KR20090081283A - a making method of bedclothes emitting an anion - Google Patents

a making method of bedclothes emitting an anion Download PDF

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Publication number
KR20090081283A
KR20090081283A KR1020080007268A KR20080007268A KR20090081283A KR 20090081283 A KR20090081283 A KR 20090081283A KR 1020080007268 A KR1020080007268 A KR 1020080007268A KR 20080007268 A KR20080007268 A KR 20080007268A KR 20090081283 A KR20090081283 A KR 20090081283A
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South Korea
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mica
powder
cotton
mineral
illite
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KR1020080007268A
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Korean (ko)
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홍종열
박월식
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홍종열
박월식
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Priority to KR1020080007268A priority Critical patent/KR20090081283A/en
Publication of KR20090081283A publication Critical patent/KR20090081283A/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B68SADDLERY; UPHOLSTERY
    • B68GMETHODS, EQUIPMENT, OR MACHINES FOR USE IN UPHOLSTERING; UPHOLSTERY NOT OTHERWISE PROVIDED FOR
    • B68G3/00Treating materials to adapt them specially as upholstery filling
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • D01F1/103Agents inhibiting growth of microorganisms
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/02Cotton wool; Wadding
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/04Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres having existing or potential cohesive properties, e.g. natural fibres, prestretched or fibrillated artificial fibres
    • D04H1/08Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres having existing or potential cohesive properties, e.g. natural fibres, prestretched or fibrillated artificial fibres and hardened by felting; Felts or felted products
    • D04H1/10Felts made from mixtures of fibres
    • D04H1/14Felts made from mixtures of fibres and incorporating inorganic fibres
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B68SADDLERY; UPHOLSTERY
    • B68GMETHODS, EQUIPMENT, OR MACHINES FOR USE IN UPHOLSTERING; UPHOLSTERY NOT OTHERWISE PROVIDED FOR
    • B68G1/00Loose filling materials for upholstery
    • B68G2001/005Loose filling materials for upholstery for pillows or duvets
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/01Natural vegetable fibres
    • D10B2201/02Cotton
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00Physical properties
    • D10B2401/13Physical properties anti-allergenic or anti-bacterial
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2503/00Domestic or personal
    • D10B2503/06Bed linen

Abstract

A method for manufacturing cotton for bedclothes is provided to manufacture cotton for bedclothes which is capable of enhancing the health of a user by air cleaning, humidity controlling, heat keeping and deodorizing effects of a mica powder. A method for manufacturing cotton for bedclothes comprises the steps of: collecting illite presenting as a natural ore in the natural state; crushing the illite ore and heating the crushed illite ore in a drying furnace to dry water from the illite ore; finely milling the illite ore to obtain a fine ore powder; uniformly agitating the illite ore powder in clean water; pouring water and extracting the mica when silica and chlorite are settled, and mica is positioned in the uppermost layer; drying the extracted mica and uniformly mixing the dried mica with a nanosilver powder; mixing the powder mixture with a polyester powder for fiber manufacturing, injecting the mixed raw materials into an extruder to heat and melt the mixed raw materials, and extruding the molten material by a screw to spin the molten material into monofilaments; and stretching the monofilaments and combining the stretched monofilaments to manufacture cotton in the monofilament phase.

Description

침구용 솜의 제조방법{a making method of bedclothes emitting an anion}Manufacturing method of bedding batting {a making method of bedclothes emitting an anion}

본 발명은 침구용 솜의 제조방법에 관한 것으로서, 더욱 상세하게는 침구용 솜에 운모(雲母)분말이 포함되어 자연상태에서 원적외선 및 음이온을 발산하는 운모분말의 특성인 공기 세정, 습도조절, 보온, 탈취 등의 효과에 의하여 사용자의 건강을 증진시켜 줄 수 있도록 한 발명에 관한 것이다.The present invention relates to a method for producing a bedding cotton, more specifically, the mica (雲母) powder is included in the bedding cotton, which is a characteristic of the mica powder that emits far infrared rays and anions in a natural state, air cleaning, humidity control, thermal insulation It relates to an invention that can improve the health of the user by the effect of deodorization, and the like.

일반적으로 침구용 솜은 잠잘 때 필요한 물건으로 이불과 요와 베개 등으로 구성되어 있고, 이러한 침구의 내부에는 신체를 푹신하게 해주는 쿠션재인 솜이 내장되어 있다.In general, bedding cotton is composed of bedding, yo, pillows, etc. necessary for sleeping, the inside of the bedding is a cushion material that softens the body is embedded.

우리의 조상들은 목화에서 뽑은 목화 솜을 사용하여 침구용 솜으로 사용하였으나 목화 솜은 가공방법이 복잡할 뿐 아니라 많은 시간이 소요되고, 수요에 비하여 공급이 부족하여 현대에는 주로 폴리에스테르·아크릴·염화비닐·폴리프로필렌과 같은 합성섬유로 이루어진 솜이 생산되어 널리 사용되고 있다.Our ancestors used cotton swabs from cotton, but cotton swabs are not only complicated processing methods but also take a lot of time and lack of supply compared to demand. Cotton made of synthetic fibers such as vinyl polypropylene is produced and widely used.

그러나, 전술한 합성섬유 솜은 목화 솜에 비하여 인체에 유익한 기능을 부여할 수 없었으므로 사용자의 건강을 증진시켜 줄 수 있도록 하는 역할을 기대할 수 없었다.However, the above-mentioned synthetic fiber cotton was not able to give a beneficial function to the human body as compared to cotton cotton, so it could not be expected to play a role to improve the health of the user.

따라서, 이를 극복하고자 각종 운동요법, 식이요법, 건강을 위한 수맥파 및 전자파 차단재, 황토매트, 황토침대, 돌침대, 황토를 섬유사에 첨가해서 실을 만들어서 직조하여 사용케 하는 제품 등이 다수 개발되고 상품화되어 범람하고 있는 실정이다.Therefore, in order to overcome the various exercise therapy, diet, health water wave and electromagnetic wave shielding material, ocher mat, ocher bed, stone bed, loess is added to the fiber yarn to make a yarn, weaving and use a number of products, etc. Commercialized and flooded.

그러나, 이와 같은 기능성 제품들은 한결같이 하나의 용도에 국한되어 이용되었고, 박테리아균이나 세균과 같이 인체에 유해한 병원균의 항균 및 살균작용을 기대할 수 없었으며 악취를 흡착하여 탈취시키거나 분해시키지 못하였을 뿐 아니라 피로회복, 혈액순환 촉진과 같은 건강증진의 효과는 기대할 수가 없었다.However, these functional products were used only for one purpose, and they could not expect the antibacterial and bactericidal action of pathogens harmful to humans such as bacteria or bacteria, and they could not absorb or deodorize or decompose odors. The effects of health promotion such as fatigue recovery and blood circulation could not be expected.

본 발명은 상기한 문제점을 감안하여 창안한 것으로서, 그 목적은 침구용 솜에 운모(雲母)분말이 포함되어 자연상태에서 원적외선 및 음이온을 발산하는 운모분말의 특성인 공기 세정, 습도조절, 보온, 탈취 등의 효과에 의하여 사용자의 건강을 증진시켜 줄 수 있는 침구용 솜의 제조방법을 제공함에 있는 것이다.The present invention has been made in view of the above problems, the object of which is the characteristics of the mica powder to emit far-infrared rays and anions in the natural state, including the mica powder in bedding cotton, air cleaning, humidity control, thermal insulation, It is to provide a method for producing a bedding cotton that can improve the health of the user by the effect of deodorization.

상기한 목적을 달성하기 위한 본 발명의 특징은, 자연상태에서 천연광물로 존재하는 단사정계(單斜晶系)의 운모족(雲母族) 광물인 일라이트(illite)를 채취하 는 단계; 규사 50∼54중량%, 운모 35∼39중량%, 크로라이트 9∼11중량%의 성분으로 구성된 일라이트 광물을 굵은 입자들로 파쇄하여 불순물을 제거한 후 건조로에 투입하여 700∼800℃의 열을 가하면서 광물에 함유된 수분을 완전히 건조시키는 단계; 건조된 광물을 곱게 분쇄하여 1,000메시 이상의 입도(粒度)를 갖는 체로 걸러 미세 분말로 가공하는 단계; 광물 분말을 깨끗한 물에 침전시켜 고르게 저어주는 단계; 비중이 무거운 규사와 크로라이트는 가라앉고 비중이 가벼운 운모가 최상층에 위치되면 물을 버리고 운모를 추출하는 단계; 추출된 운모를 건조시킨 후 10∼100ppm의 농도와 1∼10nm의 크기를 갖는 은 나노 파우더에 고르게 혼합시키되 운모분말 88∼92중량%, 은 나노 파우더 8∼12중량%의 배합비율로 혼합시키는 단계; 고르게 혼합된 분말을 섬유제조용 폴리에스터 분말에 대해 3∼7중량%의 비율로 혼합하고, 고르게 혼합된 원료들을 압출기에 투입하여 180∼240℃의 온도로 가열하여 융해시킨 후 스크류로 압출하여 다이스에 뚫려진 방사공의 크기가 1.5∼2 데니어인 방사공으로 방사하여 모노필라멘트를 제조하는 단계; 상기 모노필라멘트를 연신하고 합사하여 멀티필라멘트상의 솜을 제조하는 단계를 포함하는 것을 특징으로 하는 침구용 솜의 제조방법에 의하여 달성될 수 있는 것이다.A feature of the present invention for achieving the above object is the step of collecting the illite which is a monoclinic mica group mineral present in the natural state as a natural mineral; An elite mineral composed of 50 to 54% by weight of silica sand, 35 to 39% by weight of mica and 9 to 11% by weight of chromite was crushed into coarse particles to remove impurities, and then introduced into a drying furnace to heat 700 to 800 ° C. Completely drying the moisture contained in the mineral while being added; Milling the dried mineral finely and filtering it into a fine powder with a sieve having a particle size of 1,000 mesh or more; Precipitating the mineral powder in clean water and stirring it evenly; If the heavy silica sand and chromite are sinking and the light gravity mica is located on the top layer, discarding water and extracting mica; The dried mica is dried and evenly mixed with silver nanopowder having a concentration of 10 to 100 ppm and a size of 1 to 10 nm, but mixed at a mixing ratio of 88 to 92 wt% of mica powder and 8 to 12 wt% of silver nano powder. ; The evenly mixed powder is mixed at a ratio of 3 to 7% by weight with respect to the polyester powder for fiber production, and the evenly mixed raw materials are introduced into an extruder, heated to a temperature of 180 to 240 ° C, melted, and extruded with a screw. Producing a monofilament by spinning with spinnerets having a size of 1.5 to 2 deniers; Stretching and weaving the monofilament to be achieved by a method for producing a bedding cotton, characterized in that it comprises the step of producing a multifilament-like cotton.

전술한 제조과정에 의하여 완성된 본 발명의 침구류용 솜은 운모에서 발산되는 음이온과 원적외선 방출효과에 의하여 사용자의 혈액순환을 촉진시켜 건강을 증진시킬 수 있을 뿐 아니라 운모와 나노 은이 갖는 강한 항균력과 살균효과에 의하 여 침구류에 기생하는 진드기나 인체에 유해한 각종 세균의 번식을 억제하는 한편 살균처리 하여 보다 위생적인 생활을 영위할 수 있고, 땀 냄새와 같은 자극성 있는 냄새를 흡착하여 제거할 수 있는 등의 이점이 있는 것이다.The bedding stuffing cotton of the present invention completed by the above-described manufacturing process can promote the blood circulation of the user by anion and far-infrared ray emission effect emitted from mica, as well as to improve the health of the mica and nano silver has strong antibacterial and sterilization By suppressing the growth of mites parasitic to bedding and various germs harmful to human body, sterilization can lead to more hygienic life, and it can absorb and remove irritating odor such as sweat smell. There is an advantage.

이하, 상기한 목적을 달성하기 위한 바람직한 실시예를 첨부된 제조공정도에 의하여 상세히 설명하면 다음과 같다.Hereinafter, described in detail by the accompanying manufacturing process drawings for a preferred embodiment for achieving the above object is as follows.

실시예Example

자연상태에서 천연광물로 존재하는 단사정계(單斜晶系)의 운모족(雲母族) 광물인 일라이트(illite)를 채취하였다.The illite, a monoclinic mica group, which exists as a natural mineral in nature, was collected.

상기 일라이트는 규사 50∼54중량%, 운모 35∼39중량%, 크로라이트 9∼11중량%의 성분으로 구성된 광물을 채취하였다.The said illite collected the mineral which consists of 50-54 weight% of silica sand, 35-39 weight% of mica, and 9-11 weight% of chromite.

이어서, 일라이트 광물을 굵은 입자들로 파쇄하여 불순물을 제거한 후 건조로에 투입하여 700∼800℃의 열을 가하면서 광물에 함유된 수분을 완전히 건조시켰다.Subsequently, the elite mineral was crushed into coarse particles to remove impurities, and then charged into a drying furnace to completely dry the moisture contained in the mineral while applying heat at 700 to 800 ° C.

이 단계에서는 파쇄된 광물 입자들을 선별한 후 물로 세척한 후 자연 건조시키는 단계가 더 포함되도록 하여 광물들의 표면에 함유된 미세한 이물질까지 깨끗하게 제거하는 것이 바람직하다.In this step, the crushed mineral particles are selected, washed with water, and then naturally dried to further remove fine foreign substances contained on the surfaces of the minerals.

상기 건조로는 열 가마 형태의 건조로 형태로 구성되어 광물을 투입하여 건조시켜도 무방하나 가마 내부를 통해 이동되는 컨베이어에 광물을 투입하여 약10∼ 20분간 이동시키면서 약750℃ 이상의 열을 가하여 건조시키면서 소성(燒成)하는 방법이 대량생산이 가능하여 바람직하다.The drying furnace is composed of a drying furnace in the form of a thermal kiln, and may be dried by adding minerals, but the mineral is put into a conveyor moving through the kiln and moved by heating for about 10 to 20 minutes while heating by applying heat of about 750 ° C. or higher to dry it. The method of forming is preferable because mass production is possible.

물론, 경우에 따라서는 경사지게 장착되어 가열되는 회전로에 광물을 투입하여 열 건조시킬 수 있는 것이므로 본 발명에서는 상기 광물들의 건조방법에 국한되는 것은 아니다.Of course, in some cases, it is possible to inject minerals into a rotary furnace that is mounted to be inclined and heated, so that the drying is not limited to the drying method of the minerals.

이어서, 건조된 광물을 곱게 분쇄하여 1,000메시 이상의 입도(粒度)를 갖는 체로 걸러 미세 분말로 가공하였다.Subsequently, the dried mineral was ground finely, and sieved through a sieve having a particle size of 1,000 mesh or more to be processed into fine powder.

상기 분쇄기는 커터들이 서로 마주보며 회전되고, 단계적으로 분쇄 입자가 작아지면 맷돌 식으로 갈아서 분쇄하는 통상적인 분쇄기를 사용하여 미세 분말로 가공한 후 필터를 이용하여 집진하여 분말을 포집하였다.The mill is rotated while the cutters face each other, and when the particles are gradually reduced, the mill is processed into a fine powder using a conventional mill that grinds and grinds to collect the powder by dust collection using a filter.

이어서, 곱게 분쇄된 광물 분말을 깨끗한 물에 침전시켜 고르게 저어주었더니 비중이 무거운 규사와 크로라이트는 가라앉고 비중이 가벼운 운모가 최상층에 위치되었다.Subsequently, finely ground mineral powder was precipitated in clean water and stirred evenly. The heavy silica sand and chromite subsided and the lighter mica was placed on the top layer.

이어서, 물은 버리고 최상층에 위치한 운모를 추출하였다.The water was then discarded and the mica located on the top layer was extracted.

이어서. 추출된 운모를 건조시킨 후 10∼100ppm의 농도와 1∼10nm의 크기를 갖는 은 나노 파우더에 고르게 혼합시켰다.next. The extracted mica was dried and evenly mixed with silver nano powder having a concentration of 10 to 100 ppm and a size of 1 to 10 nm.

이때, 이들의 배합비율은 운모분말 88∼92중량%, 은 나노 파우더 8∼12중량%가 되도록 고르게 혼합하였다.At this time, these compounding ratios were mixed evenly so that mica powder 88-92 weight% and silver nano powder 8-12 weight%.

본 발명에 사용되는 은 나노 파우더는 은(銀) 화합물 형태인 질산은(AgNO3) 0.85g를 수용액에 넣고, 이소프로판올(isopropanol) 30ml, 폴리비닐피롤리돈(polyvinylprrolidone) 5g 그리고 단량체로서 아크릴로니트릴(acrylonitrile) 85g를 넣어 질소퍼징 한 후 방사선을 조사하여 10∼100ppm의 농도와 1∼10nm의 크기를 갖는 은 나노 파우더를 제조하여 사용하였다.The silver nanopowder used in the present invention was added 0.85 g of silver nitrate (AgNO 3 ) in the form of a silver compound in an aqueous solution, 30 ml of isopropanol, 5 g of polyvinylpyrolidone, and acrylonitrile as a monomer. 85 g of acrylonitrile) was purged with nitrogen and irradiated with radiation to prepare silver nanopowder having a concentration of 10 to 100 ppm and a size of 1 to 10 nm.

물론, 상기 은 나노 파우더의 제조방법은 이미 알려져 있는 방법이므로 자세한 설명은 생략하였으며, 기타 전기적인 분해방법이나 화학적인 환원법 등을 사용하여 제조할 수 있는 것이므로 본 발명은 은 나노 파우더의 제조방법에 국한되는 것은 아니다.Of course, since the method for producing the silver nanopowder is a known method, a detailed description thereof has been omitted, and the present invention is limited to the method for preparing the silver nanopowder because it can be prepared using other electrical decomposition methods or chemical reduction methods. It doesn't happen.

은(銀) 성분은 예로부터 항균력과 살균력이 있는 것으로 밝혀져 있는 것으로, 은 나노의 강한 살균력과 항균력에 의하여 진드기, 유해세균(有害細菌) 및 곰팡이들의 번식을 억제하는 한편 살균처리 할 수 있는 것이므로 침구류를 보다 청결하게 사용할 수 있을 뿐 아니라 침구류가 세균에 감염되더라도 은 나노의 살균력에 의하여 1시간 이내에 세균이 99%이상 살균되어 제거되는 것이므로 매우 위생적으로 사용할 수 있는 것으로서 향균력을 갖는 침구용 솜의 대외 경쟁력을 최대한 높여줄 수 있는 등의 이점이 있는 것이다.Silver component has been found to have antimicrobial and bactericidal properties since ancient times, and it is capable of inhibiting the reproduction of mites, harmful bacteria and molds while sterilizing by the strong bactericidal and antimicrobial properties of silver nanos. Not only can the cleaners be used more cleanly, but even if the beddings are infected with bacteria, they can be used in a very hygienic way because the bacteria are sterilized by 99% or more within one hour by the sterilizing power of silver nano. There is an advantage such as to increase the external competitiveness as possible.

이어서, 고르게 혼합된 분말을 섬유제조용 폴리에스터 분말에 대해 3∼7중량%의 비율로 혼합하고, 고르게 혼합된 원료들을 압출기에 투입하여 180∼240℃의 온도로 가열하여 융해시킨 후 스크류로 압출하여 다이스에 뚫려진 방사공의 크기가 1.5∼2 데니어인 방사공으로 방사하여 모노필라멘트를 제조하였다.Subsequently, the evenly mixed powder is mixed at a ratio of 3 to 7% by weight based on the polyester powder for fiber production, the evenly mixed raw materials are introduced into an extruder, heated to a temperature of 180 to 240 ° C, melted, and extruded with a screw. The monofilament was prepared by spinning with a spinneret having a size of 1.5 to 2 deniers.

이어서, 상기 모노필라멘트를 연신하고 합사하여 멀티필라멘트상의 솜을 제 조하였다.Subsequently, the monofilament was stretched and spun together to prepare a multifilament-like cotton.

실험예 1 : 음이온 방출량의 측정시험Experimental Example 1 Measurement Test of Anion Release

발급번호 : KFI-110Issue Number: KFI-110

의뢰인 : 박월식· 홍종열 2008년 1월 7일Client: Park, Wol-Sik, Jong-Yeul Hong January 7, 2008

본 발명의 제조과정에 의하여 완성된 침구용 솜을 한국원적외선협회에 의뢰하여 실내온도 37℃, 습도 40%, 대기중 음이온 수 104/cc의 조건에서 음이온 방출량을 측정하였으며, 측정대상물에서 방출되는 음이온을 측정하여 단위체적 당 이온수로 표시하는 KFIA-FI-1042 시험규격을 사용하였다.Bedding cotton completed by the manufacturing process of the present invention was commissioned by the Korea Far Infrared Ray Association, the anion emission amount was measured under conditions of room temperature 37 ℃, humidity 40%, the number of anions in the air 104 / cc, anion released from the measurement object KFIA-FI-1042 test standard was used to measure and express the number of ions per unit volume.

그 결과는 표 2의 결에서 나타난 바와 같이 음이온 수가 950/cc로 나타나 대기중 음이온 수 104/cc보다는 약 9배에 가까운 음이온을 방출하는 것으로 나타났다.The results showed that the anion number was 950 / cc as shown in the result of Table 2, and it was released about 9 times more than the anion number 104 / cc in the air.

시험결과Test result 항목 시료명Item Sample Name 음이온(ION/cc)Anion (ION / cc) 기능성 화이버Functional fiber 950950

1) 시험방법 : KFIA-FI-10051) Test Method: KFIA-FI-1005

2) 시험편 : 시료의 크기 100×150×20mm2) Test piece: Sample size 100 × 150 × 20mm

실험예 2 : 원적외선 방사에너지의 측정시험Experimental Example 2 Measurement Test of Far Infrared Radiation Energy

발급번호 : KFI-108Issue Number: KFI-108

의뢰인 : 박월식· 홍종열 2008년 1월 7일Client: Park, Wol-Sik, Jong-Yeul Hong January 7, 2008

본 발명의 제조과정에 의하여 완성된 침구용 솜의 시료를 한국원적외선협회에 의뢰하여 실내온도 37℃의 조건에서 원적외선 방사에너지를 측정하였으며 그 결과는 표 3의 결과에서 나타난 바와 같이 원적외선 방사율(5∼20㎛)은 90.2%이고, 방사에너지(W/m2·㎛, 37℃)는 3.48ㅧ102으로 나타나 원적외선의 방사율이 높고 방사에너지의 양이 큰 것으로 나타났다.The sample of the cotton for bedding finished by the manufacturing process of the present invention was commissioned by the Korea Far Infrared Association to measure the far-infrared radiation energy under the condition of room temperature 37 ℃ and the result is far-infrared emissivity (5 ~ 20 µm) was 90.2%, and the radiation energy (W / m 2 · µm, 37 ° C.) was 3.48 × 10 2 , indicating that the far-infrared emissivity was high and the amount of radiation energy was large.

방사율(5~20㎛)Emissivity (5 ~ 20㎛) 방사에너지(W/m2·㎛, 37℃)Radiation energy (W / m 2 · ㎛, 37 ℃) 0.9020.902 3.48×102 3.48 × 10 2

비고) 본 시험은 의뢰자의 요구에 의하여 37℃의 조건에서 시험하였으며, ET-IR Spectrometer를 이용한 BLACK BODY 대비 측정결과임.Remarks) This test was conducted under the condition of 37 ℃ according to the request of the client, and it is the result of comparing the black body using the ET-IR Spectrometer.

시험 예 3 : 향균효과의 측정Test Example 3 Measurement of Antibacterial Effect

발급번호 : KFI-109Issue Number: KFI-109

의뢰인 : 박월식· 홍종열 2008년 1월 7일Client: Park, Wol-Sik, Jong-Yeul Hong January 7, 2008

본 발명의 제조과정에 의하여 완성된 침구용 솜의 시료를 한국원적외선협회에 의뢰하여 항균효과를 측정하였으며, 시험방법은 용기 내부에 18시간 배양한 포도상구균과 본 발명에 의하여 제조된 침구용 솜의 시료를 함께 투입하고, 다른 용기에는 포도상구균만 투입하여 18시간 후 대조시료와 시험시료의 균수를 비교하여 정균의 감소율을 측정하였다.The antimicrobial effect was measured by requesting a sample of the bedding cotton completed by the manufacturing process of the present invention to the Korea Far Infrared Association, the test method of the staphylococci cultured in a container for 18 hours and the bedding cotton prepared according to the present invention Samples were added together, and Staphylococcus aureus was added only to other containers. After 18 hours, bacterial counts of the control and test samples were compared to determine the rate of bacteriostatic reduction.

또한, 전술한 방법으로 18시간 배양한 폐렴균의 감소율을 함께 측정하였다.In addition, the reduction rate of pneumococci cultured for 18 hours by the method described above was measured together.

그 결과는 표 4의 정균 감소율(%) 시험결과에 나타난 바와 같이, 24시간 후 정균의 농도를 측정하였더니 시료가 투입된 포도상구균의 배양용기에서는 정균 감소율이 88.2%로 나타났고, 시료가 투입된 폐렴균의 배양용기에서는 정균 감소율이 84.0%로 나타나 침구용 솜 시료의 살균 및 항균효율이 매우 높은 것으로 측정되었으며, 시료가 투입되지 않은 용기에는 정균의 수가 오히려 증가되는 것으로 나타났다.As a result of the bacterium reduction rate (%) test results of Table 4, the concentration of bacteriostatic bacteria was measured after 24 hours, and the bacteriostatic rate was 88.2% in the culture vessel of Staphylococcus aureus into which the sample was added. In the culture vessel of the bacteriostatic reduction rate was 84.0%, it was determined that the sterilization and antimicrobial efficiency of the bedding cotton sample was very high, the number of bacilli was rather increased in the container without the sample.

시험항목Test Items 시료구분Sample classification 초기농도Initial concentration 24시간 후 농도Concentration after 24 hours 정균감소율(%)Bacteriostatic reduction rate (%) 포도상구에 의한 항균시험Antibacterial Test by Staphylococcus 표준표Standard Table 6.4×104 6.4 × 10 4 3.4×106 3.4 × 10 6 -- 기능성 화이버Functional fiber 4.0×104 4.0 × 10 4 88.288.2 폐렴균에 의한 항균시험Antibacterial test by pneumococcal 표준표Standard Table 7.0×104 7.0 × 10 4 4.0×106 4.0 × 10 6 -- 기능성 화이버Functional fiber 6.4×105 6.4 × 10 5 84.084.0

(주) 배지상의 균수는 희석배수를 곱하여 산출한 것임.(Note) The number of bacteria on the medium is calculated by multiplying the dilution factor.

1) 시험방법 : KS K 0693-20061) Test Method: KS K 0693-2006

2) 사용균주2) Use strain

Staphylococcus aureus ATCC 6538 Staphylococcus aureus ATCC 6538

Klebsiella pneumoniae ATCC 4352 Klebsiella pneumoniae ATCC 4352

3) 비이온계면활성제 : 접종균에 0.05% 비이온계면활성제 사용(Snogen)3) Nonionic Surfactant: 0.05% nonionic surfactant is used for inoculating bacteria (Snogen)

4) 표준포 : KS K 0905 염색견뢰도용 첨부백포(Cotton)4) Standard fabric: KS K 0905 Dyeing fastness

5)용도 품질관리5) Use Quality Control

한편, 본 발명에 사용된 운모의 특성은 다음과 같다. 즉, 운모(雲母, mica)는 화강암 중의 중요한 조암광물로서, 층상 규산염광물이다. 굳기는 2.5∼4, 비중은 2.75∼3.2, 황색, 갈색, 녹색을 띤다. 성분과 성질에 따라 백운모, 소다운모, 흑운모, 금운모, 홍운모, 진발다이트 등이 있다. On the other hand, the characteristics of the mica used in the present invention are as follows. In other words, mica is an important coarse mineral in granite, a layered silicate mineral. Hardness 2.5-4, specific gravity 2.75-3.2, yellow, brown, green. Depending on the ingredients and properties, there are muscovite, cattle down, biotite, gold mica, red mica, Jinbalite.

또한, 운모는 자연상태에서 음이온 및 원적외선을 방사하고, 미립 물질을 흡착하거나 크기가 다른 미립 물질을 분리시키는 특성에 의하여 침구류에 기생하는 진드기, 유해세균(有害細菌) 및 곰팡이들의 번식을 억제할 수 있을 뿐 아니라 땀 냄새와 같은 자극성 있는 냄새를 흡착하여 제거할 수 있는 것이다.In addition, mica can suppress the reproduction of mites, harmful bacteria and fungi parasitic in beddings by the nature of radiating anions and far infrared rays in a natural state and adsorbing particulates or separating particulates of different sizes. In addition, it can absorb and remove irritating odors such as sweat odors.

전술한 제조과정에 의하여 완성된 본 발명의 침구류용 솜은 운모에서 발산되는 음이온과 원적외선 방출효과에 의하여 사용자의 혈액순환을 촉진시켜 건강을 증진시킬 수 있을 뿐 아니라 운모와 나노 은이 갖는 강한 항균력과 살균효과에 의하여 침구류에 기생하는 진드기나 인체에 유해한 각종 세균의 번식을 억제하는 한편 살균처리 하여 보다 위생적인 생활을 영위할 수 있고, 땀 냄새와 같은 자극성 있는 냄새를 흡착하여 제거할 수 있는 등의 이점이 있는 것으로서 침구용 솜의 대외 경쟁력을 최대한 높여줄 수 있는 것이다.The bedding stuffing cotton of the present invention completed by the above-described manufacturing process can promote the blood circulation of the user by anion and far-infrared ray emission effect emitted from mica, as well as to improve the health of the mica and nano silver has strong antibacterial and sterilization By suppressing the proliferation of mites parasitic to bedding and various germs harmful to human body, sterilization can lead to more hygienic life, and it can absorb and remove irritating odor such as sweat smell. As there is an advantage that can increase the external competitiveness of the bedding cotton as possible.

이상에서는 본 발명의 바람직한 실시예에 대하여 도시하고 또한 설명하였으나, 본 발명은 상기한 실시예에 한정되지 아니하며, 청구범위에서 청구하는 본 발명의 요지를 벗어남이 없이 당해 본 발명이 속하는 분야에서 통상의 지식을 가진 자라면 누구든지 다양한 변형 실시가 가능한 것은 물론이고, 그와 같은 변경은 기재된 청구범위 내에 있게 된다.Although the preferred embodiments of the present invention have been illustrated and described above, the present invention is not limited to the above-described embodiments, and the present invention is not limited to the above-described embodiments without departing from the spirit of the present invention as claimed in the claims. Various modifications can be made by those skilled in the art, and such modifications are intended to fall within the scope of the appended claims.

도 1은 본 발명의 제조과정을 순차적으로 나열한 제조공정도.1 is a manufacturing process chart sequentially listing the manufacturing process of the present invention.

Claims (1)

자연상태에서 천연광물로 존재하는 단사정계(單斜晶系)의 운모족(雲母族) 광물인 일라이트(illite)를 채취하는 단계;Collecting illite which is a monoclinic mica group mineral present in natural state as a natural mineral; 규사 50∼54중량%, 운모 35∼39중량%, 크로라이트 9∼11중량%의 성분으로 구성된 일라이트 광물을 굵은 입자들로 파쇄하여 불순물을 제거한 후 건조로에 투입하여 700∼800℃의 열을 가하면서 광물에 함유된 수분을 완전히 건조시키는 단계;An elite mineral composed of 50 to 54% by weight of silica sand, 35 to 39% by weight of mica and 9 to 11% by weight of chromite was crushed into coarse particles to remove impurities, and then introduced into a drying furnace to heat 700 to 800 ° C. Completely drying the moisture contained in the mineral while being added; 건조된 광물을 곱게 분쇄하여 1,000메시 이상의 입도(粒度)를 갖는 체로 걸러 미세 분말로 가공하는 단계;Milling the dried mineral finely and filtering it into a fine powder with a sieve having a particle size of 1,000 mesh or more; 광물 분말을 깨끗한 물에 침전시켜 고르게 저어주는 단계;Precipitating the mineral powder in clean water and stirring it evenly; 비중이 무거운 규사와 크로라이트는 가라앉고 비중이 가벼운 운모가 최상층에 위치되면 물을 버리고 운모를 추출하는 단계;If the heavy silica sand and chromite are sinking and the light gravity mica is located on the top layer, discarding water and extracting mica; 추출된 운모를 건조시킨 후 10∼100ppm의 농도와 1∼10nm의 크기를 갖는 은 나노 파우더에 고르게 혼합시키되 운모분말 88∼92중량%, 은 나노 파우더 8∼12중량%의 배합비율로 혼합시키는 단계;The dried mica is dried and evenly mixed with silver nanopowder having a concentration of 10 to 100 ppm and a size of 1 to 10 nm, but mixed at a mixing ratio of 88 to 92 wt% of mica powder and 8 to 12 wt% of silver nano powder. ; 고르게 혼합된 분말을 섬유제조용 폴리에스터 분말에 대해 3∼7중량%의 비율로 혼합하고, 고르게 혼합된 원료들을 압출기에 투입하여 180∼240℃의 온도로 가열하여 융해시킨 후 스크류로 압출하여 다이스에 뚫려진 방사공의 크기가 1.5∼2 데니어인 방사공으로 방사하여 모노필라멘트를 제조하는 단계;The evenly mixed powder is mixed at a ratio of 3 to 7% by weight with respect to the polyester powder for fiber production, and the evenly mixed raw materials are introduced into an extruder, heated to a temperature of 180 to 240 ° C, melted, and extruded with a screw. Producing a monofilament by spinning with spinnerets having a size of 1.5 to 2 deniers; 상기 모노필라멘트를 연신하고 합사하여 멀티필라멘트상의 솜을 제조하는 단계를 포함하는 것을 특징으로 하는 침구용 솜의 제조방법.Stretching and fusing the monofilament to produce a cotton for bedding, characterized in that it comprises the step of producing a multifilament-like cotton.
KR1020080007268A 2008-01-23 2008-01-23 a making method of bedclothes emitting an anion KR20090081283A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101315633B1 (en) * 2012-04-03 2013-10-08 이동욱 Resin composition including sericite powders, manufacturing method thereof and plastic goods using the same
KR102137165B1 (en) * 2019-03-29 2020-07-23 (주)엠엠바이오 Bag comprising biotite powder having brain wave stabilization by improving blood circulation

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101315633B1 (en) * 2012-04-03 2013-10-08 이동욱 Resin composition including sericite powders, manufacturing method thereof and plastic goods using the same
KR102137165B1 (en) * 2019-03-29 2020-07-23 (주)엠엠바이오 Bag comprising biotite powder having brain wave stabilization by improving blood circulation

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