KR19990051961A - Clay brick manufacturing method - Google Patents
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- KR19990051961A KR19990051961A KR1019970071402A KR19970071402A KR19990051961A KR 19990051961 A KR19990051961 A KR 19990051961A KR 1019970071402 A KR1019970071402 A KR 1019970071402A KR 19970071402 A KR19970071402 A KR 19970071402A KR 19990051961 A KR19990051961 A KR 19990051961A
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Abstract
본 발명은 점토벽돌 제조방법에 관한 것이며, 그 목적하는 바는 점토벽돌의 구성성분으로 입도가 조정된 스텐레스 제강슬래그를 적정량 함유시킴으로써, 소성 변형율이 매우 작은 점토벽돌을 얻을 수 있는 제조방법을 제공하고자 하는데 있다.The present invention relates to a clay brick manufacturing method, and its object is to provide a method for producing a clay brick having a very small plastic strain by containing an appropriate amount of stainless steel slag whose particle size is adjusted as a component of the clay brick. It is.
상기 목적을 달성하기 위한 본 발명은 점토를 주원료로 하는 점토벽돌을 제조하는 방법에 있어서, 점토와 입도조정 스텐레스 제강슬래그의 함유비를 70중량% - 40중량%와 30중량% - 60중량%로 하여 원료배합하고, 가수 혼련하고, 진공토련시켜 성형한 다음, 1050~1150℃의 온도에서 1시간 이상 소성하는 것을 특징으로 하는 점토벽돌 제조방법에 관한 것을 그 요지로 한다.In order to achieve the above object, the present invention provides a method of manufacturing clay bricks containing clay as the main material, wherein the content ratio of clay and particle size adjusting stainless steel slag is 70% by weight-40% by weight and 30% by weight-60% by weight. The present invention relates to a clay brick production method characterized by mixing raw materials, mixing with water, kneading under vacuum, molding and then firing at a temperature of 1050 to 1150 ° C for at least 1 hour.
Description
본 발명은 점토벽돌의 제조방법에 관한 것으로, 보다 상세하게는 스텐레스 제강슬래그를 이용하여 소성 변형율이 작은 점토벽돌을 제조하는 방법에 관한 것이다.The present invention relates to a method of manufacturing a clay brick, and more particularly to a method of manufacturing a clay brick having a small plastic strain using stainless steel slag.
일반적으로 점토는 소성이 있는 성질과 가열하면 암석처럼 굳어지는 성질 때문에 공업상의 용도가 많고, 도자기, 내화물 등의 원료, 종이, 포(布) 등의 충진물, 의약용 등으로도 쓰인다.In general, clay has many industrial uses because of its sintering properties and hardening like a rock when heated, and is also used as a raw material such as ceramics and refractory materials, paper and cloth fillings, and medicines.
이와같은 점토를 주성분으로 하는 점토벽돌은 점토이외에 규사 또는/및 석분 등을 첨가하며, 원료로 하는 소지를 토련하고 건조시킨 후 소성하여 제조되어 진다. 그러나, 상기와 같은 일반적인 점토벽돌은 소성변형율이 5~10%정도로 나타나기 때문에 큰 문제점으로 지적되고 있다.Clay bricks having such clays as main components are prepared by adding silica sand or / and stone powder to clays, smelting raw materials, drying and firing. However, the above-mentioned general clay brick is pointed out as a big problem because the plastic strain is about 5-10%.
한편, 점토벽돌에 대한 제안으로는 우리나라의 공개특허 95-8410과 일본의 특개평 6-720754호를 들 수 있는데, 이러한 제안에 의한 점토벽돌 역시 소성 변형율이 상당히 높은 편이다.On the other hand, proposals for clay bricks include Korean Patent Publication No. 95-8410 and Japanese Patent Application Laid-open No. Hei 6-720754. The clay bricks by this proposal also have a high plastic strain.
이에 본 발명자들은 상기한 바와같은 점토벽돌의 문제점인 소성변형율을 낮추기 위해, 연구와 실험을 거듭하고, 그 결과에 근거하여 본 발명을 제안하게 된 것으로, 본 발명은 점토벽돌의 구성성분으로 입도가 조정된 스텐레스 제강슬래그를 적정량 함유시킴으로써, 소성 변형율이 매우 작은 점토벽돌을 얻을 수 있는 제조방법을 제공하고자 하는데, 그 목적이 있다.In order to reduce the plastic strain which is a problem of clay bricks as described above, the present inventors have repeatedly conducted research and experiments and proposed the present invention based on the results. It is an object of the present invention to provide a method for producing a clay brick having a very small plastic strain by containing an appropriate amount of adjusted stainless steel slag.
상기 목적을 달성하기 위한 본 발명은 점토를 주원료로 하는 점토벽돌을 제조하는 방법에 있어서, 점토와 5mm이하로 입도조정된 스텐레스 제강슬래그의 함유비를 70중량%~40중량%와 30중량%~60중량%로 하여 원료배합하고, 가수 혼련하고, 진공토련시켜 성형한 다음, 1050~1150℃의 온도에서 1시간 이상 소성하는 것을 특징으로 하는 점토벽돌 제조방법에 관한 것이다.In order to achieve the above object, the present invention provides a method of producing a clay brick containing clay as a main material, wherein the content ratio of clay and the stainless steel slag particle size adjusted to 5 mm or less is 70% by weight to 40% by weight and 30% by weight to It relates to a clay brick manufacturing method characterized in that the raw material is blended to 60% by weight, hydrolyzed, vacuum drilled and molded, and then calcined at a temperature of 1050 ~ 1150 ℃ for 1 hour or more.
이하, 본 발명을 상세히 설명한다.Hereinafter, the present invention will be described in detail.
일반적으로 점토벽돌을 제조하는 방법은 점토와 규사 또는 석분 등을 주원료로 하는 소지를 토련하고 건조시킨 후 소성하는데, 본 발명은 점토벽돌의 소성시 일어나는 소성변형을 크게 감소시킬 수 있도록 점토벽돌의 주원료에 대한 구성성분으로서 입도 조정 스텐레스 제강슬래그를 사용한다.In general, the method for producing clay brick is calcined, dried and calcined with the main raw material such as clay and silica sand or stone powder, the present invention is the main raw material of clay brick so as to greatly reduce the plastic deformation occurring during the firing of clay brick Particle size adjustment stainless steel slag is used as a component for
이때 사용되는 입도 조정 스텐레스 제강슬래그는 5mm이하의 입도를 갖는 것이바람직하다. 5mm를 초과하면 충진성이 떨어져 치밀한 구조를 얻지 못한다.It is preferable that the particle size adjusting stainless steel slag used has a particle size of 5 mm or less. If it exceeds 5 mm, the filling property is poor, and a compact structure is not obtained.
이와같은 입도조정 스텐레스 제강슬래그의 사용량은 30중량%이상 60중량%이하가 바람직한데, 그 이유는 입도조정 스텐레스 제강 슬래그의 사용량이 30중량%미만일 경우 점토벽돌의 소성 변형율 감소효과가 미흡하고, 입도 조정 스텐레스 제강 슬래그 사용량이 60중량%를 초과할 경우에는 슬래그의 결정화에 따른 팽창의 효과가 너무 크게 되어 전체 변형율을 크게하기 때문이다.The use of such fine grained stainless steel slag is preferably at least 30% by weight and less than 60% by weight. The reason for this is that when the amount of the grain-adjusted stainless steel slag is less than 30% by weight, the effect of reducing the plastic strain of the clay brick is insufficient. If the amount of the adjusted stainless steel slag used exceeds 60% by weight, the effect of expansion due to the crystallization of the slag is too large to increase the overall strain rate.
또한, 본 발명에서의 소성온도 범위는 1050℃이상 1150℃이하가 바람직한데, 소성온도가 1050℃미만에서는 충분한 소성반응이 일어나지 않고, 1150℃를 초과하면 성형체가 용융되기 때문이다.In the present invention, the firing temperature range is preferably 1050 ° C. or higher and 1150 ° C. or lower, since a sufficient firing reaction does not occur when the firing temperature is lower than 1050 ° C., and the molded body melts when it exceeds 1150 ° C.
상기와 같은 온도범위에서는 소성시간은 1시간이상이면 충분하고, 1시간미만에서는 균일하고 충분한 소성반응이 일어나지 않는다.In the above temperature range, the firing time is sufficient for 1 hour or more, and in less than 1 hour, a uniform and sufficient firing reaction does not occur.
이하, 실시예를 통하여 본 발명을 보다 상세히 설명한다.Hereinafter, the present invention will be described in more detail with reference to Examples.
실시예 1Example 1
5mm이하로 입도조정된 스텐레스 제강슬래그를 하기 표1과 같은 비율로 점토와 배합하여 배합원료를 얻었다. 배합원료를 가수 혼련하여 함수율 20%로하고 토련기를 이용하여 진공토련시켜 성형한 다음 1150℃의 소성온도에서 5시간동안 소성시켜 점토벽돌을 제조하였다. 슬래그 함량에 따른 점토벽돌의 변형율을 측정한 결과를 하기 표1에 나타내었다.Stainless steel slag with a particle size adjusted to 5 mm or less was mixed with clay in the ratio as shown in Table 1 below to obtain a blended raw material. The raw material was kneaded and mixed to obtain a water content of 20%, vacuum drilled using a refining machine, and then fired at a firing temperature of 1150 ° C. for 5 hours to prepare clay bricks. The results of measuring the strain of clay brick according to the slag content are shown in Table 1 below.
상기 표1에서 알 수 있는 바와같이 슬래그 함량이 30중량%(발명예 1), 60중량%(발명예 2)인 경우가 슬래그 함량 20중량% (비교예 1)와 70중량%(비교예 2)보다 소성변형율을 거의 1/2이하 수준으로 크게 감소시킬 수 있음을 알 수 있다.As can be seen in Table 1, when the slag content is 30% by weight (Invention Example 1), 60% by weight (Invention Example 2), the slag content is 20% by weight (Comparative Example 1) and 70% by weight (Comparative Example 2). It can be seen that the plastic strain can be significantly reduced to almost 1/2 or less than
실시예 2Example 2
점토 40중량%와 입도조정 스텐레스 제강슬래그 60중량%의 비율로 배합하고, 가수 혼련하여 함수율 20%로 하고, 토련기를 이용하여 진공토련시켜 성형한 다음, 소성온도 1000~1200℃에서 5시간 동안 소성시켜 점토벽돌을 제조하였다. 소성온도에 따른 점토벽돌의 변형율을 측정한 결과를 하기 표2에 나타내었다.40% by weight of clay and 60% by weight of fine-grained stainless steel slag, kneading with water to make a water content of 20%, vacuum-molding with a refining machine, and then baking at 1000-1200 ° C for 5 hours. To prepare a clay brick. The results of measuring the strain of clay bricks according to the firing temperature are shown in Table 2 below.
상기 표2에 나타낸 바와같이 1050℃이하에서는 소성이 충분히 일어나지 않고 1200℃이상에서 성형체가 용융되어 부정형으로 되기 때문에 소성온도범위는 1050~1150℃가 바람직함을 알 수 있었다.As shown in Table 2 above, it was found that the firing temperature range was 1050 ° C to 1150 ° C because the molded body was not melted sufficiently at 1200 ° C or lower and became indefinite at 1050 ° C or lower.
실시예 3Example 3
점토 50중량%와 입도 조정 스텐레스 제강 슬래그 50중량%의 비율로 배합하고 가수 혼련하여 함수율 20%로 하고 토련기를 이용하여 진공토련시켜 성형한 다음 소성온도 1150℃에서 소성시간 30분-9시간으로 변화시켜 점토벽돌을 제조하였다. 소성시간에 따른 점토벽돌의 변형율을 측정한 결과를 하기 표3에 나타내었다.50% by weight of clay and 50% by weight of stainless steel slag for adjusting the particle size, mixing with water, kneading to make water content of 20%, and molding by vacuum drilling using a refining machine and then changing the firing time from 1150 ℃ to 30 minutes-9 hours. To prepare a clay brick. Table 3 shows the results of measuring the strain of clay brick according to firing time.
표 3에 나타낸 바와같이 소성시간은 1시간 이상이면 소성변형율이 1%이하로서 소성변형율 감소효과가 크게 나타남을 알 수 있었다.As shown in Table 3, when the firing time was 1 hour or more, the plastic strain was less than 1%, and the plastic strain was greatly reduced.
상술한 바와같이, 본 발명에 의하면 점토벽돌을 제조함에 있어 입도조정 스텐레스 제강 슬래그를 사용함으로써, 소성변형율이 적은 점토벽돌이 제공되는 효과가 있을 뿐만 아니라, 스텐레스 제강슬래그를 활용하는 효과도 있다.As described above, according to the present invention, in the manufacture of clay bricks, the use of the particle size adjusting stainless steel slag makes it possible not only to provide clay bricks with low plastic strain, but also to utilize stainless steel slag.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100401091B1 (en) * | 2000-10-04 | 2003-10-10 | (주)지플러스 | Biological clay brick holding anti-mildew action and method of producing the same |
KR20030086803A (en) * | 2002-05-07 | 2003-11-12 | 백래현 | Method for manufacturing a clay block |
KR100406318B1 (en) * | 2000-10-17 | 2003-11-19 | 김진만 | Manufacture and product of High strength whangtoh Block |
-
1997
- 1997-12-20 KR KR1019970071402A patent/KR19990051961A/en not_active Application Discontinuation
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100401091B1 (en) * | 2000-10-04 | 2003-10-10 | (주)지플러스 | Biological clay brick holding anti-mildew action and method of producing the same |
KR100406318B1 (en) * | 2000-10-17 | 2003-11-19 | 김진만 | Manufacture and product of High strength whangtoh Block |
KR20030086803A (en) * | 2002-05-07 | 2003-11-12 | 백래현 | Method for manufacturing a clay block |
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