KR20090004048A - Cosmetic composition for cleansing having 3 layered structure and manufacturing method thereof - Google Patents

Cosmetic composition for cleansing having 3 layered structure and manufacturing method thereof Download PDF

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KR20090004048A
KR20090004048A KR1020070067936A KR20070067936A KR20090004048A KR 20090004048 A KR20090004048 A KR 20090004048A KR 1020070067936 A KR1020070067936 A KR 1020070067936A KR 20070067936 A KR20070067936 A KR 20070067936A KR 20090004048 A KR20090004048 A KR 20090004048A
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weight
parts
cosmetic composition
mixing
cleansing
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KR1020070067936A
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Korean (ko)
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유광호
강세훈
채희원
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한국콜마 주식회사
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/03Liquid compositions with two or more distinct layers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

A cleansing cosmetic composition having a triple layered structure, and a method for preparing the cleansing cosmetic composition are provided to prevent acidification and to improve appearance. A cleansing cosmetic composition having a triple layered structure comprises a lowermost layer part which comprises 1-10 parts by weight of water and 15-30 parts by weight of coconut oil fatty acid polyoxyethylene glycerine; a middle layer part which comprises 15-40 parts by weight of glycerin; and an uppermost layer part which comprises 20-50 parts by weight of a mineral oil. Preferably the mineral oil is liquid petroleum.

Description

3층구조를 갖는 클렌징용 화장료 조성물 및 그의 제조방법 {Cosmetic composition for cleansing having 3 layered structure and manufacturing method thereof}Cosmetic composition for cleansing having a three-layer structure and a method for manufacturing the same {Cosmetic composition for cleansing having 3 layered structure and manufacturing method

본 발명은 3층구조를 갖는 클렌징용 화장료 조성물 및 그의 제조방법에 관한 것으로 특히, 세정효과를 갖는 계면활성제로서 천연계면활성제인 야자유지방산폴리옥시에틸렌글리세린을 포함하며, 조성물 자체의 외양이 3층의 층상구조를 갖도록 하여 미려한 외관을 갖도록 한 3층구조를 갖는 클렌징용 화장료 조성물 및 그의 제조방법에 관한 것이다.The present invention relates to a cosmetic composition for cleansing having a three-layer structure and a method for manufacturing the same, and particularly, a palm oil fatty acid polyoxyethylene glycerine which is a natural surfactant as a surfactant having a cleaning effect. It relates to a cosmetic composition for cleansing having a three-layer structure to have a layered structure to have a beautiful appearance and a manufacturing method thereof.

촉촉하고 윤기 있는 피부상태를 유지하기 위해서는 피부가 적당한 양의 수분을 포함하고 있어야 하며, 이를 위해서는 피부의 청결을 유지하여야 하고, 세정 시 세정작용 뿐만 아니라 피부보호 및 보습작용을 하는 우수한 세정제의 사용이 필수적이다. 이를 위해서 널리 사용되는 비누에는 여러 종류가 있으나, 우리가 일상의 피부 세정에 사용되는 비누는 고급 지방산의 알칼리염으로서 보통 유지를 가성소다 또는 가성칼리로 비누화시켜서 제조한다. 따라서 비누의 수용액은 알칼리성이 강하고 강한 음이온성 계면활성을 나타내는데 이는 피부 등 생체에 바람직하지 못하다.In order to maintain a moist and glossy skin condition, the skin must contain an appropriate amount of moisture. For this purpose, the skin must be kept clean, and the use of an excellent detergent that protects and moisturizes the skin as well as cleaning It is essential. There are many kinds of soaps widely used for this purpose, but the soaps we use for daily skin cleansing are alkali salts of higher fatty acids and are usually prepared by saponifying fat or oil with caustic soda or caustic calories. Therefore, the aqueous solution of soap has a strong alkalinity and shows a strong anionic surface activity, which is not preferable for the living body such as skin.

피부 세정제의 일종인 보디클렌저를 살펴보면, 이는 전신 세정제로서 음이온 계면활성제와 지방산비누를 주성분으로 하고 있고, 그 외에 피부보호제로서 트리글리세라이드 오일, 모노에스테르 오일, 단백질 및 그 유도체, 보습제 등이 함유되어 있다.When looking at the body cleanser which is a kind of skin cleanser, it is a whole body cleanser, which is mainly composed of anionic surfactant and fatty acid soap, and also contains triglyceride oil, monoester oil, protein and its derivatives, and moisturizer as skin protectant. .

그러나 이러한 종래의 피부 세정제에는 많은 문제점이 있다. 비누의 경우, 우지를 원료로 한 것은 산소라디칼에 의해 일어나는 산패에 기인하는 장기간 보존시의 변취, 변색, 자극 등의 경향이 나타나서 우지의 산패를 막거나 지연시키기 위한 항산화 물질로서 페놀형의 하이드로퀴논, 피로갈롤 등을 사용하여 왔으나, 이들은 피부자극 등의 부작용을 유발하기 때문에 천연 항산화제인 비타민 E, 아스코르브산을 레시틴과 함께 사용하여 왔다. 레시틴은 하이드로퀴논과 공존할 때에는 산화 방지효력을 발휘하고 비타민 E와 공존시 비타민 E의 산화방지 능력을 상승시키는 것으로 알려져 있다.However, these conventional skin cleaners have many problems. In the case of soap, the raw material of tallow is phenolic hydroquinone as an antioxidant substance to prevent or delay the fate of tallow due to the tendency of discoloration, discoloration, and irritation during long-term storage due to rancidity caused by oxygen radicals. , Pyrogallol, and the like, but these have caused side effects such as skin irritation, and natural antioxidants such as vitamin E and ascorbic acid have been used together with lecithin. Lecithin is known to exert an antioxidant effect when coexisting with hydroquinone and to increase the antioxidant capacity of vitamin E when coexisting with vitamin E.

또한 종래의 피부용의 클렌저들은 대부분 단순히 오물을 계면활성 작용으로 세정하는 효과에 불과하며, 점점 다양화되는 소비자들의 미적인 요구들을 수용하기에는 한계가 있다는 문제가 있었다.In addition, conventional skin cleansers are merely an effect of simply cleaning the dirt by the surfactant action, there was a problem that there is a limit to accommodate the increasingly diverse aesthetic needs of consumers.

본 발명은 위와 같은 종래 기술의 문제점을 해결하기 위하여 창안한 것으로 세정효과를 갖는 계면활성제로서 천연계면활성제인 야자유지방산폴리옥시에틸렌글리세린을 포함하며, 조성물 자체의 외양이 3층의 층상구조를 갖도록 하여 미려한 외관을 갖도록 함은 물론 다층구조로 미셀화된 화장료 조성물에서 상기 천연계면활성제인 야자유지방산폴리옥시에틸렌글리세린이 3층구조의 최내층에 위치되도록 함으로써 천연물의 문제점인 산패를 예방토록 하기 위한 것이다.The present invention was devised to solve the above problems of the prior art, and includes a palm oil fatty acid polyoxyethylene glycerine which is a natural surfactant as a surfactant having a cleaning effect, so that the appearance of the composition itself has a three-layered layer structure. In order to have a beautiful appearance as well as to prevent the rancidity, which is a problem of natural products, the natural surfactant palm oil fatty acid polyoxyethylene glycerine is located in the innermost layer of the three-layer structure in the multi- micelle cosmetic composition.

상기한 바와 같이 본 발명의 목적을 달성하기 위한 3층구조를 갖는 클렌징용 화장료 조성물은, 물 1 내지 10중량부와 야자유지방산폴리옥시에틸렌글리세린 15 내지 30중량부를 포함하여 이루어지는 최하층부; 글리세린 15 내지 40중량부를 포함하여 이루어지는 중층부; 및 미네랄오일 20 내지 50중량부를 포함하여 이루어지는 상층부;들을 포함하여 이루어진다.As described above, the cosmetic composition for cleansing having a three-layer structure for achieving the object of the present invention, the lowest layer comprising 1 to 10 parts by weight of water and 15 to 30 parts by weight of palm oil fatty acid polyoxyethylene glycerin; A middle layer comprising 15 to 40 parts by weight of glycerin; And an upper layer part including 20 to 50 parts by weight of mineral oil.

상기에서 미네랄오일은 리퀴드 페트로라툼이 될 수 있다.In the mineral oil may be liquid petrolatum.

또한, 본 발명의 목적을 달성하기 위한 3층구조를 갖는 클렌징용 화장료 조성물의 제조방법은, (1) 물 1 내지 10중량부와 야자유지방산폴리옥시에틸렌글리세린 15 내지 30중량부를 혼합하는 수상부 준비단계; (2) 상기 수상부 준비단계에서 수득되는 수상부에 글리세린 15 내지 40중량부를 혼합하는 제1혼합단계; (3) 상기 제1혼합단계에서 수득되는 혼합물에 미네랄오일 20 내지 50중량부를 혼합하는 제2혼합단계;들을 포함하여 이루어진다.Moreover, the manufacturing method of the cosmetic composition for cleansing which has a three-layered structure for achieving the objective of this invention is (1) water phase preparation which mixes 1-10 weight part of water and 15-30 weight part of palm oil fatty acid polyoxyethylene glycerine. step; (2) a first mixing step of mixing 15 to 40 parts by weight of glycerin to the water phase obtained in the water phase preparation step; (3) a second mixing step of mixing 20 to 50 parts by weight of mineral oil in the mixture obtained in the first mixing step;

이하, 본 발명을 구체적인 실시예를 참조하여 상세히 설명한다.Hereinafter, the present invention will be described in detail with reference to specific examples.

본 발명에 따른 3층구조를 갖는 클렌징용 화장료 조성물은, 물 1 내지 10중량부와 야자유지방산폴리옥시에틸렌글리세린 15 내지 30중량부를 포함하여 이루어 지는 최하층부; 글리세린 15 내지 40중량부를 포함하여 이루어지는 중층부; 및 미네랄오일 20 내지 50중량부를 포함하여 이루어지는 상층부;들을 포함하여 이루어짐을 특징으로 한다. 즉, 본 발명에 따른 화장료 조성물은 최하층부, 중층부 및 상층부의 3층구조로 이루어지며, 천연의 계면활성제인 야자유지방산폴리옥시에틸렌글리세린이 최하층 내에 포함되어 산패 등이 예방됨과 동시에 3층의 구조로 이루어져 겉으로 보기에도 미려한 외관을 제공함을 특징으로 한다. 또한, 실질적으로 최하층부가 물, 바람직하게는 정제수와 세정기능을 하는 천연의 계면활성제인 야자유지방산폴리옥시에틸렌글리세린을 포함하여 이루어지며, 이들은 모두 피부에 대해 안정적이고, 무해하여 장기간 사용하는 경우에도 안전하며, 상기 최하층 상에 형성되는 중층도 천연물질의 하나인 글리세린으로 이루어지고, 상층부 역시 미네랄오일로 이루어지며, 이들 글리세린과 미네랄오일 역시 장업계에서는 전통적으로 오래전부터 피부에 적용되는 화장품의 원료로 사용될 정도로 그 안정성이 입증된 것임은 이해될 수 있는 것이다. 상기 최하층부는 상기한 수상부에 의해 형성된다.The cosmetic composition for cleansing having a three-layer structure according to the present invention comprises: a lowermost layer comprising 1 to 10 parts by weight of water and 15 to 30 parts by weight of palm oil fatty acid polyoxyethylene glycerin; A middle layer comprising 15 to 40 parts by weight of glycerin; And an upper layer part including 20 to 50 parts by weight of mineral oil. That is, the cosmetic composition according to the present invention is composed of a three-layer structure of the lowermost part, the middle part and the upper part, and the palm oil fatty acid polyoxyethylene glycerin, which is a natural surfactant, is contained in the lowermost layer to prevent rancidity and the like. It consists of providing a seemingly beautiful appearance. In addition, the bottom layer substantially contains water, preferably purified water and palm oil fatty acid polyoxyethyleneglycerin, which is a natural surfactant that has a washing function, all of which are stable to the skin and are safe for long-term use. The middle layer formed on the lowermost layer is made of glycerin, which is one of natural substances, and the upper layer is made of mineral oil, and these glycerin and mineral oil are also traditionally used as raw materials for cosmetics applied to skin for a long time in the industry. It is understood that the stability is proven to the extent. The lowermost layer portion is formed by the above water phase portion.

상기 상층부를 구성하는 미네랄오일은 바람직하게는 리퀴드 페트로라툼이 될 수 있다. 페트로라툼은 석유의 윤활유 유분(溜分)을 용제탈랍(溶劑脫蠟)하여 얻어진 연질(軟質)의 비결정성(非結晶性) 또는 미(微)결정성 왁스에, 윤활유의 중질(重質) 유분을 섞어서 반죽한 반(半)고체상태의 혼합물을 일컫는 것이며, 정제도가 가장 높은 것을 바셀린이라고도 한다. 주로 석유화학에서 쓰이는 말이며, 연고 등 의약용과 녹 방지제에 쓰인다. 정제도(精製度)가 낮은 것은 녹색이며, 백토처리(白土處理)한 것은 연한 갈색이고, 더욱 고도로 정제하면 무색에 가까워진다. 이 러한 페트로라툼은 반고체상에서 액상에까지 다양한 형태로 제품화된 것을 구입하여 사용할 수 있음은 당업자에게는 용이하게 이해될 수 있는 것이다. 본 발명에서는 특히 액상 페트로라툼(liquid petrolatum)을 사용한다.The mineral oil constituting the upper layer may be preferably liquid petrolatum. Petrolatum is a soft non-crystalline or microcrystalline wax obtained by solvent dewaxing of lubricating oil fraction of petroleum, and the heavy weight of lubricating oil. It refers to a mixture of semi-solid state kneaded with oil, and also called petrolatum with the highest degree of purification. It is mainly used in petrochemicals, and is used in medicines such as ointments and rust inhibitors. The lower the degree of refining, the greener, the more white-treated is light brown, and the more highly purified, the more colorless it becomes. Such petrolatum can be easily used by those skilled in the art can be purchased and used in a variety of forms from semi-solid to liquid phase. Especially in the present invention, liquid petrolatum is used.

본 발명에 따른 상기 조성물에서의 각 성분들의 함량은 반복적인 실험을 통하여 최적의 혼합비로 선택된 것으로서, 상대적인 함량에 따른 차이를 구분하기 어려우며, 그에 따라 상대적인 함량이 아닌 절대적인 함량기준으로서 각 성분들의 함량을 중량부로 표시하였으며, 상기한 중량부의 범위를 벗어나는 경우, 안정한 제형의 3층구조의 화장료 조성물이 수득되지 않는 문제점이 있을 수 있다.The content of each component in the composition according to the present invention is selected as the optimum mixing ratio through repeated experiments, it is difficult to distinguish the difference according to the relative content, and thus the content of each component as an absolute content standard rather than relative content If expressed in parts by weight, and outside the above parts by weight, there may be a problem that a three-layered cosmetic composition of a stable formulation is not obtained.

또한, 본 발명의 목적을 달성하기 위한 3층구조를 갖는 클렌징용 화장료 조성물의 제조방법은, (1) 물 1 내지 10중량부와 야자유지방산폴리옥시에틸렌글리세린 15 내지 30중량부를 혼합하는 수상부 준비단계; (2) 상기 수상부 준비단계에서 수득되는 수상부에 글리세린 15 내지 40중량부를 혼합하는 제1혼합단계; (3) 상기 제1혼합단계에서 수득되는 혼합물에 미네랄오일 20 내지 50중량부를 혼합하는 제2혼합단계; 들을 포함하여 이루어짐을 특징으로 한다. Moreover, the manufacturing method of the cosmetic composition for cleansing which has a three-layered structure for achieving the objective of this invention is (1) water phase preparation which mixes 1-10 weight part of water and 15-30 weight part of palm oil fatty acid polyoxyethylene glycerine. step; (2) a first mixing step of mixing 15 to 40 parts by weight of glycerin to the water phase obtained in the water phase preparation step; (3) a second mixing step of mixing 20 to 50 parts by weight of mineral oil in the mixture obtained in the first mixing step; Characterized by including them.

상기 (1)의 수상부 준비단계는 물 1 내지 10중량부와 야자유지방산폴리옥시에틸렌글리세린 15 내지 30중량부를 혼합하는 것으로 이루어진다.The water phase preparation step of (1) comprises mixing 1 to 10 parts by weight of water and 15 to 30 parts by weight of palm oil fatty acid polyoxyethylene glycerine.

상기 (2)의 제1혼합단계와 상기 (3)의 제2혼합단계에서의 혼합은 장업계에서 통상적으로 사용되는 호모믹서(HOMO MIXER)와 같은 혼합기를 사용하여 수행될 수 있음은 당업자에게는 용이하게 이해될 수 있는 것이며, 이러한 혼합기 역시 국내외 유수의 제조업자들에 의해 상용적으로 제공되는 것을 구입하여 사용할 수 있을 정 도로 공지된 것으로 이해될 수 있는 것이다. 상기 혼합에서의 혼합시간 및 혼합속도(rpm) 등은 작업장의 주변온도 및 혼합기의 용량 등에 따라 달라질 수 있으며, 이러한 혼합은 당업자에게는 경험적으로나 또는 혼합기의 제조업자의 지시에 따라 적절히 수행될 수 있음은 당연히 이해될 수 있는 것이다.The mixing in the first mixing step of (2) and the second mixing step of (3) can be carried out using a mixer such as a homomixer (HOMO MIXER) commonly used in the industry. It is to be understood that such a mixer is also known to the extent that it can be purchased and used commercially provided by leading manufacturers at home and abroad. The mixing time and mixing speed (rpm) in the mixing may vary depending on the ambient temperature of the workplace and the capacity of the mixer, and the like may be appropriately performed by those skilled in the art or according to the manufacturer's instructions of the mixer. It can be understood.

본 발명은 특히 유색화장료를 지울 수 있는 계면활성제로서 야자유지방산폴리옥시에틸렌글리세린 계면활성제를 사용하였으며, 오일로는 미네랄오일을 사용하였다. 이때 3층상의 내용물이 형성되며, 사용 시, 소비자가 본 발명에 따른 조성물을 담은 용기를 흔들어 균일하게 만들고, 즉 믹싱(Mixing)을 하여 사용할 수 있도록 한다. 그 후, 혼합된 상기 조성물을 화장이 된 피부에 도포하여 피부에 마사지 하듯이 문지르면 피부에 도포된 화장료를 제거되게 된다.In the present invention, a palm oil fatty acid polyoxyethylene glycerine surfactant was used as a surfactant for erasing colored cosmetics, and mineral oil was used as an oil. At this time, the three-layered contents are formed, and when used, the consumer shakes the container containing the composition according to the present invention to make it uniform, that is, mixing (Mixing) to be used. Thereafter, the mixed composition is applied to the skin having been makeup and rubbed as if massaged to the skin to remove the cosmetic applied to the skin.

이하에서 본 발명의 바람직한 실시예 및 비교예들이 기술되어질 것이다.Hereinafter, preferred embodiments and comparative examples of the present invention will be described.

이하의 실시예들은 본 발명을 예증하기 위한 것으로서 본 발명의 범위를 국한시키는 것으로 이해되어져서는 안될 것이다.The following examples are intended to illustrate the invention and should not be understood as limiting the scope of the invention.

실시예Example 1 One

하기 표 1에 나타낸 조성에 따라 3층상 화장료 조성물을 제조하였으며, 그 제조 방법은 실시예 1을 기준으로 다음과 같다.To prepare a three-layer cosmetic composition according to the composition shown in Table 1, the preparation method is as follows based on Example 1.

(1) 정제수 5중량부와 야자유지방산폴리옥시에틸렌글리세린 20중량부를 혼합하는 수상부 준비단계; (1) an aqueous phase preparation step of mixing 5 parts by weight of purified water and 20 parts by weight of palm oil fatty acid polyoxyethylene glycerine;

(2) 상기 수상부 준비단계에서 수득되는 수상부에 글리세린 30중량부 및 방부제 0.15중량부를 혼합하는 제1혼합단계; (2) a first mixing step of mixing 30 parts by weight of glycerin and 0.15 parts by weight of a preservative to the water phase obtained in the water phase preparation step;

(3) 상기 제1혼합단계에서 수득되는 혼합물에 미네랄오일 44.85중량부를 혼합하는 제2혼합단계;(3) a second mixing step of mixing 44.85 parts by weight of mineral oil with the mixture obtained in the first mixing step;

들을 순차적으로 수행하여 본 발명에 따른 화장료 조성물을 수득하였다.They were carried out sequentially to obtain a cosmetic composition according to the present invention.

구분division 성분ingredient 실시예1Example 1 실시예2Example 2 실시예3Example 3 수상부Award 야자유지방산 폴리옥시에틸렌글리세린Palm oil fatty acid polyoxyethylene glycerine 2020 2222 24.524.5 정제수Purified water 55 66 77 제1혼합First mixture 글리세린glycerin 3030 3030 3333 방부제antiseptic 0.150.15 0.150.15 0.150.15 제2혼합Second mixture 미네랄 오일Mineral oil 44.8544.85 41.8541.85 35.3535.35

상기한 3층상 클렌징 화장료는 실시예 1, 2 및 3들에서 나타낸 함량비로 제조하였고, 상태를 테스트 한 결과, 실시예 1, 2, 3의 경우 모두 양호한 결과를 얻었으며, 실시예 3은 실시예 2에 비해서 낮은 상층부가 생성되었으며, 실시예 2는 실시예 1에 비해서 낮은 상층부가 생성 되었다. 세정력의 경우, 실시예 1, 2, 3 모두 양호한 결과를 얻었으며, 실시예 1, 2, 3이 서로 비슷한 세정력이 나왔으나, 그 중 실시예 3이 가장 좋은 세정력을 나타냄을 확인하였다.The three-layered cleansing cosmetics were prepared at the content ratios shown in Examples 1, 2, and 3, and tested as a result, all of Examples 1, 2, and 3 obtained good results, and Example 3 was Example Lower upper layer portion was generated than in Example 2, and Example 2 produced a lower upper layer portion as compared to Example 1. In the case of the cleaning power, Examples 1, 2, and 3 all obtained good results, and Examples 1, 2, and 3 were similar to each other, but it was confirmed that Example 3 showed the best cleaning power.

또한, 본 발명에 따른 실시예들의 효과를 입증하기 위한 대조군으로서 하기 표 2에 나타낸 조성에 따라 3층상 화장료 조성물을 제조하였으며, 그 제조 방법은 상기 실시예 1과 동일하게 수행하였다.In addition, a three-layer cosmetic composition was prepared according to the composition shown in Table 2 as a control for demonstrating the effect of the embodiments according to the present invention, the preparation method was performed in the same manner as in Example 1.

구분division 성분(중량%)Ingredient (% by weight) 비교예1Comparative Example 1 비교예2Comparative Example 2 수상부Award 야자유지방산 폴리옥시에틸렌글리세린Palm oil fatty acid polyoxyethylene glycerine 3030 1010 정제수Purified water 1010 2020 제1혼합First mixture 글리세린glycerin 1010 3030 방부제antiseptic 0.150.15 0.150.15 제2혼합Second mixture 미네랄 오일Mineral oil 49.8549.85 39.8539.85

상기한 유화타입 형태의 클렌징 화장료는 실시예 1, 2 및 3들과 비교예 1 및 2들에서 나타낸 함량비로 제조하였고, 상태를 테스트 한 결과, 실시예 1, 2, 3의 경우 모두 양호한 결과를 얻었다.The emulsion-type cleansing cosmetics were prepared in the content ratios shown in Examples 1, 2, and 3 and Comparative Examples 1 and 2, and tested as a result, and in the case of Examples 1, 2, and 3, all of them showed good results. Got it.

그러나 비교예 1과 같은 경우에는 3층상으로 분리가 되지 않는 현상이 있었으며, 비교예 2의 경우는 수상부와 혼합 1부가 서로 분리가 되지 않아서 2층상 형태가 되는 현상이 있었다. 따라서 실시예 1, 2, 3의 함량비로 제조 시 시각적으로 차별화되어 종래의 제형과는 차별화된 클렌징 화장료를 얻을 수 있음을 확인할 수 있었다.However, in the same case as in Comparative Example 1, there was a phenomenon that the separation into three layers was not possible. In Comparative Example 2, there was a phenomenon in which the water phase part and the mixed one part were not separated from each other and thus became a two-layered shape. Therefore, it could be confirmed that the cleansing cosmetics differentiated from the conventional formulations were visually differentiated when prepared in the content ratios of Examples 1, 2, and 3, respectively.

따라서 본 발명에 따르면 특히, 세정효과를 갖는 계면활성제로서 천연계면활성제인 야자유지방산폴리옥시에틸렌글리세린을 포함하며, 조성물 자체의 외양이 3층의 층상구조를 갖도록 하여 미려한 외관을 갖도록 한 3층구조를 갖는 클렌징용 화장료 조성물 및 그의 제조방법을 제공하는 효과가 있다.Therefore, according to the present invention, in particular, the surfactant having a washing effect includes a palm oil fatty acid polyoxyethylene glycerin which is a natural surfactant, and has a three-layer structure that has a beautiful appearance by having the appearance of the composition itself has a three-layered layered structure. It has the effect of providing the cosmetic composition for cleansing which has, and its manufacturing method.

이상에서 본 발명은 기재된 구체예에 대해서만 상세히 설명되었지만 본 발명의 기술사상 범위 내에서 다양한 변형 및 수정이 가능함은 당업자에게 있어서 명백한 것이며, 이러한 변형 및 수정이 첨부된 특허청구범위에 속함은 당연한 것이다.Although the present invention has been described in detail only with respect to the described embodiments, it will be apparent to those skilled in the art that various modifications and variations are possible within the technical scope of the present invention, and such modifications and modifications are within the scope of the appended claims.

Claims (3)

물 1 내지 10중량부와 야자유지방산폴리옥시에틸렌글리세린 15 내지 30중량부를 포함하여 이루어지는 최하층부; 글리세린 15 내지 40중량부를 포함하여 이루어지는 중층부; 및 미네랄오일 20 내지 50중량부를 포함하여 이루어지는 상층부;들을 포함하여 이루어짐을 특징으로 하는 3층구조를 갖는 클렌징용 화장료 조성물.The lowest layer part containing 1-10 weight part of water and 15-30 weight part of palm oil fatty acid polyoxyethylene glycerol; A middle layer comprising 15 to 40 parts by weight of glycerin; And an upper layer comprising 20 to 50 parts by weight of mineral oil; a cosmetic composition for cleansing having a three-layer structure comprising a. 제 1 항에 있어서,The method of claim 1, 상기에서 미네랄오일이 리퀴드 페트로라툼임을 특징으로 하는 3층구조를 갖는 클렌징용 화장료 조성물.The cosmetic composition for cleansing having a three-layer structure, characterized in that the mineral oil is liquid petrolatum. (1) 물 1 내지 10중량부와 야자유지방산폴리옥시에틸렌글리세린 15 내지 30중량부를 혼합하는 수상부 준비단계; (1) a water phase preparation step of mixing 1 to 10 parts by weight of water and 15 to 30 parts by weight of palm oil fatty acid polyoxyethylene glycerine; (2) 상기 수상부 준비단계에서 수득되는 수상부에 글리세린 15 내지 40중량부를 혼합하는 제1혼합단계; 및(2) a first mixing step of mixing 15 to 40 parts by weight of glycerin to the water phase obtained in the water phase preparation step; And (3) 상기 제1혼합단계에서 수득되는 혼합물에 미네랄오일 20 내지 50중량부를 혼합하는 제2혼합단계; (3) a second mixing step of mixing 20 to 50 parts by weight of mineral oil in the mixture obtained in the first mixing step; 들을 포함하여 이루어짐을 특징으로 하는 3층구조를 갖는 클렌징용 화장료 조성물의 제조방법.Method of producing a cosmetic composition for cleansing having a three-layer structure comprising a.
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WO2014018543A1 (en) * 2012-07-25 2014-01-30 Elc Management Llc Three-layered hair conditioning composition and consumer product
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WO2022208395A1 (en) 2021-03-30 2022-10-06 L'oreal Two phase water-based smudge-resistant make-up remover
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US9824051B2 (en) 2012-04-04 2017-11-21 Avocent Huntsville, Llc Access appliance providing direct display data channel (DDC) interface connection and stored monitor calibration information
WO2014018543A1 (en) * 2012-07-25 2014-01-30 Elc Management Llc Three-layered hair conditioning composition and consumer product
WO2022208395A1 (en) 2021-03-30 2022-10-06 L'oreal Two phase water-based smudge-resistant make-up remover
WO2022208394A1 (en) 2021-03-30 2022-10-06 L'oreal Multi-phase water-based smudge-resistant make-up remover
US11633332B2 (en) 2021-03-30 2023-04-25 L'oreal Multi-phase water-based smudge-resistant make-up remover
FR3125221A1 (en) 2021-07-13 2023-01-20 L'oreal TWO-PHASE, WATER-BASED, SMOKE-RESISTANT MAKE-UP REMOVER
FR3125222A1 (en) 2021-07-16 2023-01-20 L'oreal water-based, smudge-resistant multi-phase makeup remover

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