KR102632794B1 - 분자체 ssz-113, 이의 합성 및 용도 - Google Patents

분자체 ssz-113, 이의 합성 및 용도 Download PDF

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KR102632794B1
KR102632794B1 KR1020207022124A KR20207022124A KR102632794B1 KR 102632794 B1 KR102632794 B1 KR 102632794B1 KR 1020207022124 A KR1020207022124 A KR 1020207022124A KR 20207022124 A KR20207022124 A KR 20207022124A KR 102632794 B1 KR102632794 B1 KR 102632794B1
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molecular sieve
reaction mixture
following
composition
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KR20200122311A (ko
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스테이시 이안 존스
단 씨에
콩-얀 첸
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셰브런 유.에스.에이.인크.
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/047—Germanosilicates; Aluminogermanosilicates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/34—Reaction with organic or organometallic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/30—Scanning electron microscopy; Transmission electron microscopy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/30—Three-dimensional structures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
KR1020207022124A 2018-02-20 2018-11-19 분자체 ssz-113, 이의 합성 및 용도 Active KR102632794B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201862632694P 2018-02-20 2018-02-20
US62/632,694 2018-02-20
PCT/IB2018/059086 WO2019162745A1 (en) 2018-02-20 2018-11-19 Molecular sieve ssz-113, its synthesis and use

Publications (2)

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KR20200122311A KR20200122311A (ko) 2020-10-27
KR102632794B1 true KR102632794B1 (ko) 2024-02-02

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US (1) US10384951B1 (enExample)
EP (1) EP3755660B1 (enExample)
JP (1) JP7097950B2 (enExample)
KR (1) KR102632794B1 (enExample)
CN (1) CN111032572B (enExample)
WO (1) WO2019162745A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4090627A1 (en) * 2020-01-16 2022-11-23 Chevron U.S.A. Inc. Molecular sieve ssz-117, its synthesis and use
JP7490783B2 (ja) * 2020-01-16 2024-05-27 シェブロン ユー．エス．エー． インコーポレイテッド 分子篩ｓｓｚ－１１６、その合成及び使用
US11161749B1 (en) 2020-05-22 2021-11-02 Chevron U.S.A. Inc. Molecular sieve SSZ-120, its synthesis and use
JP7622098B2 (ja) * 2020-05-28 2025-01-27 シェブロン ユー．エス．エー． インコーポレイテッド アルミノゲルマノケイ酸塩分子ふるいｓｓｚ－１２１、その合成及び使用
WO2023235700A1 (en) * 2022-05-31 2023-12-07 Chevron U.S.A. Inc. Molecular sieve boron ssz-113
US20230382745A1 (en) * 2022-05-31 2023-11-30 Chevron U.S.A. Inc. Molecular sieve ssz-113 with high acidity, its synthesis and use
KR20250016327A (ko) * 2022-05-31 2025-02-03 셰브런 유.에스.에이.인크. 고산도 분자체 SSZ-117x
EP4532416A1 (en) * 2022-05-31 2025-04-09 Chevron U.S.A. Inc. Molecular sieve ssz-121 with high acidity, its synthesis and use
CN120077012A (zh) * 2022-11-01 2025-05-30 雪佛龙美国公司 分子筛ssz-124、其合成和用途

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110011810A1 (en) 2007-11-12 2011-01-20 Ifp Im-18 crystalline solid and process for its preparation
US20120041210A1 (en) 2008-12-18 2012-02-16 IFP Energies Nouvelles Im-20 crystalline solid and process for its preparation
US20150202603A1 (en) 2014-01-22 2015-07-23 California Institute Of Technology Novel methods for producing crystalline microporous solids with the heu topology and compositions derived from the same
US20180207625A1 (en) 2017-01-20 2018-07-26 California Institute Of Technology Enantiomerically enriched, polycrystalline molecular sieves

Family Cites Families (10)

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US4483835A (en) * 1983-11-14 1984-11-20 Chevron Research Company Process for preparing molecular sieves using imidazole template
US6043179A (en) * 1997-08-13 2000-03-28 California Institute Of Technology Zeolite CIT-5 and method of making
US7157075B1 (en) * 2005-08-30 2007-01-02 Chevron U.S.A. Inc. Process for preparing MTT zeolites using nitrogen-containing organic compounds
FR2918979B1 (fr) 2007-07-20 2011-05-27 Inst Francais Du Petrole Solide cristallise im-16 et son procede de preparation
US7820141B2 (en) * 2008-10-10 2010-10-26 Chevron U.S.A. Inc. Molecular sieve SSZ-82 composition of matter and synthesis thereof
US8500991B2 (en) * 2008-12-16 2013-08-06 Exxonmobil Research And Engineering Company High activity MTT framework type molecular sieves
CA2757854A1 (en) 2009-04-09 2010-10-14 California Institute Of Technology Molecular sieves and related methods and structure directing agents
KR101757402B1 (ko) * 2010-06-25 2017-07-13 셰브런 유.에스.에이.인크. 분자체 ｓｓｚ-81
WO2011163016A2 (en) * 2010-06-25 2011-12-29 Chevron U.S.A. Inc. Processes using molecular sieve ssz-81
US9266744B2 (en) * 2013-10-10 2016-02-23 Chevron U.S.A. Inc. Synthesis of borosilicate ton-framework type molecular sieves

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110011810A1 (en) 2007-11-12 2011-01-20 Ifp Im-18 crystalline solid and process for its preparation
US20120041210A1 (en) 2008-12-18 2012-02-16 IFP Energies Nouvelles Im-20 crystalline solid and process for its preparation
US20150202603A1 (en) 2014-01-22 2015-07-23 California Institute Of Technology Novel methods for producing crystalline microporous solids with the heu topology and compositions derived from the same
US20180207625A1 (en) 2017-01-20 2018-07-26 California Institute Of Technology Enantiomerically enriched, polycrystalline molecular sieves

Also Published As

Publication number Publication date
JP2021513944A (ja) 2021-06-03
JP7097950B2 (ja) 2022-07-08
US20190256364A1 (en) 2019-08-22
US10384951B1 (en) 2019-08-20
KR20200122311A (ko) 2020-10-27
EP3755660A1 (en) 2020-12-30
WO2019162745A1 (en) 2019-08-29
EP3755660B1 (en) 2024-10-09
CN111032572A (zh) 2020-04-17
CN111032572B (zh) 2023-01-24

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