KR20110086220A - Apparatus for plasma surface treatment - Google Patents
Apparatus for plasma surface treatment Download PDFInfo
- Publication number
- KR20110086220A KR20110086220A KR1020100005833A KR20100005833A KR20110086220A KR 20110086220 A KR20110086220 A KR 20110086220A KR 1020100005833 A KR1020100005833 A KR 1020100005833A KR 20100005833 A KR20100005833 A KR 20100005833A KR 20110086220 A KR20110086220 A KR 20110086220A
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- KR
- South Korea
- Prior art keywords
- plasma
- surface treatment
- rotating
- treatment apparatus
- fine particles
- Prior art date
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/223—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating specially adapted for coating particles
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/50—Substrate holders
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/54—Controlling or regulating the coating process
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F7/00—Magnets
- H01F7/02—Permanent magnets [PM]
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/67—Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
- H01L21/67005—Apparatus not specifically provided for elsewhere
- H01L21/67011—Apparatus for manufacture or treatment
- H01L21/67155—Apparatus for manufacturing or treating in a plurality of work-stations
- H01L21/67207—Apparatus for manufacturing or treating in a plurality of work-stations comprising a chamber adapted to a particular process
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Power Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Electromagnetism (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Computer Hardware Design (AREA)
- General Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Plasma Technology (AREA)
Abstract
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a plasma surface treatment apparatus, and more particularly, to a plasma surface treatment apparatus capable of surface treatment by exposing the surface to plasma more uniformly by spatially moving a surface treatment object in a reaction chamber during plasma application. It is about.
According to the present invention, in the plasma surface treatment apparatus for generating a plasma by using the gas supply device and the plasma generating device, and then using the same to treat the surface of the fine particles, the inlet and discharge to which the fine particles as the surface treatment object is introduced A reaction chamber having an outlet configured to be at least one end of which is fixed in a cylindrical shape and a rotating part rotating the central axis of the cylinder as a rotation axis in a state in which the fixing part is sealed; And first driving means connected to the rotating part to support and rotate the rotating part.
In the plasma surface treatment apparatus according to the present invention, fine particle substrates such as fiber / powder / capsule phase are evenly dispersed by the driving means during plasma application. Therefore, the plasma surface treatment of the fine particles can be more uniformly and efficiently.
Description
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a plasma surface treatment apparatus, and more particularly, to a plasma surface treatment apparatus capable of surface treatment by exposing the surface to plasma more uniformly by spatially moving a surface treatment object in a reaction chamber during plasma application. It is about.
Plasma means ionized gas. Discharge by using electrical energy to a gas composed of atoms or molecules forms a plasma composed of electrons, ions, decomposed gases, photons, and the like.
Surface treatment using such plasma is a plasma surface treatment method. The plasma surface treatment method is a surface treatment method in which a predetermined source gas such as oxygen is converted into plasma gas, and then reacted with the surface of the object to be treated physically and chemically to modify the surface thereof.
Surface treatments used throughout the present specification include grafting, crosslinking, dissociation, surface modification, etching, and deposition.
The surface treatment method using the plasma has the advantage that the surface can be treated more uniformly and precisely than the wet method, and is easy to control. In addition, since the plasma surface treatment method uses gas such as oxygen and argon, there is an advantage that the generation of pollutants is almost less than that of the wet surface treatment method.
Hereinafter, the surface treatment apparatus by plasma is demonstrated schematically.
The plasma surface treatment apparatus may be classified into a capacitively coupled plasma method and an inductively coupled plasma method according to the type of plasma generating electrode. Among these, widely used is a capacitive coupling method, which is called a capacitively coupled plasma generator.
This capacitively coupled plasma generator utilizes the principle of charge storage of a capacitor and opposes two electrodes inside a chamber to apply high frequency power, low frequency power, direct current power, or time-modulated power to one electrode. It is structured to be able to do it. The other electrode is grounded. Alternatively, the other electrode may be grounded through a combination of a capacitor, a coil (inductor), and a capacitor and a coil.
These parallel plate electrode structures accelerate charged particles such as electrons and ions by means of an electrostatic field between two electrodes, and the plasma is reacted by the collision of charged particles and charged particles, or charged particles and electrodes. Create and maintain.
In addition to this high frequency power, DC power, pulsed DC power, and microwave power may be used to generate the plasma.
In addition, the surface of the object can be treated by selecting a vacuum or atmospheric pressure atmosphere as necessary.
Even with the advantages of the plasma surface treatment described above, it is not easy to uniformly treat the fiber / powder / capsule particles using plasma. This is because all surfaces of the material must be homogeneously exposed to the plasma in order for the plasma to react uniformly with the surface of fine particles comprising fibers / powders / capsules.
Conventionally, like the surface treatment of a thin film, the base material was put on the sample support and the surface of the fine particle was plasma-surface-treated. However, powders / capsules have a wider surface area and are more reactive than thin film materials. As a result, the fine particles of the powder / capsules tend to clump together to lower the surface energy, becoming one large cluster. When the clustered powder / capsules are subjected to plasma surface treatment in a condition where the surface position of the sample exposed to the plasma is fixed as in the conventional thin film surface treatment, the plasma reacts only with the exposed surface, so that each particle of the powder / capsules It becomes difficult to give a homogeneous and efficient plasma treatment over the entire surface. The fibers are also generally linear, so they are easily entangled and clumped together, making it difficult to achieve a uniform surface finish.
In order to solve this problem, a method of surface treatment of plasma was developed while floating the fine powder using gas. However, since the powder has a particle size distribution, when the powder is suspended and conveyed at a constant gas flow rate, the smaller the particle size is faster. The time to pass through the plasma zone is short, and the larger the particle size is, the slower the time is to pass and the longer the time to pass, there is a problem that non-uniformity occurs in the plasma (plasma) treatment of the whole powder. Japanese Patent Laid-Open Nos. 6-228739, 7-68382, and 7-328427 disclose the above-described inventions.
Thus, the present invention allows the fine particles such as fibers / powders / capsules to be separated in the process of moving in space by vibrating, rotating, etc. using a driving element during the plasma surface treatment, and as a result the surface is more uniformly plasma In order to increase the plasma surface treatment efficiency.
The present invention is to improve the above-mentioned conventional problems, according to the present invention, after generating a plasma by using a gas supply device and a plasma generating device, using the plasma surface treatment apparatus for treating the surface of the fine particles using the same The rotary part includes an inlet through which fine particles, which are surface treatment objects, and an outlet are discharged, and at least one end of which is fixed in a cylindrical shape, and a rotating part rotating the central axis of the cylinder as a rotating shaft while the fixing part is sealed. A reaction chamber having a; And first driving means connected to the rotating part to support and rotate the rotating part.
In addition, there is provided a plasma surface treatment apparatus further comprising a first dispersing means extending from the rotating part toward the fixing part to disperse the fine particles.
In addition, the second dispersing means is installed so as to rotate in the reaction chamber to disperse the fine particles; And a second driving means for supporting and rotating the second dispersing means.
In addition, there is provided a plasma surface treatment apparatus further comprising a vibration means connected to the second dispersion means to vibrate the second dispersion means.
In the plasma surface treatment apparatus according to the present invention, fine particle substrates such as fiber / powder / capsule phase are evenly dispersed by the driving means during plasma application. Therefore, the plasma surface treatment of the fine particles can be more uniformly and efficiently.
1 is a schematic diagram of a plasma surface treatment apparatus according to a first embodiment of the present invention.
2 is a schematic diagram of a plasma surface treatment apparatus according to a second embodiment of the present invention.
3 is a schematic diagram of a plasma surface treatment apparatus according to a third embodiment of the present invention.
4 is a schematic diagram of a plasma surface treatment apparatus according to a fourth embodiment of the present invention.
Hereinafter, a plasma surface treatment apparatus according to an embodiment of the present invention will be described with reference to the accompanying drawings. Embodiments herein are for the purpose of describing the invention only and are not intended to limit the scope thereof.
1 is a schematic diagram of a plasma surface treatment apparatus according to a first embodiment of the present invention. Referring to FIG. 1, the plasma surface treatment apparatus according to the first embodiment of the present invention includes a
The
The
The
The
The gas may be used by directly connecting a gas such as oxygen to the
The gas may be a gas containing an oxygen component such as air, O 2 , N 2 O, etc .; A gas containing a fluorine component such as CF 4 and SF 6 ; A gas containing a chlorine component such as Cl 2 and BCl 3 ; An inert gas such as Ar, N 2 may be used alone or in combination.
The
The internal pressure of the
The
The
The rotary feed through 33 has a
The
Each
The
The second dispersing means 35 is disposed in the
The
In addition, the second dispersing means 35 can vibrate. When the second dispersing means 35 rotates, the second dispersing means 35 vibrates while colliding with the rod-shaped collision means 315 extending from the fixing
The
The
2 is a schematic diagram of a plasma surface treatment apparatus according to a second embodiment of the present invention. Since it is the same as the first embodiment except the vibration means 80 for vibrating the second dispersion means 35, only the vibration means 80 will be described in detail. The same component number is attached | subjected about the same component, and description is abbreviate | omitted.
In this embodiment, the vibration means 80 includes a
3 is a schematic diagram of a plasma surface treatment apparatus according to a third embodiment of the present invention. Since it is the same as the first embodiment except the vibration means 90 for vibrating the second dispersion means 35, only the vibration means will be described in detail.
In the present embodiment, the vibrating means includes a
4 is a schematic diagram of a plasma surface treatment apparatus according to a fourth embodiment of the present invention. The vibration of the second dispersing means 35 using the
In the above, the embodiments of the plasma surface treatment apparatus for fine particles including the fiber / powder / capsules of the present invention have been described with reference to the drawings, but those skilled in the art to which the present invention pertains are based on the above contents. It will be possible to make various applications and modifications within the scope of the invention.
For example, it was described as sealing using a magnetic fluid bearing, but depending on the application, oil seals, bellows seals, O-rings, wilson seals, and Visco seals seals, magnetic-coupling seals, and a variety of dynamic seals are available.
10: plasma generator 20: gas supply device
30: reaction chamber 31: fixed part
32: rotary part 33: rotary feed through
34: first dispersion means 35: second dispersion means
40: first driving means 50: second driving means
60: exhaust unit 70: control unit
Claims (11)
It has an inlet through which the fine particles, which are surface treatment objects, and an outlet are discharged, and having a cylinder-shaped fixing part having at least one end opened and a rotating part rotating the central axis of the cylinder as a rotating shaft in a state where the fixing part is sealed. A reaction chamber; And
And a first driving unit connected to the rotating unit to support the rotating unit and rotate the rotating unit.
And a first dispersing means extending from the rotating part toward the fixing part so as to disperse the fine particles.
Second dispersing means installed to rotate in the reaction chamber to disperse the fine particles; And
Second driving means for supporting and rotating the second dispersing means;
Plasma surface treatment apparatus further comprising a.
And vibrating means connected to said second dispersing means to vibrate said second dispersing means.
The vibration means,
Plasma surface treatment apparatus, characterized in that the impact means is installed in the reaction chamber so as to collide with the rotating second dispersion means.
The vibration means,
motor; A shaft penetrating the fixing part; And an eccentric cam coupled to the shaft and colliding with the second dispersing means while rotating as the motor rotates.
The vibration means,
Plasma surface treatment apparatus is disposed between the fixing portion and the second dispersing means, the vibrator is fixed to the inner surface of the fixing portion so as to vibrate the second dispersing means.
Plasma surface treatment apparatus further comprising a control unit for controlling the drive means and the vibration means, respectively.
The first driving means,
Plasma surface treatment apparatus comprising a motor and a shaft connecting the rotating unit and the motor.
The second driving means,
And a shaft connecting the second dispersing means and the motor through a rotary feed through through the motor and the fixing part.
The second driving means,
Further comprising a hollow shaft for connecting the shaft and the second dispersion means,
The vibration means,
Plasma surface treatment apparatus, characterized in that the vibrator disposed in the inner hollow of the hollow shaft.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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KR1020100005833A KR20110086220A (en) | 2010-01-22 | 2010-01-22 | Apparatus for plasma surface treatment |
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KR1020100005833A KR20110086220A (en) | 2010-01-22 | 2010-01-22 | Apparatus for plasma surface treatment |
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Publication Number | Publication Date |
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KR20110086220A true KR20110086220A (en) | 2011-07-28 |
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KR1020100005833A KR20110086220A (en) | 2010-01-22 | 2010-01-22 | Apparatus for plasma surface treatment |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101507532B1 (en) * | 2012-12-28 | 2015-04-07 | 주식회사 선익시스템 | Thin Film Deposition Apparatus with Vibrator |
KR20200028689A (en) * | 2018-09-07 | 2020-03-17 | 한국기초과학지원연구원 | Plasma equipment for treating powder using vibration |
KR20220000588A (en) * | 2020-06-26 | 2022-01-04 | 한국생산기술연구원 | sputtering device for coating floating fine powder and the coating method thereof |
KR20220072822A (en) * | 2020-11-25 | 2022-06-02 | 울산과학기술원 | Plasma device for surface treatment of powder using flat filter electrode |
-
2010
- 2010-01-22 KR KR1020100005833A patent/KR20110086220A/en not_active Application Discontinuation
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101507532B1 (en) * | 2012-12-28 | 2015-04-07 | 주식회사 선익시스템 | Thin Film Deposition Apparatus with Vibrator |
KR20200028689A (en) * | 2018-09-07 | 2020-03-17 | 한국기초과학지원연구원 | Plasma equipment for treating powder using vibration |
KR20220000588A (en) * | 2020-06-26 | 2022-01-04 | 한국생산기술연구원 | sputtering device for coating floating fine powder and the coating method thereof |
KR20220072822A (en) * | 2020-11-25 | 2022-06-02 | 울산과학기술원 | Plasma device for surface treatment of powder using flat filter electrode |
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