KR20030069659A - Preparation of Body Nutritional Cream Prepared by Natural Herb and Seaweeds - Google Patents

Preparation of Body Nutritional Cream Prepared by Natural Herb and Seaweeds Download PDF

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KR20030069659A
KR20030069659A KR1020020009581A KR20020009581A KR20030069659A KR 20030069659 A KR20030069659 A KR 20030069659A KR 1020020009581 A KR1020020009581 A KR 1020020009581A KR 20020009581 A KR20020009581 A KR 20020009581A KR 20030069659 A KR20030069659 A KR 20030069659A
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seaweeds
preparation
natural herbal
nutritional cream
seaweed
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KR1020020009581A
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Korean (ko)
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박영호
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박영호
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/06—Emulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706—Algae
    • A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82—Preparation or application process involves sonication or ultrasonication

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Cosmetics (AREA)

Abstract

PURPOSE: Provided is a preparation of body nutritional cream using natural herbs including Morus bombycis, Lingusticum chuangxiong Hort, Rheum undulatum and the like and seaweeds including sea tangle, brown seaweed, starfish and the like. CONSTITUTION: A preparation of body nutritional cream using natural herbs and seaweeds comprises the steps of: treating natural herbs including Morus bombycis, Lingusticum chuangxiong Hort, Rheum undulatum and the like and seaweeds including sea tangle, brown seaweed, starfish and the like with ultrasonic wave; concentrating the obtained extract by ultrafiltration; and concentrating the concentrate again by nano-filtration.

Description

천연 생약 및 해조류를 이용한 바디 영양크림 제조방법{Preparation of Body Nutritional Cream Prepared by Natural Herb and Seaweeds}Preparation of Body Nutritional Cream using Natural Herbs and Seaweeds {Preparation of Body Nutritional Cream Prepared by Natural Herb and Seaweeds}

본 발명은 천연 생약 및 해조류를 이용하여 바디 영양 크림을 제조하는 방법에 관한 것으로서 더욱 상세히는 상백피, 천궁, 번사엽 및 대황과 같은 천연 생약과 톳, 다시마, 미역, 불가사리와 같은 해조류를 이용하여 그 특정 유효 성분을 여러 추출방법(초음파, 한외여과법(ultrafiltration), 나노여과법(nanofiltration) 열수, 에탄올등)에 의하여 추출하여 피부에 그 성분들을 공급하여 피부를 통하여 직접 그 안전성 및 효과 증대를 바탕으로 피부 노화 및 신체의 여러 균형을 유지할 수 있도록 하는 것에 대한 제조방법이다.The present invention relates to a method for producing a body nutrition cream using natural herbal medicines and seaweeds, and more particularly, using natural herbal medicines such as baekbaekpi, cheonggung, fir leaf and rhubarb and seaweeds such as 톳, kelp, seaweed and starfish The specific active ingredient is extracted by various extraction methods (ultrasound, ultrafiltration, nanofiltration, hydrothermal, ethanol, etc.) and the ingredients are supplied to the skin to increase the safety and effectiveness directly through the skin. It is a manufacturing method for aging and maintaining the various balance of the body.

이에 유사한 선행 기술은 국내 특허 공고 제97-73572호(출원번호 97-43853) 에는 "바디 화장용 안료 조성물 및 그 조성물의 제조 방법"에 관하여 기재되어 있는 바, 이는 미역, 다시마, 염화나트륨 및 황토로부터 그 유효 성분을 추출하여 근육 탄력 부여 및 피부노화 방지 등의 목적으로 한 제조 방법을 개시하고 있는 것이다.Similar prior art is described in Korean Patent Publication No. 97-73572 (Application No. 97-43853) with reference to "body cosmetic pigment compositions and methods for preparing the compositions", which are prepared from seaweed, kelp, sodium chloride and loess. The present invention discloses a production method for the purpose of extracting the active ingredient and providing muscle elasticity and preventing skin aging.

그러나 이러한 선행 기술은 그 추출 과정에서 유기물 추출 및 무기물 추출, 혼합물에서 부터 순수 용액 추출, 색소 추출을 위해 -7±5℃ 의 동결실에서 3~8시간 해동 조작 1∼5회의 반복 조작 등 그 공정상의 복잡성과 경제성, 효과성 등의 문제점이 있다고 판단되는 것이다.However, these prior arts include organic extraction and inorganic extraction, pure solution extraction from the mixture, and 3-8 hours thawing in a freezing chamber at -7 ± 5 ℃ for pigment extraction. It is judged that there are problems such as complexity, economic feasibility, and effectiveness.

이에 본 발명에서는 인체에 유익한 천연 생약과 해조류를 이용하여 그 유효성분을 추출하고 혼합하여 바디 영양크림을 제조하는 제조방법을 제공하되, 보다 이상적인 제품을 제조하는 것이다.Accordingly, the present invention provides a manufacturing method for producing a body nutrition cream by extracting and mixing the active ingredient using natural herbal medicine and seaweed beneficial to the human body, to produce a more ideal product.

상기 목적을 달성하기 위하여 본 발명은 바디 영양크림을 제조함에 있어서, 천연 생약 및 해조류를 초음파처리하여 천연 생약 및 해조류에 함유된 유효성분을 추출하고, 상기 추출액을 이용하여 바디 영양크림으로 제조하는 것을 특징으로 하는 천연 생약 및 해조류를 이용한 바디 영양크림의 제조방법을 제공하고자 하는 것이다.In order to achieve the above object, the present invention, in the manufacture of body nutrition cream, to extract the active ingredient contained in the natural herbal medicine and seaweed by ultrasonic treatment of natural herbal medicine and seaweed, and to prepare a body nutrition cream using the extract solution It is to provide a method for producing a body nutrition cream using natural herbal and algae characterized in that.

도 1 : 본 발명의 바람직한 일실시예를 보인 제조공정도1 is a manufacturing process showing an embodiment of the present invention

도 1은 본 발명의 제조 방법을 보인 공정도로서, 본 발명은 바디 영양크림을 제조시 천연 생약 성분 및 해조류를 이용하여 선별, 세척 과정을 거쳐 초음파를 이용하여 그 대상물에 단계적 추출 방법을 적용함으로 원료 추출시 그 유효 및 특정 성분의 추출을 극대화하는 방법으로 제조할 수 있도록 한 것이다.1 is a process chart showing a manufacturing method of the present invention, the present invention is a raw material by applying a step-by-step extraction method to the object by using ultrasonic waves through the screening, washing process using natural herbal ingredients and seaweeds when manufacturing the body nutrition cream It is to be prepared in a way that maximizes the effective and extraction of specific components during extraction.

즉 본 발명에서는 각 재료(천연 생약 및 해조류)를 선별 후 추출 시 초음파(28khz)를 이용하여 약 5∼240분간 처리하였다.That is, in the present invention, each material (natural herbal medicine and seaweed) was treated for about 5 to 240 minutes using ultrasonic waves (28khz) at the time of selection and extraction.

추출된 유효성분들은 다시 한외여과법(ultrafiltration, MWCO, 20,000)을 이용해서 1차 추출 및 농축을 시킨 후, 나노여과법(nanofiltration, MWCO, 1,000)을 통해서 2차로 분자량에 따른 추출 및 농축을 하였다.The extracted active ingredients were first extracted and concentrated using ultrafiltration (ultrafiltration, MWCO, 20,000), and then extracted and concentrated according to molecular weight through nanofiltration (nanofiltration, MWCO, 1,000).

이하 본 발명의 실시예를 설명한다.Hereinafter, embodiments of the present invention will be described.

본 발명을 실현함에 있어서 사용되는 기기 및 재료 pH측정, 색상, 관능검사 등은 다음과 같다.Instrument and material pH measurement, color, sensory test and the like used in realizing the present invention are as follows.

사용기기는 아래와 같다.The equipment used is as follows.

본 발명의 실시예에서 사용한 초음파기기(Ultrasonic cleaner, UTA-152, Japan)의 크기는 가로×세로×높이가 32×12×14(단위:cm)로써 출력은 150W이며, 주파수는 28KHz 였다.The size of the ultrasonic cleaner (Ultrasonic cleaner, UTA-152, Japan) used in the embodiment of the present invention was 32 x 12 x 14 (unit: cm) in width x length x height, output was 150W, and frequency was 28KHz.

한외여과법(ultrafiltration)으로 사용된 membrane cartridge는 MPS-U20-P(MWCO 20,000, Max. Temp 70℃, 2.0 in. dia. by 25 in. long, KOCH Membrane System, Inc. 850 Main street Wilmington, MA. USA)를 사용하였다.Membrane cartridges used for ultrafiltration were MPS-U20-P (MWCO 20,000, Max. Temp 70 ° C, 2.0 in.dia. By 25 in.long, KOCH Membrane System, Inc. 850 Main street Wilmington, MA. USA).

나노여과법 (nanofiltration)으로 사용된 membrane cartridge는 MPS-36(MWCO 1,000, Max. Temp. 70℃, 2.0 in. dia. by 20 in. long, KOCH Membrane System, Inc. 850 Main street Wilmington, MA. USA)을 사용하였다.Membrane cartridges used for nanofiltration were MPS-36 (MWCO 1,000, Max. Temp. 70 ° C, 2.0 in.dia. By 20 in.long, KOCH Membrane System, Inc. 850 Main street Wilmington, MA.USA) ) Was used.

재료는 아래와 같다.The material is as follows.

상백피(한국산), 천궁(한국산), 번사엽(중국산), 대황(한국산) 등을 시중 약업사에서 구입하였고 톳, 미역, 다시마, 불가사리는 일반 시장에서 구입하여 사용하였다.Sangbaekpi (Korean), Cheonggung (Korean), Bunsa-Yeop (Chinese), and Rhubarb (Korean) were purchased from commercial pharmaceutical companies.

시료 추출은 다음과 같다.Sampling is as follows.

시료(상백피, 천궁, 번사엽, 대황, 톳, 미역, 다시마, 불가사리) 추출액 재료는 선별 후 초음파 기기를 이용하여 5∼240분간 처리하고 그 처리액을 추출시간별로 취하여 고형물을 포함한 것을 추출물로 하였다.After extracting the sample extracts (cephaly vulgaris, celery, fir leaf, rhubarb, shellfish, seaweed, seaweed, seaweed, starfish), the sample was treated for 5 to 240 minutes using an ultrasonic device, and the treated solution was taken for each extraction time to obtain an extract containing solids. .

본 발명에서 pH측정은 pH meter(Metrohm 632, Switzerland)를 사용하였으며, 색상측정은 색차계(CR-200, Minolta)를 사용하여 L. a. b. 값을 측정하였다.In the present invention, pH measurement was performed using a pH meter (Metrohm 632, Switzerland), color measurement using a colorimeter (CR-200, Minolta) L. a. b. The value was measured.

관능검사는 본 발명에 의해 제조된 크림의 관능검사는 잘 훈련된 10명의 패널요원에 의해서 냄새(시큼한 냄새, 비린 냄새, 청량한 냄새)등을 5점 강도법(아주 강하다 : 1점, 강하다 : 2점, 보통이다 : 3점, 약하다 : 4점, 아주 약하다 : 5점)으로 평점하여 유의성을 검증하였다.The sensory test of the cream prepared by the present invention was performed by ten well trained panelists, and the five-point intensity method (very strong: one point, strong: 2 points, normal: 3 points, weak: 4 points, very weak: 5 points).

사용감과 안정성 비교는 최종 제조된 제품에 대해 피시험자(30명)에게 5점 법(평점 : 5점(매우 우수), 4점(우수), 3점(우수), 2점(불량), 1점(매우 불량)에 의하여 평가하였다.In comparison with the feeling of use and stability, the 5-point method (Score: 5 points (very good), 4 points (good), 3 points (good), 2 points (bad), 1) It evaluated by the point (very bad).

또한 통계처리를 위한 모든 Data는 3반복한 것을 평균하였으며 결과는 표(1)(2)(3)(4)와 같다.In addition, all data for statistical processing averaged 3 repetitions and the results are shown in Table (1) (2) (3) (4).

<결과> 추출시간에 따른 pH의 변화는 큰 차이를 보이지 않았다.<Result> There was no significant difference in pH change with extraction time.

<결과> L(밝기 : Lightness) 값은 추출처리시간에 따라서 값이 떨어졌으나 a(색상 : Hue)과 b(색도 : Chroma)는 큰 변화를 보이지 않았다.<Results> L (Lightness) values decreased with extraction time, but a (Color: Hue) and b (Color: Chroma) did not show significant changes.

<결과> 시큼한 냄새는 처리시간에 따라 처리시간 30분 이 후부터 약하게 나타났고, 비린 냄새의 경우 처리시간 30분 이 후부터 약하게 나타났으며 청량한 냄새 역시 60분 이후부터 조금 나타났다.<Results> The sour smell was weak after 30 minutes of treatment time, and the smell of fishy smell was weak after 30 minutes of treatment time.

1) 사용감 : 지방 등에 의해 늘어진 피시험자의 피부가 지방의 감소로 피부의 탄력이 회복된 정도1) Feeling: The extent to which the skin of the test subjects whose elasticity has decreased due to fat recovers the elasticity of the skin due to the decrease of fat.

2) 안전성 : 피 시험자의 피부에 염증, 반점 등에 의한 부작용 정도2) Safety: The degree of side effects caused by inflammation, spots, etc. on the subject's skin

3) 지속성 : 사용감이 유지되는 정도3) Persistence: The degree to which the feeling of use is maintained

<결과> 최종제품을 피시험자 피부에 직접 사용감, 지속성, 안전성 모두 우수하게 평가되었다.<Results> The final product was evaluated for its ease of use, sustainability and safety.

이상에서 상세히 설명하는 바와 같이 본 발명에서 제공하는 제조방법은 천연 생약(상백피, 천궁, 번사엽, 대황 등)과 해조류(미역, 다시마, 톳, 불가사리 등)을 선별 세척후 초음파를 이용하여 재료에 맞게 5~240분간 처리시 각 재료의 최대 유효성분 추출시간을 적용하여 추출한 추출물을 적당한 혼합 처리함으로서 안전성과 경제성이 고려된 새로운 바디 영양크림을 제조하였다.As described in detail above, the manufacturing method provided by the present invention is characterized in that the natural herbal medicines (e.g., baekpipi, cheonggung, bunsaeng, rhubarb, etc.) and seaweeds (seaweed, kelp, 톳, starfish, etc.) are screened and cleaned using ultrasonic waves. By applying the maximum effective ingredient extraction time of each material during the treatment for 5 to 240 minutes, a new body nutrition cream was prepared considering the safety and economic efficiency by appropriately mixing the extracted extract.

이로서 천연 생약과 해조류의 부가 가치 향상 및 국민 건강 및 미용증진에 크게 일조할 수 있게 되는 등의 효과가 있는 매우 유용한 발명이었다.This is a very useful invention that has the effect of improving the added value of natural herbs and algae, and greatly contribute to the improvement of national health and beauty.

Claims (3)

바디 영양크림을 제조함에 있어서, 천연 생약 및 해조류를 초음파처리하여 천연 생약 및 해조류에 함유된 유효성분을 추출하고, 상기 추출액을 이용하여 바디 영양크림으로 제조하는 것을 특징으로 하는 천연 생약 및 해조류를 이용한 바디 영양크림의 제조방법.In the manufacture of body nutrition cream, natural herbal medicines and seaweeds are ultrasonicated to extract the active ingredients contained in the natural herbal medicines and seaweeds, and the natural herbal medicines and seaweeds are characterized in that the body nutrition cream is prepared using the extract. Method of making body nutrition cream. 제1항에 있어서, 천연 생약 및 해조류는 상백피, 천궁, 번사엽, 대황, 톳, 미역, 다시마, 불가사리인것을 특징으로 하는 천연 생약 및 해조류를 이용한 바디 영양크림의 제조방법.[Claim 2] The method of claim 1, wherein the natural herbal medicine and algae are baekbaekpi, Cheongung, Bunsa leaf, rhubarb, 톳, seaweed, kelp, starfish. 제1항에 있어서, 초음파 처리로 얻어진 추출물을 한외여과법을 통하여 농축하고, 다시 나노여과법을 통하여 2차농축하여 추출하는 것을 특징으로 하는 천연 생약 및 해조류를 이용한 바디 영양크림의 제조방법.The method of claim 1, wherein the extract obtained by sonication is concentrated by ultrafiltration and secondly concentrated through nanofiltration to extract the body nutrition cream using natural herbal medicines and seaweeds.
KR1020020009581A 2002-02-22 2002-02-22 Preparation of Body Nutritional Cream Prepared by Natural Herb and Seaweeds KR20030069659A (en)

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JP2012077035A (en) * 2010-10-01 2012-04-19 Kyoei Kagaku Kogyo Kk Cosmetic
WO2012122082A2 (en) * 2011-03-08 2012-09-13 Elc Management Llc Methods for activating caspase-14 expression in human skin
US8383167B2 (en) 2011-03-08 2013-02-26 Elc Management, Llc Method for cosmetically treating caspase-14 deficiency

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JPH02191209A (en) * 1989-01-18 1990-07-27 Eikoudou:Kk Cosmetic
JPH0692864A (en) * 1992-09-14 1994-04-05 Kanebo Ltd Production of chinese medicine extract
JPH06263623A (en) * 1993-03-12 1994-09-20 Sariensu:Kk Natural ultraviolet absorber and cosmetic containing it
KR950032567A (en) * 1994-05-07 1995-12-22 전종한 Extraction method of antioxidants
WO2001026617A1 (en) * 1999-10-08 2001-04-19 Coty B.V. Cosmetic preparation of active substances with a synergistically increased radical protection factor
KR20020011842A (en) * 2000-08-04 2002-02-09 박권필 Alginic Acid Extraction from Seaweed

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Publication number Priority date Publication date Assignee Title
JPH02191209A (en) * 1989-01-18 1990-07-27 Eikoudou:Kk Cosmetic
JPH0692864A (en) * 1992-09-14 1994-04-05 Kanebo Ltd Production of chinese medicine extract
JPH06263623A (en) * 1993-03-12 1994-09-20 Sariensu:Kk Natural ultraviolet absorber and cosmetic containing it
KR950032567A (en) * 1994-05-07 1995-12-22 전종한 Extraction method of antioxidants
WO2001026617A1 (en) * 1999-10-08 2001-04-19 Coty B.V. Cosmetic preparation of active substances with a synergistically increased radical protection factor
KR20020011842A (en) * 2000-08-04 2002-02-09 박권필 Alginic Acid Extraction from Seaweed

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012077035A (en) * 2010-10-01 2012-04-19 Kyoei Kagaku Kogyo Kk Cosmetic
WO2012122082A2 (en) * 2011-03-08 2012-09-13 Elc Management Llc Methods for activating caspase-14 expression in human skin
WO2012122082A3 (en) * 2011-03-08 2012-12-27 Elc Management Llc Methods for activating caspase-14 expression in human skin
US8383167B2 (en) 2011-03-08 2013-02-26 Elc Management, Llc Method for cosmetically treating caspase-14 deficiency

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