KR20010070384A - A tea granules made from the extract of Saururus Chinensis Bail and the manufacturing method thereof - Google Patents

Abstract

PURPOSE: A gradual tea of Saururus chinensis extract is provided, which is prepared by going through two times extracting processes in alcohol to extract the active principles to the utmost. Therefore, it can be produced easily for a less time compared to the existing ways to infuse dried Saururus chinensis. CONSTITUTION: A method for preparing gradual tea of Saururus chinensis extract comprises the steps of: (i) a first step to extract dried Saururus chinensis in 65-75% ethanol; (ii) a second step to extract again the residue of extracted Saururus chinensis in 45-55% ethanol to obtain the ingredients that melt in ethanol and water; (iii) a third step to concentrate with decompression for its density to reach up to 20-25Brix; and (iv) a fourth step to mix the concentrated solution 91% with dextrin 4-6% as a drying adjuvant, and oligosaccharide 3-5%, and then dry by spraying.

Description

A tea granules made from the extract of Saururus Chinensis Bail and the manufacturing method

The present invention relates to a method for producing a granule extract tea easy to take as a health food using the three hundred medicinal herb, more specifically, the method of extracting only a part of the active ingredient by boiling only dried leaves or roots as water In order to maintain the direction of the three hundred seconds while extracting all of the active ingredient of three hundred seconds dissolved in water and alcohol, and to improve the properties of the granules, instead of extracting only pure water, it is extracted with a certain concentration of alcohol and spray-dried to make tea as granules. It is about how to.

The scientific name of the three hundred seconds is the Saururus Chinensis Lour Baill and belongs to more than three hundred. It is a perennial herb, 30-90cm high, root is white, stem is straight, and leaves are pointed eggs. Flowers are white in the form of ear white and bloom in July-August. Fruits bear in August-September. Three hundred seconds is a peculiar plant that grows green in early summer, turns three leaves under the flower white, and then returns to green.

Three hundred seconds has been widely known for its excellent medicinal effects, and this fact is well represented in books that have been handed down since ancient times.

The Chinese book, Chinese Medicinal Dictionary, describes the effect of three hundred seconds: 'The effect clears the process heat, pee, and moist heat. Eliminate small edema, edema, detoxification. Thus, it is said that it corrects the species, each, jaundice, imak, lobster, carbuncle, and persimmon. Clearing urine is most common in adults with diabetes, hepatic disease, high blood pressure, urine is turbid, this clears up to 300 seconds. Eliminating edema is because it strengthens the capillaries that provide blood to the human body by entangled like a spider's web, and the high diuretic effect of 300 seconds helps. '

Dangboncho is said to be mainly good for species and each species, and to excrete faeces smoothly, to cut sodam wave wall, sputum, and pierce the wall, to remove the trap and to remove the jongjong. Here, 'acquisition' is pathological crystals in the stomach, ie lumps of lumps, chilled bodies, lumps of blood, cancer, etc. Sodam wave wall cuts phlegm, the pathological mucus of the body, and releases hard things in the sides, such as blood clots caused by blood circulation disorders.

As a recent data, the February 25, 1988 Health Newspaper contains a press release about Kwak Jae-wook's doctoral dissertation from Kyung Hee University, a paper entitled "Three hundred Seconds of Pharmacological Research." Dr. Kwak announced that he extracted three hundred seconds of active substances and also extracted new active substances on his own. Quercetin, the active substance of 300 seconds, has already been published by the biochemical community as an anti-inflammatory and analgesic substance. Dr. Kwak said that the active substance of 300 seconds contains anti-histamine and antibacterial substance. "Histamine" is a kind of toxic substance produced in living tissues. It is known to cause diseases. An active ingredient of three hundred seconds is that it contributes to health promotion by inhibiting the production of this "histamine" in the body. There are also reports that there are active ingredients that have antibacterial activity in 300 seconds.

Because of its excellent efficacy as described above, many people want to take the medicine to take the drug, but the situation is not yet taken as a health food, such as instant tea, so that modern people can easily take it in time. Most traditional herbal tea manufacturing method is to dry the leaves or roots and, if necessary, rinse them with water to drink the active ingredients contained in the three hundred seconds and drink them like a drink or even a simpler way. ) It was difficult to store because it takes a long time to be concerned and the plant itself should be stored in a dry state because it is mostly packed and put into a mug and poured boiling water to make tea. In addition, in the process of brewing dried medicinal herbs, the amount of water or the weights of medicinal herbs are different, so it is difficult to quantitatively take effective medicine. In addition, the procedure is cumbersome to drink medicinal herbs directly, it was difficult to go to work or go out at work, or to take 300 seconds tea in time or go out coffee or green tea in addition to the 300 seconds if boiled in water Only components that are soluble in water are extracted and other active ingredients dissolved in alcohol cannot be extracted.

Three hundred vinegar has been sold as a dry product in its original form or in small pieces. Some products are sold on the market by making one-time packaging of three hundred vinegar and other medicinal herbs. Since it is a powder, taking water separately or adding water, it becomes a turbid liquid rather than drinking it as food, but only the form of powder is only taking three hundred seconds itself. Therefore, instant granule tea made by extracting all of the medicinal active ingredients contained in three hundred seconds has not been developed.

An object of the present invention is to provide a method for producing a granular solid three hundred seconds extract tea so that it is easy to take and easy to carry while extracting all the active ingredients contained in three hundred seconds and maintaining excellent drug efficacy.

In order to achieve the above object, the present invention first extracts high concentration alcohol to extract all active ingredients of 300 seconds in the process of extracting medicinal components of 300 seconds, elutes fat-soluble components, and secondly extracts to low concentration alcohols. After eluting together, the extracts of the first and second stages were collected, concentrated at low pressure, and then dried by spray drying to make granules, adding dextrin as an excipient, adding oligosaccharides for flavoring, and making tea with only 300 seconds of extract during the manufacturing process. It has its features.

The present invention is to extract the active ingredient of three hundred seconds dissolved in water and alcohol, while maintaining the unique flavor of three hundred seconds and to extract the properties of pure water to spray the granules to improve the physical properties when spray-drying only 65-75% Extract with a high concentration of alcohol and then with a low concentration of 45-55% secondary alcohol. Extraction from herbs to water alone does not extract volatile and fat-soluble fragrant substances, resulting in the fragrance of the extract dying and the extraction of high polymer starch. The three hundred scent is a medicinal herb that excels in greatly expanding the regularity of the human body by nature, as the nickname Cheon Seong-cho is known as a report of flavone-based materials, water-soluble tannins, essential amino acids, and effective minerals.

* 300 seconds outpost

Rare 8.8%, Potassium 7.9, Total 12.4%, Zinc 12.5 (mg / kg)

Germanium 0.09 (mg / kg), iron 9.3 (mg / kg) I.C.P method,

Calcium 327.1 (mg / kg) I.C.P method, Copper 7.9 (mg / kg) I.C.P method,

Crude protein 11.2%, (Korea Food Research Institute analysis)

Tannin 1.22%, lean 4.51%, crude protein 6.07%, total sugar 59.20%, fructose 6.72%

Glucose 5.38%, calcium 172.47 (mg%), potassium 1427.33 (mg%),

Iron 18.28 (mg%), copper 0.93 (mg%), zinc 1.15 (mg%), oxalic acid 1.06%,

Vitamin B1 Thiamine 1.86%, Malic Acid 0.76%, Vitamin B2 Riboflavin 0.07%,

Acetic acid 2.87%, citric acid 0.32%, glutamic acid 635.82 (mg%), succinic acid 1.06%,

Glycine 219.14 (mg%), aspartic acid 1666.5 (mg%), arginine 456.28 (mg%),

Serine 292.87 (mg%), alanine 305.33 (mg%), histithin 156.85 (mg%),

Tyrosine 170.18 (mg%), threonine 192.30 (mg%), methionine 36.62 (mg%),

Proline 132.90 (mg%), isoleucine 188.34 (mg%), valine 395.99 (mg%),

Phenylalanine 196.86 (mg%), cystine 27.54 (mg%), lysine 190.07 (mg%),

Luchin 428.55 (mg%), Sugar 2.02% (Korea Food Research Institute)

Referring to the manufacturing process of the three hundred seconds granule extraction tea according to the present invention in detail.

Three hundred seconds can extract the active ingredient from the leaves and roots, washed immediately after harvesting and dried, and hot air dried at 45 ℃ to maximize the yield of medicinal components during the extraction process. The dried leaves are crushed to allow extraction. The component analysis of three hundred seconds used in the experiment for the present invention is as follows.

(Table 1) Component Analysis of Three hundred Seconds

moisture(%) Ash (g / 100g) Protein (g / 100g) Calcium (g / 100g) Magnesium (g / 100g) Potassium (g / 100g) Phosphorous pentoxide (g / 100g) 10.8 12.6 11.5 0.83 0.47 0.95 0.66

In extracting medicinal ingredients of three hundred seconds, three hundred seconds contains low-molecular fat-soluble organic ingredients that are not soluble in water but especially in ethanol, an organic solvent. Recent studies have shown that the fat-soluble part is particularly effective in adult diseases. As a result of repeated experiments of extracting the most effective ingredients, the extracts were extracted with high concentrations of ethanol and low concentrations of ethanol twice to extract the active ingredients of 300 seconds.

The first extract is extracted from high concentration ethanol (Tethanol) of 65% to 75%, extracts the active ingredient such as proline and some fatty acids, which are mainly dissolved in ethanol, from the solute three hundred seconds. The remaining three hundred seconds are extracted again with 45% to 55% low concentration of ethanol containing about half of the water, and the remaining active ingredient dissolved in ethanol and water is extracted once more, and the concentration of serine, alanine and protein By extracting a component that is dissolved in water, such as albumin (albumin), which is the main component, all active ingredients of 300 seconds are extracted.

Therefore, conventionally, when only 300 seconds of water, we can improve the disadvantage of not obtaining the active ingredient dissolved in ethanol to extract all the active ingredients such as organic acids dissolved in ethanol.

In this case, the reason for not including 100% water extraction is that the extraction of only water is because the starch is extracted a lot of properties when making granular tea is not good. In addition, the first extract with high concentration alcohol to elute a lot of aromatic components, the second extract with 50% alcohol, and extract the remaining fat-soluble components to extract the water-soluble active ingredients with the remaining 50% water so that fat-soluble and volatile aroma components are not lost.

The extract extracted through the above process is extracted by extracting the first and second extraction extract is filtered through a filter (filter), the filtrate is concentrated under reduced pressure at 70 ~ 80 ℃, pressure 40cmHg to adjust the concentration to 20 to 25 Brix.

Thus, by extracting and concentrating at low temperature, it is possible to minimize the loss of the active ingredient due to heat generated during the extraction and concentration of three hundred seconds and maintain the inherent aroma of the herb.

The extract concentrate is spray dried to form granular solids of small particles. 4 to 6% of dextrin is added as a drying aid to 91% of the 300 sec concentrate, and 3 to 5% of the oligosaccharide is mixed.

The reason for the addition of dextrin in the above process is that the extract of Trichophyte may have a smaller physical quantity than its efficacy, so it is added as an adjuvant to increase the efficiency of granulation during spray drying, and the oligosaccharides add flavor to the Trichophyte. At the same time, it is effective in improving constipation, improving fat metabolism, and preventing tooth decay.

The three hundred seconds granulated extract tea obtained by the method of the present invention is a red brown powder having a yield (a solid content in the final extract / amount of injected raw material) 22% and a water 4.5%, and the sugar content is investigated as the sugar content of 8.6% when it is made into tea by water. As a result, all 30 respondents rated more than average, 69.2% said it was good, and 15.5% said it was very good, so that the bitter taste of herbal medicine was removed and flavored as a favorite food.

(Example 1)

1 kg of dried triticale leaf and 15 liters of 70% ethanol were placed in an extractor and extracted first at 70 ° C. for 6 hours, and 15 liters of 50% ethanol was added again and extracted for 2 hours at 70 ° C. for 2 hours. Concentrated under reduced pressure, the concentration was adjusted to 23 Brix, and 5% of dextrin was added as a drying aid to 90-92% of the concentrate, and 4% of oligosaccharides were mixed, followed by hot air injection at 130 ° C. and centrifugal force of 16,500 rpm. Using the spray drying at a flow rate of 7.5ml per minute to make a granule extraction tea.

By taking the three hundred seconds granule extraction tea according to the present invention it is possible to shorten the manufacturing time than the conventional manufacturing method that concerns the hay without losing the excellent efficacy and active ingredients of three hundred seconds during the manufacturing process. In addition, by extracting mainly the primary alcohol, eluting the fat-soluble components that are effective in adult diseases including the aromatic component of three hundred seconds, while extracting the water-soluble components together with the second low concentration alcohol and extracting all active ingredients of three hundred seconds, It has better flavor as tea than drinking method, and it can be seen more reliably because it is only 300 seconds of pure 300 seconds extract without mixing with other herbs, and the granular extract tea is portable so it can be easily quantitated even at work or out. You can take it or take it as often as coffee or green tea. Therefore, the general public can easily see the effect of three hundred seconds, it is expected to contribute to the popularization of three hundred seconds.

Claims (2)

In the herbal tea preparation, extracted with dried three hundred seconds 65-75% ethanol, the first component is dissolved in ethanol, and extracted again with 45-55% ethanol in the remaining three hundred seconds and extracted in ethanol and water After dissolving the component to be dissolved, concentrated under reduced pressure to adjust the concentration to 20 to 25 Brix, to 4% to 6% of dextrin as a drying aid to 91% of the concentrate, mixed 3 to 5% oligosaccharides as a health sweetener, and sprayed Method of producing three hundred seconds granule extract tea, characterized in that the drying. An extract of the active ingredient in 300 seconds, concentrated to 20 to 25 Brix, 90 to 92% of dextrinthine 4 to 6%, oligosaccharides 3 to 5%, characterized in that the granulated tea extract.