KR20050026648A - Beauty product manufacturing method for using very beginning milk and arbutin and thereof product - Google Patents

Abstract

A method for manufacturing functional cosmetics using very beginning milk and arbutin and the functional cosmetics thereof are provided, which functional cosmetics makes melanocytes such as discoloration and freckles to be faint due and inhibits formation of melanocytes to arbutin, and improves skin beauty. The method for manufacturing functional cosmetics comprises the steps of: heating an aqueous mixture comprising 66.8 to 80.2 wt.% of water, 0.50 wt.% of allantoin, 3 to 8.0 wt.% of butylene glycol, 1 to 5 wt.% of glycerin and 0.1 to 0.3 wt.% of methylparaben, and an oil mixture comprising 2.30 to 2.80 wt.% of cetanol, 2.0 to 2.8 wt.% of montanove, 0.7 to 1.4 wt.% of arlacel, 1 to 3 wt.% of beeswax, 1 wt.% of Apricot Kernel, 3.0 wt.% of mineral oil, 0.4 to 0.6 wt.% of squalane and 0.1 wt.% of propylparaben at 80 deg. C; adding the oil mixture into the aqueous mixture and emulsifying them for 10 minutes; cooling the mixture to 45 deg. C; adding additives comprising 1.0 wt.% of hyaluronic acid extract, 0.5 wt.% of green tea extract, 1.0 wt.% of very beginning milk and 2.0 wt.% of arbutin into the mixture and cooling the mixture to 40 deg. C; adding 0.2 wt.% of perfume into the mixture and cooling the mixture to 35 deg. C; and removing bubbles and inserting the mixture into a vessel.

Description

Method of manufacturing functional cosmetics using colostrum and arbutin and its products {BEAUTY PRODUCT MANUFACTURING METHOD FOR USING VERY BEGINNING MILK AND ARBUTIN AND THEREOF PRODUCT}

The present invention relates to a method of manufacturing functional cosmetics using colostrum and arbutin, and more particularly, to a method of manufacturing functional cosmetics using colostrum and arbutin and its products for whitening effect and skin protection and improvement.

Colostrum refers to milk secreted up to three days in freshly born cows. Colostrum contains glublins that perform the calf's immune function, and promotes the production of antibodies that can fight bacteria or toxins. In addition, colostrum not only increases muscle elasticity and strength, but also selectively dissolves body fat, so that it can be processed into diet foods, reversing skin elasticity, giving healthy skin, and promoting calcium growth and osteoporosis treatment. Effective in prevention

In addition, colostrum contains lgF-1 and GH, which stimulates brain activity, improves concentration, and increases serotonin levels to help bright and cheerful emotions.

Ingredients contained in colostrum include IgF-1, IgA, S-IgA, IgD and E, IgG, IgM and T-cell.

Looking at these factors in more detail, IgF-1 is a growth factor that contributes directly to development, which promotes energy conversion of fats, breaks down body fat, helps to concentrate brain activity, and helps concentration. As an immune factor contained in, it is a powerful antiviral antibody and acts as a broad antiviral against the invading virus.

And, S-IgA is secretory and found in saliva, tears, and mucous membranes. It works by preventing bacteria from penetrating into the body. IgD and E are highly viral resistant and control allergies.

IgG is the most important immune substance found in colostrum and is carried by lymphatic and circulatory systems to neutralize toxic substances and invaders. In 1994, clinical trials showed that not only staying in the gut, but also passing through the gut into the plasma kills the virus.

IgM, along with IgG, destroys bacteria and antibodies to the disease persist for many years or even a lifetime.

Insulin-like growth factor and transforming growth factor (TgF, IgF-1); Directly promotes the production of T-cells (viruses and cells that fight antigens), promotes wound healing, regulates blood sugar levels, lowers insulin needs, promotes muscle growth and regeneration, and strengthens fasting Prevent muscle protein disappearance It selectively burns body fat to use energy, contributes to weight control, and strengthens bones to provide treatment and prevention of osteoporosis.

As described above, colostrum secreted up to 3 days after delivery contains very useful elements compared to milk normally secreted, but the amount of colostrum is low and the effectiveness of colostrum is not recognized, and a significant amount of colostrum is not discarded or utilized.

The present invention is to provide a functional cosmetic manufacturing method and a product for the whitening effect and skin improvement using the useful elements and arbutin contained in colostrum.

As a means for implementing the functional cosmetic manufacturing method using colostrum, arbutin of the present invention, water, allantoin, butylene glycol (moisturizer), glycerin (Glycerin), methylparaben (preservative) mixed with The mixed mixture is defined as a water mixture,

Cetanol, thickeners (Beeswax, beeswax, Montanob 68EC, emulsifiers, alacel 165, emulsifiers, apricot kernel oil, skin oils, mineral oils) A mixture consisting of skin conditioning agent, squalane (skin conditioner), dimethicone (skin conditioner) and propylparaben (preservative) is defined as an oily mixture,

A mixture of hyaluronic acid extract, green tea extract, colostrum and arbutin added to protect the skin is defined as an additive.

Combination fragrance (TRW W-210291) for producing perfume is defined as fragrance.

The above-mentioned combination fragrance is a fragrance which combines bergamot oil, ylang-ylang oil, nialool, citronellol, hexylcinnamic aldehyde, gamma methylonone, lilyaldehyde, linalyl acetate, gamma decaractone, and apricincesis. Appearance is pale yellow, specific gravity is 1.004∼1.014 refractive index is 1.471∼1.481,

The sum of the water-based mixture, the oil-based mixture, the additive and the flavor is 100% by weight.

For reference, useful ingredients contained in colostrum are as follows.

Ingredients in Colostrum Number of live bacteria in colostrum Fat 3.62% Escherichia coli 22 × 10 ⁵ CFU / ML protein 11.82% Lactic acid bacteria 2.3 × 10 ⁵ CFU / ML Lactose 3.6% Yeast and Mold 2 × 10 ⁵ CFU / ML Immunoglobulin 40.04% Total bacteria 7.2 × 10 ⁵ CFU / ML Solid non fat (SNF) 15.38% Titratble Acidity 0.3% Solid content 18.94 pH 6.3%

<Example>

First, prepare an aqueous and oily mixture, additives and flavorings.

The aqueous mixture is prepared by mixing 66.8 to 80.2 wt% of water, 0.50 wt% of allantoin, 3 to 8.0 wt% of butylene glycol, 1 to 5 wt% of glycerin, and 0.1 to 0.3 wt% of methylparaben,

The oily mixture is 2.30-2.80 wt% cetanol, 2.0-2.8 wt% montanob, 0.7-1.4 wt% alacel 1-3 wt% apricot kernel oil 1 wt%, mineral oil 3.0 wt%, squalane 0.4-0.6 Prepare by mixing weight%, propylparaben 0.1% by weight,

The additive is prepared by mixing 1.0% by weight of hyaluronic acid extract, 0.5% by weight of green tea extract, 1.0% by weight of colostrum, and 2.0% by weight of arbutin, and 0.20% of fragrance (combined flavor: TRW W-210291) to flavor it. Prepared by adding%,

The additive is prepared by adding a 1.0% by weight hyaluronic acid extract, 0.5% by weight green tea extract 1.0% by weight colostrum, 2.0% by weight arbutin prepared additives, 0.20% by weight of fragrance is added.

A first step of heating the aqueous phase mixture (83.7% by weight) and the oily mixture (13.6% by weight) in each of the mixtures prepared as above to 80 ° C;

A second step of mixing and emulsifying the oil phase mixture in the aqueous phase mixture at 80 ° C. for 10 minutes;

Mixing and emulsifying for 10 minutes and then cooling to 45 ° C. while stirring;

Cooling to 45 ° C., adding an additive, and cooling the mixture to 40 ° C. again, followed by cooling;

A fifth step of cooling to 35 ° C. after adding the fragrance after cooling to 40 ° C. and

After cooling to 35 ° C., it is prepared in a sixth step of defoaming and filling into a container.

Allantoin described above is added for skin protection, and it is preferable to add 0.50% by weight. The reason for this is that when the content exceeds 0.5% by weight or more, the skin has a feeling of drying.

Butylene glycol (Butylene Glycol) is added to the skin moisturizing action, if more than 6.0% by weight, for example, if more than 10% by weight of the skin becomes greasy and oily, the face becomes heavy It may be generated, when added to 3% by weight or less, the moisturizing action is lowered, the content is preferably in the range of 3 to 8% by weight, more preferably 6.0% by weight.

Glycerin is added to moisturize the skin, and if it is added in excess of 5% by weight, the skin tends to be slippery and sticky, and is preferably in the range of 1 to 5% by weight, more preferably. 3% by weight.

Methylparaben (Methylparaben) is added as a preservative, 0.1 to 0.3% by weight is more suitable, more preferably 0.2% by weight, since if the addition amount is added more than 0.5% by weight may cause a problem that half the fragrance of the form Do.

Cetanol, Montanob 68EC, and Araxel (Arlacel 165) are added to stabilize the emulsification. As a preferred embodiment, Cetanol is 2.30 to 2.80 wt%, Montanob 68EC is 2.0 to 2.8 wt%, Ara The cell is preferably 0.7 to 1.4% by weight, more preferably 1.0% by weight.

The thickener (Beeswax) affects the viscosity of the functional cosmetics, the viscosity is increased when added to more than 3% by weight, the lower the addition ratio is lower the viscosity is thinner, so the preferred ratio is 1.0% by weight is good.

Apricot Kernel Oil, Mineral Oil Squalane, and Dimethicone have been added to provide shine to the skin. Oil is absorbed into the dermis layer of the skin to make the skin soft and supple, and also to make the skin elastic and shiny and to supply nutrition.

Propylparaben (Propylparaben) is added to maintain the efficacy and action without altering the cosmetic component is manufactured for a long time, 0.1% by weight is suitable.

The hyaluronic acid extract, green tea extract and colostrum are added to protect the skin from harmful oxygen such as fine dust, pollution and soot, and protect the skin. It acts to form a film to protect the skin from harmful external environment.

Here, the specific hyaluronic acid extract has excellent skin-friendliness and maintains moisture retention ability of the skin to maintain a long-term moisturizing condition. Green tea extract contains catechins for skin whitening, antioxidant activity and bacterial growth. It acts to suppress.

And colostrum is the IgG (immunoglobulin) contained in it provides antibacterial and antiviral action to the skin, the content is defined as 1.0% by weight for the most appropriate effect and skin improvement.

In addition, arbutin is a whitening agent with chemical structure similar to hydroquinone but with no toxicity to the human body. It is extracted from plants (mandarin orange, vineberry, and beetle) and penetrates deeply into the skin to produce melanin. It is a substance that inhibits whitening.

When the skin is exposed to ultraviolet rays, stress, or air pollution in the sun, free radicals, which are free radicals, are generated in the skin, and melanocytes (pigment cells) are activated by the stimulus. Activated pigment cells activate the action of the enzyme tyrosinase, which causes melanin pigmentation. As a result, tyrosine in melanocytes (tyrosine) is converted to melanin by tyrosinase (tyrosinase), which causes freckles and blemishes.

Arbutin acts on tyrosinea, an enzyme that produces melanin pigment, which causes freckles and blemishes, and strongly inhibits melanin pigment production.

As described above, the following results were obtained by testing the efficacy of the functional cosmetics prepared through the process in the first to sixth steps.

Contents and pH were tested in accordance with the standards and test methods for cosmetics 5, Annexes No. 2000-27 of the Korea Food and Drug Administration, and the peak retention time of the standard solution was the same in the test of arbutin of the prepared cosmetics according to the content test method.

In addition, in the arbutin content test as a functional whitening material, the cosmetics according to the present invention accurately weigh 20 mg of arbutin according to the present invention, add 50 mL of a mobile phase, disperse it with ultrasonic waves sufficiently, and then filter and put the mobile phase into exactly 100 mL. Accurately weigh 20mg and add the mobile phase to make 100ml to make standard solution. Take 10 µl of the sample solution and standard solution, and test by liquid chromatograph under the following conditions to obtain the peak areas A _T and A _s of each solution.

Amount of arbutin (C ₁₂ H ₁₆ O ₇ ) (mg) = Amount of arbutin standard (mg) × A _T / A _s

Operating conditions

Detector: UV absorbance (measuring wavelength 280 nm)

Column: A column filled with octadecylsilylated silica gel for liquid chromatograph of 5 µm in a stainless tube having an inner diameter of about 4.6 mm and a length of about 20 cm, or a similar column.

Column temperature: room temperature

Mobile phase ratio: Water: Methanol: Acetic acid mixture (5: 5: 1)

Flow rate: 0.7 mL / min

Result according to finished product content test

pH Meter: HANNA pH 211 Microprossor pH Meter

HPLC: Pump: Shimadzu LC-10AT VP

     Column: VPODS-Ⅱ (4.6mm × 250mm)

     Detector: Shimadzu LC-10AT VP

*Experiment result

Specimen Test Items Average Experiment 1 Experiment 2 Experiment 3 CLS11 Constellation fitness fitness fitness fitness Capacity - - - - pH 5.56 5.67 5.66 5.67 Test fitness fitness fitness fitness Content test 2.0029 1.9965 2.00121 2.0001 CLS12 Constellation fitness fitness fitness fitness Capacity - - - - pH 5.64 5.65 5.64 5.64 Test fitness fitness fitness fitness Content test 1.9915 1.9940 1.9944 1.9991 CLS13 Constellation fitness fitness fitness fitness Capacity - - - - pH 5.66 5.67 5.66 5.64 Test fitness fitness fitness fitness Content test 2.0050 1.9991 2.0067 2.0093

* Analysis

Arbutin Lot No. Sample amount Quantity of standard product Sample area (At) Standard standard area (As) Effective amount (mg) content(%) Average content (%) CLS11-1 1145 20.73 698382 633325 22.8594 1.9965 2.0029 CLS11-2 1135 697701 22.8372 2.0121 CLS11-3 1142 697836 22.8416 2.0001 CLS12-1 1137 692664 22.6723 1.9940 1.9915 CLS12-2 1140 694626 22.7365 1.9944 CLS12-3 1143 693545 22.7011 1.9861 CLS13-1 1135 693207 22.6901 1.9991 2.0050 CLS13-2 1129 692160 22.6558 2.0067 CLS13-3 1128 692429 22.6646 2.0093

As described above, the present invention manufactures functional cosmetics using colostrum and arbutin to cloud the melanocytes (pigment cells) such as freckles and freckles by whitening action of arbutin and to suppress the occurrence of bright and transparent skin. Not only does it work very beneficially, it is excellent in spreading, shine, and moisturizing, so that the skin can be fine and moist, not pull or shine, but also provide non-slip functional cosmetics.

Claims (2)

In the functional cosmetics manufacturing method having a whitening effect, Water phase mixtures were prepared by mixing 66.8-8.2% by weight of water, 0.50% by weight of allantoin, 3-8.0% by weight of butylene glycol, 1-5% by weight of glycerin, and 0.1-0.3% by weight of methylparaben, and prepared with 2.30-2.80% by weight of cetanol. %, Montanob 2.0 to 2.8% by weight, Aracel 0.7 to 1.4% by weight Thickener 1-3% by weight Apricot kernel oil 1% by weight, mineral oil 3.0% by weight, 0.4-0.6% by weight squalane, 0.1% by weight propylparaben To prepare an oil-based mixture by mixing, prepare a prepared additive mixture of 1.0% by weight of hyaluronic acid extract, 0.5% by weight of green tea extract 1.0% by weight of colostrum and 2.0% by weight of arbutin, add 0.20% by weight to flavor After preparing the spices, A first step of heating the aqueous phase mixture and the oil phase mixture to 80 ° C. in each of the prepared mixtures; A second step of mixing and emulsifying the oil phase mixture in the aqueous phase mixture at 80 ° C. for 10 minutes; Mixing and emulsifying for 10 minutes and then cooling to 45 ° C. while stirring; Cooling to 45 ° C., adding an additive, and cooling the mixture to 40 ° C. again, followed by cooling; A fifth step of cooling to 35 ° C. after adding the fragrance after cooling to 40 ° C. and Method for producing functional cosmetics using colostrum and arbutin, which is prepared by cooling to 35 ° C. and degassing and filling the container. Functional cosmetics, characterized in that prepared according to claim 1.