KR20110062495A - Granulated powder for thin rice gruel and preparation method thereof - Google Patents
Granulated powder for thin rice gruel and preparation method thereof Download PDFInfo
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- KR20110062495A KR20110062495A KR1020090119237A KR20090119237A KR20110062495A KR 20110062495 A KR20110062495 A KR 20110062495A KR 1020090119237 A KR1020090119237 A KR 1020090119237A KR 20090119237 A KR20090119237 A KR 20090119237A KR 20110062495 A KR20110062495 A KR 20110062495A
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/143—Cereal granules or flakes to be cooked and eaten hot, e.g. oatmeal; Reformed rice products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/198—Dry unshaped finely divided cereal products, not provided for in groups A23L7/117 - A23L7/196 and A23L29/00, e.g. meal, flour, powder, dried cereal creams or extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/16—Extrusion
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- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
Description
본 발명은 영양이 강화된 인스턴트 쌀미음을 제조할 수 있을 뿐 아니라, 과립화 하지 않은 분말에 비해 재수화능을 향상시킬 수 있는, 압출미 및 유지혼합분말을 포함하는 쌀미음용 과립분말 및 이의 제조방법에 관한 것이다. The present invention not only can produce nutritious instant rice flour, but also can improve the rehydration ability compared to the non-granulated powder, granulated powder for rice fine, including extruded rice and oil and fat mixed powder and its manufacturing method It is about.
최근 국내 쌀 소비량이 지속적인 하락세를 보이고 있는 가운데 우리쌀 살리기에 관한 관심이 급증하면서 다양한 쌀 소비방안의 마련을 통해 새로운 쌀 수요 창출 및 쌀 제품의 개발이 진행되고 있다. 하지만 현재 쌀 가공은 다양한 분야에 적용되고 있지 않아 가공 기술의 향상과 신제품 개발을 통해서 활용성을 제고해 나갈 필요가 있다. Recently, as domestic rice consumption continues to decline, interest in revitalizing our rice has soared, creating new rice demand and developing rice products through various rice consumption plans. However, since rice processing is not applied to various fields, it is necessary to improve its utilization through improvement of processing technology and development of new products.
최근에는 기존의 밀가루를 대체한 쌀 제품의 확장을 통해 쌀 소비 형태를 늘리고자 하는 연구가 활발히 진행되고 있으며, 영양과 건강, 그리고 편의성까지 고려한 인스턴트쌀 가공품은 쌀의 소비를 제고할 수 있는 방안으로 고려되고 있다. Recently, researches to increase the consumption of rice through the expansion of rice products replacing the flour have been actively conducted, and instant rice processed products considering nutrition, health, and convenience are ways to increase the consumption of rice. Is being considered.
환자식은 수술 후 환자가 질병에서 회복되는 정도와 소화 능력에 맞추어 단계적으로 공급되는 식사로 유동식, 연식, 회복식 순으로 주어진다. 이 중 유동식 은 미음이 주가 되어 수술 후 환자, 소화기능이 약화된 환자, 고체음식을 삼키기 힘든 환자 등에게 처음으로 영양분을 공급하는 식사로 3대 영양소와 필수 영양소가 고루 공급되어야 한다. The patient's diet is a diet that is fed in stages according to the degree to which the patient recovers from the disease and his digestive ability. Among them, the formula is the food that provides the first nutrients to patients after surgery, patients with weak digestive function, and patients who have difficulty in swallowing solid foods after surgery, and should be supplied with three major nutrients and essential nutrients.
국내외의 환자식 대부분은 유청 단백질과 같은 우유 단백질을 주요 에너지 급원으로 이용하고 있다. 하지만 국내의 경우에는 곡류 중 특히 쌀을 주요 에너지 급원으로 하는 환자식을 제공하는 것이 쌀이 주식인 한국인에게 더 바람직하다고 판단되며, 이 외의 다른 영양소를 균형있게 제공함으로써 고른 영양섭취가 필요한 환자들을 위한 환자식을 제조할 수 있다. 이외에도 환자식에서는 균형있는 열량공급, 빠른 소화 및 흡수 특성을 지닌 제품을 제조하는 것이 관건인데, 이는 원재료의 선정과 배합비 및 가공방법에 달려있다.Most domestic and international patient foods use milk protein, such as whey protein, as their main source of energy. In Korea, however, the provision of a patient diet with rice as the main source of energy is more desirable for Koreans whose rice is staple, and for patients who need even nutrition by providing a balanced supply of other nutrients. Patient food can be prepared. In addition, the patient's formula is to produce a product with balanced calorie supply, fast digestion and absorption characteristics, which depends on the selection of raw materials, the mixing ratio and the processing method.
환자식에 쌀을 이용하기 위해서는 호화된 쌀가루로 이용할 수 있어야 하며, 분말 형태의 환자식을 제조하는 데에 사용되는 지방 급원인 유지들은 액상이기 때문에 적용하기 어렵고 저장 중 지방산패로 인한 제품의 변질이 쉬운 문제가 있다. 또한, 분말 형태의 식품 원료들이 가지는 단점 중 하나는 입자의 크기가 매우 작으면 표면적이 증가해 입자들끼리 강한 응집력과 케이킹 현상이 일어난다. 예를 들어, 입자의 크기가 20~30 ㎛ 이하일 경우는 반데르발스(Van der waals) 인력과 상호반응력에 의해 입자들끼리 엉기는 현상이 발생할 수 있다. 이렇게 케이킹이 된 입자들은 재수화 시 물의 침투가 어려워져 물에 잘 분산되지 않고 덩어리로 존재하여 제품의 품질 저하에 주요 요인이 된다. In order to use rice for patient food, it must be available as luxurious rice flour, and fat source oils used to make powdered patient food are difficult to apply because they are liquid and easy to deteriorate the product due to fatty acid plaque during storage. there is a problem. In addition, one of the disadvantages of the food ingredients in the form of powder is that when the particle size is very small, the surface area is increased, resulting in strong cohesion and caking phenomenon between the particles. For example, when the particle size is 20 ~ 30 ㎛ or less, the particles may be entangled by the van der waals attraction force and the mutual reaction force. This caking particles are difficult to penetrate the water during rehydration, so they are not dispersed in the water and are present as lumps, which is a major factor in the deterioration of product quality.
상기 종래기술의 문제점을 해결하기 위하여, 본 발명자는 환자식을 압출미로 대체하고자 압출성형 공정을 통해 압출 쌀가루를 제조하였고, 분무건조를 통해 유지를 캡슐화 하였으며, 재수화능 향상을 위해 과립화 함으로써 본 발명을 완성하였다.In order to solve the problems of the prior art, the present inventors manufactured the extruded rice powder through the extrusion molding process to replace the patient's meal with the extruded rice, encapsulated the oil through spray drying, and the present invention by granulating to improve the rehydration capacity Was completed.
이에, 본 발명의 목적은 재수화능이 향상된 쌀미음용 과립분말 및 이의 제조방법을 제공하는 데에 있다.Accordingly, it is an object of the present invention to provide a granulated powder for rice fine rice with improved rehydration ability and a preparation method thereof.
상기 목적을 달성하기 위하여, 본 발명은 압출성형을 통해 얻어진 압출미 60 내지 80 중량% 및 분무건조를 통해 캡슐화한 유지혼합분말 20 내지 40 중량%를 포함하는 것을 특징으로 하는 쌀미음용 과립분말을 제공한다.In order to achieve the above object, the present invention provides granulated powder for rice fine rice, characterized in that it comprises 60 to 80% by weight of the extruded rice obtained through extrusion molding and 20 to 40% by weight of the oil-mixed powder encapsulated through spray drying. do.
상기 유지혼합분말은 중쇄사슬지방, 미강유, 참기름, 들기름, 대두유, 옥수수유, 채종유, 홍화유, 팜유, 올리브유, 해바라기유 및 소맥배아유로 이루어진 군에서 선택된 어느 하나 또는 둘 이상을 포함할 수 있고, 바람직하게는 중쇄사슬지방, 미강유 및 참기름을 포함할 수 있으며, 유청단백질을 코팅 소재로 이용하여 상기 유지혼합분말을 캡슐화 할 수 있다.The oil-mixed powder may include any one or two selected from the group consisting of medium chain chain fat, rice bran oil, sesame oil, perilla oil, soybean oil, corn oil, rapeseed oil, safflower oil, palm oil, olive oil, sunflower oil and wheat germ oil. Preferably, it may include heavy chain fat, rice bran oil and sesame oil, and may use the whey protein as a coating material to encapsulate the oil-mixed powder.
또한, 본 발명의 쌀미음용 과립분말은 추가로 현미가루, 검은콩 분말, 검은깨 분말, 브로콜리 분말, 전란 분말, 양파 분말, 당근 분말, 표고버섯 분말, 양송이버섯 분말, 자일리톨 및 소금으로 이루어진 군에서 선택된 어느 하나 또는 둘 이 상을 포함할 수 있다.In addition, the granule powder for rice brewing of the present invention is in the group consisting of brown rice flour, black bean powder, black sesame powder, broccoli powder, whole egg powder, onion powder, carrot powder, shiitake mushroom powder, mushroom mushroom powder, xylitol and salt It may include any one or more than two selected.
또한, 본 발명의 쌀미음용 과립분말은 압출미 30 내지 60 중량%, 현미가루 5 내지 20 중량%, 검은콩 분말 1 내지 10 중량%, 중쇄사슬지방 1 내지 10 중량%, 미강유 1 내지 10 중량%, 유청단백질 5 내지 20 중량% 및 자일리톨 10 내지 20 중량%를 포함할 수 있다.In addition, the granulated powder for rice wine of the present invention is 30 to 60% by weight extruded rice, 5 to 20% by weight brown rice powder, 1 to 10% by weight black bean powder, 1 to 10% by weight heavy chain fat, 1 to 10% by weight rice bran oil , 5 to 20 wt% whey protein and 10 to 20 wt% xylitol.
바람직하게는, 상기 과립분말은 압출미 40 내지 55 중량%, 현미가루 5 내지 15 중량%, 검은콩 분말 2 내지 8 중량%, 검은깨 분말 0.5 내지 1 중량%, 브로콜리 분말 0.5 내지 1 중량%, 전란 분말 2 내지 5 중량%, 양파 분말 0.5 내지 1 중량%, 당근 분말 0.5 내지 1 중량%, 표고버섯 분말 0.2 내지 0.5 중량%, 양송이버섯 분말 0.2 내지 0.5 중량%, 중쇄사슬지방 2 내지 3 중량%, 미강유 1.5 내지 2.5 중량%, 참기름 0.1 내지 0.5 중량%, 유청단백질 8 내지 15 중량%, 자일리톨 10 내지 15 중량% 및 소금 2 내지 2.5 중량%를 포함할 수 있다.Preferably, the granulated powder is 40 to 55% by weight extruded rice, 5 to 15% by weight brown rice flour, 2 to 8% by weight black bean powder, 0.5 to 1% by weight black sesame powder, 0.5 to 1% by weight broccoli powder, 2-5 wt% of whole egg powder, 0.5-1 wt% of onion powder, 0.5-1 wt% of carrot powder, 0.2-0.5 wt% of shiitake mushroom powder, 0.2-0.5 wt% of mushroom mushroom powder, 2-3 wt% of medium chain fat It may include 1.5 to 2.5 wt% of rice bran oil, 0.1 to 0.5 wt% of sesame oil, 8 to 15 wt% of whey protein, 10 to 15 wt% of xylitol, and 2 to 2.5 wt% of salt.
또한, 본 발명은 압출성형을 이용하여 압출한 압출쌀을 분쇄하는 압출미 제조단계; 분무건조를 이용하여 유지혼합물을 캡슐화하는 유지혼합분말 제조단계; 및 압출미와 유지혼합분말을 혼합한 혼합분말을 유동층 과립건조를 통해 과립화하는 과립단계를 포함하여 이루어지는 것을 특징으로 하는 쌀미음용 과립분말의 제조방법을 제공한다.In addition, the present invention is an extruded rice manufacturing step of grinding the extruded rice extruded using extrusion molding; Oil-mixing powder manufacturing step of encapsulating the oil-fat mixture by spray drying; And a granulating step of granulating the mixed powder obtained by mixing the extruded rice and the oil mixed powder through fluid bed granulation drying.
상기 압출미 제조단계는 원료공급량 18 내지 30 kg/h 및 분쇄선속도 80 내지 100 m/s의 조건 하에서 압출쌀을 분쇄할 수 있고, 상기 유지혼합분말 제조단계는 유청단백질을 물에 용해시키는 용해단계; 상기 유청단백질 용액에 유지를 첨가하는 첨가단계; 상기 용액을 분산시켜 수중유적형 유화액을 제조하는 분산단계; 및 상기 수중유적형 유화액을 분무건조하는 분무건조단계를 포함하여 이루어질 수 있다.The extruded rice manufacturing step may grind the extruded rice under the conditions of the raw material feed amount of 18 to 30 kg / h and the crushing wire speed of 80 to 100 m / s, the oil-mixed powder manufacturing step is dissolved to dissolve whey protein in water step; Adding an oil or fat to the whey protein solution; A dispersion step of dispersing the solution to prepare an oil-in-water emulsion; And a spray drying step of spray drying the oil-in-water emulsion.
이하, 본 발명을 보다 상세하게 설명한다.Hereinafter, the present invention will be described in more detail.
환자식에 쌀을 이용하기 위해서는 압출성형하여 호화된 쌀을 가루화하여 이용하는 것이 바람직하며, 이때 압출성형 공정은 비용이 적게 들고 연속적으로 제조할 수 있는 장점이 있다. 또한 고온단시간 공정을 거치기 때문에 적은 양의 수분으로도 전분의 호화가 가능하다. 압출미 분말의 기능성과 소화 특성은 제품의 부가가치를 향상시키는데 사용될 수 있다.In order to use the rice in the patient formula, it is preferable to use the powdered rice by extruding and luxury, wherein the extrusion process has the advantage of being able to manufacture continuously and low cost. In addition, because of the high temperature and short time process, starch can be gelatinized even with a small amount of moisture. The functionality and extinguishing properties of the extruded fine powder can be used to enhance the added value of the product.
본 발명에서 사용되는 압출미는 일정한 수분을 지닌 쌀을 110 내지 130℃의 고온 및 3.62 내지 6.98 Mpa의 압력 하에서 압출성형한 후 얻어진 압출물을 18 내지 30 kg/h 및 분쇄선속도 80 내지 100 m/s의 조건 하에서 분쇄하고, 35 mesh 이하의 압출 쌀가루를 선별함으로써 제조할 수 있다. The extruded rice used in the present invention is 18 to 30 kg / h and grinding wire speed 80 to 100 m / after extruding the rice having a constant moisture at a high temperature of 110 to 130 ℃ and pressure of 3.62 to 6.98 Mpa It can be prepared by grinding under the conditions of s, and sorting extruded rice flour of 35 mesh or less.
이때, 상기 온도 및 압력 범위를 벗어나 압출 성형하면 호화가 완전히 일어나지 않아 재수화능이 떨어지는 문제가 야기될 수 있고, 상기 분쇄 조건을 벗어나 분쇄하면 수율과 수용성이 떨어지는 문제가 야기될 수 있다.At this time, if the extrusion molding outside the temperature and pressure range does not completely occur gelatinization may cause a problem that the rehydration capacity is lowered, when the grinding is out of the grinding conditions may cause a problem that the yield and water solubility falls.
한편, 환자식은 액상 유동식과 더불어 유통과 저장, 편의성을 위해 분말화하여 온수에 타서 음용될 수 있는 형태로 제조된다. 환자식에서 이러한 분말 형태의 환자식을 제조하는데 있어서 대부분의 원료들이 가루인 반면 지방 급원인 유지들은 액상이기 때문에 적용하기 어렵고 저장 중 지방산패로 인한 제품의 변질이 쉽다. 특히, 지방 급원의 대부분은 소화와 흡수가 빠른 중쇄사슬지방(medium chain triglyceride, MCT), 식물성 유지 등을 사용하며, 이러한 유지에 저장 안정성 부여를 위하여 유지를 유화시킨 후 유화액을 분무건조하여 분말화 할 수 있다. 분무건조를 통해 캡슐화된 유지 분말은 원료 배합시 공정이 간편하고 최종 제품의 저장성이 증대될 수 있다. On the other hand, the patient's formula is prepared in a form that can be drinkable by burning in hot water powdered for distribution, storage, and convenience along with the liquid flow. While most of the raw materials are powders in the production of patient forms in patient forms, fat-sourced fats and oils are liquid and therefore difficult to apply and the product is easily deteriorated due to fatty plaques during storage. In particular, most of the fat source uses medium chain triglycerides (MCT), vegetable oils, etc., which are quickly digested and absorbed, and the oils are emulsified to impart storage stability to these oils, followed by spray-drying the emulsion to be powdered. can do. The fat or oil powder encapsulated through spray drying may be easy to process the raw materials and increase the shelf life of the final product.
유지의 캡슐화에 사용될 O/W 유화액 제조를 위하여 유화 특성이 좋고 단백질 급원으로 이용할 수 있는 유청단백질(whey protein isolate, WPI)을 바람직한 코팅 소재로 이용할 수 있다. 이때, 유지 1 중량부에 대하여 유청단백질을 65 내지 90 중량부로 사용할 수 있고, 만약 상기 범위를 벗어나 유청단백질을 과량 또는 소량 사용하면 O/W 유화액의 혼합이 완전히 되지 않고 층이 분리되는 문제가 야기될 수 있다.Whey protein isolate (WPI), which has good emulsification properties and can be used as a protein source, can be used as a preferred coating material for the preparation of O / W emulsions to be used for encapsulation of fats and oils. At this time, the whey protein may be used in an amount of 65 to 90 parts by weight based on 1 part by weight of oil, and if the whey protein is used in an excessive or small amount out of the above range, the O / W emulsion may not be completely mixed and the layers may be separated. Can be.
또한, 상기 유화액을 투입구 온도 170 내지 185℃, 토출구 온도 75 내지 85℃의 조건 하에서 분무건조하여 캡슐화된 유지분말을 제조할 수 있다.In addition, the emulsion may be spray-dried under the conditions of the inlet temperature of 170 to 185 ℃, the outlet temperature of 75 to 85 ℃ can be prepared an encapsulated fat powder.
또한, 분말 형태의 식품 원료들이 가지는 단점인 강한 응집력과 케이킹 현상을 방지하기 위하여, 유동층 과립기를 이용하여 분말을 과립화할 수 있다. 과립화를 하면 가해진 수분에 의해 입자들이 수분을 흡착함으로써 입자 사이 공극에 수분층이 형성되며, 건조과정을 통해 수분이 기화되면 수분이 있던 자리는 공기층이 형성되어 궁극적으로 다공성 및 수분의 재흡수에 용이한 구조가 된다. 이러한 분말은 차후 가수 시 수분 흡착을 용이하게 하여 재수화능이 향상될 수 있다.In addition, the powder may be granulated using a fluidized bed granulator to prevent strong cohesion and caking, which are disadvantages of the food ingredients in powder form. When granulation, the moisture adsorbs the moisture by the added moisture, forming a moisture layer in the pores between the particles. When moisture is vaporized through the drying process, an air layer is formed in the place where the moisture was present, ultimately facilitating the resorption of porosity and moisture. It becomes a structure. Such powders may facilitate moisture adsorption during subsequent hydrolysis, thereby improving rehydration ability.
보다 상세하게는, 압출미와 유지혼합분말을 혼합한 혼합분말을 유동층 과립 건조기에 넣고 투입구 온도 70 내지 90℃, 분무 시간 2 내지 5초, 건조 시간 40 내 지 50 초, 총 과립 시간 40 내지 100 분의 조건 하에서 과립화를 수행할 수 있다.More specifically, the mixed powder mixed with the extruded rice and the oil-mixed powder is placed in a fluidized bed granule dryer, and the inlet temperature 70 to 90 ℃,
물론, 압출미와 유지혼합분말 혼합 시에는 추가로 현미가루, 검은콩 분말, 검은깨 분말, 브로콜리 분말, 전란 분말, 양파 분말, 당근 분말, 표고버섯 분말, 양송이버섯 분말, 자일리톨 및 소금으로 이루어진 군에서 선택된 어느 하나 또는 둘 이상을 포함할 수 있으며, 균형있는 영양을 제공할 수 있다면 상기 재료 이외의 다른 재료가 추가될 수 있음은 당연하다. Of course, when mixing the extruded rice and oil-mixed powder in the group consisting of brown rice powder, black bean powder, black sesame powder, broccoli powder, whole egg powder, onion powder, carrot powder, shiitake powder, mushroom mushroom powder, xylitol and salt It may be any one or two or more selected, it is natural that other materials than the above may be added if it can provide a balanced nutrition.
본 발명의 쌀미음용 과립분말에 포함되는 재료들은 3대 영양소 함량에 따라 크게 탄수화물과 단백질, 지방 급원으로 분류하여 조절할 수 있다. 탄수화물 급원으로는 압출미, 현미가루가 사용되었는데 현미는 영양소가 풍부하고 혈중 콜레스테롤을 낮추는 기능을 한다. The ingredients included in the granulated powder for rice bran of the present invention can be classified and controlled into carbohydrates, proteins, and fat sources according to three major nutrient contents. Extruded rice and brown rice flour were used as carbohydrate sources. Brown rice is rich in nutrients and functions to lower blood cholesterol.
단백질 급원으로 사용된 유청단백질, 검은콩 분말, 전란 분말 중 유청단백질은 단백질 함량을 90% 이상 농축시킨 제품으로 유화작용 외에 우수한 단백질 급원 뿐 아니라 항산화 효과도 있다. 또한 환자에게 있어 질 좋은 단백질의 공급이 무엇보다 중요한데 육류보다 콩류에서 얻는 단백질은 암 예방에도 도움이 된다. Whey protein among whey protein, black soybean powder and whole egg powder used as protein source is a product with more than 90% concentration of protein. In addition to emulsification, it has excellent protein source as well as antioxidant effect. In addition, the supply of quality protein is most important for patients, protein from legumes rather than meat can help prevent cancer.
지방 급원으로는 MCT, 미강유, 참기름 등이 사용될 수 있고, MCT는 기존의 장쇄사슬지방(long chain triglyceride, LCT)과는 다르게 분해시 췌장 리파아제나 담즙산을 필요로 하지 않는다. 따라서, 간까지 도달하는 시간이 짧아 빠른 소화와 흡수가 가능한 장점 때문에 대부분의 환자식에서 지방 급원으로 사용된다. 토코트리엔올(tocotrienol)이 많이 함유된 미강유는 콜레스테롤 합성을 방해하여 혈중 LDL수치를 낮추는 기능을 한다. 참기름은 항산화 효과와 향미 개선 차원에서 첨가 할 수 있고, 마지막으로 양파분말, 당근분말, 브로콜리 분말, 검은깨분말, 버섯 분말은 미량 첨가하여 맛과 영양을 향상시킬 수 있다. As a fat source, MCT, rice bran oil, sesame oil, etc. may be used, and unlike conventional long chain triglycerides (LCT), MCT does not require pancreatic lipase or bile acid. Therefore, it is used as a fat source in most patient foods because of the short time to reach the liver, which enables fast digestion and absorption. Rice bran oil, which is high in tocotrienol, interferes with cholesterol synthesis and lowers LDL levels in the blood. Sesame oil can be added for antioxidant and flavor improvement. Finally, a small amount of onion powder, carrot powder, broccoli powder, black sesame powder, and mushroom powder can be added to improve taste and nutrition.
또한, 미음의 맛을 조절하기 위하여 자일리톨과 소금이 사용될 수 있고, 자일리톨은 대표적인 당알코올로 낮은 칼로리와 낮은 GI(Glycemic Index)로 인해 당뇨병 환자가 섭취해도 무리가 없으면서 설탕과 감미도가 비슷하다.In addition, xylitol and salt may be used to control taste of taste, and xylitol is a representative sugar alcohol due to low calories and low GI (Glycemic Index).
환자식은 목적에 따라 성분과 함량이 각기 다르며 일반적으로 3대 영양소를고루 함유하고 있어야 한다. 특히 단백질 공급이 일반 식이보다 약간 높아야 한다. 한국인영양섭취기준에 의한 에너지 적정 비율은 20세 이상 성인을 기준으로 단백질:지방:탄수화물의 비율이 7∼20 : 15∼25 : 55∼70이며(한국영양학회, 2005), 본 발명에서는 이를 근거로 에너지 비율이 적절하게 구성되도록 설계하였다. Patient foods vary in composition and content depending on the purpose and should generally contain three major nutrients. In particular, the protein supply should be slightly higher than the regular diet. The ratio of energy titration according to the Korean nutrient intake standard is 7-20: 15-25: 55-70 based on adults over 20 years old (Korea Nutrition Society, 2005), and the present invention The furnace energy ratio is designed to be properly configured.
본 발명에 따른 쌀미음용 과립분말은 과립화 하지 않은 분말보다 지방 함량과 단백질 함량이 각각 0.9, 1.9% 높게 나타난 반면, 탄수화물 함량은 상대적으로 3.2% 낮게 나타났다. 과립분말의 단백질 조성은 71.1 내지 118.5 g으로 1일 권장 단백질 섭취량 45 내지 55 g보다 많았는데, 이는 일반적인 환자식이 지니는 공통적인 특성이다. In the rice flour granule powder according to the present invention, the fat content and the protein content were 0.9 and 1.9% higher than the non-granulated powder, respectively, while the carbohydrate content was relatively 3.2% lower. The protein composition of the granular powder was 71.1 to 118.5 g, which was higher than the recommended daily protein intake of 45 to 55 g, which is a common feature of the general patient diet.
또한, 분말 입자의 침강 속도를 보여주는 분산성의 경우 과립분말(93.7%)은 과립화 하지 않은 혼합분말(77.0%)보다 높게 나타났고, 재수화에 걸리는 시간도 과립분말(122.3 초)이 과립화 하지 않은 혼합분말(305.3 초)보다 빨랐으며 이러한 결과들로부터 과립공정이 분말의 재수화능을 향상시킬 수 있음을 나타낸다.In addition, in the case of dispersibility showing the sedimentation rate of the powder particles, the granulated powder (93.7%) was higher than the non-granulated mixed powder (77.0%), and the time required for rehydration was not granulated (122.3 seconds). It was faster than the mixed powder (305.3 seconds), and these results indicate that the granulation process can improve the powder's rehydration ability.
본 발명에 따른 쌀미음용 과립분말을 이용하면, 영양과 건강, 그리고 편의성까지 고려한 인스턴트 쌀가공 제품을 개발할 수 있어 기존의 우유단백질 위주의 환자식을 압출미로 대체하여 영양이 강화된 인스턴트 쌀미음을 제조할 수 있을 뿐 아니라, 과립화 하지 않은 분말에 비해 재수화능을 향상시킬 수 있다. Using rice granule powder according to the present invention, it is possible to develop instant rice processing products considering nutrition, health, and convenience to manufacture instant rice taste with enhanced nutrition by replacing existing milk protein-oriented patient food with extruded rice. Not only can this be done, but the rehydrating ability can be improved compared to the non-granulated powder.
이하, 하기 실시예를 통해 본 발명을 보다 상세하게 설명한다. 다만, 이러한 실시예에 의해 본 발명이 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to the following examples. However, the present invention is not limited by these examples.
<실시예 1> 압출미의 제조Example 1 Preparation of Extruded Rice
실험에 사용된 쌀은 ㈜화촌농산(수라벼, 2008)에서 구입하여 실온에 보관하며사용하였다. 압출성형 공정은 특별히 세척을 하지 않아도 고온 고압에서 공정이 이루어지기 때문에 충분한 살균효과를 줄 수가 있다. 따라서 수분조건 27%의 쌀을 압출성형기의 투입구를 통하여 공급되었다. Rice used in the experiment was purchased from Hwachon Nongsan (Sura Rice, 2008) and stored at room temperature. Extrusion process can give a sufficient sterilization effect because the process is performed at high temperature and high pressure even without special washing. Therefore, rice of 27% of moisture condition was supplied through the inlet of the extruder.
사용된 장비는 이축 압출성형기(co-rotating intermeshing type twin-screw extruder, STS-25HS, Hankook E.M. Ltd., Gyeonggi-do, Korea)로서 총 8개의 section이 연결된 형태의 배럴(barrel)을 가지고 있으며, L/D의 비가 32:1 이고 축(screw)의 직경은 32 mm였다. 다이(die)는 직경이 4 mm, L/D 7인 원형타입을 사용하였다. 제조 조건은 배럴온도 120℃, 원료수분함량 27%, 축 회전속도 300 rpm으로 작동되었다. The equipment used is a co-rotating intermeshing type twin-screw extruder (STS-25HS, Hankook EM Ltd., Gyeonggi-do, Korea) and has a barrel with a total of eight sections. The ratio of L / D was 32: 1 and the diameter of the screw was 32 mm. The die used was a circular type having a diameter of 4 mm, L / D 7. The production conditions were operated at a barrel temperature of 120 ° C., a water content of 27%, and an axis rotation speed of 300 rpm.
제조된 압출물은 기류식 초미분쇄기(HKP-05, Korea Energy Technology, Seoul, Korea)를 이용하여 원료공급량 18∼30 kg/h, 분쇄선속도 80∼100 m/s의 조건하에 분쇄 되었으며, 35 mesh 이하의 압출 쌀가루만을 선별하여 냉장 보관하면서 사용하였다.The produced extrudate was pulverized under the conditions of 18 ~ 30 kg / h raw material feed rate and 80 ~ 100 m / s grinding speed by using an airflow ultra fine grinding machine (HKP-05, Korea Energy Technology, Seoul, Korea). Only the extruded rice powder below the mesh was selected and used while refrigerated.
<실시예 2> 유화액의 제조 및 분무건조Example 2 Preparation of Emulsion and Spray Drying
유지 형태의 재료와 분말 형태인 나머지 재료들을 동시에 섞으면 엉김현상이 일어나고 재수화시 기름 층과 물 층이 분리되는 현상이 일어나며, 또한 유지는 그 자체로 저장 중 쉽게 산패되어 산패취가 발생할 수 있다. 따라서 유지 원료의 변질억제 및 혼합성을 향상시키기 위하여 캡슐화 과정을 수행하였다. Mixing the fat and oil materials with the rest of the powder at the same time results in entanglement and separation of the oil and water layers during rehydration, and fats and fats can easily dissipate during storage, causing rancidity. Therefore, the encapsulation process was performed in order to improve the quality control and miscibility of fats and oils.
이를 위하여 코팅 물질로 분리유청단백(whey protein isolate, WPI)을 이용하여 캡슐화하였고 이로 인해 지방의 산패 방지와 특유의 이취를 억제하는 효과를 얻을 수 있었다. To this end, encapsulation was carried out using whey protein isolate (WPI) as a coating material, which prevented the rancidity of fat and suppressed the off-flavor.
구체적인 캡슐화 공정은 다음과 같다. 즉, 증류수 900 mL에 WPI 70 g을 넣고 교반기(overhead stirrer, MS3040, Mtops, Gyeonggi-do, Korea)를 이용하여 완전히 용해될 때까지 400 rpm에서 30분간 교반한 후 WPI 용액에 MCT:미강유:참기름이 50:45:5 (중량%)로 혼합된 유지를 30 g 첨가하였다. 이 후 초음파 파쇄기(VCX750, Sonics & Materials Inc., Newtown, CT, USA)를 이용하여 750 W에서 20분간 분산시켰다. Specific encapsulation process is as follows. In other words, add 70 g of WPI to 900 mL of distilled water and stir for 30 minutes at 400 rpm until completely dissolved using a stirrer (overhead stirrer, MS3040, Mtops, Gyeonggi-do, Korea), and then add MCT: rice bran oil to sesame oil. 30 g of the fats and oils mixed at this 50: 45: 5 (weight%) were added. This was followed by dispersion for 20 minutes at 750 W using an ultrasonic crusher (VCX750, Sonics & Materials Inc., Newtown, CT, USA).
제조된 수중유적형(oil-in-water, O/W) 유화액은 분무건조기(SD-1000, EYELA, Tokyo, Japan)를 이용하여 투입구 온도 180℃, 토출구 온도 80℃, 아토마이저 공기 압력 20 kPa, 원료액 투입 속도 50-55 mL/min의 조건에서 분무건조 하였 다. 제조된 분말은 유지혼합분말로 명명되었다.The prepared oil-in-water (O / W) emulsion was spray-dried (SD-1000, EYELA, Tokyo, Japan) using an inlet temperature of 180 ° C, an outlet temperature of 80 ° C, and an atomizer air pressure of 20 kPa. Spray drying was carried out at 50-55 mL / min. The prepared powder was named as a fat-mixed powder.
<실시예 3> 원료 혼합 레시피 결정 및 혼합분말 제조<Example 3> Raw material mixed recipe crystal and mixed powder preparation
실시예 1에서 제조된 압출미 57 g, 현미가루 10 g, 검은콩 분말 5 g, 검은깨 분말 1 g, 브로콜리 분말 1 g, 전란 분말 3 g, 양파 분말 1 g, 당근 분말 1 g, 표고버섯 분말 0.5 g, 양송이버섯 분말 0.5 g 및 실시예 2에서 제조된 유지혼합분말 15 g을 함께 믹서기에 넣고 5분간 섞고 2분간 쉬는 방식으로 총 15분간 고루 섞어 주었다. 이렇게 만들어진 혼합분말은 4℃에서 냉장보관 하며 사용하였다. 57 g extruded rice prepared in Example 1, brown rice powder 10 g, black bean powder 5 g, black sesame powder 1 g, broccoli powder 1 g, whole egg powder 3 g, onion powder 1 g, carrot powder 1 g, shiitake mushroom 0.5 g of powder, 0.5 g of mushroom mushroom powder, and 15 g of the oil-mixed powder prepared in Example 2 were put together in a blender and mixed for 5 minutes and mixed for a total of 15 minutes by resting for 2 minutes. The mixed powder thus prepared was used while refrigerated at 4 ℃.
<실시예 4> 유동층 과립기를 이용한 과립화Example 4 Granulation Using a Fluidized Bed Granulator
혼합분말의 재수화능을 개선하기 위하여 실시예 3에서 제조한 혼합분말을 이용해 추가로 과립화를 하였다. 과립화 공정은 혼합분말 200 g을 유동층 과립 건조기(fluid bed spray granulator, DK-FGP, DooKoo machine, Seoul, Korea)에 넣어 투입구 온도 80℃, 분무 시간 3 초, 건조 시간 50 초 조건에서 수행하였으며 결착제로는 60℃의 온수만을 이용하여 50분간 과립화하였다. In order to improve the rehydration ability of the mixed powder it was further granulated using the mixed powder prepared in Example 3. The granulation process was carried out at 200 ° C. in a fluid bed spray granulator (DK-FGP, DooKoo machine, Seoul, Korea) at an inlet temperature of 80 ° C., spray time 3 seconds, and drying time 50 seconds. Zero was granulated for 50 minutes using only hot water at 60 ° C.
과립화한 분말 중 40 mesh 이하인 것을 선별하여 4℃의 온도에서 냉장보관 하며 사용하였다. 이렇게 얻어진 과립분말에서는 육안으로 확인했을 때 거의 관찰되지 않았다.Among the granulated powder, those which were 40 mesh or less were selected and refrigerated at 4 ° C. It was hardly observed in the granule powder thus obtained when visually confirmed.
<실험예 1> 일반성분 및 열량비 분석Experimental Example 1 Analysis of General Components and Calorie Ratio
1) 일반성분 분석1) General Ingredient Analysis
실시예에서 제조한 과립분말의 수분함량은 105℃ 상압 가열 건조법, 조지방 함량은 Soxhlet법, 조단백질 함량은 Kjeldahl법, 조회분 함량은 550℃에서 직접회 화법으로 분석하였다(AOAC, 1995). 모든 결과는 3회 반복 실험한 측정치의 평균값으로 나타내었다. 이를 바탕으로 총 탄수화물 함량은 회분, 조단백질, 조지방, 수분의 함량을 제외한 나머지 부분으로 산출하였다.The moisture content of the granule powder prepared in Example was analyzed by direct heating method at 105 ° C atmospheric pressure drying, crude fat content by Soxhlet method, crude protein content by Kjeldahl method, and crude ash content by 550 ° C (AOAC, 1995). All results are expressed as the mean value of three repeated experiments. Based on this, the total carbohydrate content was calculated as the remainder except ash, crude protein, crude fat, and water content.
그 결과, 하기 표 1과 같이, 과립분말과 혼합분말의 탄수화물이 각각 68.4%, 71.6%로 가장 많이 함유되어 있었고, 수분은 각각 2.9±0.2% 및 2.8±0.2%, 조단백질은 각각 17.2±0.3% 및 15.2±0.3%, 조회분은 각각 3.2±0.1% 및 3.0±0.0%, 그리고 조지방은 각각 8.3±0.5% 및 7.4±0.2% 함유된 것으로 분석되었다. As a result, as shown in Table 1, the carbohydrate of the granulated powder and the mixed powder was the most contained 68.4%, 71.6%, respectively, the water content of 2.9 ± 0.2% and 2.8 ± 0.2%, crude protein 17.2 ± 0.3%, respectively And 15.2 ± 0.3%, crude ash contained 3.2 ± 0.1% and 3.0 ± 0.0%, and crude fat contained 8.3 ± 0.5% and 7.4 ± 0.2%, respectively.
두 시료의 배합비는 동일하지만 일반성분에서 이와 같은 차이가 나는 이유는 과립공정의 차이 때문으로 판단된다. 유동층 과립 공정은 결착제로 수분을 이용하기 때문에 수분함량이 약 0.2% 증가하였고, 과립화 시 형성된 수분층은 지질에 대한 보호 역할을 제공하기 때문에 지질의 산패를 억제할 수 있다. 따라서, 과립 후의 시료가 과립 전보다 약 0.9%의 지방 함량이 증가하였고, 단백질 함량도 약 1.9% 증가하였다. 탄수화물의 함량이 3.2% 감소한 것은 탄수화물의 함량이 감소한 것이 아니라 지방과 단백질의 양이 증가해 상대적으로 감소한 것으로 나타난 것이다. The mixing ratio of the two samples is the same, but the reason for this difference in the general ingredients is considered to be due to the difference in granulation process. In the fluidized bed granulation process, the water content increased by about 0.2% due to the use of water as a binder, and the water layer formed during granulation provides a protective role for lipids, thereby suppressing the rancidity of lipids. Thus, the sample after the granulation increased the fat content by about 0.9% and the protein content by about 1.9% than before the granulation. The 3.2% reduction in carbohydrates was not a decrease in carbohydrates, but rather a decrease in fat and protein.
2) 열량비 분석2) Calorie Ratio Analysis
일반성분분석을 통한 시료의 열량비는 하기 표 2와 같다. 즉, 과립분말의 열량비는 16.5 : 17.9 : 65.6, 배합분말의 열량비는 14.7 : 16.2 : 69.1 로 분석되었다. Calorie ratio of the sample through the general component analysis is shown in Table 2 below. That is, the calorie ratio of the granular powder was 16.5: 17.9: 65.6, and the calorie ratio of the blended powder was 14.7: 16.2: 69.1.
이 결과는 20세 이상 성인을 기준으로 조사된 한국인영양섭취기준에 의한 에너지적정비율 즉, 단백질:지방:탄수화물 7~20:15~25:55~70 측면에 부합하였다. 입원환자, 또는 암, AIDS, 결핵, 흡수불량증, 신장과 간질환, 식욕감퇴증이 있는 환자들에게서 단백질 결핍이 자주 발생한다. 체내에 질소평형 유지 외에 체단백질의 축적 등의 요인에 의한 추가 단백질이 필요하기 때문이다. 그렇기 때문에 환자식은 단백질 공급량이 일반 식이보다 높아야 한다. The results were in line with the energy-adjusted ratio according to the Korean nutrient intake standard surveyed for adults over 20 years old, that is, protein: fat: carbohydrate 7 ~ 20: 15 ~ 25: 55 ~ 70. Protein deficiency often occurs in hospitalized patients, or in patients with cancer, AIDS, tuberculosis, malabsorption, kidney and liver disease, and loss of appetite. This is because in addition to maintaining nitrogen balance in the body, additional proteins are required due to factors such as accumulation of body proteins. For this reason, the patient's diet should be higher than the normal diet.
30세 성인 남녀의 에너지 필요추정량에 따르면 평균 1800~3000 kcal/일 의 에너지가 필요하다. 본 발명에서 제조한 과립분말의 경우 100 g 당 417.1 kcal/g의 열량이 공급되므로 하루에 431.6~719.3 g 씩 공급한다고 가정했을 때 단백질 공급량이 71.1~118.5 g/일로 기준치(45~55 g/일)보다 높은 수준을 보였다. Estimates of energy needs for men and women of 30 years of age require an average of 1800 to 3000 kcal / day. Since the granule powder prepared in the present invention is supplied with 417.1 kcal / g of calories per 100 g, the protein supply amount is 71.1 to 118.5 g / day based on assuming that 431.6 to 719.3 g is supplied per day (45 to 55 g / day). Higher than).
열량비는 시료의 단백질, 지방, 탄수화물의 비율에 Atwater 계수 즉, 단백질4 kcal/g, 지방 9 kcal/g, 탄수화물 4 kcal/g을 각각 곱하여 3대 영양소를 100%로 환산하여 계산하였다.The calorie ratio was calculated by multiplying the ratio of protein, fat and carbohydrate by the Atwater coefficient, that is,
<실험예 2> 재수화능 분석Experimental Example 2 Rehydration Analysis
1) 분산성 측정1) Dispersibility Measurement
혼탁도를 통한 분산성의 측정은 시료 0.1 g을 pH 7.4의 인산 완충 생리식염수(D-PBS D5652, Sigma-Aldrich, Steinheim, Germany) 용액 50 mL에 넣고 500 rpm에서 10분 간 교반한 후, 3 mL를 cuvette에 넣고 분광광도계(DU 730, Beckman Coulter Inc., Fullerton, CA, USA)로 650 nm에서 혼탁도를 측정하였다. 혼탁도는 매 1분 간격으로 총 10분간 측정되었다.To measure the dispersibility through turbidity, 0.1 g of the sample was added to 50 mL of a solution of phosphate buffered saline (D-PBS D5652, Sigma-Aldrich, Steinheim, Germany) at pH 7.4, stirred at 500 rpm for 10 minutes, and then 3 mL. The turbidity was measured at 650 nm in a cuvette and spectrophotometer (DU 730, Beckman Coulter Inc., Fullerton, CA, USA). Turbidity was measured every 10 minutes for a total of 10 minutes.
재수화능 분석을 위한 분산성 측정은 A/S Niro Atomizer(1978)의 방법을 변형하여 사용하였다. 즉, 증류수 30 mL를 50 mL 비커에 담고 자석교반기(MS-MP4, DAIHAN Scientific, Co., Ltd., Seoul, Korea) 500 rpm으로 교반 시키면서 시료 약 2 g을 위에서 천천히 가해주었다. 시료가 처음 들어가는 순간부터 30 초가 지나면 25 mesh의 sieve에 모두 걸러 미리 항량된 알루미늄 접시에 담았다. 시료가 담긴 알루미늄 접시를 건조 오븐에 넣어 105℃에서 4 시간 동안 건조시킨 후 무게를 측정하였고, 분산성은 다음과 같이 계산하였다.Dispersibility measurement for rehydration analysis was used by modifying the method of A / S Niro Atomizer (1978). That is, 30 mL of distilled water was added to a 50 mL beaker, and about 2 g of the sample was slowly added thereto while stirring at 500 rpm with a magnetic stirrer (MS-MP4, DAIHAN Scientific, Co., Ltd., Seoul, Korea). After 30 seconds from the beginning of the sample, all were filtered through 25 mesh sieve and placed in a pre-weighed aluminum dish. The aluminum dish containing the sample was put in a drying oven and dried at 105 ° C. for 4 hours, and then weighed. The dispersibility was calculated as follows.
여기서, a=시료양 (g), b=시료의 수분 함량, c=체를 통과한 분산액을 건조한 후 고형분의 양 (g)Where a = sample amount (g), b = water content of the sample, c = amount of solids after drying the dispersion passed through the sieve (g)
도 1은 물 속에 분산된 혼합분말과 과립분말의 시간에 따른 안정도를 나타낸 것으로, 분산성이 좋은 분말은 수중에 고르게 분산되어 오랫동안 침전이나 부유 없이 상태를 유지하기 때문에 시간에 따른 혼탁도의 변화가 적다. 반대로 분산도가 나쁜 분말은 시간에 따라 분말이 침강하거나 부유하기 때문에 층 분리가 생겨 결과적으로 시료의 혼탁도가 작아지게 된다. 혼합분말과 과립분말 모두 시간이 지남에 따라 혼탁도가 감소하는 결과를 얻었다. 이는 분말이 시간이 지남에 따라 점차 가라앉는다는 것을 의미한다. 인스턴트 쌀 미음에는 압출을 통해 알파화한 쌀가루가 45% 이상이 첨가되어 있기 때문에 시간에 따른 이들의 침전이 주요 원인이다. 이러한 결과는 곡류를 기반으로 한 미음, 스프 등의 점성 식품에서 공통적인 특징이라고 할 수 있다. 또한, 첨가된 검은콩, 검은깨 등의 부재료들도 분산성을 저해하는데 영향을 미치고 있다. Figure 1 shows the stability of the mixed powder and granule powder dispersed in water according to the time, the powder having a good dispersibility is uniformly dispersed in water to maintain the state without precipitation or floating for a long time, so the change in turbidity with time little. On the contrary, the powder having poor dispersibility is sedimented or suspended over time, resulting in layer separation, resulting in a low turbidity of the sample. Both the mixed powder and granulated powder resulted in a decrease in turbidity over time. This means that the powder gradually sinks over time. Instant rice taste is the main cause of the precipitation over time, since more than 45% of the alpha powdered through the extrusion is added. This result is a common feature in viscous foods such as rice-based tastes and soups. In addition, added ingredients such as black soybeans, black sesame seeds also affect the dispersibility.
도 1에 도시된 바와 같이 과립분말과 혼합분말의 분산도는 큰 차이가 없이 거의 유사한 특징을 나타내었다. 이는 과립화 공정이 분산도를 향상시키지는 못하는 것으로 결론을 내릴 수 있다.As shown in FIG. 1, the dispersion degree of the granulated powder and the mixed powder showed almost similar characteristics without a big difference. It can be concluded that the granulation process does not improve the degree of dispersion.
2) 재수화능 측정2) Rehydration Measurement
하지만 분말의 재수화 특성은 분산성(dispersibility) 하나의 특성만으로는 설명할 수 없으며 젖음성(Wettability), 침강도(Sinkability), 용해도(Solubility) 등과 관련되어 있다. 이들 특징은 수분흡수지수(water absorption index, WAI), 수분용해도(water solubility, WS), 팽윤력(swelling power, SP) 등 분석하는 방법은 다양하나 본 실험에서는 분말 입자가 물속에서 서로 엉기지 않고 얼마나 잘 풀어지는지를 확인하는 목적으로, 기존의 실험들과는 성격이 맞지 않아 새로운 방법을 시도하였다. 즉, 가수시 혼합분말과 과립분말이 물에 잘 풀어지는 정도를 비교 확인하였다. However, the rehydration properties of the powder cannot be explained by only one property of dispersibility, and are related to wettability, sinkability, solubility, and the like. These characteristics can be analyzed in various ways such as water absorption index (WAI), water solubility (WS), and swelling power (SP), but in this experiment, powder particles do not clump together in water. In order to check how well it solved, I tried a new method because it did not fit with existing experiments. That is, the degree of loosening of the mixed powder and the granular powder in water was compared and confirmed.
즉, 시료의 재수화에 걸리는 시간을 통해 재수화능을 비교 분석하기 위한 방법으로 Omobuwajo et al. (2000)의 방법을 변형하여 사용하였다. 즉, 100 mL 비커에 증류수 30 mL를 넣고 자석교반기(MS-MP4, Daihan Scientific, Co., Ltd., Seoul, Korea) 500 rpm으로 교반시키면서 시료 약 2 g을 위에서 천천히 가해주었다. 시료가 처음 들어가는 순간부터 시간을 재어 시료가 완전히 녹을 때까지의 시간을 기록하였다. 모든 결과는 3회 반복 실험한 측정치의 평균값으로 나타내었다.That is, Omobuwajo et al. As a method for comparative analysis of the rehydration ability through the time taken to rehydrate the sample. The method of (2000) was modified. That is, 30 mL of distilled water was added to a 100 mL beaker and about 2 g of the sample was slowly added thereto while stirring at 500 rpm with a magnetic stirrer (MS-MP4, Daihan Scientific, Co., Ltd., Seoul, Korea). The time from the first sample entry was measured and the time until the sample completely dissolved was recorded. All results are expressed as the mean value of three repeated experiments.
육안으로 관찰했을 때 혼합분말은 과립분말에 비해 덩어리진 것이 훨씬 많았고, 25 mesh체에 통과시킬 때 많은 양이 통과되지 못하고 걸러졌다. 반면에 과립분말은 체에 통과시킬 때 대부분이 통과 되었다. 이를 수치로 나타낸 결과, 두 시료의 재수화 특성은 표 3과 같이 나타났다. 과립분말의 분산성이 93.7±0.1%으로, 혼합분말 77.0±5.0% 에 비해 약 16.7% 증가하였다. 또한 재수화 시간을 분석한 결과, 과립분말을 모두 물에 녹였을 때 걸리는 시간이 평균 122.3±28.1 초로 혼합분말 305.3±4.2 초에 비해 약 183 초 빨랐다. When visually observed, the mixed powder was much more agglomerated than the granulated powder, and when passed through a 25 mesh sieve, a large amount was filtered out. On the other hand, most of the granular powder was passed through the sieve. The numerical results show that the rehydration characteristics of the two samples are shown in Table 3. The dispersibility of the granular powder was 93.7 ± 0.1%, which was about 16.7% higher than that of the mixed powder 77.0 ± 5.0%. As a result of analyzing the rehydration time, it took 122.3 ± 28.1 seconds when the granule powder was dissolved in water, which was about 183 seconds faster than 305.3 ± 4.2 seconds of mixed powder.
이러한 결과를 토대로 분말을 과립화 하였을 때 재수화능 향상에 영향을 미치는 것으로 나타났다.Based on these results, it was shown that the granulation of the powder affects the rehydration performance.
도 1은 물 속에 분산된 혼합분말과 과립분말의 시간에 따른 안정도를 나타낸 것이다.Figure 1 shows the stability over time of the mixed powder and granule powder dispersed in water.
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