KR20020026805A - coarse liquor and rice wine brewage method by means of acanthopanax - Google Patents
coarse liquor and rice wine brewage method by means of acanthopanax Download PDFInfo
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Abstract
Description
쌀 등의 곡물을 주원료로 오가피 등의 한약재를 부원료로 하는 전통 탁약주 제조에 있어서의, 종래에는 탁·약주 담금시에는 한약재를 원료와 함께 첨가하여 발효할 경우 발효 기간이 짧아 한약재의 충분한 추출이 이루어지지 않으며 오가피, 모과와 같이 수분이 많은 식물의 껍질, 열매 등은 건조중 오염으로 인한 탁·약주의 변질과 품질저하가 자주 일어나는 단점이 있다.Traditionally in the manufacture of traditional medicinal liquor made from rice and other grains as the main ingredient, medicinal herbs such as Ogapi, conventionally, when medicinal herbs are added and fermented with medicinal herbs, the fermentation period is short. It is not made and the bark, fruit, etc. of juicy plants, such as cucumbers and quince, have the disadvantage that deterioration and deterioration of quality of the turbid and weak liquor due to contamination during drying often occur.
또한 곡물로 만드는 탁·약주 원료처리에 있어서 수도수 등으로 침적하므로 침적시의 변질로 인한 사고(쉬는 현상)가 가끔 있으며, 곡물류에 포함되어 있는 불필요한 잡미를 없애고 풍미를 좋게 하기 위하여 도정비율을 높일 경우 경제적인 손실이 많다.In addition, in the processing of raw materials of grains and herbs made of grains, they are deposited with tap water, which sometimes causes accidents due to deterioration at the time of sedimentation.In order to remove unnecessary blemishes contained in grains and improve flavor, There are many economic losses.
또한 원료를 증자하여 발효하므로 곡물의 열 변성으로 맛이 떨어지며 액기스분이 증가하고 또한 그 만큼 열에너지가 소요된다.In addition, since the raw material is increased by fermentation, the taste is degraded due to the heat denaturation of grains, and the amount of extract increases, and heat energy is required as much.
이에 본 발명에서는 상기 문제점들을 해결하여 안전한 제조와 오가피를 주재로하는 한약재의 향미가 풍부하고, 잡미나 이취가 없으며 신선하고 부드러운 맛의 탁·약주 제조방법을 제공하려는 것이다.Therefore, the present invention is to solve the above problems to provide a safe manufacturing and aroma of herbal medicine mainly to oopi, there is no nasty or odor and fresh and soft taste of the preparation method of turk, Yakju.
도1은 본 발명의 제조공정도로서,상세하게는 오가피를 주재로 하는 한약재를 미리 당류와 구연산수에 침출하여 사용하며 곡물을 구연산수로 침적 세미 분쇄한 원료와 따로 배양한 주모, 생전분 분해력이 우수한 액체증식배양을 거쳐 생밀기울 고체배양후 건조하여 만들어진 발효제를 혼합 발효하고 1차여과한 탁주와 정밀여과한 약주를 제조하는 제조하는 공정도이다.1 is a manufacturing process diagram of the present invention, in detail, the medicinal herb used as a predominantly used for leaching in sugars and citric acid in advance, and sedimentation and semi-crushing of grains with citric acid, cultivated raw rice, excellent starch decomposition power It is a process of manufacturing fermentation agent made by mixing and fermenting the dried wheat bran solid culture through liquid growth culture and preparing primary filtered Takju and fine filtered Yakju.
본 발명은 오가피를 주로하는 한약재를 당류와 구연산 혼합물료로 침출하여 만드는 침출공정과 쌀 등의 곡물류의 침적방법 생전분 분해균으로 생배양한 발효제 제조와 주모제조, 한약제 침출물 등을 혼합하여 발효하는 공정으로 구성되어 있다.The present invention is a leaching process of leaching herbal medicine mainly oolong with a mixture of sugars and citric acid and a method of dipping of grains such as rice. Fermentation by mixing fermentation agent prepared with live starch decomposition bacteria, main hair preparation, herbal leach, etc. It consists of the process to make.
이하 본발명을 공정별로 설명하면Hereinafter, the present invention will be described by process.
[한약재 침출공정][Medicinal Herb Leaching Process]
포도당, 설탕, 등의 당류 50∼55%,구연산 2∼3% 의 용액에 오가피 120g,모과 20g, 당귀 15g, 사인 15g, 구기자 소회향 산사자 하수오 복분자 오미자 등을 각 2g으로 합계 180g을 혼합, 20∼30일간 상온에서 충분히 침출한 뒤 탁·약주 부원료로 사용한다.In a solution of 50-55% of saccharides such as glucose, sugar, etc., 2-3% citric acid, 180 g of Ogapi, 20 g of Chinese quince, 15 g of Angelica, 15 g of signature, 15 g of Goji berry, small hawthorn hawthorn, sesame seed schizophrenic Schizandra chinensis, etc. After sufficiently leaching at room temperature for 30 days, it is used as a subsidiary material of Tak and Yak.
한약재의 종류 상태에 따라 다소간의 차이는 있으나 오가피를 주로 할 경우 pH는 2.0 내외였으며, 당류를 증가할 경우 점도가 높아 침출이 용이치 않았으며 줄일 경우 야생효모가 증식하므로 50% 내외가 적당하였다.Depending on the type of medicinal herb, there were some differences, but the pH of Ogapi was about 2.0, and it was not easy to leach because the viscosity of the sugar was increased.
담금에서 대부분의 한약재는 야생효모 세균 곰팡이등의 오염이 극심하며 특히 야생효모의 오염은 술맛을 나쁘게 하는데 크게 작용하였으며 물로 씻는 방법을 사용하였으나 풍미가 떨어지는 결과를 초래하였다.Most medicinal herbs in the immersion are severely contaminated with wild yeast bacteria and fungi. Especially, the contamination of wild yeast has a great effect on the bad taste and washes with water, but the flavor is decreased.
또한 발효기간이 15-20일 정도로는 한약 성분이 완전히 추출되지 않아 한약재의 낭비를 줄이기 위하여 미리 침출하는 방법을 고안하게 되었다.In addition, the fermentation period of 15-20 days is not completely extracted from the herbal medicines to devise a method of pre-leaching to reduce the waste of herbal medicines.
먼저 당류만으로 침출 하였던바,세균은 번식 하지 않았지만 내당성 야생 효모류는 죽지않고 10일 정도 지나면 조금씩 활성을 보이는 현상을 나타내므로 당과 함께 구연산을 첨가하여 pH를 떨어뜨리므로 해결하였다.First leached only with saccharides, bacteria did not breed, but the sugar-resistant wild yeast did not die, and showed a little phenomenal activity after about 10 days, so the solution was solved by adding citric acid with sugar.
아래의 표1은 침출용액과 한약재의 구성을 적었으며 일부 거친 한약재는 분쇄하여 사용하였다.Table 1 below shows the composition of the leaching solution and herbal medicines, and some of the rough herbal medicines were used by grinding.
※정제 포도당 사용※ Use of purified glucose
※침출 중 pH 2.0※ pH 2.0 during leaching
표2는 당류만으로 침출시 약재추출은 양호하나 야생효모의 대부분이 죽지않고 활성을 나타내었으며, 구연산 1% 첨가에서는 외관상 오염은 없었으나 20일 후의 맥아배지에 도말하여 야생효모의 활성여부를 검사한 결과 극히 소수나마 존재하며 구연산 2% 첨가시는 추출과 오염에 문제가 없었다.Table 2 shows that medicinal extracts were good when leached only with sugars, but most of the wild yeasts did not die and showed no contamination when 1% citric acid was added, but smeared with malt medium after 20 days was tested for wild yeast activity. As a result, only a few were present and there was no problem in extraction and contamination when 2% citric acid was added.
또한 일반적으로 한약재추출주는 2∼3개월 침출하여야만 약재성분 및 향취가 충분히 추출되어 약효를 발휘하는 것으로 알려져왔다. (참조. 병을 치료하는 민간약술.권혁세지음)In addition, herbal medicine extracts have been known to exert medicinal medicinal properties and sufficient medicinal ingredients extracted only after 2-3 months leaching. (See folk medicine to cure illness.
실제 탁약주 제조공정에서 발효완료시 한약재 첨가된 상태로 장시간 방치숙성하면 효모의 자가소화등으로 맛과 향취의 변화가 크므로 반드시 여과하여 숙성한다. 그러므로, 짧은 발효기간동안 한약재성분 및 향취의 침출이 충분치 못한 단점을 보완하기 위하여 미리 당 및 구연산에 충분히 침출하여 담금에 사용하므로 한약재의 낭비를 줄이고 충분히 추출된 좋은 술을 만들 수 있다.When the fermentation is completed in the process of manufacturing the medicinal liquor, if it is left to mature for a long time in the state of adding medicinal herbs, it must be filtered and matured because the change of taste and smell is great due to self-extinguishing of yeast. Therefore, in order to make up for the shortcoming of the shortcoming of the medicinal herb ingredient and odor leaching, it is used in immersion by sufficiently dipping in sugar and citric acid in advance to reduce the waste of medicinal herb and to make a good sake extracted.
[곡물류의 침적방법][Sedimentation method of cereals]
백미등의 곡류를 구연산 0.3∼1% 첨가수로 pH 3.0∼3.6 내외로 유지시켜 5∼12시간 침미하므로 하절기 변질을 방지하며, 쌀의 외피,씨눈 등에 함유되어 중성에는 녹지않으나 산성에 녹는 엑기스성분을 제거한다. 청주양조시 주질을 향상하기 위하여 도정율을 높여 품질 저하에 관련된 물질을 제거하는 것과 비슷한 효과를 가져온다. 실제 주질을 좋게하는 성분도 유실될 수 있으나, 오가피 등의 한약재첨가 탁·약주의 경우 곡물향을 줄이고 약재의 향을 강하게 하기 위하여서는 좋은 방법이라 생각된다.Cereals such as white rice are maintained at pH 3.0-3.6 with citric acid 0.3 ~ 1% added water and soaked for 5-12 hours to prevent deterioration in the summer.Extract ingredients that are not soluble in neutrality but are not soluble in neutrality because they are contained in rice skin and seeds. Remove it. In order to improve the quality of sake brewing, it has a similar effect to the removal of substances related to quality deterioration by increasing the coating rate. In fact, the ingredients that improve the quality can be lost, but it is considered a good way to reduce the aroma of grains and to strengthen the scent of the medicinal herbs, such as ogapi, etc.
실제 구연산수로 침미시 30℃ 12시간 유지하여도 쌀이 변질(쉬는) 현상은 볼수 없었으며 또한, 술의 곡물향이 줄어드는 현상을 확인하였다.Indeed, when the rice was kept at 30 ° C for 12 hours, the deterioration (rest) of rice was not observed, and the grain aroma of alcohol was reduced.
침적이 완료된 쌀은 1시간 물을 빼고 구연산 수로 1,2회 세척하여 압착분쇄기로 분쇄하여 사용한다.After immersion, the rice is drained for 1 hour, washed 1, 2 times with citric acid water and crushed with a crusher.
[발효제 제조공정][Fermentation agent manufacturing process]
본 발명에 따른 발효제는 Aspergillus.Shiroussamii 균의 포자를 멸균수 (Tween80미량첨가)에 충분히 분산시킨 후 10㎝거리에 UV등(San Kyo Den Ki Co.일본제 살균등)에 10분간 조사하여 감자 한천배지에 도말, 생존균을 밀기울배지에 배양하여 생전분 역가를 검사하여 우수균을 선별하였다.The fermentation agent according to the present invention is sufficiently dispersed in aspergillus.Shiroussamii spores in sterile water (added Tween 80) and irradiated with UV light (San Kyo Den Ki Co., Japan) for 10 minutes at 10 cm distance to potato agar. The smear and viable bacteria were cultured in a bran medium to check the starch titer and the excellent bacteria were selected.
선별된 우수균은 30∼35℃,10% 밀기울액체배지(pH 4.0)에 배양하여 균체를 증식시킨 후 생밀기울 원료와 1:1로 배합하여 상자에 엷게 펴서 48시간 배양하여 건조 사용한다.Selected rainwater bacteria are incubated in 30 ~ 35 ℃, 10% wheat bran liquid medium (pH 4.0) to grow the cells and then mixed with raw wheat bran raw material 1: 1, spread thinly in a box and incubated for 48 hours to dry.
대체로 이때의 생전분역가는 200∼400sp, 호화전분역가는 2,000∼3,000sp정도였다.Generally, the starch titer was 200-400sp and the luxury starch titer was 2,000-3,000sp.
생전분역가 측정 방법은 호화전분역가 측정법을 응용하여 본 발명자가 아래와 같이 임의로 행하였다.The raw starch titer was determined by the present inventors by applying gelatinized starch titer.
[주모제조][Master production]
주모제조는 실험실에서 배양한 효모(Sacharomyces Servisea)를 구연산수를 처리한 쌀가루 200g과 물 300㎖를 혼합하고, 구연산 등으로 pH 2.4∼2.8로 조절하여 여기에 생전분발효제를 혼합하여 20℃에서 5∼10일간 배양한다.Main hair production is the yeast (Sacharomyces Servisea) cultured in the laboratory mixed with 200g of citric acid-treated rice flour and 300ml of water, adjusted to pH 2.4 ~ 2.8 with citric acid, etc. mixed with this starch fermentation agent at 20 ℃ 5 Incubate for 10 days.
[발효공정]Fermentation Process
상기의 공정을 거친 쌀가루와 한약재 침출액 대원료 10∼50%, 발효제 6%, 주모 5%. 급수 대원료 150% 한약재 추출액은 당 농도를 환산하여 물과 1 : 1 로 희석하여 사용하였으며 20℃ 내외로 15∼20일간 저온발효한다.Rice flour and medicinal herb leaching raw material 10-50%, fermentation agent 6%, chimney 5%. The 150% herbal medicine extract of feedwater raw material was diluted with water and converted to 1: 1 in terms of sugar concentration. It is fermented at 20 ℃ for 15-20 days at low temperature.
단계별 담금을 하지 않고 한꺼번에 담금하여 가끔씩 저어주고 용기의 뚜껑을 덮어 향취의 발산을 막으며 발효한다.Do not step by step soaking at once and stir occasionally and cover the lid of the container to prevent the release of odor and ferment.
[탁약주 제조][Takko wine production]
비교예 : 원료미 1,000g을 통상적인 방법에 따라 2시간 침미, 1시간 물빼기, 1시간 증자 처리하고 냉각 후 실시예1과 동일비율의 한약재 56g, 배양효모 50㎖,물1,600㎖을 효소제(역가2,000sp) 60g 첨가하여 20℃에서 15일간 발효하였으므로 17.2%의 알콜분과 2,500㎖의 숙성 술덧을 얻었다.Comparative Example: 1,000 g of raw rice was treated with 2 hours of immersion, 1 hour of water draining, 1 hour of steaming according to a conventional method, and cooled, followed by cooling of 56 g of herbal medicine, 50 ml of culture yeast, and 1600 ml of water in the same ratio as in Example 1. 60 g of the titer 2,000sp) was added and fermented at 20 ° C. for 15 days, yielding 17.2% alcohol content and 2,500 ml of fermentation.
실시예 1 : 비교예와 동일한 방법으로 제조하되 원료를 구연산수에 5시간 침미, 1시간 물빼기 구연산수 1∼2회 세척 압착분쇄기에 2회 분쇄하여 배양효모 50㎖, 한약재침출액 500㎖, 생전분효소제 60g, 물 2,100㎖를 첨가,발효하였다. 17.4%의 알콜분과 3,400㎖의 숙성 술덧을 얻었다.Example 1: Prepared in the same manner as in Comparative Example, but the raw material was soaked in citric acid for 5 hours, 1 hour drained citric acid 1 to 2 times crushed twice in a crushing grinder and cultured yeast 50ml, herbal medicine leaching solution 500ml, live 60 g of powder enzyme and 2,100 ml of water were added and fermented. 17.4% alcohol content and 3,400 ml of ripening powder were obtained.
실시예 2 : 실시예1과 동일하게 하되 한약재 침출액을 250㎖ 첨가하고 물을 1,850㎖ 첨가하여 17.2%의 알콜분과 2,100㎖의 숙성 술덧을 얻었다.Example 2 The same procedure as in Example 1 was performed except that 250 ml of medicinal herb leachate was added and 1,850 ml of water was added to obtain 17.2% alcohol content and 2,100 ml of aged powder.
실시예 3 : 실시예1과 동일하게 하되 한약재 침출액 100㎖ 첨가하고 1,700㎖의 물을 첨가하여 17.1%의 알콜분과 2,700㎖의 숙성 술덧을 얻었다.Example 3 In the same manner as in Example 1, 100 ml of medicinal herb leachate was added, and 1,700 ml of water was added to obtain 17.1% alcohol content and 2,700 ml of aged powder.
표 4는 한약재 침출액 첨가비율에 따라 담금을 비교하였으며 급수량이 다른 것을 한약재 침출액의 당의량에 따라 급수를 계산, 증가하였다.Table 4 compares the immersion according to the ratio of medicinal herb leaching, and the water supply was calculated and increased according to the sugar content of the medicinal herb leaching.
표 5는 쌀을 원료로 발효시킨 비교예의 발효비율이 83.5%로 높고 한약재 침출액이 많이 들어간 것이 대체로 발효비율이 낮은 것은 설탕의 수분이 많았던 관계로 사료된다.Table 5 shows that the fermentation rate of the comparative example in which the fermented rice was used as a raw material was high as 83.5%, and that the fermentation rate was large was low because the medicinal leachate contained a lot of water.
대부분이 비교예와 큰 차이가 없으며 표7에서와 같이 오염도에서 현저한 차이를 보이며 현미경상 세균의 오염과 야생효모의 오염으로 구분, 관찰하여 보았다.Most of them were not significantly different from the comparative example and showed a significant difference in pollution degree as shown in Table 7, and were classified and observed under microscopic bacterial contamination and wild yeast contamination.
주 1)이론알콜생성량 : 원료중 발효가능한 유효성분으로부터 생산가능한 순수이론 적수량으로 전분일 경우 원료사용량×원료미전분가×0.715,당분일 경우 (원료사용량÷0.95)×0.6435임.Note 1) The amount of theoretical alcohol produced: The amount of pure theoretical product that can be produced from fermentable active ingredients in raw materials.
주 2)숙성술덧 총알콜량 : 숙성술덧중의 순수알콜량으로 숙성술덧량×숙성술덧의 알콜분.Note 2) Total alcohol content in aged liquor: The amount of pure alcohol in aged liquor.
참고로 본실험에서는 숙성술덧의 양이 한약재 및 발효제의 양이 차이가 많이나므로 거친 체로(약1㎝의 크기) 1차 걸러 잘 짠 후의 술덧량과 알콜분을 계산하였으므로 다소간의 유실이 있어 한약재의 첨가량이 많은 것이 발효비율이 조금 떨어지는 것으로 사료됨.For reference, in this experiment, the amount of medicinal herbs and fermenters differed a lot, so the amount of alcohol and the amount of alcohol after squeezing well after squeezing the fine sieve (about 1cm) were calculated. It is considered that the fermentation ratio is a little lower with a large amount of addition.
주 3)발효비율 : 숙성술덧의 총알콜생성량과 이론알콜생성량의 비율Note 3) Fermentation ratio: ratio of total alcohol production and theoretical alcohol production
발효시의 오염내용은 아래 표 6과 같다.The contamination contents during fermentation are shown in Table 6 below.
< 오염내용 : 야생효모 o , 세균 + ><Pollution content: wild yeast o, bacteria +>
※ 참고: 야생효모는 편의상 첨가효모와는 달리 현미경상 긴 타원형의 효모를 말한다.※ Note: Unlike yeast for convenience, wild yeast refers to long oval yeast under the microscope.
표 7에서 보는 바와 같이 맛과 향취 에서는 비교예에 비하여 실시예가 한약취가 강하고 곡물취와 알콜의 자국취가 현저히 줄어드는 결과가 나왔다. 즉, 술이 순하고 한약취가 강한 현상을 나타내었다.As shown in Table 7, in the taste and scent, the results of the Examples were stronger than the Comparative Example, and the odor of grain and alcohol was significantly reduced. In other words, the alcohol is mild and the herbal medicine showed a strong phenomenon.
본 발명의 방법에 의해 한약재 첨가 탁·약주 제조에서는 곡물취와 자극취가 줄어들고 오가피를 중심으로 한 독특한 향취가 강하면서도 순하고 부드러운 술을 제조하므로 동양의 특성을 잘 살려 세계화 할수 있는 가능성과 오가피를 위시한 한약재 소비로 인한 농민소득증대에 기여하는 효과가 있다.Herbal medicine added turk and medicinal herbs by the method of the present invention reduces grain odor and irritation odor and produces a strong and gentle alcoholic beverage with a unique scent mainly around agap, so that the oriental medicine and the possibility of globalization utilizing the oriental characteristics well It has the effect of contributing to the increase of farmers' income from consumption.
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