KR102312069B1 - Natural cosmetic containing esters oil - Google Patents
Natural cosmetic containing esters oil Download PDFInfo
- Publication number
- KR102312069B1 KR102312069B1 KR1020190179097A KR20190179097A KR102312069B1 KR 102312069 B1 KR102312069 B1 KR 102312069B1 KR 1020190179097 A KR1020190179097 A KR 1020190179097A KR 20190179097 A KR20190179097 A KR 20190179097A KR 102312069 B1 KR102312069 B1 KR 102312069B1
- Authority
- KR
- South Korea
- Prior art keywords
- weight
- oil
- cosmetic composition
- composition containing
- present
- Prior art date
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
- C12N11/00—Carrier-bound or immobilised enzymes; Carrier-bound or immobilised microbial cells; Preparation thereof
- C12N11/02—Enzymes or microbial cells immobilised on or in an organic carrier
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
- C12N9/00—Enzymes; Proenzymes; Compositions thereof; Processes for preparing, activating, inhibiting, separating or purifying enzymes
- C12N9/14—Hydrolases (3)
- C12N9/16—Hydrolases (3) acting on ester bonds (3.1)
- C12N9/18—Carboxylic ester hydrolases (3.1.1)
- C12N9/20—Triglyceride splitting, e.g. by means of lipase
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
Abstract
본 발명은 식물성 에스테르 오일이 함유된 천연화장품 조성물에 관한 것으로, 보다 상세하게는 식물성 오일를 에스테르화시켜 오일 베이스를 제조하고, 그 오일 베이스를 이용하여 무독성이면서도 피부주름개선 효과, 피부톤 개선 효과, 피부멜리닌 개선 효과를 갖는 천연 화장품을 제조할 수 있는 식물성 에스테르 오일이 함유된 천연화장품 조성물에 관한 것이다.
본 발명에 따른 바이오 촉매를 이용한 식물성 에스테르 오일 제조 방법은, 식물성 오일과 에탄올을 혼합하여 에스테르화 반응시켜 에스테르 화합물을 얻되, 리파제 효소(Lipase enzyme)가 촉매로 이용되는 것을 특징으로 한다. 또한, 본 발명에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물은 상기와 같이 바이오 촉매를 이용하여 제조된 에스테르 화합물이 베이스 오일로 함유된 것을 특징으로 한다.The present invention relates to a natural cosmetic composition containing vegetable ester oil, and more particularly, by esterifying vegetable oil to prepare an oil base, and using the oil base to improve skin wrinkles, improve skin tone, and improve skin tone while being non-toxic It relates to a natural cosmetic composition containing vegetable ester oil capable of producing natural cosmetics having a nin improvement effect.
The method for producing vegetable ester oil using a biocatalyst according to the present invention is characterized in that a vegetable oil and ethanol are mixed to obtain an ester compound by an esterification reaction, and a lipase enzyme is used as a catalyst. In addition, the natural cosmetic composition containing vegetable ester oil according to the present invention is characterized in that the ester compound prepared using the biocatalyst as described above is contained as a base oil.
Description
본 발명은 식물성 에스테르 오일이 함유된 천연화장품 조성물에 관한 것으로, 보다 상세하게는 식물성 오일를 에스테르화시켜 오일 베이스를 제조하고, 그 오일 베이스를 이용하여 무독성이면서도 피부주름개선 효과, 피부톤 개선 효과, 피부멜리닌 개선 효과를 갖는 천연 화장품을 제조할 수 있는 식물성 에스테르 오일이 함유된 천연화장품 조성물에 관한 것이다.The present invention relates to a natural cosmetic composition containing vegetable ester oil, and more particularly, by esterifying vegetable oil to prepare an oil base, and using the oil base to improve skin wrinkles, improve skin tone, and improve skin tone while being non-toxic It relates to a natural cosmetic composition containing vegetable ester oil capable of producing natural cosmetics having a nin improvement effect.
화장품 산업에서의 자연주의 트렌드는 수년 전부터 친환경적인 식물유래 제품 개발로 나타나고 있다. 따라서, 대한민국 등록특허 제10-1595921호(2016.02.15, 천연화장품 조성물의 제조방법)나 대한민국 공개특허 제10-2018-0066348호(2018.06.19, 식물유래 피부미용 기능성 소재를 이용한 천연화장품)에서와 같이 다양한 소재와 방법으로 천연 화장품이 개발되고 있다. 천연 원료로 만들어진 화장품은 효능과 안정성 면에서 기존 제품보다 뛰어난 장점을 지니고 있기 때문에 피부 주름 개선, 미백 등 각종 기능성 화장품 개발에 활발히 이용되고 있다.The naturalism trend in the cosmetic industry has been showing up for several years in the development of eco-friendly plant-derived products. Therefore, in Korean Patent Registration No. 10-1595921 (2016.02.15, method of manufacturing a natural cosmetic composition) or Korean Patent Publication No. 10-2018-0066348 (2018.06.19, natural cosmetics using plant-derived functional materials for skin care) Natural cosmetics are being developed with various materials and methods. Cosmetics made from natural ingredients have superior advantages over existing products in terms of efficacy and stability, so they are actively used in the development of various functional cosmetics such as skin wrinkle improvement and whitening.
그러나, 현재 사용되고 있는 천연 화장품은 천연 소재를 혼합하고 있으나 대부분 알코올이나 정제수 및 글리세린 등의 화학성분도 포함하고 있어 민감한 피부 및 외상 피부질환을 가진 사람이 사용할 경우에는 오히려 피부에 염증이 발생하고 트러블에 의한 부작용으로 오히려 피부가 손상되는 경우가 발생하고 있다.However, natural cosmetics currently used contain natural ingredients, but most of them also contain chemical components such as alcohol, purified water, and glycerin. As a side effect, the skin is damaged.
본 발명은 상기와 같은 점을 인식하여 안출된 것으로 본 발명의 목적은 식물성 오일를 에스테르화시켜 오일 베이스를 제조하고, 그 오일 베이스를 이용하여 무독성이면서도 피부주름개선 효과, 피부톤 개선 효과, 피부멜리닌 개선 효과를 갖는 천연 화장품을 제조할 수 있는 식물성 에스테르 오일이 함유된 천연화장품 조성물을 제공하기 위한 것이다.The present invention has been devised in recognition of the above points, and an object of the present invention is to prepare an oil base by esterifying vegetable oil, and use the oil base to improve skin wrinkles, skin tone, and skin melinin while being non-toxic. An object of the present invention is to provide a natural cosmetic composition containing vegetable ester oil that can produce natural cosmetics having an effect.
상기와 같은 목적을 달성하기 위하여 본 발명에 따른 바이오 촉매를 이용한 식물성 에스테르 오일 제조 방법은, 식물성 오일과 에탄올을 혼합하여 에스테르화 반응시켜 에스테르 화합물을 얻되, 리파제 효소(Lipase enzyme)가 촉매로 이용되는 것을 특징으로 한다.In order to achieve the above object, the method for producing vegetable ester oil using a biocatalyst according to the present invention is a method for producing an ester compound by mixing vegetable oil and ethanol to obtain an ester compound, a lipase enzyme is used as a catalyst. characterized in that
또한, 본 발명에 따른 바이오 촉매를 이용한 식물성 에스테르 오일 제조 방법은, 상기 식물성 오일은 동백나무씨 오일이나 올리브 오일인 것을 특징으로 한다.In addition, the method for producing a vegetable ester oil using a biocatalyst according to the present invention is characterized in that the vegetable oil is camellia seed oil or olive oil.
또한, 본 발명에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물은 상기와 같이 바이오 촉매를 이용하여 제조된 에스테르 화합물이 베이스 오일로 함유된 것을 특징으로 한다.In addition, the natural cosmetic composition containing vegetable ester oil according to the present invention is characterized in that the ester compound prepared using the biocatalyst as described above is contained as a base oil.
상기와 같은 구성에 의하여 본 발명에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물에 관한 것으로, 보다 상세하게는 식물성 오일를 에스테르화시켜 오일 베이스를 제조하고, 그 오일 베이스를 이용하여 무독성이면서도 피부주름개선 효과, 피부톤 개선 효과, 피부멜리닌 개선 효과를 갖는 천연 화장품을 제조할 수 있는 장점을 갖는다.It relates to a natural cosmetic composition containing vegetable ester oil according to the present invention by the above configuration, and more specifically, an oil base is prepared by esterifying vegetable oil, and the oil base is used to improve skin wrinkles while being non-toxic. , has the advantage of being able to manufacture natural cosmetics having an effect of improving skin tone and improving skin melinin.
도 1은 본 발명의 일실시예에 따른 바이오 촉매를 이용한 식물성 에스테르 오일 제조 과정을 도시한 흐름도
도 2는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선 효과를 도시한 그래프
도 3은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선율을 도시한 그래프
도 4는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선 효과에 대한 임상 사진
도 5는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선 효과를 도시한 그래프
도 6은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선율을 도시한 그래프
도 7은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선 효과에 대한 임상 사진
도 8은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 측정 결과를 도시한 그래프
도 9는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 개선율을 도시한 그래프
도 10은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 개선 효과에 대한 임상 사진1 is a flowchart illustrating a process for producing vegetable ester oil using a biocatalyst according to an embodiment of the present invention;
Figure 2 is a graph showing the skin wrinkle improvement effect of the natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
Figure 3 is a graph showing the improvement rate of skin wrinkles of the natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
4 is a clinical photograph of the skin wrinkle improvement effect of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
5 is a graph showing the skin tone improvement effect of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
6 is a graph showing the skin tone improvement rate of the natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
7 is a clinical photograph of the skin tone improvement effect of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
8 is a graph showing the measurement result of skin melanin of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
9 is a graph showing the skin melanin improvement rate of the natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
10 is a clinical picture of the skin melanin improvement effect of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention;
이하에서는 도면 및 실시예를 참조하여 본 발명에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물을 보다 상세하게 설명하기로 한다.Hereinafter, a natural cosmetic composition containing vegetable ester oil according to the present invention will be described in more detail with reference to the drawings and examples.
본 발명의 이해를 돕기 위하여 실시예등을 들어 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 용이하게 실시할 수 있도록 상세히 설명한다. 그러나, 본 발명은 여러 가지 상이한 형태로 변형될 수 있으며, 본 발명의 범위가 하기 실시예들에 한정되는 것은 아니다.In order to help the understanding of the present invention, examples, etc., will be described in detail so that those of ordinary skill in the art can easily carry out the present invention. However, the present invention may be modified in many different forms, and the scope of the present invention is not limited to the following examples.
도 1은 본 발명의 일실시예에 따른 바이오 촉매를 이용한 식물성 에스테르 오일 제조 과정을 도시한 흐름도이고, 도 2는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선 효과를 도시한 그래프이며, 도 3은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선율을 도시한 그래프이고, 도 4는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선 효과에 대한 임상 사진이며, 도 5는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선 효과를 도시한 그래프이고, 도 6은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선율을 도시한 그래프이며, 도 7은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선 효과에 대한 임상 사진이고, 도 8은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 측정 결과를 도시한 그래프이며, 도 9는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 개선율을 도시한 그래프이고, 도 10은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 개선 효과에 대한 임상 사진이다.1 is a flowchart illustrating a process for manufacturing vegetable ester oil using a biocatalyst according to an embodiment of the present invention, and FIG. 2 is a skin wrinkle improvement of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention. It is a graph showing the effect, and FIG. 3 is a graph showing the skin wrinkle improvement rate of the natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention, and FIG. 4 is a vegetable ester according to an embodiment of the present invention. It is a clinical picture of the skin wrinkle improvement effect of a natural cosmetic composition containing oil, and FIG. 5 is a graph showing the skin tone improvement effect of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention, FIG. is a graph showing the skin tone improvement rate of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention, and FIG. 7 is a skin tone improvement of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention. It is a clinical picture of the effect, and FIG. 8 is a graph showing the skin melanin measurement result of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention, and FIG. 9 is a vegetable according to an embodiment of the present invention. It is a graph showing the skin melanin improvement rate of the natural cosmetic composition containing the ester oil, and FIG. 10 is a clinical photograph of the skin melanin improvement effect of the natural cosmetic composition containing the vegetable ester oil according to an embodiment of the present invention.
도 1을 참조하면, 본 발명의 일실시예에 따른 바이오 촉매를 이용한 식물성 에스테르 오일의 제조 방법은 동백나무씨 오일이나 올리브 오일과 같은 식물성 오일과 에탄올을 혼합하여 에스테르화 반응시킨다. 특히 본 발명은 리파제 효소(Lipase enzyme)를 촉매로 이용함으로써 에스테르화 반응이 이루어진다. 에스테르화 반응은 50℃의 온도에서 2hr 정도 이루어지며, 이 화합물을 여과하여 촉매를 분리함으로써 에스테르 화합물을 얻는다.Referring to FIG. 1 , in the method for producing a vegetable ester oil using a biocatalyst according to an embodiment of the present invention, a vegetable oil such as camellia seed oil or olive oil and ethanol are mixed and subjected to an esterification reaction. In particular, in the present invention, the esterification reaction is performed by using a lipase enzyme as a catalyst. The esterification reaction is carried out at a temperature of 50° C. for about 2 hours, and the ester compound is obtained by filtering the compound to separate the catalyst.
상기와 같이 얻어진 에스테르 화합물은 항노화 천연화장품 조성물의 베이스 오일로 이용된다.The ester compound obtained as described above is used as a base oil for an anti-aging natural cosmetic composition.
<실시예 1 : 화장품 조성물 제조><Example 1: Preparation of cosmetic composition>
에스테르화 식물성 베이스 오일과 아래의 보조 성분을 혼합하여 화장품 조성물을 제조하였다. 보조 성분은 조성은 아래와 같다.A cosmetic composition was prepared by mixing the esterified vegetable base oil and the following auxiliary ingredients. The auxiliary ingredients are as follows.
매실추출물(30중량%), 동백나무씨오일에틸에스터즈(4중량%), 녹차씨오일(3중량%), 올리브오일에틸에스터즈(2중량%), 세라마이드엔피(1.8중량%), 옥틸도데칸올(0.2중량%), 카보머(8중량%), 세테아릴올리베이트(1.5중량%), 솔비탄올리베이트(1중량%), 스위트브라이어씨오일(1중량%), 호호바씨오일(1중량%), 아데노신(0.04중량%), 나이아신아마이드(1중량%), 메도우폼씨오일(1중량%), 달맞이꽃오일(1중량%), 시어버터(1중량%), 호호바버터(0.5중량%), 하이드로제네이티드복숭아커넬오일(0.5중량%), 소듐하이알루로네이트(0.3중량%), 소듐아세틸레이티드하이알루로네이트(0.3중량%), 하이드롤라이즈드하이알루로닉애씨드(0.3중량%), 글리세린(1.5중량%), 다이글리세린(1.5중량%), 베타인(1중량%), 캐비아추출물(1중량%), 달팽이점액여과물(1중량%), 토코페롤(1중량%), 판테놀(1중량%), 알로에베라잎즙(3중량%), 부틸렌글라이콜(1중량%), 칸데릴라왁스(0.3중량%), 합성비즈왁스(0.3중량%), 스테아릭애씨드(0.3중량%), 세테아릴알코올(1중량%), 정제수(26.66중량%)Plum extract (30% by weight), camellia seed oil ethyl esters (4% by weight), green tea seed oil (3% by weight), olive oil ethyl esters (2% by weight), ceramide NP (1.8% by weight), octyl dodecanol (0.2% by weight), carbomer (8% by weight), cetearylolivate (1.5% by weight), sorbitan olivate (1% by weight), sweet briar seed oil (1% by weight), jojoba seed Oil (1% by weight), adenosine (0.04% by weight), niacinamide (1% by weight), meadowfoam seed oil (1% by weight), evening primrose oil (1% by weight), shea butter (1% by weight), jojoba butter (0.5% by weight), hydrogenated peach kernel oil (0.5% by weight), sodium hyaluronate (0.3% by weight), sodium acetylated hyaluronate (0.3% by weight), hydrolyzed hyaluronate Nick acid (0.3% by weight), glycerin (1.5% by weight), diglycerin (1.5% by weight), betaine (1% by weight), caviar extract (1% by weight), snail mucus filtrate (1% by weight), tocopherol (1% by weight), panthenol (1% by weight), aloe vera leaf juice (3% by weight), butylene glycol (1% by weight), candelilla wax (0.3% by weight), synthetic beeswax (0.3% by weight), Stearic acid (0.3% by weight), cetearyl alcohol (1% by weight), purified water (26.66% by weight)
<실시예 2 : 항노화 천연 화장품의 피부주름 개선 효과> <Example 2: Skin wrinkle improvement effect of natural anti-aging cosmetics>
상기와 같이 실시예 1에서 제조된 항노화 천연 화장품의 효능 검증을 위하여 20명의 피험자(만 31-54세 여성)를 선발하여 사용전, 2주 및 4주 후 Antera에 의한 피부주름 평가, 시험 대상자에 의한 주관적 설문평가, 피부과 전문의 및 시험담당자와 시험대상자에 의한 이상 반응 평가를 실시하였다. 도 2는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선 효과를 도시한 그래프이며, 도 3은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선율을 도시한 그래프이고, 도 4는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부주름 개선 효과에 대한 임상 사진이다. 또한, 표 1은 피부주름 개선 설문 평가를 정리한 것이다. 도 2 내지 도 4 및 표 1에 따르면, 본 발명에 따른 항노화 천연 화장품을 사용한 대상자는 13.12중량% 피부주름 개선율을 보였다.To verify the efficacy of the anti-aging natural cosmetics prepared in Example 1 as described above, 20 subjects (aged 31-54 years old) were selected and skin wrinkle evaluation by Antera before, 2 weeks and 4 weeks after use, test subjects Subjective questionnaire evaluation by the dermatologist, and adverse reaction evaluation by dermatologists and test subjects and test subjects were conducted. 2 is a graph showing the skin wrinkle improvement effect of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention, and FIG. 3 is a natural cosmetic containing vegetable ester oil according to an embodiment of the present invention. It is a graph showing the skin wrinkle improvement rate of the composition, and FIG. 4 is a clinical picture of the skin wrinkle improvement effect of the natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention. In addition, Table 1 summarizes the skin wrinkle improvement questionnaire evaluation. According to FIGS. 2 to 4 and Table 1, the subjects using the anti-aging natural cosmetics according to the present invention showed a 13.12% by weight skin wrinkle improvement rate.
<실시예 3 : 항노화 천연 화장품의 피부톤 개선 효과> <Example 3: Anti-aging natural cosmetics Skin tone improvement effect>
20명의 피험자(평균 41.7세 여성)를 대상으로 피부톤 개선효과를 검정한 결과 4주 후 피부톤 결과값이 통계적으로 유의하게 감소하였다. 또한 사용자에 대한 주관적 설문 평가를 실시한 결과 대부분 항목에서 좋음 이상으로 평가하였다. As a result of testing the skin tone improvement effect on 20 subjects (average 41.7 years old female), the skin tone result value decreased statistically significantly after 4 weeks. In addition, as a result of subjective survey evaluation of users, most items were rated as good or higher.
도 5는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선 효과를 도시한 그래프이고, 도 6은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선율을 도시한 그래프이며, 도 7은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부톤 개선 효과에 대한 임상 사진이다. 또한, 표 2는 피부톤 개선 효과 설문조사를 정리한 표이다.5 is a graph showing the skin tone improvement effect of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention, and FIG. 6 is a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention. is a graph showing the skin tone improvement rate of , and FIG. 7 is a clinical photograph of the skin tone improvement effect of the natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention. In addition, Table 2 is a table summarizing the skin tone improvement effect questionnaire.
<실시예 4 : 항노화 천연 화장품의 피부멜라닌 개선 효과> <Example 4: Anti-aging natural cosmetics Skin melanin improvement effect>
20명의 피험자(31-54세 여성)를 대상으로 피부멜라닌 개선효과를 검정하였다. 피부멜라닌을 확인한 결과, Average level 결과 값은 사용 2주 후 및 4주 후에 각각1.93중량% 및 2.64중량%의 개선율을 보였으며, 통계적으로 유의미하게 감소하였다. 피험자를 대상으로 제품 사용 후 유효성에 대한 설문 평가를 실시하였는데 대부분 항목에서 좋음 이상으로 평가하였다. 도 8은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 측정 결과를 도시한 그래프이고, 도 9는 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 개선율을 도시한 그래프이며, 도 10은 본 발명의 일실시예에 따른 식물성 에스테르 오일이 함유된 천연화장품 조성물의 피부 멜라닌 개선 효과에 대한 임상 사진또한, 표 3은 피부멜라닌 개선 효과 설문 조사 결과를 정리한 표이다.The skin melanin improvement effect was tested on 20 subjects (31-54 years old female). As a result of confirming skin melanin, the average level result showed improvement rates of 1.93% by weight and 2.64% by weight, respectively, after 2 weeks and 4 weeks of use, and decreased statistically significantly. After using the product, a questionnaire evaluation was conducted on the subjects, and most of the items were rated as good or higher. 8 is a graph showing the measurement results of skin melanin of a natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention, and FIG. 9 is a natural cosmetic containing vegetable ester oil according to an embodiment of the present invention. It is a graph showing the skin melanin improvement rate of the composition, and FIG. 10 is a clinical picture of the skin melanin improvement effect of the natural cosmetic composition containing vegetable ester oil according to an embodiment of the present invention. Also, Table 3 is a skin melanin improvement effect questionnaire This is a table summarizing the survey results.
Claims (3)
매실추출물(30중량%), 동백나무씨오일에틸에스터즈(4중량%), 녹차씨오일(3중량%), 올리브오일에틸에스터즈(2중량%), 세라마이드엔피(1.8중량%), 옥틸도데칸올(0.2중량%), 카보머(8중량%), 세테아릴올리베이트(1.5중량%), 솔비탄올리베이트(1중량%), 스위트브라이어씨오일(1중량%), 호호바씨오일(1중량%), 아데노신(0.04중량%), 나이아신아마이드(1중량%), 메도우폼씨오일(1중량%), 달맞이꽃오일(1중량%), 시어버터(1중량%), 호호바버터(0.5중량%), 하이드로제네이티드복숭아커넬오일(0.5중량%), 소듐하이알루로네이트(0.3중량%), 소듐아세틸레이티드하이알루로네이트(0.3중량%), 하이드롤라이즈드하이알루로닉애씨드(0.3중량%), 글리세린(1.5중량%), 다이글리세린(1.5중량%), 베타인(1중량%), 캐비아추출물(1중량%), 달팽이점액여과물(1중량%), 토코페롤(1중량%), 판테놀(1중량%), 알로에베라잎즙(3중량%), 부틸렌글라이콜(1중량%), 칸데릴라왁스(0.3중량%), 합성비즈왁스(0.3중량%), 스테아릭애씨드(0.3중량%), 세테아릴알코올(1중량%), 정제수(26.66중량%)이 배합되어 제조된 것을 특징으로 하는 특징으로 하는 식물성 에스테르 오일이 함유된 천연화장품 조성물.In a natural cosmetic composition containing a vegetable ester oil obtained by mixing each of camellia seed oil and olive oil in ethanol and esterification reaction using a lipase enzyme as a catalyst,
Plum extract (30% by weight), camellia seed oil ethyl esters (4% by weight), green tea seed oil (3% by weight), olive oil ethyl esters (2% by weight), ceramide NP (1.8% by weight), octyl dodecanol (0.2% by weight), carbomer (8% by weight), cetearylolivate (1.5% by weight), sorbitan olivate (1% by weight), sweet briar seed oil (1% by weight), jojoba seed Oil (1% by weight), adenosine (0.04% by weight), niacinamide (1% by weight), meadowfoam seed oil (1% by weight), evening primrose oil (1% by weight), shea butter (1% by weight), jojoba butter (0.5% by weight), hydrogenated peach kernel oil (0.5% by weight), sodium hyaluronate (0.3% by weight), sodium acetylated hyaluronate (0.3% by weight), hydrolyzed hyaluronate Nick acid (0.3% by weight), glycerin (1.5% by weight), diglycerin (1.5% by weight), betaine (1% by weight), caviar extract (1% by weight), snail mucus filtrate (1% by weight), tocopherol (1% by weight), panthenol (1% by weight), aloe vera leaf juice (3% by weight), butylene glycol (1% by weight), candelilla wax (0.3% by weight), synthetic beeswax (0.3% by weight), A natural cosmetic composition containing vegetable ester oil, characterized in that it is prepared by mixing stearic acid (0.3% by weight), cetearyl alcohol (1% by weight), and purified water (26.66% by weight).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020190179097A KR102312069B1 (en) | 2019-12-31 | 2019-12-31 | Natural cosmetic containing esters oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020190179097A KR102312069B1 (en) | 2019-12-31 | 2019-12-31 | Natural cosmetic containing esters oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20210085723A KR20210085723A (en) | 2021-07-08 |
| KR102312069B1 true KR102312069B1 (en) | 2021-10-13 |
Family
ID=76893852
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020190179097A KR102312069B1 (en) | 2019-12-31 | 2019-12-31 | Natural cosmetic containing esters oil |
Country Status (1)
| Country | Link |
|---|---|
| KR (1) | KR102312069B1 (en) |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB0725266D0 (en) * | 2007-12-28 | 2008-02-06 | Innospec Ltd | Novel esters and compositions and uses thereof |
| US8796217B2 (en) * | 2008-01-25 | 2014-08-05 | HallStar Italia S.r.l. | Use of transesterified olive oil in the cosmetic field |
| ES2462548T3 (en) * | 2010-03-01 | 2014-05-23 | Trans Bio-Diesel Ltd. | A process for the enzymatic synthesis of fatty acid alkyl esters |
| KR101595921B1 (en) | 2014-01-17 | 2016-02-19 | 박노면 | Method for manufacturing natural cosmetic |
| KR20160130421A (en) * | 2014-03-04 | 2016-11-11 | 바스프 에스이 | Method for degumming and esterification of an oil |
| EP3517619B1 (en) * | 2016-09-23 | 2022-07-27 | CJ Cheiljedang Corporation | Method for preparing fatty acid ethyl ester |
| KR20180066348A (en) | 2016-12-08 | 2018-06-19 | 경일대학교산학협력단 | Plant-derived natural cosmetics |
-
2019
- 2019-12-31 KR KR1020190179097A patent/KR102312069B1/en active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| KR20210085723A (en) | 2021-07-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| AU2008334527B2 (en) | Use of a novel natural agent in cosmetic compositions | |
| CN105997735B (en) | A kind of natural hair-washing hair-care articles and its preparation method and application | |
| KR102625288B1 (en) | Anti-aging, antioxidant cosmetic composition comprising broccoli exosome as an active ingredient, and functional cosmetic comprising the same | |
| KR102312069B1 (en) | Natural cosmetic containing esters oil | |
| CA3007694A1 (en) | Personal care formulations comprising carmin protein | |
| KR102040688B1 (en) | Cosmetic composition containing extract of Sea Buckthorn Fruit | |
| EP3787752B1 (en) | Haircare composition comprising modified vegetable waxes | |
| KR100955572B1 (en) | Cosmetic composition comprising a supercritical fluid extract of Morinda citrifolia | |
| FR2928549A1 (en) | USE OF AN EXTRACT OF BRASSOCATTLEYA MARCELLA KOSS ORCHIDEE AS AN AGENT TO PREVENT OR DELAY THE APPEARANCE OF SIGNS OF SKIN AGING | |
| KR20160036123A (en) | Cosmetic composition containing extracts consisting of Tremella fuciformis Berk., Caulerpa lentillifera J. Agardh, Trichosanthes kirilowii Maxim, Camellia Sinensis, Nelumbo nucifera Gaertn., Helichrysum angustifolium DC., and colloidal gold | |
| KR20150105721A (en) | Skin-antiaging cosmetical composition containing mixed extract of lycium chinense mill as an active ingredient | |
| KR20160024675A (en) | Cosmetic composition for skin-moisturization comprising the extract of hydrangea macrophylla var. thunbergii and manufacture of the same | |
| EP4221678A1 (en) | Novel use of a peptide to improve the comfort of skin and/or mucous membranes and/or the appearance of dander | |
| KR102398406B1 (en) | Novel deep sea water equisetum hyemale extract and the preparation method of the same | |
| KR102092728B1 (en) | Two part cosmetic composition, Cosmetics containing the same and manufacturing method thereof | |
| KR102131361B1 (en) | Cosmetic composition for hair and scalp comprising keratin peptides as active ingredients | |
| KR20180027772A (en) | Cosmetic composition for preventing near infrared ray containing extract of ganoderma lucidum | |
| CN112618405A (en) | Oligopeptide-containing composition and application thereof in eye mask | |
| CN110585091A (en) | Preparation method of skin care product raw material containing desert rose leaf cell extract | |
| KR20160055118A (en) | Cosmetic composition comprising of the mixed herb fermentes and preparation method of the same | |
| KR20160036124A (en) | Cosmetic composition containing extracts consisting of Dioscorea japonica Thunb., Aloe vera (L.) Burm. f., Daucus carota subsp. sativa (Hoffm.) Arcang., Pinus densiflora Siebold and Zucc. and Eulota Peliomphala Pfr. with nano emulsion process | |
| KR20160036122A (en) | Cosmetic composition containing extracts consisting of Achillea milleforium L., Swiftlet Nest extract, Hypericum perforatum, Euterpe oleraceal, Aspalathus linearis, Rosa canina, gold | |
| JP4748962B2 (en) | Moisturizer, cell activator, whitening agent, and antioxidant | |
| KR101499168B1 (en) | Composition for improving Hair Damage containing Propolis extract and Method Of Composition for improving Hair Damage | |
| JP3923438B2 (en) | Cosmetics and cleaning materials |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| E701 | Decision to grant or registration of patent right | ||
| GRNT | Written decision to grant |