KR20150033811A - Method for manufacturing forged magnesium alloy mebmer having enhanced hardness and forged magnesium alloy member manufactured thereby - Google Patents

Method for manufacturing forged magnesium alloy mebmer having enhanced hardness and forged magnesium alloy member manufactured thereby Download PDF

Info

Publication number
KR20150033811A
KR20150033811A KR20130113382A KR20130113382A KR20150033811A KR 20150033811 A KR20150033811 A KR 20150033811A KR 20130113382 A KR20130113382 A KR 20130113382A KR 20130113382 A KR20130113382 A KR 20130113382A KR 20150033811 A KR20150033811 A KR 20150033811A
Authority
KR
South Korea
Prior art keywords
magnesium alloy
forging
manufacturing
forged
compressive stress
Prior art date
Application number
KR20130113382A
Other languages
Korean (ko)
Inventor
김세종
이영선
윤종헌
이정환
윤은유
권용남
김지훈
김대용
김상우
이광석
이호원
강성훈
Original Assignee
한국기계연구원
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 한국기계연구원 filed Critical 한국기계연구원
Priority to KR20130113382A priority Critical patent/KR20150033811A/en
Publication of KR20150033811A publication Critical patent/KR20150033811A/en

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C23/00Alloys based on magnesium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/06Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of magnesium or alloys based thereon

Abstract

The present invention relates to a method to manufacture a forged magnesium alloy member having enhanced hardness, and comprises: (a) a step of preparing the forged magnesium alloy member; (b) a step of permitting a compressive stress to the said forged member, and a forged magnesium alloy member manufactured using the same. According to the method of manufacturing the forged magnesium alloy member in the present invention, compressive stress is permitted to the forged magnesium alloy member to induce twinning within magnesium alloy to improve hardness of the said forged magnesium alloy member.

Description

TECHNICAL FIELD The present invention relates to a method of manufacturing a magnesium alloy forging member having improved hardness and a magnesium alloy forging member manufactured thereby,

The present invention relates to a method of manufacturing a magnesium alloy forging member and a magnesium alloy forged member manufactured thereby.

Magnesium alloys are the most densely lightweight metal materials among the available structural materials, and are attracting attention in the automotive and electronic parts industries due to their excellent properties such as high nobleness, excellent machinability, vibration absorbing ability and electromagnetic wave shielding.

The molding method for such a magnesium alloy is casting such as die casting, but the casting method is excellent in moldability, while a large number of internal defects such as shrinkage pores are generated, And its surface is very coarse, which requires a lot of time and cost in the post-treatment process for the post-casting surface, making it unsuitable for producing high quality magnesium alloy products requiring high strength.

On the other hand, forging as a plastic working process is suitable for producing a magnesium alloy of high quality having a dense microstructure with minimal defects, so that various magnesium alloy forging members are manufactured, and a scroll compressor equipped with a scroll compressor Scrolling, engine parts for automobiles (such as valve lifters for engine intake and exhaust valves), and the like.

However, since the magnesium alloy forging member such as the scroll has hardness less than expected, there is a need for a manufacturing method of a magnesium alloy forging member having improved hardness.

The present invention provides a method for manufacturing a magnesium alloy forging member having improved hardness by controlling the microstructure of a magnesium alloy forging member and a magnesium alloy forging member manufactured by the method.

According to an aspect of the present invention, there is provided a method of manufacturing a semiconductor device, comprising: (a) preparing a forging member made of a magnesium alloy; And (b) applying a compressive stress to the forged member. The present invention also provides a method of manufacturing a magnesium alloy forged member, the method comprising:

Further, the present invention proposes a method for producing a magnesium alloy forging member having improved hardness, wherein the magnesium alloy is AZ31, AZ61 or AZ80.

Also, in the step (b), a compressive stress is applied in a direction parallel to the basal plane of the magnesium alloy crystal, and a method for manufacturing the magnesium alloy forging member with improved hardness is proposed.

Further, in the step (b), twinning is caused in the microstructure of the magnesium alloy constituting the forging member by applying compressive stress, thereby proposing a method of manufacturing a magnesium alloy forging member with improved hardness.

Further, the present invention proposes a method of manufacturing a magnesium alloy forged member with improved hardness, wherein the forging member is a scroll.

Further, in the step (b), the compressive stress is applied to the wrap portion of the scroll, and a method for manufacturing the magnesium alloy forged member with improved hardness is proposed.

Further, the strain of the wrap portion is 0.5 to 6%. The method for manufacturing the magnesium alloy forging member with improved hardness is proposed.

Further, a magnesium alloy forging member manufactured by the above manufacturing method is proposed.

Further, a scroll produced by the above production method is proposed.

According to the method of manufacturing a magnesium alloy forging member according to the present invention, a compressive stress is applied to a magnesium alloy forging member to induce twinning in the magnesium alloy, thereby improving the hardness of the magnesium alloy forging member Can be produced.

Figs. 1 (a) and 1 (b) are a plan view and a cross-sectional view, respectively, of a scroll used for preparing a specimen in Examples and Comparative Examples of the present invention.
2 (a) to 2 (c) are graphs showing the relationship between the three points (the top, the top, and the bottom) of the specimen along the length direction of the specimen in the magnesium alloy forging specimens prepared in Examples 1, Center, and bottom) of the microstructure of the microstructure.
Fig. 3 is a photograph showing the result of observation of a crystal structure of a cross section of a scroll used for preparing a specimen in Examples and Comparative Examples of the present invention. Fig.
4 is a graph showing Vickers hardness (H V ) measurement results of the magnesium alloy forgings produced in Examples 1 and 2 and Comparative Examples of the present invention.

Hereinafter, the present invention will be described in detail.

A method of manufacturing a high strength magnesium alloy sheet according to the present invention comprises the steps of: (a) preparing a forged member made of a magnesium alloy; And (b) applying compressive stress to the forging member, wherein each step is described in detail below.

Step (a) of the manufacturing method according to the present invention is a step of preparing a forging member made of a magnesium alloy by molding a billet or the like made of a magnesium alloy through a forging process.

The method of preparing the magnesium alloy forging member through the forging process in this step is not particularly limited. That is, in the case of the means for performing the forging, it can be done by any method such as press forging or hammer forging, and the hot forging or the cold forging It can be done by either.

Also, the shape of the forged member prepared through this step is not particularly limited. That is, various kinds of forged members can be prepared through known methods such as free forging or die forging using a magnesium alloy.

For example, commercially available magnesium alloys such as AZ31 (Mg-3Al-1Zn), AZ61 (Mg-3Al-1Zn), and the like may be used as the forging member. 6Al-1Zn), AZ80 (Mg-8Al-0.5Zn), and the like.

Step (b) of the manufacturing method according to the present invention is a step of applying a compressive stress to the magnesium alloy forging member prepared in the step (a) to improve the hardness of the magnesium alloy forging member.

By carrying out this step, the microstructure of the magnesium alloy constituting the forging member can be controlled. More specifically, tensile twinning is induced in the microstructure of the magnesium alloy by applying compressive stress to the magnesium alloy forging member, thereby improving the hardness of the magnesium alloy forging member by reducing the grain size of the magnesium alloy. Can be achieved.

Meanwhile, it is preferable that the compressive stress applied to the forging member in this step is applied in a direction parallel to the basal plane of the magnesium alloy crystal forming the forging member, that is, in a direction perpendicular to the basal pole, When compressive stress is applied in this manner, more twinning can be induced in the magnesium alloy.

Further, when compressive stress is applied to the magnesium alloy member through this step, the strain of the forging member is preferably 0.5 to 6%. When the strain is less than 0.5%, sufficient magnesium alloy grain refinement is not achieved to improve the hardness of the forged member. When the strain exceeds 6%, the effect of improving the hardness due to refinement of the magnesium alloy grain is insignificant. There is a problem that additional processing may be required depending on the deformation.

The magnesium alloy forging member manufactured according to the above manufacturing method can be substituted for various forging members made of conventional steel materials such as a scroll and the like by having magnesium alloy itself not only light weight but also high hardness, It is expected that the application field of magnesium alloy will be greatly expanded.

Hereinafter, the present invention will be described in detail on the basis of embodiments. The presented embodiments are illustrative and are not intended to limit the scope of the invention.

< Example  1>

After the wrap portion is cut from a scroll produced by hot forging a commercial magnesium alloy (A6) shown in the plan and sectional views in Figs. 1 (a) and 1 (b) Was subjected to a compressive stress such that a strain of 1% was generated in the longitudinal direction at room temperature using a gleeble tester, thereby producing a magnesium alloy forging specimen subjected to compressive stress.

< Example  2>

After the wrap portion is cut from a scroll produced by hot forging a commercial magnesium alloy (A6) shown in the plan and sectional views in Figs. 1 (a) and 1 (b) Was subjected to compressive stress by using a gleeble tester so that a strain of 3% in the longitudinal direction was generated at room temperature, thereby producing a magnesium alloy forging specimen under compressive stress.

< Comparative Example >

A wrap portion was cut from a scroll produced by hot forging a commercial magnesium alloy (A6) shown in a plan view and a sectional view in Figs. 1 (a) and 1 (b) to manufacture a magnesium alloy forging specimen Respectively.

< Experimental Example  1> Example  One, Example  2 and In the comparative example  Observation of Microstructure of Forged Magnesium Alloy Specimens

Figs. 2 (a) to 2 (c) are graphs showing the relationship between the three points of the specimen (top, middle and bottom) of the magnesium alloy forging specimens prepared in Examples 1, 2, (center) and bottom (bottom)) of the microstructure.

According to Fig. 2 (a) to Fig. 2 (c), in the case of the specimens prepared in the comparative examples, twinning tissues were hardly found, but in the specimens prepared in Examples 1 and 2, In particular, twinning tissues were more frequently found in the specimen prepared in Example 2, where deformation due to compressive deformation was larger than that in the specimen prepared in Example 1.

The microstructure observation results show that the compressive stress is applied in the longitudinal direction of the lap since the basal plane shown in red is located horizontally or horizontally close to the longitudinal direction of the lap, This is because tensile twinning is induced.

From the above results, it can be confirmed that miniaturization of the magnesium alloy grain was achieved by generating twin crystal structure in the specimen as compressive stress is applied to the magnesium alloy forging specimen.

< Experimental Example  2> Example  One, Example  2 and In the comparative example  Measurement of mechanical properties of fabricated specimens

As a result of conducting Vickers hardness (H V ) test (test load: 500 gf, dwell time: 5 sec) on the magnesium alloy specimen in Examples 1, 2 and Comparative Example, It can be seen that the hardness at each measurement point increases as the strain due to stress increases.

That is, when the magnesium forged member is manufactured according to the present invention, the magnesium alloy forging member having improved hardness can be manufactured by controlling the microstructure of the magnesium alloy through twinning induction.

Claims (9)

(a) preparing a forging member made of a magnesium alloy; And
(b) applying a compressive stress to the forging member, wherein the hardness is improved.
The method of claim 1, wherein the magnesium alloy is AZ31, AZ61 or AZ80. The method of claim 1, wherein the compressive stress is applied in a direction parallel to a basan plane of the magnesium alloy grains in the step (b). The method for manufacturing a magnesium alloy forging member according to claim 1, wherein twisting of the microstructure of the magnesium alloy forming the forging member is caused by applying compressive stress in the step (b) . The method of claim 1, wherein the forging member is a scroll. 6. The method of claim 5, wherein the compressive stress in step (b) is applied to the wrap portion of the scroll. [7] The method of claim 6, wherein the strain of the wrap portion is 0.5 to 6%. A magnesium alloy forging member produced by the manufacturing method according to any one of claims 1 to 4. A scroll produced by the production method according to any one of claims 5 to 7.
KR20130113382A 2013-09-24 2013-09-24 Method for manufacturing forged magnesium alloy mebmer having enhanced hardness and forged magnesium alloy member manufactured thereby KR20150033811A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR20130113382A KR20150033811A (en) 2013-09-24 2013-09-24 Method for manufacturing forged magnesium alloy mebmer having enhanced hardness and forged magnesium alloy member manufactured thereby

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR20130113382A KR20150033811A (en) 2013-09-24 2013-09-24 Method for manufacturing forged magnesium alloy mebmer having enhanced hardness and forged magnesium alloy member manufactured thereby

Publications (1)

Publication Number Publication Date
KR20150033811A true KR20150033811A (en) 2015-04-02

Family

ID=53030912

Family Applications (1)

Application Number Title Priority Date Filing Date
KR20130113382A KR20150033811A (en) 2013-09-24 2013-09-24 Method for manufacturing forged magnesium alloy mebmer having enhanced hardness and forged magnesium alloy member manufactured thereby

Country Status (1)

Country Link
KR (1) KR20150033811A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108754365A (en) * 2018-05-25 2018-11-06 湖南工学院 A kind of high density twin structure ZK21 magnesium alloy block materials preparation methods
US11286544B2 (en) * 2017-01-11 2022-03-29 The Boeing Company Calcium-bearing magnesium and rare earth element alloy and method for manufacturing the same
KR20230103010A (en) * 2021-12-30 2023-07-07 주식회사 엠에프알씨 Manufacturing method for mounting bracket for transport equipment

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11286544B2 (en) * 2017-01-11 2022-03-29 The Boeing Company Calcium-bearing magnesium and rare earth element alloy and method for manufacturing the same
CN108754365A (en) * 2018-05-25 2018-11-06 湖南工学院 A kind of high density twin structure ZK21 magnesium alloy block materials preparation methods
KR20230103010A (en) * 2021-12-30 2023-07-07 주식회사 엠에프알씨 Manufacturing method for mounting bracket for transport equipment

Similar Documents

Publication Publication Date Title
JP5082483B2 (en) Method for producing aluminum alloy material
CN103695817B (en) One can synchronously to be quenched heat forming technology by heat-treatable aluminum alloy
KR101324715B1 (en) A method for increasing formability of magnesium alloy sheet and magnesium alloy sheet prepared by the same method
Joshi et al. Mechanical properties and microstructural evolution in Al 2014 alloy processed through multidirectional cryoforging
JP6492057B2 (en) High strength copper-nickel-tin alloy
Lu et al. Modification of grain refinement and texture in AZ31 Mg alloy by a new plastic deformation method
Xu et al. Hardness homogeneity and micro-tensile behavior in a magnesium AZ31 alloy processed by equal-channel angular pressing
Qiu et al. Microstructures and mechanical properties of titanium alloy connecting rod made by powder forging process
JP5723878B2 (en) Method for producing processed magnesium alloy material with improved low cycle fatigue life using pre-compression deformation
Azadi et al. Fatigue lifetime of AZ91 magnesium alloy subjected to cyclic thermal and mechanical loadings
US20140166165A1 (en) High-strength aluminum alloy extruded shape exhibiting excellent corrosion resistance, ductility, and hardenability, and method for producing the same
JPWO2014016875A1 (en) Die forging crankshaft manufacturing method
KR20150033811A (en) Method for manufacturing forged magnesium alloy mebmer having enhanced hardness and forged magnesium alloy member manufactured thereby
JP6718219B2 (en) Method for manufacturing heat resistant aluminum alloy material
KR101502751B1 (en) Method for manufacturing cold rolled magnesium alloy sheet having enhanced formability, yield strength and tensile strength and cold rolled magnesium alloy sheet having enhanced formability, yield strength and tensile strength manufactured thereby
JP5588884B2 (en) Magnesium alloy forged piston manufacturing method and magnesium alloy forged piston
KR102069361B1 (en) Method of manufacturing for magnesium alloy sheet with improved total elongation
JP7096226B2 (en) Process for the production of hot-worked spinodal alloys with uniform particle size
Tokutomi et al. Changes in mechanical characteristics of pre-annealed wires of Cu–Sn alloy manufactured by continuous draw bending
RU2692539C1 (en) Method of obtaining volumetric blanks of high-manganese steel with recrystallized fine-grained structure
RU2013126799A (en) METHOD FOR PRODUCING A SHAPED PANEL FROM AI ALLOY FOR AEROSPACE APPLICATIONS
KR101648847B1 (en) Method for manufacturing of magnesium alloy sheet and the magnesium alloy sheet thereby
Umezawa Mechanical Properties of Thermomechanical Treated Hyper-Eutectic Al–Si–(Fe, Mn, Cu) Materials
Lee et al. Effects of {10–12} twins on dynamic torsional properties of extruded AZ31 magnesium alloy
KR101495500B1 (en) Composite sheet having enhanced ductility during cold rolling, method for cold rolling using the same, method for manufacturing rolled sheet using the same, and rolled sheet manufactured thereby

Legal Events

Date Code Title Description
A201 Request for examination
E902 Notification of reason for refusal
AMND Amendment
E601 Decision to refuse application