KR20100052946A - Preventer of sick house syndrome using effective microorganisms and it's making method - Google Patents
Preventer of sick house syndrome using effective microorganisms and it's making method Download PDFInfo
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Abstract
Description
본 발명은 새집증후군의 원인 물질인 포름알데히드와 휘발성유기화합물(VOC)를 효과적으로 제거할 수 있는, EM이라는 유용미생물군의 분해능력을 이용하여 새집증후군의 원인물질을 제거하는 것으로 기존의 기술과는 차별화 되고 진일보한 신개념의 새집증후군 제거제와 그 제조방법에 관한 것이다.The present invention is to remove the causative agent of sick house syndrome by using the decomposition ability of the useful microorganism group called EM, which can effectively remove the formaldehyde and volatile organic compounds (VOC), the causative agent of sick house syndrome. The present invention relates to a new concept of a new house syndrome remover and a method of manufacturing the same.
새집증후군 제거제와 관련된 기술로는, 금속과 무기산화물 미립자, 산화티탄, 실리카 및 지르코니아 등을 이용하여 새집증후군의 원인 물질인 포름알데히드와 휘발성유기화합물을 제거하도록 한 '항균성 소취제 및 그 제조방법'(한국 공개특허공보 10-2006-0046901)이 공개된 바 있다.As a technology related to a sick house syndrome remover, an antibacterial deodorant and a method of manufacturing the same, which removes formaldehyde and volatile organic compounds, which are the causative agents of the sick house syndrome, using metals and inorganic oxide fine particles, titanium oxide, silica, and zirconia ( Korean Unexamined Patent Publication No. 10-2006-0046901) has been published.
또, 무기산 아민염 분말을 이용한 '소취제 및 소취성 제품'(한국 공개특허공보 10-2006-0107778)이 공개되기도 하였다.In addition, 'deodorant and deodorant product' (Korean Patent Publication No. 10-2006-0107778) using an inorganic acid amine salt powder has been disclosed.
상기와 같은 제품들은 모두 무기질의 구성요소를 이용한 것으로 특히, '항균 성 소취제 및 그 제조방법'은 고가의 금속 산화물을 이용하는 점, 금속 산화물의 2차 오염 등의 문제점이 있었다.All of the above products are made of inorganic components. In particular, the 'antibacterial deodorant and its manufacturing method' have problems such as the use of expensive metal oxides and secondary contamination of metal oxides.
본 발명의 이엠유용미생물군을 이용한 새집증후군 제거제 제조방법은 상기와 같은 종래 기술에서 발생되는 문제점을 해소하기 위한 것으로, 강력한 항산화 능력을 갖고 있는 이엠(EM : Effective microorganisms)을 이용하여 포름알데히드와 휘발성유기화합물(VOC)를 신속하고 손쉽게 제거하려는 것이다.The method for preparing a sick house syndrome remover using the EM utility microorganism group of the present invention is to solve the problems occurring in the prior art as described above. Formaldehyde and volatility using EM (Effective microorganisms) having powerful antioxidant ability To remove organic compounds (VOC) quickly and easily.
아울러, 미생물 집합체인 이엠(EM : Effective microorganisms)을 이용함으로써 포름알데히드와 휘발성유기화합물(VOC)를 제거한 후 발생되는 2차 오염이 발생되지 않게 하려는 것이다.In addition, by using the effective microorganisms (EM: microorganism aggregate) is to prevent secondary pollution generated after removing formaldehyde and volatile organic compounds (VOC).
본 발명의 이엠유용미생물군을 이용한 새집증후군 제거제 제조방법은 상기와 같은 과제를 해결하기 위하여, 용기에 물 91 중량% 투입한 후 용기 내 물의 온도를 38도로 유지시키는 단계; 쌀겨 1 중량 %를 준비한 후 망태에 넣은 다음 용기에 투입하고 수중에서 비벼주는 단계; EM 원액 3 중량 %, 당밀 3 중량 %, 설탕 1 중량 %, EM 발효숙성염 1 중량%를 용기에 투입한 후 교반하는 단계; 6 ~ 8 일간 온도를 유지한 채 배양하여 EM 발효액을 제조하는 발효액제조단계와; EM세라믹나노파우더를 준비하는 파우더준비단계와; 발효액제조단계에서 제조된 EM 발효액 99.5 중량 %와, EM세라믹나노파우더 0.5 중량 %을 혼합하는 혼합단계;로 구성된다.Method for manufacturing a sick house syndrome remover using EM utility microorganisms of the present invention, in order to solve the above problems, the step of maintaining the temperature of the water in the container to 38 degrees after 91% by weight of water in the container; Preparing 1% by weight of rice bran, put it in the mantle, and then putting it in a container and rubbing in water; Adding 3% by weight of EM stock solution, 3% by molasses, 1% by weight sugar, and 1% by weight EM fermented mature salt to a container, followed by stirring; A fermentation broth production step of preparing an EM fermentation broth by culturing the temperature for 6 to 8 days; A powder preparation step of preparing an EM ceramic nano powder; Consisting of mixing 99.5% by weight of EM fermentation broth prepared in the fermentation broth manufacturing step and 0.5% by weight of EM ceramic nano powder.
이때, 상기 EM 발효숙성염은, EM 원액 또는 EM-X 중 선택된 어느 하나 또는 양자의 혼합물에 천일염을 넣고 1 ~ 3개월 숙성한 후 정제하여 제조한 것을 특징으로 한다.At this time, the EM fermentation aging salt, characterized in that prepared by refining after adding the natural salt to any one or a mixture of selected EM stock or EM-X and aged for 1 to 3 months.
또, EM세라믹나노파우더는, 점토에 EM 원액을 첨가하여 숙성한 뒤 1300 ~ 1700 도의 온도로 소성한 후 분말화 시킨 것을 다시 10nm이하로 나노화한 것을 특징으로 한다.In addition, the EM ceramic nano powder is characterized in that after aging by adding the EM stock solution to the clay, and then calcined to a temperature of 1300 ~ 1700 degrees and then powderized to nano 10 nm or less again.
아울러, EM 발효액에는 1 ㎖ 당 효모가 1.1 ~ 1.7×104cfu, 유산균이 1.3 ~ 1.9 ×106cfu, 광합성세균이 4.0 ~ 4.8 ×105cfu, 방선균이 2.0 ~ 2.6 ×104cfu 정도의 복합미생물이 포함된 것을 특징으로 한다.In addition, EM fermentation broth contains yeast from 1.1 to 1.7 × 10 4 cfu, lactic acid bacteria from 1.3 to 1.9 × 10 6 cfu, photosynthetic bacteria from 4.0 to 4.8 × 10 5 cfu, actinomycetes from 2.0 to 2.6 × 10 4 cfu. Characterized in that it contains a complex microorganism.
본 발명에서 EM(EM : Effective microorganisms)의 기존 발효방법에 쌀겨를 이용한 것은, 기존의 EM 배양방법에서 볼 수 없었던 방선균 등의 분해미생물의 밀도를 높이는 작용을 하게 되며, 다른 미생물들과 결합을 통해 난분해성 물질로 알려진 포름알데히드와 휘발성유기화합물(VOC)를 신속하게 제거할 수 있게 된다.In the present invention, the use of rice bran in the existing fermentation method of EM (EM: Effective microorganisms), acts to increase the density of microorganisms such as actinomycetes that were not seen in the conventional EM culture method, through the combination with other microorganisms Formaldehyde and volatile organic compounds (VOCs), known as hardly degradable substances, can be quickly removed.
아울러, 천연물질로 이루어진 미생물 집합체인 이엠(EM : Effective microorganisms)을 이용함으로써 포름알데히드와 휘발성유기화합물(VOC)를 제거한 후 발생되는 2차 오염이 발생되지 않게 된다.In addition, by using the effective microorganisms (EM), a microbial aggregate made of natural materials, secondary pollution generated after removing formaldehyde and volatile organic compounds (VOC) is not generated.
이엠(EM)은 Effective microorganisms의 머리글자를 딴 약자로서 여기서 유용 미생물이란 뜻으로 여기에는 일반적으로 효모, 유산균, 광합성 세균 등 인류가 오래 전부터 식품의 발효 등에 이용해 왔던 미생물들이 포함되어 있다.EM stands for Effective microorganisms, which means useful microorganisms, which include microorganisms such as yeast, lactic acid bacteria, and photosynthetic bacteria that humans have long used for food fermentation.
이러한 미생물들은 서로 공존공생하면서 대사산물을 만들어 내는데 이것이 강력한 천연의 항산화물질로서 산화와 부패를 억제하는 것으로 알려져 있으며, 특히 사람을 포함한 생명체에 무해유익(無害有益)하면서 비옥한 토양 속에 존재하는 통성 혐기성(通性 嫌氣性 : 혐기성과 호기성, 양쪽 성질을 가지나 대체적으로 공기를 별로 좋아하지 않는 성질) 미생물과 미호기성(微好氣性 : 공기를 어느 정도 좋아하는 것) 미생물들을 합성과 배양과정을 거쳐 상승효과를 나타내도록 만든 복합 유효미생물의 합성체를 말한다.These microorganisms coexist symbioticly to produce metabolites, which are known as powerful natural antioxidants that are known to inhibit oxidation and decay, and are especially known for their anaerobic anaerobic properties, which are harmless to life, including humans. (通性 嫌 氣 性: anaerobic and aerobic, both properties but generally do not like the air) Microorganisms and micro-aerobic (微 好: 性: Some like the air) Microorganisms rise through the synthesis and culture process Refers to a composite of a composite effective microorganism made to produce an effect.
이러한 이엠(EM)에 대해서는 악취를 없애고 물을 깨끗이 하며, 철, 식품 등의 산화를 방지하고 곰팡이 균을 제거하는 효과를 갖는 것으로 알려져 있다.EM is known to have an effect of removing odors and cleaning water, preventing oxidation of iron, food, and the like and removing fungi.
본 발명에서는 이러한 이엠(EM)을 다른 재료와 혼합하여 발효시키거나 세라믹나노파우더에 적용하여 특정 성분 비로 혼합하여 새집증후군의 원인이 되는 포름알데히드와 휘발성유기화합물을 제거할 수 있도록 하였다.In the present invention, it is possible to remove the formaldehyde and volatile organic compounds that cause the sick house syndrome by mixing the EM (EM) and mixed with other materials and fermented or applied to a ceramic nano powder in a specific component ratio.
이하 본 발명의 이엠유용미생물군을 이용한 새집증후군 제거제 제조방법의 세부 공정에 대해 설명하면 다음과 같다.Hereinafter, a detailed process of the method for preparing a sick house syndrome remover using EM utility microorganism of the present invention will be described.
1.발효액제조단계1. Fermentation solution manufacturing step
1) 용기에 물 91 중량% 투입한 후 용기 내 물의 온도를 38도로 유지시킨다.1) After adding 91% by weight of water to the container, maintain the water temperature in the container at 38 ° C.
물의 온도를 38도로 유지시키는 것은 EM 원액의 발효율을 높이기 위한 것이다.Maintaining the water temperature of 38 degrees is to increase the efficiency of EM stock solution.
2) 쌀겨 1 중량 %를 준비한 후 망태에 넣은 다음 용기에 투입하고 수중에서 비벼준다.2) Prepare 1% by weight of rice bran, put it in the mantle, put it in a container and mix it in water.
3) EM 원액 3 중량 %, 당밀 3 중량 %, 설탕 1 중량 %, EM 발효숙성염 1 중량%를 용기에 투입한 후 교반한다.3) 3% by weight of EM stock solution, 3% by molasses, 1% by weight sugar, 1% by weight EM fermented salt is added to the container and stirred.
여기서 EM 발효숙성염은 EM 원액 또는 EM-X 중 선택된 어느 하나 또는 양자의 혼합물에 천일염을 넣고 1 ~ 3개월 숙성한 후 정제하여 제조한 것을 특징으로 한다.Wherein EM fermented salt is characterized in that prepared by adding the natural salt to any one or a mixture of selected EM stock or EM-X and aged for 1 to 3 months and then purified.
4) 6 ~ 8 일간 온도를 유지한 채 배양하여 EM 발효액을 제조한다.4) The fermentation broth is prepared by incubating for 6-8 days while maintaining the temperature.
상기와 같은 EM 발효액은 EM 원액, 당밀, 설탕, 쌀겨, EM 발효숙성염, 물을 3 : 3 : 1 : 1 : 1 : 91의 비율로 혼합한 것으로 공지된 EM 발효액의 조성 비와는 다른 비율을 가진다.EM fermentation broth as described above is different from the composition ratio of EM fermentation broth, which is known to be mixed in the ratio of EM stock, molasses, sugar, rice bran, EM fermentation maturation salt, water 3: 3: 1: 1: 1: 191 Has
이로 인해 상기 EM 발효액에는 EM 발효액 1 ㎖ 당 효모가 1.1 ~ 1.7×104cfu, 유산균이 1.3 ~ 1.9 ×106cfu, 광합성세균이 4.0 ~ 4.8 ×105cfu, 방선균이 2.0 ~ 2.6 ×104cfu 포함된 것이 특징이다. For this reason, the EM fermentation broth contains yeast 1.1 to 1.7 × 10 4 cfu, lactobacillus 1.3 to 1.9 × 10 6 cfu, photosynthetic bacteria 4.0 to 4.8 × 10 5 cfu, actinomycetes 2.0 to 2.6 × 10 4 It is characterized by the inclusion of cfu.
즉, 일반적인 EM 배양방법에 비해 방선균 등의 분해 미생물의 조성이 높아져 난분해 물질인 휘발성유기화합물의 분해를 촉진시키도록 한 것이다.That is, the composition of decomposing microorganisms such as actinomycetes is increased compared to the general EM culture method to promote the decomposition of volatile organic compounds, which are difficult to decompose.
2. 파우더준비단계2. Powder Preparation Step
EM세라믹나노파우더를 준비한다.Prepare an EM ceramic powder.
EM세라믹나노파우더는 EM세라믹파우더를 나노화 시킨 것으로, 점토에 EM 원액을 첨가하여 숙성한 뒤 1300 ~ 1700 도의 온도로 소성한 후 분말화 시킨 것이다.EM ceramic nano powder is a nano-ceramic EM ceramic powder, which is aged by adding EM stock solution to clay, and then sintered to a temperature of 1300 to 1700 degrees and then powdered.
EM세라믹파우더는 기존의 세라믹 파우더에 비해 뛰어난 항산화 기능을 갖고 있으며, 일본에서 전래되어 사용되고 있으며, 주로 건축물의 내구성 강화 등의 목적으로 사용되고 있다.EM ceramic powder has superior antioxidant function compared to the conventional ceramic powder, and has been used in Japan and is mainly used for the purpose of strengthening the durability of buildings.
세라믹의 나노화 기술은 이미 공지된 것으로 등록특허공보 제10-573295호 '나노 금속 또는 세라믹 분말의 생성장치' 등에 공지된 것이므로 EM세라믹파우더를 나노화 시켜 EM세라믹나노파우더로 제조하는 구성에 대해서는 생략하기로 한다.Ceramic nanonization technology is already known, and is known in the Patent Publication No. 10-573295, 'Generating device for nano metal or ceramic powder', etc., so that the configuration for manufacturing the EM ceramic powder to the EM ceramic nano powder will be omitted. do.
3. 혼합단계3. Mixing Step
상기 발효액제조단계에서 제조된 EM 발효액 99.5 중량 %와, 상기 EM세라믹나노파우더 0.5 중량 %을 혼합하여 본 발명의 새집증후군 제거제를 제조한다.99.5% by weight of the EM fermentation broth prepared in the fermentation broth manufacturing step and 0.5% by weight of the EM ceramic nanopowder is mixed to prepare a bird house syndrome remover of the present invention.
이하 본 발명의 실시예에 대해 설명하기로 한다.Hereinafter, embodiments of the present invention will be described.
<실시예 1> 새집증후군 제거제 제조Example 1 Preparation of Sick House Syndrome Remover
1. EM발효숙성염 준비1. Preparation of EM Fermented Salt
시중에서 EM 원액과 EM-X(이엠 코퍼레이션에서 제조한 EM-X Gold)를 구입하여 반씩 넣고 혼합한 후 여기에 신안앞바다 천일염을 넣고 2달간 숙성한 후 정제하여 EM발효숙성염을 준비하였다.Commercially prepared EM stock solution and EM-X (EM-X Gold manufactured by EM Corporation) were added in half, mixed, mixed with sea salt in front of Sinan and then aged for 2 months, and then purified to prepare EM fermented salt.
2. EM세라믹나노파우더 준비2. Preparation of EM Ceramic Nano Powder
점토에 EM 원액을 첨가하여 숙성한 뒤 약 1300 ~ 1700 도의 온도로 소성한 후 분말화 시켜 EM세라믹파우더를 제조한 뒤 이를 나노화장치를 이용하여 나노화시켰다.After the EM stock solution was added to the clay and aged, it was calcinated at a temperature of about 1300 to 1700 degrees, and then powdered to prepare an EM ceramic powder.
3. EM 발효액 제조3. EM fermentation broth manufacture
히터가 설치된 용기에 정제수 91 kg을 담아 하루동안 방치한 후 히터를 가동시켜 물의 온도를 38도로 유지시킨 상태에서 망태에 넣은 쌀겨 1 kg을 용기에 넣고 수중에서 망태를 비벼주었다.91 kg of purified water was placed in a container equipped with a heater and left for one day, and the heater was operated to keep the water temperature at 38 degrees, and 1 kg of rice bran in the mantle was put in the container and rubbed with water.
그런 다음 시중에서 EM 원액을 구입한 후 용기에 EM 원액 3 kg, 당밀 3 kg, 설탕 1 kg을 투입하였다.Then, commercial EM stock was purchased, and then 3 kg of EM stock, 3 kg of molasses, and 1 kg of sugar were added to a container.
아울러, 준비된 EM발효숙성염 1kg을 용기에 투입한 후 교반시켰다.In addition, 1kg of the prepared EM fermented salt was added to the vessel and stirred.
재료의 투입이 끝난 후 용기 내부 물의 온도를 38도로 유지하면서 7일간 배양하여 EM 발효액을 제조하였다.EM fermentation broth was prepared by incubating for 7 days while maintaining the temperature of the water in the container after the addition of the material.
4. 준비된 EM 발효액에서 995 g을 새로운 용기에 넣고 EM세라믹나노파우더를 새 용기에 5 g 투입한 후 교반하여 본 발명의 새집증후군 제거제를 제조하였다.4. In the prepared EM fermentation broth, 995 g was placed in a new container, and 5 g of an EM ceramic nano powder was added to a new container, followed by stirring to prepare a bird house syndrome remover of the present invention.
<실험예 1> 새집증후군 제거제의 탈취 성능 테스트<
제조된 새집증후군 제거제에 대하여 한국 건자재시험연구원에 포름알데히드의 저감 효과를 확인해본 결과 도 2에 도시된 것처럼 실험시작 50시간 후에 포름알데히드의 99.9 %이상의 탈취 효과를 얻는 것을 알 수 있었다.As a result of confirming the reduction effect of formaldehyde on the prepared new house syndrome remover, it was found that more than 99.9% of formaldehyde deodorizing effect was obtained after 50 hours of the experiment as shown in FIG.
아울러, 도시하지는 않았으나, 벤젠 및 톨루엔에 대해서도 각각 51.2 %, 56.2 %의 탈취 효과를 갖는 것을 확인할 수 있었다.In addition, although not shown, it was confirmed that the deodorizing effect of 51.2% and 56.2% for benzene and toluene, respectively.
<실험예 2> 신축 아파트 실험 결과Experimental Example 2 New Apartment Apartment Experimental Results
실험예 1의 결과를 토대로 (재)서해환경과학연구소에 의뢰하여 전주시 중화산동에 소재한 신축아파트(오페라하우스) 44평 현장에서 발생되는 포름알데히드와 VOC의 저감효과를 테스트하였으며, 테스트 결과를 도 3에 도시하였다.Based on the results of Experimental Example 1, we commissioned the Seohae Environmental Science Research Institute to test the reduction effect of formaldehyde and VOC generated at the 44 pyeong site of the new apartment (opera house) located in Junghwasan-dong, Jeonju-si. Shown.
도 3에 도시된 바와 같이 토탈 VOC가 63 % 이상 감소되는 것으로 확인되어 우수한 탈취 효과를 갖는 것을 알 수 있었다.As shown in FIG. 3, the total VOC was confirmed to be reduced by 63% or more, and it was found to have an excellent deodorizing effect.
본 발명의 새집증후군 제거제는 기본적으로 새건축물의 새집증후군 제거의 용도에 사용될 수 있으며, 본드, 페이트 등 건축자재 제조시 혼합원료로도 이용 가능하며, 신규 차량 등 각종 합성수지 제품이 신규 채용된 각종 환경에 적용할 수 있다 할 것이다.Birdhouse syndrome remover of the present invention can be basically used for the removal of birdhouse syndrome of a new building, can also be used as a mixed raw material in the manufacture of building materials such as bonds, paints, various environments where new synthetic resin products such as new vehicles are newly adopted It will be applicable to.
도 1은 본 발명의 새집증후군 제거제의 제조공정을 나타낸 공정도.1 is a process chart showing the manufacturing process of the birdhouse syndrome remover of the present invention.
도 2는 본 발명의 새집증후군 제거제에 대한 한국건자재시험연구원의 시험 결과를 나타낸 사진.Figure 2 is a photograph showing the test results of the Korea Building Materials Testing Institute for the new house syndrome remover of the present invention.
도 3은 본 발명의 새집증후군 제거제를 건축 현장에서 사용한 결과를 나타낸 시험결과표Figure 3 is a test result table showing the results of using the new house syndrome removal agent of the present invention in the building site
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