KR20140060424A - Aromatheraphy solution oil anti-bac composition and processing make the same - Google Patents

Abstract

The present invention relates to a solution oil anti-bac composition for aromatherapy and a method for producing the same. More specifically, the composition consists of natural antibacterial essential oil (eucalyptus, peppermint, tea tree, pine, lemon, rosemary, bergamot, lavender, orange, cinnamon, spearmint, mandarin, citronella, basil, geranium, juniper berry, sage, and thyme), a surfactant, a preserving agent, a fragrance-maintaining agent, a solvent, a plant extract, and purified water. The composition especially has an improved fragrance retention rate and provides a special effect of aromatherapy having excellent air purification, humidifying, deodorizing, and antibacterial effects.

Description

Technical Field [0001] The present invention relates to an anti-bacterial composition for aromatherapy,

The present invention relates to a solution of an oil anti-foaming composition and a method for preparing the solution, and a method of preparing a solution anti-bacterial solution by immersing 4 g of solution anti- (Contaminated air, bacteria, odor, bacteria) and sterilizing action of viruses and harmful substances. It is sprayed in a mist form when air is discharged to the outside, The present invention relates to a solution of an oil anti-foaming composition and a method of using the same, which can relieve psychological stability, cool feeling, tension, fatigue, and deterioration of efficiency of human by continuously radiating a unique fragrance of natural essential oil for a long period of time.

▷ Cosmetic composition containing semi-solid capsule containing natural aroma oil

Korea Application No.: 10-2004-0060461 (Jul. 30, 2004)

▷ Indoor air purifier fragrance / so-called component divergent sustained-directional gel composition

Korea Application No.: 10-2001-0023891 (May 1, 2001)

Natural essential oil composition for aromatherapy and method for producing nanoparticles of transparent state using the same

Korea Application No.: 10-2004-0078816 (2004.10.04)

 Aromatherapy uses natural essential oil extracted from each part of a natural (aromatic) plant (flower, woody, roots, fruit, peel, etc.) and promotes human body, spirit and psychological health And maintains and promotes vitality. When the fragrance delivery system of natural essential oil by respiration of the aroma therapy is examined, if the receptor in the olfactory nerve cell receives the fragrance molecule after the fragrance molecule enters the nose, the fragrance molecule passing through the olfactory nerve enters the tonsil nucleus, Signals are sent to the limbic system of the cerebrum to promote hormone secretion, and limbic structures that control emotions and memory are also stimulated by the transmission signals. The aromatherapy effect promotes circulation, strengthens the immune system, relieves muscle tension and muscle aches, destroys fat deposits, excretes waste in tissues, increases relaxation, and has a variety of effects. Natural essential oils with aromatherapy effects have been used as fragrances or as cosmetics, and have been used as a form of massage oil blended with a small amount of essential oils in carrier oils using mainly vegetable oils. In recent years, natural essential oils have been used in cosmetics Directly applied studies are being published and products are being launched.

 Essential oils are composed of hundreds of natural materials that can not be imitated by artificial synthetic materials, and they are applied to the human body with only about 30% of the currently known ingredients.

 Essential oils in plant biochemical structure play a pivotal role and function in the plant, play the role of hormones between cells, control physiological function and transmit information. In other words, it can be said that plants protect themselves from pests and diseases and adapt to environment by coping with stress situations.

 The lives of urban people living in modern times are becoming increasingly serious due to the overcrowding of highly dense buildings, cars and population density. In particular, in order for human beings to have life, the atmospheric air, which is essential for respiration, It is being threatened. In order to prevent pollution of atmospheric air, a method to reduce the emission of harmful substances is a basic measure, but as the society expands, it is impossible to reduce the amount of harmful substances in the present state. Therefore, it is required to develop a device that can purify and disinfect air as an alternative. In advanced countries, technology development is actively promoted in order to improve the quality of human life, and many products are being released.

 Generally, the indoor air purifiers use an electric dust collecting system and a carbon filter to purify the indoor air by removing the dust and dust of the air introduced into the fan. However, directional composition-related products comprising various formulations have been introduced as a method for emotionally stabilizing the urban people who have to live indoors most of the time, rather than merely cleansing indoor air, and as a method for promoting work efficiency Excepting the area where only the smell is enjoyed, therapies such as stress and aging of the modern life, relaxation of tension, enhancement of concentration and the like are attracting attention, and the fragrance and the composition including the perfume are being actively developed. The use of an air purifier for purifying the indoor air, and an oil composition for a natural antimicrobial solution which can emit the aroma into the room to give a refreshing feeling of the indoor air and can show the humidification effect of the mist dispersed in the air If done, consumers using it would be very beneficial.

 Fragrance is a volatile compound such as odor, but it is composed of structure and functional group different from odor and refers to a good smell emitted from flowers and perfume. This fragrance is used as a fragrance to neutralize the odor, and it is used as a fragrance, and it shows excellent effect on the mental and physical treatment caused by the stress which is the biggest problem of modern people, and it is already attracting attention as an alternative medicine in developed countries. In addition, its side effects are small, and it is easy to use by anyone. Its popularity is rising in Korea and it gives an air purification and refreshing to the indoor atmosphere as an aroma of antibacterial essential oil, refreshing the mood and sometimes relaxing feeling of mind and body .

 In particular, incense capsules have the advantage of controlling the divergence time according to the type of capsule material, the type of capsule material, and the thickness of the capsule wall, and the particle size can be variously varied from several millimeters to tens of degrees, It can be applied to perfume products, fragrant wallpaper, clothes, and the like.

  However, incense capsules can not be manufactured with various appearance and color, and their manufacturing cost is high, so there are some problems to be solved in order to use incense capsules alone. In order to directly apply the natural essential oil to cosmetics, there is a method of directly applying the natural essential oil to an emulsion formulation or a dispersion formulation. In order to apply it to a cosmetic composition of a transparent formulation such as a skin, a gel, etc., a micelle is formed using a surfactant, It must go through the solubilization method. However, when the content of the essential oil is increased in order to exhibit a sufficient aromatherapy effect, a large amount of the solubilizing agent should be used, thereby causing unstability of the formulation, deterioration in feeling, and stimulation. Natural essential oils are used in cosmetic formulations of transparent formulations, and studies on how to safely apply them to skin are needed.

 In recent years, for example, humidifier disinfectants, which are widely used at home, have become a social issue. Humidifiers were added to the spray liquor while humidifiers were used, causing people who suffered from lung disease to die. In 2011, the disease was first diagnosed as unknown lung disease, and the lungs were implanted due to problems in the lungs of pregnant women and infants, and as a result of the epidemiological survey, it was found to be caused by the humidifier disinfectant. Humectant disinfectants are mainly polyhexamethylene guanidine (PHMG) and oligo (2- (2-ethoxy) ethoxyethyl guanidine chloride (PGH) Toxicity is only about 5 to 10 times lower than other disinfectants, so it is used in various products such as shampoo, wet tissue as well as humidifier disinfectant. However, the toxicity that occurs when these components are inhaled into the respiratory tract is studied In the case of foreign countries, there is no case where these ingredients are used as humidifier disinfectants, and because the humidifier disinfectants are classified as industrial products, they are not covered by the Food Sanitation Law or the Pharmaceutical Affairs Law, Only the general safety standards according to the management law were applied and the damage could not be prevented. In order to maintain the fragrance for a long time, it is necessary to mix the fragrance with an inorganic powder or a cyclohexanone in order to maintain the fragrance for a long time in a natural state because it has a constant boiling point, A microencapsulation method of adsorbing on the dextrin or encapsulating the fragrance ingredient with a polymer substance is used.

 The inventor of the present invention has found that by using the natural antimicrobial essential oil which can purify the indoor air (contaminated air, bacteria, odor, bacteria) and sterilize the fragrance for a long time, The present invention has been completed as a result of studies on a composition and a manufacturing method using the same.

 In the present invention, among the essential oils of more than 200 kinds, a kind that can most effectively express a desired antimicrobial function is selected and used. In this case, when more than 10 kinds of oils are mixed, the effect can be increased. However, the method of using various natural essential oils as described above is effective in controlling the amount of each oil to be mixed in order to prevent excessively excessive or inadequate amount of natural components contained in each oil when they act on the human body In addition, the retarder and the solvent were mixed and stirred to enhance the transparency and delayed synergy effect.

 In order to achieve the above object, the present invention provides a natural antimicrobial essential oil composition for aromatherapy, comprising: a) 1.0 to 15.0% by weight of eucalyptus, b) 1.0 to 20.0% by weight of peppermint, c) 1.0 to 10.0% F) Rosemary 5.0 to 20.0 wt%, g) Bergamot 2.0 to 8.0 wt%, h) Lavender 2.0 to 8.0 wt%, i) Orange 2.0 to 8.0 wt%, e) Lemon 0.1 to 5.0 wt% M) citralella 3.0 - 10.0 wt.%, N) basil 0.5 - 3.0 wt.%, And mixtures thereof. 0.5 to 5.0% by weight of geranium, 0.5 to 3.0% by weight of juniper berries, 5.0 to 10.0% by weight of sage, and 0.1 to 5.0% by weight of time. The present invention provides a natural antimicrobial essential oil composition. The present invention also relates to a method for producing a natural antimicrobial essential oil composition for aromatherapy comprising the steps of: 5.0 to 20.0% by weight of a natural antimicrobial essential oil composition for aromatherapy, 10.0 to 40.0% by weight of a surfactant, 5.0 to 15.0% by weight of a retarder, 5.0 to 10.0% 0.1 to 2.0% by weight of a plant extract, and a remaining amount of purified water are mixed and solubilized and dissolved at room temperature, followed by micro-homogenization to provide a solution of an oil antipust solution.

An object of the present invention is to provide an oil antisubstance composition for aromatherapy solution which has uniformity and long-lasting efficiency by using the fragrance of natural essential oil and which is excellent in humidification, deodorization and antibacterial effect, and a method of using the same.

INDUSTRIAL APPLICABILITY The present invention provides an effective natural solution of an oil anti-foaming solution capable of uniformly controlling the divergence of fragrant materials over a long period of time. The initial strength is too strong and the fragrance strength of fragrance is weakened to a high rate, Which can suppress the volatilization of the volatile oil, and which can uniformly spray the fragrance with a long period of time, and to provide a manufacturing method using the same.

 Also, it is aimed to provide a method of using natural antimicrobial essential oil in which the volatility of each antioxidant is vaporized and volatilized to diffuse in the air and to control the diffusion rate.

 The natural solution of the oil anti-foaming solution of the present invention is applied to the antibacterial wet-type air cleaner by applying a retarding agent and the air is blown out to the outside while passing through the aqueous liquid phase by rotating at more than 2,000RPM, And a composition which emits a fragrance which is uniform and long enough for the human to feel the fragrance at an effective concentration, and has an excellent effect of feeling the fragrance while keeping the fragrance duration for a long time.

 Although the present invention has been described in connection with the above-mentioned preferred embodiments, it is possible to make various modifications and variations without departing from the spirit and scope of the invention. Accordingly, the appended claims are intended to cover such modifications or changes as fall within the scope of the invention.

 In addition, as mentioned above, solution oil anti-foaming solution is uniformly and continuously diffused and at the same time exhibits a direction effect. By using a unique therapeutic effect of aromatherapy alone, it can be used in home, offices, hospitals, nursing homes, kindergartens, I am sure that it will be available to public institutions and will solve the problems of existing humidifiers.

FIG. 1 shows the manufacturing process of the solution oil antibiotic composition in Example 1-5,
FIG. 2 shows the results of GC-MS analysis of the samples of the solution oil anti-foaming solution in Example 8 at 1 hour, 3 hours, 5 hours, 7 hours and 12 hours.
FIG. 3 shows data obtained by analyzing the data of FIG. 2 in 1 hour, 3 hours, 5 hours, 7 hours, and 12 hours by setting the range from 0 to 10 minutes.
FIG. 4 shows data obtained by analyzing the data of FIG. 2 in 1 hour, 3 hours, 5 hours, 7 hours, and 12 hours by setting the range from 10 to 16 minutes.
FIG. 5 shows the data obtained by analyzing the data of FIG. 2 in 1 hour, 3 hours, 5 hours, 7 hours, and 12 hours by setting the range from 16 to 21 minutes.
FIG. 6 shows data obtained by analyzing the data of FIG. 2 in 1 hour, 3 hours, 5 hours, 7 hours, and 12 hours by setting the range from 21 to 28 minutes.

As for the production method of the present invention,

1. Natural antimicrobial essence oil is added to the surfactant, and the solubilization is carried out while stirring.

2. Step of completely dissolving the solubilized raw material by adding a natural preservative.

3. Mixing the solvent and the retarder in the molten raw material and completely dissolving the molten raw material, followed by stirring so as to be uniformly combined.

4. Put the plant extract and purified water in the fully stirred state, slowly stir the solution, homogenize and dissolve completely.

5. When the reaction is complete, it can be summarized as cooling, defoaming, and stabilizing and filling the solution.

  [Specification of LED antibacterial humidifier purifier measuring sample]

  1. Product name and model name: Antibacterial water purifier purifier

  2. Specification: 200mm (W) x 200mm (D) x 190mm (H)

  3. Purification method:

  4. Test mode: S / W ON (rated air flow rate)

 In the following example, a solution of the oil anti-foaming solution was prepared, and then 1 liter of water was weighed into the container using an LED antibacterial humidifier purifier. 4 g of solution anti-foaming solution was taken into the container, power was turned on, , And the strength of the fragrance which is sprayed while being dissolved is confirmed by the sensory test. [Sensory Test Reference]

 As the equipment used in this example, the speed range (200 ~ 3,000 rpm) was used for the MISUNG SCIENTIFIC (Model MS3040) and the MISUNG SCIENTIFIC (Model MS300HS) for the hot plate and magnetic stirrer. The maximum RPM (1,500 rpm) up to 380). For pH measurement, the microprocessor pH meter was measured with Hana Instruments (Model pH213).

 [Example 1]

 In Example 1-1, the solution oil antibiotic composition was prepared and the fragrance delay time test was performed. However, the transparency was remarkably decreased within 3 hours, and the transparency of 1-2 was improved but the delay time was lower. Example 1-3.1-4 Experiments were carried out to confirm that the delay time was improved by 6 hours or more by completing the compounding amount of Example 1-5.

Ingredient 1-1 1-2 1-3 1-4 1-5 Functional Essential Oil 20 17 17 20 17 Polysorbate-80 34 34 34 38 34 Octanediol, Ethylhexylglycerin, Citrus Paradisi (Grapefruit) Seed Extract, Artemisia princeps Extract
0.6
0.6
0.6
0.6
0.6 Glycerine 10 10 10 10 15 Ethyl Alcohol 5 5 10 8 10 Dipropylene Glycol 10 15 10 10 10 Algae Extract 1.0 - 1.0 - 1.0 D.I water 19.4 18.4 17.4 13.4 12.4   Sum 100 100 100 100 100

[Example 2]

 4 g of each of Examples 1-5 were taken into 1,000 ml of the solution, and the LED antibacterial and humidifier air cleaner was operated to inhale the sprayed air at intervals of 1 hour, 3 hours, 5 hours, 6 hours, and 8 hours, The results of the strong, medium, weak, weak, and odorless tests are shown in the table below.

  [how to write ; Strong - A, medium - B, weak - C, weak - D, odorless - F]

(Sensory test of the subject)  name age gender After 1 hour After 3 hours After 5 hours After 6 hours After 8 hours Hong Sung * 40s south A A A B C More than * 30s south B B C D D Imhun * 30s south A B C D D Hwang, Chun * 40s female B C C D D Park Min * 30s south A C C C D Hwang Tae * 50s south B B D D F Upstairs * 40s female B B B C  C already * 40s female A C C C D * 30s female A B C C D Noh * 40s female A B C C D Adjusting * 40s female A B B C D

 As shown in the above table, the sensory test of the subject continued to show that the duration of the fragrance continued even after 6 hours, and the subjects could feel the fragrance even after 8 hours.

[Example 3]

The deodorization rates of ammonia (NH ₃ ), acetaldehyde (CH ₃ CHO), and acetic acid (CH ₃ COOH) were measured according to elapsed time using the samples of Examples 1-5. It was tested according to the test method of the Air Purifier Association, and the deodorization efficiency is very excellent as 30 ~ 50% of the test result.

Test Items

unit
division
Test result
Test Methods
Deodorization efficiency (ammonia, NH ₃ )

%
One
36
SPS-KACA002-132: 2006
Deodorization efficiency (acetaldehyde, CH ₃ CHO)

%
One
30
SPS-KACA002-132: 2006
Deodorization efficiency (acetic acid, CH ₃ COOH)

%
One
50
SPS-KACA002-132: 2006

[Example 4]

 The antibacterial test with Escherichia coli and Pseudomonas aeruginosa was carried out using the samples of Examples 1-5.

 1. Test results (concentration after 5 minutes)

Escherichia coli ATCC 25922 and Pseudomonas aeruginosa ATCC 15442 were used as the inoculum bacteria concentration (CFU / mL) of Escherichia coli 1.6 × 10 ⁶ and P. aeruginosa 1.8 × 10 ⁶ . The sample volume was 1 mL, the test method was KCL-FIR-1002 (2011), and the bacterial incubation time was 5 minutes. The bacterial reduction rate was 99.9%.

Test Items
Test result
Test Methods Initial concentration
(CFU / mL) Concentration after 5 minutes
(CFU / mL) Bacterial reduction rate
(%)
By E. coli
Antibacterial test
BLANK 1.6 x 10 ⁴
1.6 x 10 ⁴         -


Present the client Solution oil
(ANTI + BAC) 1.6 x 10 ⁴       <10        99.9
By Pseudomonas aeruginosa
Antibacterial test    BLANK 1.8 x 10 ⁴ 1.8 x 10 ⁴         - Solution oil
(ANTI + BAC) 1.8 x 10 ⁴       <10        99.9

  2. Test results (concentration after 1 hour)

Escherichia coli ATCC 25922 and Pseudomonas aeruginosa ATCC 15442 were used as the inoculum bacteria concentration (CFU / mL) of Escherichia coli 1.6 × 10 ⁶ and P. aeruginosa 1.8 × 10 ⁶ . The sample volume was 1 mL, and the test method was KCL-FIR-1002 (2011). The incubation time was 1 hour. As a result, the bacterial reduction rate was 99.9%.

Test Items Test result
Test Methods Initial concentration
(CFU / mL) Concentration after 1 hour
(CFU / mL) Bacterial reduction rate
(%)
By E. coli
Antibacterial test
BLANK
1.6 x 10 ⁴ 1.7 x 10 ⁴ -


Present the client Solution oil
(ANTI + BAC) 1.6 x 10 ⁴ <10 99.9
By Pseudomonas aeruginosa
Antibacterial test
BLANK
1.8 x 10 ⁴ 2.0 x 10 ⁴ - Solution oil
(ANTI + BAC) 1.8 x 10 ⁴ <10 99.9

 [Example 5]

 The samples of Examples 1-5 were taken and measured for the amount of water dispersed in the air using an LED antibacterial wet scrub cleaner before the first stirring by using a balance [Chosun Instrument, HS210 Model, 0.01 g] After each hour, the amount of water was measured and the results were shown.

 As a result, the amount of water of about 20.6 g per hour was sprayed into the air, and the humidifying effect was confirmed.

Example

1-5

After 1 hour
After 2 hours
After 3 hours
After 4 hours
After 5 hours
After 6 hours
After 7 hours
After 8 hours
After 9 hours
Content quantity
(g)
1004

986
973
958
945
916
900
886
855
818
Evaporation amount
(g)
0
18
13
15
13
29
16
14
31
37

[Example 6]

 The specimens of Examples 1-5 were measured by FT-IR (infrared spectroscopy), and the charts are shown below. The experimental equipment is a FT-Infrared Spectrometer for solid-liquid measurement and the standard is Wavenumber ange (4000 ~ 650 cm-1) and the manufacturer is Sumiths Detection / USA, model name (Travel IR). This IR system is a system that can directly analyze solid image, liquid image, and owder state by placing a sample on a diamond sensor and observing a video image using a microscope without sample preprocessing. Especially, it is a device that is excellent in analyzing samples which are difficult to analyze with IR and difficult to measure permeability, that is, surface analysis of coated film and thin film coating on metal plate, foreign matter analysis of rubber, plastic, and chemical analysis of drugs.

                 <Solution oil anti-foil FT-IR measurement data>

Solution 4 g of the antioxidant solution was put into 1 liter of water, and after 1 hour, 3 hours, 5 hours, 7 hours, and 12 hours elapsed, the samples were collected by stirring, and the results were measured using FT-IR equipment.

                   <Measurement data after 1 hour>

                   <Measurement data after 3 hours>

                   <Measurement data after 5 hours>

                   <Measurement data after 7 hours>

                   <Measurement data after 12 hours>

                   <Comparison with existing data after sample analysis>

As a result of analyzing the measurement data using the FT-IR instrument, only 1 hour to 9 hours after the elapse of the peak, H ₂ O was present, and the present inventors conducted an incense-persistence experiment using a GC-MS measuring instrument.

(Example 8)

[Example 7]

The samples of Examples 1-5 were added to the solution and stirred to measure the residual amount in the solution relative to the residual amount. After stirring for 1 hour, 5 ml of each sample was taken and the absorbance and the permeability were measured using UV Spectrum there was.

Absorbance DATA time Wavelength range (nm) Absorbance (ABS) Change over 1 hour (ABS) After 1 hour
Near 1033 0.114 - Near 343 0.009 - After 2 hours
Near 1033 0.082 -0.032 Near 343 0.009 0 After 3 hours
Near 1033 0.066 -0.048 Near 343 0.009 0 After 4 hours
Near 1033 0.023 -0.091 Near 343 0.009 0 After 5 hours
Near 1033 0.047 -0.067 Near 343 0.009 0 After 6 hours
Near 1033 0.031 -0.083 Near 343 0.088 0.079 After 7 hours
Near 1033 0.027 0.079 Near 343 0.088 -0.062 After 9 hours
Near 1033 0.052 0.079 Near 343 0.088 -0.07 After 12 hours
Near 1033 0.044 0.079 Near 343 0.088 -

Transmittance measurement DATA time Wavelength range Transmittance (T%) Change over 1 hour (T%)
After 1 hour
Near 1042 1.1 0 Near 996 2.1 0 Near 920 1.3 0
After 2 hours
Near 1042 1.4 0.3 Near 996 1.9 0.2 Near 920 1.1 0.2
After 3 hours
Near 1042 1.3 0.2 Near 996 2.1 0 Near 920 1.3 0
After 4 hours
Near 1042 1.3 0.2 Near 996 2.1 0 Near 920 1.3 0
After 5 hours
Near 1042 1.2 0.1 Near 996 2.2 0.1 Near 920 1.4 0.1
After 6 hours
Near 1042 1.4 0.3 Near 996 2.0 0.1 Near 920 1.5 0.2
After 7 hours
Near 1042 1.4 0.3 Near 996 1.9 0.2 Near 920 1.2 0.1
After 9 hours
Near 1042 1.3 0.2 Near 996 2.1 0 Near 920 1.4 0.1
After 12 hours
Near 1042 0.2 0.9 Near 996 3.3 1.2 Near 920 3.4 2.1

[Example 8]

The samples of Example 7 were analyzed for the samples containing 1 hour, 3 hours, 5 hours, 7 hours, and 12 hours after the elapse of 12 hours by using a gas chromatograph / mass spectrometer (GC-MS) The results of measurement of the fragrance residue by the material analysis are shown below, and the analysis conditions are as follows.

- MS ion source: EI

- Ionization energy: 5-241eV

- Scan rate: 10,000 amu / sec

- Max. Molecular Weight; GC, 600: MS, 800

- Wiley library (275,000)

- Stan pesticide library (340)

- NIST structure DB Oven temp: 4-450 ° C

- Colume: DB5

- Carrier gas: Helium

- Standard Solution: C ₄ H ₁₀ O

                 (DATA after 1 hour)

                (DATA after 3 hours)

                 (DATA after 5 hours)

                  (DATA after 7 hours)

                  (DATA after 12 hours)

As a result of analysis based on the above data, the residual fractions of the organic materials were calculated using the peak area values as follows.

  1. DATA after 1 hour; Total Peak Area value (732112037): 100.0%

  2. DATA after 3 hours; Total Peak Area value (389520412): 53.2%

  3. DATA after 5 hours; Total Peak Area value (184319766): 25.2%

  4. DATA after 7 hours; Total Peak Area value (118507254): 16.2%

  5. DATA after 12 hours; Total Peak Area value (57522095): 7.9%

               (Fragrance retention rate with time)

The solution of the oil antibiotic composition prepared according to the present invention is characterized in that the preparation method is simple, the shape stability is stable and the fragrance retention rate can be maintained for a long time. Although it was measured using GC-MS analysis equipment, Which is a natural essential oil. Provides the solution of oil anti-foaming composition that dissipates the fragrance retardation effect for more than 6 hours. Using LED antibacterial and humidifier purifier, it is possible to provide a variety of aromatherapy products such as psychological stability, cooling sensation, air purification, relieve stress, Effect can be expected.

While the invention has been described in detail above, it will be understood by those skilled in the art that various changes and modifications may be made therein without departing from the spirit and scope of the invention as defined in the following claims.

Claims (3)

d) from 0.1 to 5.0% by weight of e) lemon from 0.1 to 5.0% by weight, f) from rosemary to rosemary, from 5.0 to 15.0% by weight of a) eucalyptus, b) from 1.0 to 20.0% by weight of peppermint, I) 2.0 to 8.0% by weight of orange, j) 1.0 to 7.0% by weight of cinnamon, k) 4.0 to 15.0% by weight of spearmint, , j) 1.0 to 5.0% by weight of mandarin, m) 3.0 to 10.0% by weight of citrulla, n) 0.5 to 3.0% by weight of basil, 0.5 to 5.0% by weight of geranium, 0.5 to 3.0% ) 5.0 to 10.0% by weight of sage, and r) 0.1 to 5.0% by weight of time. The composition has a stable effect and is a natural antimicrobial essential oil composition for aromatherapy. The composition according to claim 1, which comprises 9 to 20% by weight of the natural antimicrobial essential oil composition, 20 to 40% by weight of a surfactant, 5 to 20% by weight of a perfume bottle, 0.05 to 2.0% by weight of a natural preservative, 2.0 to 15.0% 0.001 to 5.0% by weight, and the balance purified water. The method according to claim 2, wherein
a) Mixing natural antimicrobial essential oil and surfactant and stirring at room temperature for solubilization.
b) adding to a mixture of natural preservative a), mixing and stirring to homogenize.
c) Mixing the flame retardant and the solvent, followed by stirring to homogenize.
d) adding the mixture of step c) to step a), followed by stirring to homogenize.
e) homogenizing the plant extract and purified water, d) adding the mixture to the step mixture, stirring, mixing, and homogenizing with stirring at 3,000 RPM.
f) Stirring sufficiently, cooling, filtering, defoaming and filling.

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