KR20100087968A - Manufacturing method of shampoo composition using fermented liquid and shampoo composition thereof - Google Patents

Abstract

PURPOSE: A method for manufacturing a shampoo composition using fermentation liquid containing herb materials and mud is provided to relieve dandruff and prevent hair loss without side effects. CONSTITUTION: A method for manufacturing a shampoo composition using fermentation liquid comprises: a step of dissolving alkali in fermentation liquid and heating; a step of mixing a base oil and glycerin in an alkali solution and stirring; a step of mixing together salicornia herbacea extract, purslane, and honey; and a step of adding ginger powder. The fermentation liquid is obtained by maturing a mixture of herb powder, grape juice, paprika juice, and mud, mixing with floral water, and maturing again.

Description

Manufacturing method of shampoo composition using fermentation liquid and shampoo composition using the same {Manufacturing method of shampoo composition using fermented liquid and shampoo composition

The present invention relates to a method for preparing a shampoo composition using a fermentation broth and a shampoo composition using the same, and a method for preparing a shampoo composition which can prevent or improve hair loss and dandruff while being environmentally friendly using a fermentation broth based on herbal medicine and mud. It relates to a shampoo composition used.

In general, modern industrialized societies with improved living standards use shampoo almost every day, causing side effects such as damaging hair.

In other words, commercially available shampoos are manufactured and sold with a focus on cleansing power rather than hair protection purposes, which causes damage to hair when shampooed daily. In addition, dandruff is also formed in the scalp refers to the dead cells of the scalp come off in the form of hard keratin, sebum secreted from the scalp, sweat and agglomerates formed into a large mass.

In general, dandruff is accompanied by itching of the scalp, at this time to scratch the scalp hard to hurt and eventually cause inflammation, eczema, hair loss occurs. The root cause of severe dandruff is known to be caused by the vigorous growth of microorganisms in the scalp, which may be thought of as a bactericidal preservative that can eliminate microorganisms in the scalp, but it is not the case. .

The reason is that the microorganisms affect the metabolism of the scalp cells, but for some other reasons, such as endocrine hormone imbalances, nutrient metabolism imbalances, stress, fatigue, etc. Even before keratinization, it comes off and several scalp cells come together and eventually cause a lot of dandruff.

Therefore, in order to treat and prevent dandruff and itching should use anti-dandruff shampoo containing a component that has the effect to normalize abnormal metabolic activity of the scalp cells as well as bactericidal antiseptic effect.

Among these ingredients, zinc pyrithione, the most commonly used anti-dandruff shampoo, is water insoluble and has a high specific gravity, which makes it very difficult to maintain a uniform dispersion in shampoo solution, and zinc pyrithione is highly irritating to eyes. Severe.

In addition to the dandruff problem described above, as society becomes more complex and diversified, factors such as environmental pollution, stress, and various chemicals, such as hair loss and hair damage, are gradually increasing. Specifically, damage to hair loss or hair damage is caused by environmental damage; Damage from strong sunlight, heat, acid rain and various pollutants; Mechanical damage, ie damage by dryers, curling irons, hot rollers, etc .; Chemical damage, ie damage due to permanent, coloring, bleaching, and the like.

Among these factors, the damage caused by chemical factors is also increasing. In other words, many people want to have their own unique styles and colors these days when personality is important. In order to satisfy these needs, more and more people are wearing permalinks and dyes regardless of age or gender. Thanks to their own personality, but because of frequent perming and dyeing, the hair loses luster, crumbs, cracks and breaks, causing many problems. In addition, the hair becomes thinner and weaker, and even more severe hair loss can occur.

Hair cosmetics, such as hair growth agents, include vitamins such as vitamin E, amino acids such as serine or methionine, vasodilators such as aceylcholine derivatives, anti-inflammatory agents such as ritsperum root extract, female hormones such as estradiol, and skin function promoters such as ceparatin. And various components that exhibit hair growth effects such as melanin synthesis catalysts such as copper pantothenate and keratin dissolving agents such as salicylic acid. These ingredients are also used to help prevent and treat alopecia.

However, when using various chemical compounds as in the prior art, it is difficult to expect a naturally adjustable soothing and purifying action of the scalp and hair, as well as it may cause abnormal irritation to the scalp and hair.

The present invention was created to improve the above-described problems, using a fermentation broth based on herbal medicine and mud to prevent dandruff or hair loss without damaging the scalp or hair, and a shampoo composition and a method for producing the same The purpose is to provide.

Method for producing a shampoo composition using a fermentation broth of the present invention for achieving the above object comprises a heating step of heating after dissolving alkali in the fermentation broth; A first mixing step of mixing and stirring the base oil and glycerin in the alkaline solution; A second mixing step of further mixing fertilizer extract, fermented aging solution and fertilizer which are matured by mixing the perilla extract and purslane with honey after completion of the first mixing step; And a post-adding step of adding an additive including a ginger powder after the second mixing step is completed.

The fermentation broth is characterized in that it is obtained by first aging the mixture of the dried herbal medicine powder, grape juice, paprika juice, mud, and then dried and pulverized fermentation powder with a floral water and then secondary aging.

The first aging is aged by injecting the third mixture into the inside of the pottery, but the inside of the pottery is provided with a mesh installed on the upper side spaced apart from the third mixture, and a plurality of germanium balls supported on the mesh It features.

The mud is finely pulverized mudstone and ball milled to be finely divided into a powder having a size of 200 to 300 mesh particle size, and then left to pour water and discarded the supernatant, characterized in that obtained by recovering the precipitate.

And the shampoo composition using the fermentation broth of the present invention for achieving the above object is characterized in that it is prepared by the above method.

As described above, the present invention is based on a fermentation broth based on dry herbs and mud, so it can be safely used without side effects on the human body.

Shampoo composition using such a fermentation broth can improve the scalp conditions and effective at preventing hair loss and at the same time can relieve dermatitis and dandruff.

Hereinafter, a method for preparing a shampoo composition using a fermentation broth according to a preferred embodiment of the present invention will be described in detail.

The method for producing a sampu composition of the present invention includes a heating step, a first mixing step, a second mixing step, and a post-adding step.

First, the alkali is dissolved in the fermentation broth in the heating step and then heated.

The fermentation broth applied to the present invention is obtained by first aging a mixture of dry herbal powder, grape juice, and mud, and then drying and pulverizing the fermented powder mixed with a floral water and then aging second.

Herbal medicines used in the present invention, for example, Sokdan, dragon's meat, Sanjoin, cheonhwabun, snakeberry, thistle, odor, echidna, baekbaek, mokdanpi, rhubarb, blue rice vine, machihyeon, gold is used. These herbal medicines can be used alone or in combination of two or more. The herbal medicines are excellent in antioxidant and antimicrobial effects to prevent hair loss and to improve dandruff and scalp. In addition, other herbal medicines may be used. Hair loss prevention and dandruff, scalp to improve scalp, creation, safflower, licorice, Angelica can be added.

The herbs are ground in a dry state and used in powder form. When using a mixture of two or more of the medicinal materials are natural materials, so the composition ratio can be arbitrarily adjusted.

Grape juice and paprika juice are obtained by juice of raw grapes and raw paprika. Grape juice and paprika juice is mixed 20 to 30 parts by weight with respect to 100 parts by weight of dry herbal medicine powder.

Phenolics and tannins contained in the grape juice prevent virus aging and prevent aging of the scalp, and other materials facilitate the absorption into the scalp. Paprika juice is rich in vitamins A, E, carotene, iron, calcium, and minerals.

Mud is formed by the decomposition products, soils, salts, etc. of plants and animals, which have been subjected to geological and chemical reactions for many years and the decomposition of microorganisms. Because of this, mud contains numerous inorganic and trace elements such as carbon, nitrogen, phosphorus, sulfur, iron and silicate compounds. It also contains organic substances, hormone-like substances such as prolan and estrogen, as well as vitamins such as thiamin, ascorbic acid, hydrochloric acid, vitamin B12 and riboflavin. Since mud with various ingredients is rich in minerals, it can have the same effect as a hot spring depending on the method of use. Also, it is a good treatment for metabolism, circulation, and nervous system of human body due to hormones and vitamins. It may work for me.

In addition, mud contains colloids and crystals, which can be widely used in physical treatment methods such as sand steaming, water bathing, and sea bathing. In addition, there is an antibacterial, antifungal effect is excellent in the treatment of trauma. Generally speaking, mud therapy is widely known to have effects such as inflammation, promoting metabolism, promoting the growth and regeneration of cells, tissues, nerves, immune function, analgesic function, and hormone function.

Preferably the mud is obtained from mud stone. Mudstone is a type of sedimentary rock that is hardened by the accumulation of fine mud. The main component is clay mineral. The mudstone is composed of quartz, feldspar, carbonate mineral, organic substance and bentonite in addition to the clay mineral which accounts for about 60%.

In order to use such mudstone, the mud mass is roughly coarse firstly in a conventional crusher. This is for facilitating micronization. The coarsely crushed mudstone is milled into a powder having a particle size of 200 to 300 mesh by ball milling and then poured with water and left to stand for about one day. Then discard the supernatant and recover only the precipitate. The recovered precipitate can be used as is or dried and then ground to use in powder form. By using mudstone as described above, various nutrient supply components such as mineral components can be used, and when used, it is alkaline and can easily absorb harmful substances such as skin waste and sebum, as well as neutralize the absorbed waste.

The mud is mixed with 60 to 80 parts by weight based on 100 parts by weight of the dry herbal medicine powder.

The dried herbal medicine powder, grape juice, paprika juice, and mud prepared as described above are first aged. Preferably, the mixture is half-filled with pottery and then first aged at 2 to 3 ° C. for 5 to 7 months. Onggi is a myriad of fine pores are formed to ensure the constant circulation of fresh air into the Onggi for optimal fermentation.

A square cylindrical net is installed inside the pottery during the first aging. The mesh can be used a conventional wire mesh, etc., but it is preferable to use a mesh made of woven fabric. This net is installed in the upper part of the pot after filling the mixture inside the pot. In this case, the net is installed at a position kept a certain distance from the mixture. And the inside of the mesh is filled with a number of germanium balls.

Germanium ball is a porous material with numerous pores on the surface and inside, it is very useful to remove the bad odor generated during the aging process. In particular, the soil odor generated from the mud mixed in the mixture during the first aging can be effectively removed.

Germanium may use natural germanium ores or pure GeO ₂ . Natural germanium ores contain various materials in addition to germanium. Using these germanium ores is much cheaper than using pure GeO ₂ . Germanium balls are manufactured by pulverizing germanium ore by ball milling (ball milling) and then molding them into balls having a diameter of 10 to 40 mm and firing at 800 to 1000 ° C.

The total volume of germanium balls upon aging is preferably about 1/20 to 1/10 of the total volume of the mixture.

When the primary aging is completed, dried and pulverized to obtain a fermented powder. The fermented powder is secondly aged at the same temperature and time as the first maturation after mixing in the floral water. 100 to 200 parts by weight of floral water are mixed with 100 parts by weight of fermented powder.

Floral water refers to a water-soluble substance hydrosol obtained by distilling essential oils from flowers or herbs and is a by-product of essential oils. This floral water has the effect of soothing, moisturizing, converging, anti-inflammatory. As floral water, one or two or more of aloe water, tea tree water, and rosemary water may be used.

In the second aging process, as in the first aging process, it can be matured in Onggi using a mesh and germanium balls. After the second ripening is completed, the resultant is filtered through a strainer to obtain fermentation broth.

Then, a heating step of dissolving alkali in the prepared fermentation broth and heating is performed. As alkali, potassium hydroxide or sodium hydroxide can be used. 20-30 parts by weight of potassium hydroxide are mixed with 100 parts by weight of the fermentation broth, followed by complete dissolution of potassium hydroxide. And it is heated to about 80 ℃ for rapid emulsification to obtain an alkaline solution.

When the heating is completed, the first mixing step is performed. In the first mixing step, the base oil and glycerin are mixed with the alkaline solution, followed by stirring until thick emulsification to prepare a stirred product. In this case, the base oil can be stirred while heated to 80 ° C. Base oil is mixed 80 to 90 parts by weight based on 100 parts by weight of the fermentation broth, glycerin is mixed 12 to 20 parts by weight.

In the present invention, coconut oil extracted from palm fruit is used as the base oil. Coconut oil has excellent foaming power and is suitable for hardness. In addition to coconut oil, vegetable oils such as grape seed oil, castor oil and olive oil may be mixed with coconut oil. In this case, however, it is preferable to use soybean oil, castor oil, olive oil mixed with coconut oil alone. When mixing, the mixing ratio is 20 to 25 parts by weight of soybean oil, castor oil, olive oil with respect to 100 parts by weight of coconut oil, respectively.

Glycerin is mixed for the effect of moisturizing, betaine, diepanthenol and the like extracted from sugar cane can be used.

When the emulsification is sufficiently progressed by stirring in the first mixing step, a second mixing step of further mixing the nachosium extract, fermented saturated fermentation with fermentation of honey and fertilized with honey, and the first egg are further mixed. In this case, preferably, 8 to 12 parts by weight of the seaweed extract, 12 to 20 parts by weight of fermented manure, and 30 to 35 parts by weight of eggs are mixed with respect to 100 parts by weight of the agitated substance.

Hamchoe is an annual herb that grows on Gaepearl on the west coast of Korea. Its main ingredients are enzymes and minerals such as calcium, magnesium, potassium, iron, phosphorus, manganese, zinc, iodine, copper, nickel, chromium, cobalt, vanadium, sodium, chlorine, It contains a large amount of uronic acid and natural fiber, and contains general ingredients such as water, ash, crude protein, crude fat, carbohydrate, and vitamin B1, B2, vitamin C, vitamin E, niacin and alkaloids. In addition, amino acids (glutamic acid, aspartic acid, tyrosine, lysine, taurine, betaine, choline and proline are contained in a large amount. In addition, it contains various minerals in seawater. Various trace elements and enzymes contained in seaweed are expected to have various useful effects.

Using the above-mentioned seaweed, the seaweed extract is obtained by a method such as ethanol solvent, hot water, and compression. The above-mentioned seaweed extract is obtained by extracting in ethanol or hot water, filtering, concentrating and processing the liquid phase. Here, the hot seaweed extract is 40 to 60 parts by weight based on 100 parts by weight of freshly washed raw seaweed. After heating for 1 hour in a pressure cooker at 90 ℃ extracted by filtration and processed into a liquid phase, the ethanol extract of seaweed is concentrated by immersing purslane in ethanol at room temperature for 5 hours or more. In addition, the pressing extracts of the seaweeds are squeezed with purslane in a green juice, sterilized the collected juice for 1 minute at 98 ℃, cooled and centrifuged to concentrate the supernatant.

These seaweed extracts improve the blood circulation of the scalp and help hair shine.

Purslane can reduce heat, detoxify, remove inflammation and boils on the scalp, and prevent hair loss by removing Demodex in the scalp. Purslane maturation liquid is obtained by mixing 20 to 40 parts by weight of purslane juice obtained by grinding fertilizer with respect to 100 parts by weight of honey and aged for about 3 months at 2 to 3 ° C. Honey is a nutrient source for microorganisms during ripening.

Eggs are made by immersing raw eggs in a vinegar solution, which can be stored at room temperature with a pH of about 4.0. It is known that egg which has been mixed with the original ingredient of vinegar and vinegar to become nutritious alkaline food is especially good for patients in recovery period. In particular, when the egg is soaked in the vinegar solution, the egg is dissolved in the eggshell component, which reacts with acid to produce carbon dioxide, and the shell part is kept soft.

As an example of egg production, after putting 20 egg eggs in 3L of brown rice vinegar, about 9 days have elapsed, the eggs are stirred, the shell is popped, the shell is taken out, and the contents are mixed well to prepare the mixture. This disturbance softens the hair in the present invention and makes the hair elastic and shiny.

In the second mixing step, the above materials are mixed and slowly heated in a low heat to ensure sufficient mixing. After the second mixing step is completed, it is cooled until it cools down to about 30 ° C. and then an additive is added to carry out the post-adding step.

The additive is for adding functionality, and the additive in the present invention preferably includes a ginger powder.

The ginger powder is excellent in antibacterial and bactericidal action to prevent hair loss by removing hair follicles of the scalp. In addition to ginger powder, cellulose to adjust viscosity with additives, silky base to give silk texture to hair, honey powder to increase moisturizing effect of scalp, tocopherol as antioxidant, herbal oil to increase odor and functionality, etc. Can be. Herbal oils include ylang-ylang, tea tree, rosemary, rosemary antioxidants, and peppermint.

Hereinafter, the method for producing a shampoo composition using the fermentation broth of the present invention through the examples. However, the following examples are intended to illustrate the present invention in detail, and the scope of the present invention is not limited to the following examples.

Example 1

25 parts by weight of grape juice, paprika juice, 100 parts by weight of dried herbal medicine powder mixed with same ratio of Sokdan, longan meat, Sanjoin, natural flower, snakeberry, thistle, odor, barkwood, cypress, velvet, rhubarb, blue rice vine, machi, and golden After mixing 25 parts by weight, 70 parts by weight of mud obtained from mudstone, and half-filled in a plastic container, the first aging for 5 months at 2.5 ℃, dried and pulverized to obtain a fermented powder. And 150 parts by weight of floral water mixed with aloe water, tea tree water, and rosemary water in 100 parts by weight of fermented powder were mixed in a plastic container, and then aged for 2 months at 2.5 ° C. for 5 months, and then filtered through a strainer. Fermentation broth was prepared.

85 parts by weight of base oil and 16 parts by weight of glycerin were mixed in an alkaline solution in which 25 parts by weight of potassium hydroxide was dissolved per 100 parts by weight of the prepared fermentation broth. Left for a while. At this time, soybean oil, castor oil, and olive oil 22 parts by weight were all mixed with 100 parts by weight of coconut oil as a base oil.

And after mixing 10 parts by weight of the seaweed hot water extract, 16 parts by weight of purslane aging solution, and 32 parts by weight of egg eggs after mixing with 100 parts by weight of the agitated mixture, while slowly heating in a weak fire and cooled to 30 ℃ and then the 3 parts by weight of ginger powder, 3 parts by weight of cellulose and 3 parts by weight of herb oil were added based on 100 parts by weight of the stirred substance, and then aged in a well-ventilated place for about 2 weeks to prepare a shampoo composition.

(Example 2)

To prepare a shampoo composition in the same manner as in Example 1, but instead of using a plastic container during the first aging was used an onggi installed inside the germanium ball-filled network.

(Comparative Example)

A commercially available hair shampoo was used.

Experimental Example 1: Skin Irritation Experiment

In order to determine the degree of skin irritation for the shampoo composition according to the present invention, the skin test was performed for Examples 1 and 2 and Comparative Examples. For skin testing, a small sample was placed on the upper arm against five women from each age group from five to ten years of age. After 1 hour, the skin reaction was first visually examined, and after 24 hours, the second visual The test results are shown in Table 1 below.

division Skin irritation degree Example 1 1st: ○, 2nd: ○ Example 2 1st: ○, 2nd: ○ Comparative example Primary: △, Secondary: △

(○: no skin change, △: slight erythema appears, ×: distinct erythema appears)

Looking at the results of Table 1, in the case of a typical shampoo composition of the comparative example it can be seen that the mild erythema appeared irritating to the skin, while the shampoo composition of the present invention can be used safely without irritation to the skin.

Experimental Example 2: Inertia Test

Experiments were carried out to confirm the moisturizing effect, the anti-dandruff, and the anti-hair loss effect for the Examples and Comparative Examples.

To do this, 30 male and female adults were selected. The ages ranged from 25 to 55 years, with 12 males and 18 females. The subjects were divided into three groups of 10 people each, using the shampoo composition of Example 1 in the first group, the shampoo composition of Example 2 in the second group, and the shampoo composition of the comparative group in the third group, once daily by a conventional method. After two months, the skin's moisturizing effect, dandruff prevention, and hair loss prevention were evaluated by a 5-point scale method.

The results are shown in Table 2 below.

division Moisturizing effect Anti dandruff Hair loss prevention incense Example 1 4.2 4.3 4.5 3.9 Example 2 4.1 4.5 4.5 4.3 Comparative example 3.4 2.8 2.6 3.2

(1: Very bad, 2: Bad, 3: Normal, 4: Good, 5: Very good)

Looking at the results of Table 2, it can be seen that the shampoo composition of the present invention is significantly effective in moisturizing effect, anti-dandruff, hair loss prevention compared to the comparative example of a conventional shampoo composition.

And the effect of Example 2 and Example 1 was shown similarly. However, Example 2 was found to be better than Example 1 in the odor of the shampoo composition.

From the above results, it can be seen that the shampoo composition using the fermentation broth of the present invention has an effect on preventing hair loss and at the same time a moisturizing effect and an antidandruff effect.

In the above, the present invention has been described with reference to one embodiment, which is merely exemplary, and it will be understood by those skilled in the art that various modifications and equivalent embodiments are possible.

Therefore, the true scope of protection of the present invention should be defined only by the appended claims.

Claims (5)

A heating step of dissolving alkali in the fermentation broth and then heating it; A first mixing step of mixing and stirring the base oil and glycerin in the alkaline solution; A second mixing step of further mixing fertilizer extract, fermented aging solution and fertilizer which are matured by mixing the perilla extract and purslane with honey after completion of the first mixing step; After the second mixing step is completed, the post-adding step of adding an additive including a ginger powder; Method of producing a shampoo composition using a fermentation broth, characterized in that it comprises a. The method of claim 1, wherein the fermentation broth is obtained by first aging a mixture of dry medicinal herb powder, grape juice, paprika juice, and mud, and then drying and pulverizing the fermented powder mixed with a floral water, followed by secondary aging. Method for producing a shampoo composition using a fermentation broth. The method of claim 2, wherein the first aging of the third mixture is put into the inside of the pottery aging, the inside of the pottery spaced apart from the third mixture and the mesh installed on the upper side, a plurality of supported on the network Method for producing a shampoo composition using a fermentation broth, characterized in that germanium balls are provided. The fermentation broth according to claim 2, wherein the mud is obtained by roughly crushing mudstone and ball milling the fine powder into powder having a particle size of 200 to 300 mesh, then pouring water and leaving the supernatant to recover the precipitate. Method for producing a shampoo composition using. Shampoo composition using a fermentation broth, characterized in that prepared by the method of any one of claims 1 to 4.