KR102551315B1 - Composition for har coloring containing hydroxytyrosol - Google Patents
Composition for har coloring containing hydroxytyrosol Download PDFInfo
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- KR102551315B1 KR102551315B1 KR1020220096186A KR20220096186A KR102551315B1 KR 102551315 B1 KR102551315 B1 KR 102551315B1 KR 1020220096186 A KR1020220096186 A KR 1020220096186A KR 20220096186 A KR20220096186 A KR 20220096186A KR 102551315 B1 KR102551315 B1 KR 102551315B1
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- JUUBCHWRXWPFFH-UHFFFAOYSA-N Hydroxytyrosol Chemical compound OCCC1=CC=C(O)C(O)=C1 JUUBCHWRXWPFFH-UHFFFAOYSA-N 0.000 title claims abstract description 92
- 239000000203 mixture Substances 0.000 title claims abstract description 56
- 229940095066 hydroxytyrosol Drugs 0.000 title claims abstract description 27
- 235000003248 hydroxytyrosol Nutrition 0.000 title claims abstract description 27
- 238000004040 coloring Methods 0.000 title 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 63
- 244000299461 Theobroma cacao Species 0.000 claims description 46
- 239000000843 powder Substances 0.000 claims description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 27
- 239000008213 purified water Substances 0.000 claims description 26
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Natural products OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 24
- 229940094952 green tea extract Drugs 0.000 claims description 21
- 235000020688 green tea extract Nutrition 0.000 claims description 21
- 241000405414 Rehmannia Species 0.000 claims description 20
- 239000001509 sodium citrate Substances 0.000 claims description 20
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 20
- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 claims description 18
- 235000005767 Theobroma cacao ssp. sphaerocarpum Nutrition 0.000 claims description 18
- 235000001046 cacaotero Nutrition 0.000 claims description 18
- 239000006000 Garlic extract Substances 0.000 claims description 17
- 235000020706 garlic extract Nutrition 0.000 claims description 17
- 241001107116 Castanospermum australe Species 0.000 claims description 16
- 229940069765 bean extract Drugs 0.000 claims description 16
- 235000021279 black bean Nutrition 0.000 claims description 16
- 239000000118 hair dye Substances 0.000 claims description 5
- 235000013399 edible fruits Nutrition 0.000 claims description 4
- 244000111388 Rubus occidentalis Species 0.000 claims 1
- 235000003942 Rubus occidentalis Nutrition 0.000 claims 1
- 210000004209 hair Anatomy 0.000 abstract description 102
- 238000004043 dyeing Methods 0.000 abstract description 87
- GGNQRNBDZQJCCN-UHFFFAOYSA-N benzene-1,2,4-triol Chemical compound OC1=CC=C(O)C(O)=C1 GGNQRNBDZQJCCN-UHFFFAOYSA-N 0.000 abstract description 16
- 210000004761 scalp Anatomy 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 3
- 230000000052 comparative effect Effects 0.000 description 94
- 235000009470 Theobroma cacao Nutrition 0.000 description 28
- 244000269722 Thea sinensis Species 0.000 description 24
- 235000006468 Thea sinensis Nutrition 0.000 description 21
- 240000002234 Allium sativum Species 0.000 description 19
- 244000068988 Glycine max Species 0.000 description 19
- 235000010469 Glycine max Nutrition 0.000 description 19
- 235000004611 garlic Nutrition 0.000 description 19
- 238000002474 experimental method Methods 0.000 description 18
- 238000001035 drying Methods 0.000 description 15
- 238000005406 washing Methods 0.000 description 13
- 230000006378 damage Effects 0.000 description 9
- 238000001816 cooling Methods 0.000 description 7
- 239000007788 liquid Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 239000002244 precipitate Substances 0.000 description 7
- 229940079990 rubus coreanus fruit extract Drugs 0.000 description 7
- 239000007787 solid Substances 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- 231100000640 hair analysis Toxicity 0.000 description 6
- 238000007654 immersion Methods 0.000 description 6
- 239000002453 shampoo Substances 0.000 description 6
- 239000008399 tap water Substances 0.000 description 6
- 235000020679 tap water Nutrition 0.000 description 6
- 240000007651 Rubus glaucus Species 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 238000001556 precipitation Methods 0.000 description 5
- 238000010298 pulverizing process Methods 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 235000020712 soy bean extract Nutrition 0.000 description 4
- 239000000975 dye Substances 0.000 description 3
- 235000009569 green tea Nutrition 0.000 description 3
- NAJVRARAUNYNDX-UHFFFAOYSA-N picamilon Chemical compound OC(=O)CCCNC(=O)C1=CC=CN=C1 NAJVRARAUNYNDX-UHFFFAOYSA-N 0.000 description 3
- 235000016623 Fragaria vesca Nutrition 0.000 description 2
- 240000009088 Fragaria x ananassa Species 0.000 description 2
- 235000011363 Fragaria x ananassa Nutrition 0.000 description 2
- 235000011034 Rubus glaucus Nutrition 0.000 description 2
- 235000009122 Rubus idaeus Nutrition 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 210000001519 tissue Anatomy 0.000 description 2
- 241001116389 Aloe Species 0.000 description 1
- 241000512259 Ascophyllum nodosum Species 0.000 description 1
- 229920002261 Corn starch Polymers 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- 240000001972 Gardenia jasminoides Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 240000007049 Juglans regia Species 0.000 description 1
- 235000009496 Juglans regia Nutrition 0.000 description 1
- 235000002789 Panax ginseng Nutrition 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 244000046146 Pueraria lobata Species 0.000 description 1
- 235000010575 Pueraria lobata Nutrition 0.000 description 1
- 241000219161 Theobroma Species 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 235000011399 aloe vera Nutrition 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 230000003700 hair damage Effects 0.000 description 1
- 230000003699 hair surface Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000014571 nuts Nutrition 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 210000003625 skull Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
- A61Q5/065—Preparations for temporary colouring the hair, e.g. direct dyes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Cosmetics (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Emergency Medicine (AREA)
Abstract
Description
본 발명은 하이드록시티로솔을 포함하는 모발 염색용 조성물에 관한 것으로, 더욱 구체적으로 인체에 무해하며, 모발 염색력이 우수하고, 다양한 환경에 노출되어도 장기간 모발 염색상태에 변화가 거의 없으며, 잦은 사용으로도 두피 또는 모발을 손상시키지 않는 모발 염색용 조성물에 관한 것이다.The present invention relates to a hair dyeing composition containing hydroxytyrosol, and more specifically, is harmless to the human body, has excellent hair dyeing power, has little change in hair dyeing state for a long period of time even when exposed to various environments, and frequently It relates to a composition for hair dyeing that does not damage the scalp or hair even when used.
모발은 태양빛, 강우, 바람, 추위 또는 외부 충격 등으로 부터 사람의 두개골과 두피 부분을 보호해 줌과 동시에 다양한 색상이나 모양으로 모발의 형태에 변화를 줌으로써 개개인의 개성을 표현하는 수단이 되기도 하는 매우 중요한 신체 기관이며 일종이 피부 조직에 해당한다.Hair protects the human skull and scalp from sunlight, rain, wind, cold or external shocks, and at the same time, it is a means of expressing individual individuality by changing the shape of hair into various colors or shapes. It is a very important organ of the body and one type corresponds to skin tissue.
이러한 모발은 피부의 표피 조직 등과 같이 평생 동안 지속적으로 자라나는 특성이 있으며, 나이가 들어감에 따라 모발이 가늘어지거나 전체 모발의 개수가 서서히 줄어들기도 하며, 일정 연령대에 도달하면, 태성적인 개개인 고유의 모발의 색상이 점차적으로 흰색 또는 회색으로 변색되는 과정을 거치게 된다.Such hair has a characteristic of continuously growing throughout life, such as the epidermal tissue of the skin, and with age, the hair thins or the total number of hairs gradually decreases. It goes through a process where the color gradually changes to white or gray.
따라서, 이와 같이 나이가 들어감에 따라 흰색 또는 회색으로 변색되는 모발을 특정 색상으로 염색하거나 이와 같이 노화에 따른 모발의 변색이 아니더라도 각자의 개성을 표현하기 위한 수단으로 모발을 다양한 색상으로 염색하기도 한다.Therefore, hair that is discolored to white or gray with age is dyed with a specific color, or hair is dyed with various colors as a means of expressing individuality even if the hair is not discolored due to aging.
그러나, 종래 사용되던 모발의 염색약에 필수적으로 함유되는 성분인 1,2,4-트라이하이드록시벤젠(THB) 성분은 현재에도 의료계, 학계 및 산업계에서 각종 유해성 논쟁이 벌어지고 있는 유해성 의심물질에 해당하며, 이와 같이 각종 유해성 논란이 끊이지 않는 상황에서도 모발을 빠른 시간 내에 효율적으로 염색하는 것이 가능하다는 이유만로 현재도 대부분의 모발 염색용 화장품이나 모발 염색제에 1,2,4-트라이하이드록시벤젠(THB)이 포함되어 유통되고 있는 실정이다.However, 1,2,4-trihydroxybenzene (THB), which is an essential ingredient in hair dyes that have been used in the past, is a suspected harmful substance that is still subject to various harmfulness debates in the medical, academic, and industrial world. 1,2,4-trihydroxybenzene (THB) is still used in most hair dye cosmetics or hair dyes just because it is possible to dye hair efficiently in a short time even in the situation where various harmfulness controversies continue. ) is included and distributed.
한편, 하기 특허문헌 1은 이러한 문제점을 해결하고자 천연성분인 흑홍삼, 콩파우더, 옥수수전분, 칡, 호두피, 참나무가시, 알로에, 치자, 녹차잎, 다시마, 오배자 분말을 포함하는 천연물로 조성된 염모제를 개시하고 있으나, 이러한 천연성분의 조합만으로는 모발의 염색력 및 염색지속력이 상대적으로 낮은 한계를 지니고 있었다.On the other hand, Patent Document 1 below is composed of natural ingredients including black red ginseng, soybean powder, corn starch, kudzu, walnut skin, oak thorn, aloe, gardenia, green tea leaves, kelp, gall nut powder, which are natural ingredients to solve these problems However, the combination of these natural ingredients alone has relatively low dyeing power and dyeing durability.
따라서, 1,2,4-트라이하이드록시벤젠(THB)을 사용하지 않아 인체에 무해하며, 1,2,4-트라이하이드록시벤젠(THB) 없이도 우수한 모발 염색력을 나타낼 수 있으며, 다양한 환경에 노출되어도 장기간 모발 염색상태에 변화가 거의 없으며, 잦은 사용으로도 두피 또는 모발을 손상시키지 않는 모발 염색용 조성물에 관한 개발이 절실히 요구되는 실정이다.Therefore, it is harmless to the human body because 1,2,4-trihydroxybenzene (THB) is not used, and excellent hair dyeing power can be displayed without 1,2,4-trihydroxybenzene (THB), and it can be used in various environments. Even when exposed, there is little change in the hair dyeing state for a long time, and there is an urgent need to develop a hair dyeing composition that does not damage the scalp or hair even with frequent use.
이에 본 발명에서는 상기 문제점 등을 해결하고자 1,2,4-트라이하이드록시벤젠(THB)을 전혀 사용하지 않고, 하이드록시티로솔을 이용하여 인체에 무해하며, 우수한 모발 염색력을 나타낼 수 있으며, 다양한 환경에 노출되어도 장기간 모발 염색상태에 변화가 거의 없고, 잦은 사용으로도 두피 또는 모발을 손상시키지 않는 모발 염색용 조성물을 개발하게 되었다.Accordingly, in the present invention, in order to solve the above problems, 1,2,4-trihydroxybenzene (THB) is not used at all, and hydroxytyrosol is used, which is harmless to the human body and can exhibit excellent hair dyeing power. , It has been developed a hair dyeing composition that has little change in the state of hair dyeing for a long period of time even when exposed to various environments and does not damage the scalp or hair even with frequent use.
따라서, 본 발명의 하나의 관점은 하이드록시티로솔을 포함함으로써, 인체에 무해하며, 우수한 모발 염색력을 나타낼 수 있고, 다양한 환경에 노출되어도 장기간 모발 염색상태에 변화가 거의 없고, 잦은 사용으로도 두피 또는 모발을 손상시키지 않는 모발 염색용 조성물을 제공하는 데 있다.Therefore, one aspect of the present invention is that by including hydroxytyrosol, it is harmless to the human body, can exhibit excellent hair dyeing power, has little change in the long-term hair dyeing state even when exposed to various environments, and frequent use It is also an object of the present invention to provide a composition for dyeing hair that does not damage the scalp or hair.
본 발명의 일 구현예에 따른 모발 염색용 조성물은 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol)을 포함하는 것을 특징으로 한다.The hair dyeing composition according to one embodiment of the present invention is characterized in that it contains hydroxytyrosol (3,4-dihydroxyphenylethanol).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 카카오추출물(Theobroma Cacao (Cocoa) Extract) 및 카카오씨추출물 (Theobroma Cacao (Cocoa) Seed Extract) 중 하나 이상을 더 포함하는 것을 특징으로 한다.The hair dyeing composition according to one embodiment of the present invention is characterized in that it further comprises at least one of cacao extract (Theobroma Cacao (Cocoa) Extract) and cacao seed extract (Theobroma Cacao (Cocoa) Seed Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 녹차추출물(Camellia Sinensis Leaf Extract)을 더 포함하는 것을 특징으로 한다.The hair dyeing composition according to one embodiment of the present invention is characterized in that it further comprises a green tea extract (Camellia Sinensis Leaf Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 복분자딸기열매추출물(Rubus Coreanus Fruit Extract)을 더 포함하는 것을 특징으로 한다.The hair dyeing composition according to one embodiment of the present invention is characterized in that it further comprises a raspberry strawberry fruit extract (Rubus Coreanus Fruit Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 검정콩추출물(Glycine Soja Seed Extract)을 더 포함하는 것을 특징으로 한다.The hair dyeing composition according to one embodiment of the present invention is characterized in that it further comprises black soybean extract (Glycine Soja Seed Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 마늘추출물(Allium Sativum Bulb Extract)을 더 포함하는 것을 특징으로 한다.The hair dyeing composition according to one embodiment of the present invention is characterized in that it further comprises garlic extract (Allium Sativum Bulb Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 지황뿌리추출물(Rehmannia Chinensis Root Extract)을 더 포함하는 것을 특징으로 한다.The hair dyeing composition according to one embodiment of the present invention is characterized in that it further comprises Rehmannia Chinensis Root Extract.
본 발명에 따른 모발 염색용 조성물은 1,2,4-트라이하이드록시벤젠(THB)을 전혀 사용하지 않아 인체에 무해하며, 1,2,4-트라이하이드록시벤젠(THB) 없이도 우수한 모발 염색력을 나타낼 수 있으며, 다양한 환경에 노출되어도 장기간 모발 염색상태에 변화가 거의 없으며, 잦은 사용으로도 두피 또는 모발을 손상시키지 않는 장점을 갖는다.The hair dyeing composition according to the present invention does not use 1,2,4-trihydroxybenzene (THB) at all, so it is harmless to the human body and has excellent hair dyeing power even without 1,2,4-trihydroxybenzene (THB). It can represent, and even when exposed to various environments, there is little change in the hair dyeing state for a long time, and it has the advantage of not damaging the scalp or hair even with frequent use.
본 발명을 좀 더 구체적으로 설명하기 전에, 본 명세서 및 청구범위에 사용된 용어나 단어는 통상적이거나 사전적인 의미로 한정되어서는 아니되며, 발명을 가장 최선의 방법으로 설명하기 위해 용어의 개념을 적절하게 정의할 수 있다는 원칙에 입각하여 본 발명의 기술적 사상에 부합하는 의미와 개념으로 해석되어야만 한다. 따라서, 본 명세서에 기재된 실시 예의 구성은 본 발명의 바람직한 하나의 예에 불과할 뿐이고, 본 발명의 기술적 사상을 모두 대변하는 것은 아니므로, 본 출원시점에 있어서 이들을 대체할 수 있는 다양한 균등물과 변형 예들이 있을 수 있음을 이해하여야 한다. Before describing the present invention in more detail, the terms or words used in this specification and claims should not be limited to their usual or dictionary meanings, and the concept of terms is appropriately used to describe the invention in the best way. It should be interpreted as a meaning and concept consistent with the technical spirit of the present invention based on the principle that it can be defined in the following way. Therefore, the configuration of the embodiments described in this specification is only one preferred example of the present invention, and does not represent all of the technical spirit of the present invention, so various equivalents and modifications that can replace them at the time of the present application It should be understood that there may be
이하, 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 본 발명을 용이하게 실시할 수 있도록, 본 발명의 바람직한 실시 예들을 상세히 설명한다. 아울러, 본 발명을 설명함에 있어서, 본 발명의 요지를 불필요하게 흐릴 수 있는 관련된 공지기술에 대한 상세한 설명은 생략한다.Hereinafter, preferred embodiments of the present invention will be described in detail so that those skilled in the art can easily practice the present invention. In addition, in describing the present invention, detailed descriptions of related known technologies that may unnecessarily obscure the gist of the present invention will be omitted.
본 발명의 일 구현예에 따른 모발 염색용 조성물은 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol)을 포함한다.The hair dyeing composition according to one embodiment of the present invention includes hydroxytyrosol (3,4-dihydroxyphenylethanol).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 카카오추출물(Theobroma Cacao (Cocoa) Extract) 및 카카오씨추출물 (Theobroma Cacao (Cocoa) Seed Extract) 중 하나 이상을 더 포함할 수 있다.The hair dyeing composition according to one embodiment of the present invention may further include at least one of cacao extract (Theobroma Cacao (Cocoa) Extract) and cacao seed extract (Theobroma Cacao (Cocoa) Seed Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 녹차추출물(Camellia Sinensis Leaf Extract)을 더 포함할 수 있다.The hair dyeing composition according to one embodiment of the present invention may further include a green tea extract (Camellia Sinensis Leaf Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 복분자딸기열매추출물(Rubus Coreanus Fruit Extract)을 더 포함할 수 있다.The composition for hair dyeing according to one embodiment of the present invention may further include Rubus Coreanus Fruit Extract.
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 검정콩추출물(Glycine Soja Seed Extract)을 더 포함할 수 있다.The hair dyeing composition according to one embodiment of the present invention may further include black soybean extract (Glycine Soja Seed Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 마늘추출물(Allium Sativum Bulb Extract)을 더 포함할 수 있다.The hair dyeing composition according to one embodiment of the present invention may further include garlic extract (Allium Sativum Bulb Extract).
본 발명의 일 구현예에 따른 상기 모발 염색용 조성물은 지황뿌리추출물(Rehmannia Chinensis Root Extract)을 더 포함할 수 있다.The hair dyeing composition according to one embodiment of the present invention may further include Rehmannia Chinensis Root Extract.
한편, 본 발명의 다른 구현예에 따른 모발 염색용 조성물은 상기 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol), 카카오추출물(Theobroma Cacao (Cocoa) Extract), 카카오씨추출물 (Theobroma Cacao (Cocoa) Seed Extract), 녹차추출물(Camellia Sinensis Leaf Extract), 복분자딸기열매추출물(Rubus Coreanus Fruit Extract), 검정콩추출물(Glycine Soja Seed Extract), 마늘추출물(Allium Sativum Bulb Extract), 지황뿌리추출물(Rehmannia Chinensis Root Extract) 이외에 시트릭애씨드(Citric Acid), 소듐시트레이트(Sodium Citrate), 포타슘하이드록사이드(Potassium Hydroxide), 또는 하기 화학식 1의 N-니코티노일-가바(N-nicotynoyl-GABA)를 더욱 포함할 수 있다.On the other hand, the hair dyeing composition according to another embodiment of the present invention includes the hydroxytyrosol (3,4-dihydroxyphenylethanol), the cacao extract (Theobroma Cacao (Cocoa) Extract), the cacao seed extract (Theobroma Cacao ( Cocoa Seed Extract), Camellia Sinensis Leaf Extract, Rubus Coreanus Fruit Extract, Glycine Soja Seed Extract, Allium Sativum Bulb Extract, Rehmannia Chinensis Root Extract), Citric Acid, Sodium Citrate, Potassium Hydroxide, or N-nicotinoyl-GABA of Formula 1 below can include
[화학식 1][Formula 1]
본 발명에서 정제수 1,000중량당 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol)은 1 내지 150중량, 카카오추출물(Theobroma Cacao (Cocoa) Extract) 1 내지 150중량, 카카오씨추출물 (Theobroma Cacao (Cocoa) Seed Extract) 1 내지 150중량, 녹차추출물(Camellia Sinensis Leaf Extract) 1 내지 150중량, 복분자딸기열매추출물(Rubus Coreanus Fruit Extract) 1 내지 150중량, 검정콩추출물(Glycine Soja Seed Extract) 1 내지 150중량, 마늘추출물(Allium Sativum Bulb Extract) 1 내지 150중량, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 1 내지 150중량, 시트릭애씨드(Citric Acid) 1 내지 100중량, 소듐시트레이트(Sodium Citrate) 1 내지 100중량, 포타슘하이드록사이드(Potassium Hydroxide) 1 내지 100중량, N-니코티노일-가바(N-nicotynoyl-GABA) 1 내지 150중량의 비율로 혼합하는 것이 가능하다.In the present invention, hydroxytyrosol (3,4-dihydroxyphenylethanol) per 1,000 weight of purified water is 1 to 150 weight, cacao extract (Theobroma Cacao (Cocoa) Extract) 1 to 150 weight, cacao seed extract (Theobroma Cacao ( Cocoa) Seed Extract 1 to 150 weight, green tea extract (Camellia Sinensis Leaf Extract) 1 to 150 weight, raspberry strawberry fruit extract (Rubus Coreanus Fruit Extract) 1 to 150 weight, black bean extract (Glycine Soja Seed Extract) 1 to 150 weight , Allium Sativum Bulb Extract 1 to 150 weight, Rehmannia Chinensis Root Extract 1 to 150 weight, Citric Acid 1 to 100 weight, Sodium Citrate 1 to 100 It is possible to mix in a ratio of 1 to 100 weight of potassium hydroxide and 1 to 150 weight of N-nicotinoyl-GABA.
본 발명에서 상기 카카오씨추출물(Theobroma Cacao Seed Extract)은 카카오씨를 채취하여 건조과정 없이 세척하고, 잘게 분쇄한 후, 분쇄된 카카오씨 100중량당 약 1,000중량의 정제수를 가하여 약 30분동안 가열하고 실온(25℃)으로 냉각한 후, 200메쉬의 필터를 통과시켜 고형성분을 제거하고, 약 4℃의 온도에서 약 24시간 동안 침전과정을 진행한 후, 침전물을 제거하고 나머지 상층부의 액상추출물을 수득하는 방법으로 얻었다.In the present invention, the cacao bean extract (Theobroma Cacao Seed Extract) is obtained by collecting cacao seeds, washing without drying, pulverizing, adding about 1,000 weight of purified water per 100 weight of pulverized cacao seeds, heating for about 30 minutes, and room temperature After cooling to (25 ° C), solid components were removed by passing through a 200 mesh filter, and precipitation was performed at a temperature of about 4 ° C for about 24 hours, and then the precipitate was removed and the liquid extract of the upper layer was obtained. got it in a way
본 발명에서 상기 카카오추출물(Theobroma Cacao Extract)은 카카오 과육을 준비하여 건조과정 없이 세척하고, 잘게 분쇄한 후, 분쇄된 카카오 과육 100중량당 약 1,000중량의 정제수를 가하여 약 30분동안 가열하고 실온(25℃)으로 냉각한 후, 200메쉬의 필터를 통과시켜 고형성분을 제거하고, 약 4℃의 온도에서 약 24시간 동안 침전과정을 진행한 후, 침전물을 제거하고 나머지 상층부의 액상추출물을 수득하는 방법으로 얻었다.In the present invention, the cacao extract (Theobroma Cacao Extract) is prepared by preparing cacao pulp, washing without drying, finely pulverizing, adding about 1,000 weight of purified water per 100 weight of pulverized cacao pulp, heating for about 30 minutes, and room temperature ( After cooling to 25 ° C), solid components were removed by passing through a 200 mesh filter, and precipitation was performed at a temperature of about 4 ° C for about 24 hours, and then the precipitate was removed and the liquid extract of the remaining upper layer was obtained. got it in a way
본 발명에서 상기 녹차추출물(Camellia Sinensis Leaf Extract)은 녹차잎을 채취하여 건조과정 없이 세척하고, 잘게 분쇄한 후, 분쇄된 녹차잎 100중량당 약 1,000중량의 정제수를 가하여 약 30분동안 가열하고 실온(25℃)으로 냉각한 후, 200메쉬의 필터를 통과시켜 고형성분을 제거하고, 약 4℃의 온도에서 약 24시간 동안 침전과정을 진행한 후, 침전물을 제거하고 나머지 상층부의 액상추출물을 수득하는 방법으로 얻었다.In the present invention, the green tea extract (Camellia Sinensis Leaf Extract) is obtained by collecting green tea leaves, washing without drying, pulverizing finely, adding about 1,000 weight of purified water per 100 weight of pulverized green tea leaves, heating for about 30 minutes, and room temperature After cooling to (25 ° C), solid components were removed by passing through a 200 mesh filter, and precipitation was performed at a temperature of about 4 ° C for about 24 hours, and then the precipitate was removed and the liquid extract of the upper layer was obtained. got it in a way
본 발명에서 상기 복분자딸기열매추출물(Rubus Coreanus Fruit Extract)은 복분자딸기 과육을 채취하여 건조과정 없이 세척하고, 잘게 분쇄한 후, 분쇄된 복분자딸기 과육 100중량당 약 1,000중량의 정제수를 가하여 약 30분동안 가열하고 실온(25℃)으로 냉각한 후, 200메쉬의 필터를 통과시켜 고형성분을 제거하고, 약 4℃의 온도에서 약 24시간 동안 침전과정을 진행한 후, 침전물을 제거하고 나머지 상층부의 액상추출물을 수득하는 방법으로 얻었다.In the present invention, the raspberry raspberry fruit extract (Rubus Coreanus Fruit Extract) is obtained by collecting raspberry raspberry flesh, washing without drying, pulverizing finely, and then adding about 1,000 weight of purified water per 100 weight of raspberry raspberry pulp for about 30 minutes After heating for a while and cooling to room temperature (25℃), solid components were removed by passing through a 200-mesh filter, and after a precipitation process at a temperature of about 4℃ for about 24 hours, the precipitate was removed and the remaining upper layer It was obtained by a method for obtaining a liquid extract.
본 발명에서 상기 검정콩추출물(Glycine Soja Seed Extract)은 검정콩을 채취하여 건조과정 없이 세척하고, 잘게 분쇄한 후, 분쇄된 검정콩 100중량당 약 1,000중량의 정제수를 가하여 약 30분동안 가열하고 실온(25℃)으로 냉각한 후, 200메쉬의 필터를 통과시켜 고형성분을 제거하고, 약 4℃의 온도에서 약 24시간 동안 침전과정을 진행한 후, 침전물을 제거하고 나머지 상층부의 액상추출물을 수득하는 방법으로 얻었다.In the present invention, the black soybean extract (Glycine Soja Seed Extract) is collected from black beans, washed without drying, finely ground, and then added with about 1,000 weight of purified water per 100 weight of ground black beans, heated for about 30 minutes, and room temperature (25 After cooling to ° C), passing through a 200 mesh filter to remove solid components, precipitating at a temperature of about 4 ° C for about 24 hours, removing the precipitate and obtaining the remaining upper liquid extract got by
본 발명에서 상기 마늘추출물(Allium Sativum Bulb Extract)은 마늘을 채취하여 건조과정 없이 세척하고, 잘게 분쇄한 후, 분쇄된 마늘 100중량당 약 1,000중량의 정제수를 가하여 약 30분동안 가열하고 실온(25℃)으로 냉각한 후, 200메쉬의 필터를 통과시켜 고형성분을 제거하고, 약 4℃의 온도에서 약 24시간 동안 침전과정을 진행한 후, 침전물을 제거하고 나머지 상층부의 액상추출물을 수득하는 방법으로 얻었다.In the present invention, the garlic extract (Allium Sativum Bulb Extract) is collected from garlic, washed without drying, finely pulverized, and then added with about 1,000 weight of purified water per 100 weight of crushed garlic, heated for about 30 minutes, and room temperature (25 After cooling to ° C), passing through a 200 mesh filter to remove solid components, precipitating at a temperature of about 4 ° C for about 24 hours, removing the precipitate and obtaining the remaining upper liquid extract got by
본 발명에서 상기 지황뿌리추출물(Rehmannia Chinensis Root Extract)은 지황뿌리를 채취하여 건조과정 없이 세척하고, 잘게 분쇄한 후, 분쇄된 지황뿌리 100중량당 약 1,000중량의 정제수를 가하여 약 30분동안 가열하고 실온(25℃)으로 냉각한 후, 200메쉬의 필터를 통과시켜 고형성분을 제거하고, 약 4℃의 온도에서 약 24시간 동안 침전과정을 진행한 후, 침전물을 제거하고 나머지 상층부의 액상추출물을 수득하는 방법으로 얻었다.In the present invention, the Rehmannia Chinensis Root Extract is obtained by collecting Rehmannia Chinensis Root, washing it without drying, pulverizing it finely, adding about 1,000 weight of purified water per 100 weight of pulverized Rehmannia root, heating for about 30 minutes, After cooling to room temperature (25 ° C), solid components were removed by passing through a 200 mesh filter, and precipitation was performed at a temperature of about 4 ° C for about 24 hours, and then the precipitate was removed and the liquid extract of the upper layer was removed. Obtained by the method of obtaining.
이하, 다양한 실시예 및 비교예를 통하여 본 발명의 효과를 실험한 실험 및 그 결과를 설명하기로 한다.Hereinafter, experiments and results of testing the effects of the present invention through various examples and comparative examples will be described.
[실시예 1][Example 1]
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, Citric Acid powder 20g, Sodium Citrate powder 20g , Potassium Hydroxide (Potassium Hydroxide) powder 20g was evenly mixed to prepare a composition for hair dyeing.
[실시예 2][Example 2]
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, citric acid powder 20g , 20 g of sodium citrate powder and 20 g of potassium hydroxide powder were evenly mixed to prepare a composition for hair dyeing.
[실시예 3][Example 3]
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g , 20 g of Citric Acid powder, 20 g of Sodium Citrate powder, and 20 g of Potassium Hydroxide powder were evenly mixed to prepare a composition for hair dyeing.
[실시예 4][Example 4]
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g , Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Citric Acid Powder 20g, Sodium Citrate Powder 20g, Potassium Hydroxide ) A composition for hair dyeing was prepared by evenly mixing 20 g of the powder.
[실시예 5][Example 5]
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g, 복분자딸기열매추출물(Rubus Coreanus Fruit Extract) 50g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g , Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Citric Acid Powder 20g, Sodium Citrate Powder 20g, Potassium Hydroxide ) 20 g of powder and 50 g of Rubus Coreanus Fruit Extract were evenly mixed to prepare a composition for hair dyeing.
[실시예 6][Example 6]
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g, 복분자딸기열매추출물(Rubus Coreanus Fruit Extract) 50g, N-니코티노일-가바(N-nicotynoyl-GABA) 50g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g , Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Citric Acid Powder 20g, Sodium Citrate Powder 20g, Potassium Hydroxide ) 20 g of powder, 50 g of Rubus Coreanus Fruit Extract, and 50 g of N-nicotinoyl-GABA were evenly mixed to prepare a composition for hair dyeing.
[비교예 1] - 실시예 4에서 하이드록시티로솔 제외[Comparative Example 1] - Excluding hydroxytyrosol in Example 4
정제수 1,000g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, Green Tea Extract (Camellia Sinensis Leaf Extract) 50g, Black Bean Extract (Glycine Soja Seed Extract) 50g, Garlic Extract (Allium Sativum Bulb Extract) 50g, Rehmannia Chinensis Root Extract 50g, Cacao Seed Extract (Theobroma) 50 g of Cacao Seed Extract, 20 g of Citric Acid powder, 20 g of Sodium Citrate powder, and 20 g of Potassium Hydroxide powder were evenly mixed to prepare a composition for hair dyeing.
[비교예 2] - 실시예 4에서 녹차추출물 제외[Comparative Example 2] - Excluding green tea extract in Example 4
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g, Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Citric Acid powder 20g, Sodium Citrate powder 20g, Potassium Hydroxide powder 20g mixed evenly for hair dyeing A composition was prepared.
[비교예 3] - 실시예 4에서 검정콩추출물 제외[Comparative Example 3] - Excluding black soybean extract from Example 4
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g, Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Citric Acid powder 20g, Sodium Citrate powder 20g, Potassium Hydroxide powder 20g mixed evenly for hair dyeing A composition was prepared.
[비교예 4] - 실시예 4에서 마늘추출물 제외[Comparative Example 4] - Excluding garlic extract from Example 4
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Citric Acid powder 20g, Sodium Citrate powder 20g, Potassium Hydroxide powder 20g mixed evenly for hair dyeing A composition was prepared.
[비교예 5] - 실시예 4에서 지황뿌리추출물 제외[Comparative Example 5] - Excluding Rehmannia root extract from Example 4
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g , Hair dye composition by evenly mixing 50g of Theobroma Cacao Seed Extract, 20g of Citric Acid powder, 20g of Sodium Citrate powder, and 20g of Potassium Hydroxide powder was manufactured.
[비교예 6] - 실시예 4에서 카카오씨추출물 제외[Comparative Example 6] - Except for cacao seed extract in Example 4
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g , Rehmannia Chinensis Root Extract 50g, Citric Acid powder 20g, Sodium Citrate powder 20g, Potassium Hydroxide powder 20g mixed evenly to form a composition for hair dyeing. was manufactured.
[비교예 7] - 실시예 4에서 시트릭애씨드분말 제외[Comparative Example 7] - Excluding citric acid powder from Example 4
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g For hair dyeing, evenly mix Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Sodium Citrate powder 20g, Potassium Hydroxide powder 20g A composition was prepared.
[비교예 8] - 실시예 4에서 소듐시트레이트분말 제외[Comparative Example 8] - Excluding sodium citrate powder in Example 4
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g For hair dyeing, evenly mix Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Citric Acid powder 20g, Potassium Hydroxide powder 20g A composition was prepared.
[비교예 9] - 실시예 4에서 포타슘하이드록사이드분말 제외[Comparative Example 9] - Excluding potassium hydroxide powder in Example 4
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 검정콩추출물(Glycine Soja Seed Extract) 50g, 마늘추출물(Allium Sativum Bulb Extract) 50g, 지황뿌리추출물(Rehmannia Chinensis Root Extract) 50g, 카카오씨추출물(Theobroma Cacao Seed Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, green tea extract (Camellia Sinensis Leaf Extract) 50g, black bean extract (Glycine Soja Seed Extract) 50g, garlic extract (Allium Sativum Bulb Extract) 50g , Rehmannia Chinensis Root Extract 50g, Theobroma Cacao Seed Extract 50g, Citric Acid powder 20g, Sodium Citrate powder 20g mixed evenly to form a composition for hair dyeing. was manufactured.
[비교예 10] - 실시예 1에서 하이드록시티로솔 제외[Comparative Example 10] - Excluding hydroxytyrosol in Example 1
정제수 1,000g, 녹차추출물(Camellia Sinensis Leaf Extract) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.1,000g of purified water, 50g of Camellia Sinensis Leaf Extract, 20g of Citric Acid powder, 20g of Sodium Citrate powder, and 20g of Potassium Hydroxide powder were mixed evenly to dye the hair. A composition was prepared.
[비교예 11] - 실시예 1에서 녹차추출물(Camellia Sinensis Leaf Extract) 제외[Comparative Example 11] - Excluding the green tea extract (Camellia Sinensis Leaf Extract) in Example 1
정제수 1,000g, 하이드록시티로솔(hydroxytyrosol)(3,4-dihydroxyphenylethanol) 50g, 시트릭애씨드(Citric Acid)분말 20g, 소듐시트레이트(Sodium Citrate)분말 20g, 포타슘하이드록사이드(Potassium Hydroxide)분말 20g을 고르게 혼합하여 모발 염색용 조성물을 제조하였다.Purified water 1,000g, hydroxytyrosol (3,4-dihydroxyphenylethanol) 50g, Citric Acid powder 20g, Sodium Citrate powder 20g, Potassium Hydroxide powder 20 g was evenly mixed to prepare a composition for hair dyeing.
[실험 1][Experiment 1]
상기 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물을 이용하여 모발 염색력을 테스트하는 실험을 수행하였다.An experiment was performed to test hair dyeability using the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11.
모발 염색력 테스트는 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물에 흰색 자연모 샘플(각각 10g)을 15분간 완전히 침지시키는 방법으로 수행하였고, 15분간의 침지가 종료된 후 흐르는 수돗물에 3회 세척하고 1시간 동안 자연 바람으로 건조시킨 후 모발의 염색 정도를 측정하였고, 염색된 정도는 모발의 명도값(100: 가장 밝음, 0: 가장 어두움, 즉 명도값이 낮을수록 우수한 염색력을 나타냄)를 측정하는 방법으로 수행하였으며, 그 결과를 하기 표 1에 나타내었다.The hair dyeability test was carried out by completely immersing white natural hair samples (10g each) in the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11 for 15 minutes, and the 15 minutes of immersion was completed. After washing with flowing tap water three times and drying with natural wind for 1 hour, the degree of dyeing of the hair was measured. It was performed by a method for measuring the higher dyeing power), and the results are shown in Table 1 below.
(100: 가장 밝음, 0: 가장 어두움)brightness value
(100: brightest, 0: darkest)
상기 표 1의 결과를 살펴보면, 비교예 10 및 11에 비하여 실시예 1 내지 6의 경우 우수한 염색력을 발휘함을 확인할 수 있다.Looking at the results of Table 1, it can be confirmed that Examples 1 to 6 exhibit excellent dyeing power compared to Comparative Examples 10 and 11.
또한, 비교예 1 내지 9에 비하여 실시예 4가 우수한 염색력을 발휘함을 확인할 수 있다.In addition, it can be confirmed that Example 4 exhibits excellent dyeing power compared to Comparative Examples 1 to 9.
또한, 실시예 1 내지 3에 비하여 실시예 4의 경우 더욱 우수한 염색력을 나타냄을 확인할 수 있다.In addition, it can be confirmed that Example 4 exhibits more excellent dyeing power than Examples 1 to 3.
또한, 실시예 6의 경우 가장 우수한 염색력을 나타냄을 확인할 수 있다.In addition, it can be seen that Example 6 exhibits the best dyeing power.
[실험 2][Experiment 2]
상기 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물을 이용하여 고온 환경에서 모발 염색력이 어느 정도 유지되는지 확인하는 실험을 수행하였다.Using the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11, an experiment was performed to determine how much hair dyeing ability was maintained in a high-temperature environment.
고온 환경 염색력 유지 실험은 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물에 흰색 자연모 샘플(각각 10g)을 15분간 완전히 침지시키고, 15분간의 침지가 종료된 후 흐르는 수돗물에 3회 세척하고 1시간 동안 자연 바람으로 건조시킨 후 45℃로 유지되는 챔버에 20일간 보관한 후에 꺼내어 모발의 염색 상태를 측정하였고, 모발 염색 정도는 모발의 명도값(100: 가장 밝음, 0: 가장 어두움, 즉 명도값이 낮을수록 우수한 염색력을 나타냄)를 측정하는 방법으로 수행하였으며, 그 결과를 하기 표 2에 나타내었다.In the high-temperature environment dyeability maintenance experiment, white natural hair samples (each 10g) were completely immersed in the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11 for 15 minutes, and after the 15 minutes of immersion was completed, After washing with flowing tap water three times, drying with natural wind for 1 hour, and storing it in a chamber maintained at 45 ° C for 20 days, it was taken out and the dyed state of the hair was measured. , 0: the darkest, that is, the lower the brightness value, the better dyeing power) was performed, and the results are shown in Table 2 below.
(100: 가장 밝음, 0: 가장 어두움)brightness value
(100: brightest, 0: darkest)
상기 표 2의 결과를 표 1의 결과와 비교하여 살펴보면, 실시예 4 내지 6의 경우 모발의 염색 정도가 전혀 변하지 않았음을 확인할 수 있다.Comparing the results of Table 2 with the results of Table 1, it can be seen that the degree of dyeing of the hair in Examples 4 to 6 did not change at all.
[실험 3][Experiment 3]
상기 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물을 이용하여 고염분 대기 환경에서 모발 염색력이 어느 정도 유지되는지 확인하는 실험을 수행하였다.Using the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11, an experiment was performed to determine how much hair dyeing ability was maintained in a high salt air environment.
고염분 대기 환경 염색력 유지 실험은 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물에 흰색 자연모 샘플(각각 10g)을 15분간 완전히 침지시키고, 15분간의 침지가 종료된 후 흐르는 수돗물에 3회 세척하고 1시간 동안 자연 바람으로 건조시킨 후 공기중의 염분(NaCl) 농도가 3g/㎥로 유지되는 염분 대기 상태가 조성되어 유지되는 챔버에 20일간 보관한 후에 꺼내어 모발의 염색 상태를 측정하였고, 모발 염색 정도는 모발의 명도값(100: 가장 밝음, 0: 가장 어두움, 즉 명도값이 낮을수록 우수한 염색력을 나타냄)를 측정하는 방법으로 수행하였으며, 그 결과를 하기 표 3에 나타내었다.In the test for maintaining dyeing power in a high salt air environment, white natural hair samples (10 g each) were completely immersed in the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11 for 15 minutes, and the 15 minutes of immersion was completed. After washing with flowing tap water three times and drying with natural wind for 1 hour, the concentration of salt (NaCl) in the air is maintained at 3g/m3 in a chamber where a salt atmosphere is created and maintained for 20 days. The dyeing state was measured, and the degree of hair dyeing was performed by measuring the lightness value of the hair (100: the brightest, 0: the darkest, that is, the lower the lightness value, the better the dyeing power), the results are shown in the table below 3.
(100: 가장 밝음, 0: 가장 어두움)brightness value
(100: brightest, 0: darkest)
상기 표 3의 결과를 표 1의 결과와 비교하여 살펴보면, 실시예 4 내지 6의 경우 모발의 염색 정도가 전혀 변하지 않았음을 확인할 수 있다.Comparing the results of Table 3 with the results of Table 1, it can be seen that the degree of dyeing of the hair in Examples 4 to 6 did not change at all.
[실험 4][Experiment 4]
상기 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물을 이용하여 고습 대기 환경에서 모발 염색력이 어느 정도 유지되는지 확인하는 실험을 수행하였다.Using the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11, an experiment was performed to determine how much hair dyeability was maintained in a high-humidity air environment.
고습 대기 환경 염색력 유지 실험은 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물에 흰색 자연모 샘플(각각 10g)을 15분간 완전히 침지시키고, 15분간의 침지가 종료된 후 흐르는 수돗물에 3회 세척하고 1시간 동안 자연 바람으로 건조시킨 후 공기중의 습도가 70%로 유지되는 고습 대기 상태가 조성되어 유지되는 챔버에 20일간 보관한 후에 꺼내어 모발의 염색 상태를 측정하였고, 모발 염색 정도는 모발의 명도값(100: 가장 밝음, 0: 가장 어두움, 즉 명도값이 낮을수록 우수한 염색력을 나타냄)를 측정하는 방법으로 수행하였으며, 그 결과를 하기 표 4에 나타내었다.In the high-humidity air environment dyeability maintenance experiment, white natural hair samples (each 10g) were completely immersed in the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11 for 15 minutes, and the 15 minutes of immersion was completed. After washing with flowing tap water three times, drying with natural wind for 1 hour, and storing in a chamber where a high-humidity atmospheric condition is maintained at 70% for 20 days, it was taken out and the dyeing state of the hair was measured. , The degree of hair dyeing was performed by measuring the lightness value of the hair (100: the brightest, 0: the darkest, that is, the lower the lightness value, the better the dyeing power), and the results are shown in Table 4 below.
(100: 가장 밝음, 0: 가장 어두움)brightness value
(100: brightest, 0: darkest)
상기 표 4의 결과를 표 1의 결과와 비교하여 살펴보면, 실시예 4 내지 6의 경우 모발의 염색 정도가 전혀 변하지 않았음을 확인할 수 있다.Comparing the results of Table 4 with the results of Table 1, it can be seen that the degree of dyeing of the hair in Examples 4 to 6 did not change at all.
[실험 5][Experiment 5]
상기 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물을 이용하여 잦은 샴푸 사용 후에 모발 염색력이 어느 정도 유지되는지 확인하는 실험을 수행하였다.Using the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11, an experiment was performed to determine how much hair dyeability was maintained after frequent shampoo use.
잦은 샴푸 사용 후의 염색력 유지 실험은 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물에 흰색 자연모 샘플(각각 10g)을 15분간 완전히 침지시키고, 15분간의 침지가 종료된 후 흐르는 수돗물에 3회 세척하고 1시간 동안 자연 바람으로 건조시킨 후 매번 동일한 양의 샴푸를 이용하여 1분간 물 및 샴푸를 이용하여 거품을 내고 세척한 후 자연 건조시키는 과정을 24시간 간격으로 20회 반복하는 방법으로 수행하였고, 그 후 모발의 염색 상태를 측정하였고, 모발 염색 정도는 모발의 명도값(100: 가장 밝음, 0: 가장 어두움, 즉 명도값이 낮을수록 우수한 염색력을 나타냄)를 측정하는 방법으로 수행하였으며, 그 결과를 하기 표 5에 나타내었다.In the test for maintaining dyeability after frequent shampoo use, white natural hair samples (each 10g) were completely immersed in the hair dyeing composition prepared in Examples 1 to 6 and Comparative Examples 1 to 11 for 15 minutes, and the 15-minute immersion was completed. After washing with flowing tap water three times, drying with natural wind for 1 hour, using the same amount of shampoo for 1 minute each time, lathering with water and shampoo for 1 minute, washing, and drying naturally after 20 It was performed by repeating the method twice, and then the dyeing state of the hair was measured, and the degree of hair dyeing was determined by the lightness value of the hair (100: the brightest, 0: the darkest, that is, the lower the lightness value, the better the dyeing power). It was performed as a measuring method, and the results are shown in Table 5 below.
(100: 가장 밝음, 0: 가장 어두움)brightness value
(100: brightest, 0: darkest)
상기 표 5의 결과를 표 1의 결과와 비교하여 살펴보면, 실시예 4 내지 6의 경우 모발의 염색 정도가 전혀 변하지 않았음을 확인할 수 있다.Comparing the results of Table 5 with the results of Table 1, it can be seen that the degree of dyeing of the hair in Examples 4 to 6 did not change at all.
[실험 6][Experiment 6]
상기 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물을 이용하여 잦은 샴푸 사용 후에 모발이 손상되는지 여부를 확인하는 실험을 수행하였다.Using the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11, an experiment was performed to determine whether or not hair was damaged after frequent shampoo use.
모발 손상여부 확인 실험은 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물에 흰색 자연모 샘플(각각 10g)을 15분간 완전히 침지시키고, 15분간의 침지가 종료된 후 흐르는 수돗물에 3회 세척하고 1시간 동안 자연 바람으로 건조시킨 후 매번 동일한 양의 샴푸를 이용하여 1분간 물 및 샴푸를 이용하여 거품을 내고 세척한 후 자연 건조시키는 과정을 24시간 간격으로 20회 반복하는 방법으로 수행하였고, 그 후 모발 표면을 현미경으로 관찰하여 손상 상태를 확인하였고, 그 결과를 하기 표 6에 나타내었다.In the hair damage test, white natural hair samples (each 10 g) were completely immersed in the hair dyeing compositions prepared in Examples 1 to 6 and Comparative Examples 1 to 11 for 15 minutes, and after the 15 minutes of immersion, flowing After washing with tap water 3 times, drying with natural wind for 1 hour, using the same amount of shampoo for 1 minute each time, lathering, washing, and drying naturally is repeated 20 times at 24 hour intervals. After that, the hair surface was observed under a microscope to confirm the damage state, and the results are shown in Table 6 below.
최초 샘플의 표면 사진과 비교하여 추가적인 손상이 없는 경우 X로 표시하였고, 추가적인 손상이 발생한 경우 O로 표시하였다.Compared to the surface photograph of the original sample, if there is no additional damage, it is marked as X, and if additional damage occurs, it is marked as O.
상기 표 6의 결과를 살펴보면, 모든 경우 모발의 손상이 전혀 발생하지 않았음을 확인할 수 있다.Looking at the results of Table 6, it can be confirmed that no damage to the hair occurred in all cases.
[실험 7][Experiment 7]
한편, 실험 참가자 160명 (남자 80명, 여자 80명)(16명을 1개 그룹으로 구성하고, 1개 그룹당 각 참가자별로 각각 상기 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물을 이용하도록 함)(10개 그룹 반복 실험)을 대상으로 상기 실시예 1 내지 6 및 비교예 1 내지 11을 통하여 제조된 모발 염색용 조성물을 이용하여 30일간 매일 머리에 염색을 수행하도록 하였으며, 30일이 경과하는 동안 실험 참가자의 두피 상태를 확인하였고, 160명 중 어느 누구도 두피에 피부 발적, 가려움, 염증 등과 같은 부작용이 전혀 발생하지 않았다.On the other hand, 160 test participants (80 males, 80 females) (16 people were composed of 1 group, and each participant per group had hair manufactured through Examples 1 to 6 and Comparative Examples 1 to 11, respectively. To dye the hair every day for 30 days using the hair dyeing composition prepared through Examples 1 to 6 and Comparative Examples 1 to 11 for subjects (10 groups repeated experiments) During the 30 days, the scalp condition of the experiment participants was checked, and none of the 160 participants had any side effects such as redness, itching, or inflammation on the scalp.
Claims (7)
Hair dye containing purified water, hydroxytyrosol, green tea extract, black bean extract, garlic extract, Rehmannia root extract, cacao seed extract, citric acid powder, sodium citrate powder, potassium hydroxide powder, and black raspberry fruit extract composition for.
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