KR101991226B1 - Manufacturing method of eco fomentation device containing red clay - Google Patents

Abstract

According to the present invention, a method of manufacturing an eco-friendly loess fomentation device containing a loess base comprises: a loess base manufacturing step of manufacturing a loess base including loess, charcoal powder, and calcium phosphate; a main body preparation step of preparing a main body having an internal space into which the loess base is injected; and an injection step of completing a loess fomentation device by injecting the loess base into the internal space, wherein the loess base is manufactured by additionally including 60 to 80 wt% of loess, 10 to 20 wt% of charcoal powder, 5 to 15 wt% of calcium phosphate, and 0.1 to 10 wt% of antibacterial agent including tetraethylorthosilicate (TEOS) and a silane-based organic material, with respect to the total weight of the loess base.

Description

TECHNICAL FIELD [0001] The present invention relates to a method for producing an eco-friendly loess fomentation apparatus containing a loess base,

The present invention relates to a method for manufacturing an environmentally friendly loess apparatus comprising a loess base, and more particularly, to a method for manufacturing an environmentally friendly loess apparatus comprising the steps of: applying far infrared rays from a loess base in a loess fomentation equipment, The present invention relates to a method for producing an eco-friendly loess fomentation apparatus containing a loess base.

The padding is classified into a hot padding and a cold padding. The hot padding helps promote blood circulation, and is effective in relieving muscular pain and bruising. It is effective in relieving tension headaches and stressful symptoms. Lt; / RTI >

Regarding the technique for manufacturing the above-described warming apparatus, Korean Patent No. 10-1746919 (entitled "A warming apparatus for preventing electromagnetic waves and easy to use") is brought into contact with a human body conveniently in a lying state, The present invention relates to a warm feminine care appliance having an electromagnetic wave prevention and use convenience.

The present invention has been proposed to provide a warm fomentation apparatus capable of exerting an effect of adding a medicinal material or a magnet when warming the feminine body and of preventing the electromagnetic wave from being easily brought into contact with the human body even in a lying state.

Regarding the technology for manufacturing the portable warm fomentation apparatus, Korean Patent Registration No. 10-1380927 (entitled "portable warm fomentation apparatus") minimizes the generation of harmful electromagnetic waves to the human body, radiates far-infrared rays, So that the user can easily perform hot fumigation.

The present invention has a simple structure and can freely adjust the heat generation temperature to a desired temperature without any risk of burning, and a heat-resistant pad is wrapped around the heat generation body by using a heat-resistant pad. Thus, there is no risk of fire, The present invention proposes a portable warm fomentation apparatus that has the effect of removing the toxicity and the effect of removing the impurities of the skin by forming the body of the feminine body of the pegmatite.

The two inventions of the present invention have a problem that they commonly have a feature of reducing the electromagnetic waves generated from the feminine warming apparatus and providing convenience to the user, but simply providing warmth.

Accordingly, there is a need to develop a method for manufacturing a feminine care appliance containing a loess base, which not only provides a hot firming effect but also a skin beauty and a blood purification effect by irradiating the far-infrared rays with the ocher base inside the loess fomentation device.

Disclosure of Invention Technical Problem [8] The present invention has been made to overcome the problems of the prior art, and it is an object of the present invention to provide not only hot fomenting effect but also skin beauty and cosmetic effect due to irradiation of far-infrared rays.

Another object of the present invention is to manufacture a clayey base by additionally containing apatite hydroxide.

A further object of the present invention is to further prepare a clayey base by further comprising a preservative containing an effective amount of sea weed.

In order to accomplish the above object, the present invention provides a method for manufacturing an eco-friendly loess fomentation apparatus comprising a loess base, comprising the steps of: preparing a loess base comprising an ocher, a charcoal powder and calcium phosphate as active ingredients; A body preparing step of preparing a body provided with an inner space into which the loess base is injected; And injecting the loess base into the inner space to complete the loess fomentation equipment.

Further, the loess base is characterized in that it is produced by additionally including a preservative containing an effective amount of sea anionite.

In addition, the above-mentioned preservative may be a primary solution preparation step in which a primary solution is prepared by mixing 50 to 70% by weight of water, 20 to 40% by weight of hemp stone, and 1 to 15% by weight of a foaming agent, based on the weight of the entire primary solution. 50 to 70% by weight of the primary solution, 5 to 20% by weight of aluminum silicate, 5 to 20% by weight of asbestos and 1 to 15% by weight of oxalic acid are mixed at 800 to 1500 rpm, A secondary solution preparation step; Wherein the third solution is prepared by mixing 70 to 90% by weight of the secondary solution, 1 to 15% by weight of the adhesive and 1 to 15% by weight of the thickener, based on the weight of the total tertiary solution, Obtaining; And a preservative preparation step in which the third solution is heat-treated at 50 to 150 ° C for 2 to 15 hours to complete the preservative.

A method of manufacturing an eco-friendly loess fomentation apparatus containing a loess base according to the present invention comprises the steps of:

1) It is possible to manufacture a loess base which not only provides a hot fomenting effect but also provides a beauty and a blood-

2) It is possible to manufacture an ocher base which can effectively prevent the propagation of fungi and bacteria inside the ocher base,

3) Not only is it possible to produce a loess base which can maximize the far-infrared effect of loess,

4) It is possible to manufacture the loess base which is high in heat retention and can be stored without heat and high, and is effective in energy saving.

BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a conceptual diagram showing various embodiments of a fomentation apparatus containing a loess base according to the present invention. FIG.
2 is a conceptual view showing still another embodiment of a fomentation apparatus containing a loess base according to the present invention.
FIG. 3 is a flowchart showing a method for manufacturing an environmentally friendly loess fomentation apparatus containing a loess base according to the present invention.
4 is a flowchart showing a process for producing the adjuvant of the present invention.
5 is a flow chart showing a process for producing the antibacterial agent of the present invention.

Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings. The accompanying drawings are not drawn to scale and wherein like reference numerals in the various drawings refer to like elements.

FIG. 1 and FIG. 2 are conceptual diagrams showing various embodiments of a fomentation apparatus containing a loess base according to the present invention, and FIG. 3 is a flowchart showing a method of manufacturing an environmentally friendly loess fomentation apparatus containing a loess base according to the present invention.

The fomentation can be classified into two types: hot and cold. The hot fomentation helps promote blood circulation, helps to relieve muscle aches and bruises, and is effective in relieving tension headaches and stressful symptoms. The hot fomentation can be carried out through a fomentation apparatus. In the present invention, a loess fomentation apparatus is manufactured by adding a fomentation base as a constitution of a fomentation apparatus, and when the fomentation (when the hot soil is injected with thermal energy) .

Here, as far as the effect of the far-infrared ray irradiation is concerned, it has a skin cosmetic effect by smoothly discharging wastes, and has a preventive effect on women's diseases (menstrual cramps, menstrual irregularities, afterbirth, etc.) as well as a blood-

Referring to FIG. 1, (a) is an embodiment in which a power source unit capable of injecting thermal energy is provided with a loess fomentation device made of plastic, (b) is a neck pillow type, And the inside of the loess fomentation apparatus is filled with the loess base in the form of loess balls.

Referring to FIG. 2, (a) is a packed loess fomentation apparatus in which a power source unit is not provided separately, so that thermal energy is supplied from a microwave oven and can be used as a loess fomentation equipment. (B) (C) has a trough shape, and it does not have a separate power supply unit, so it supplies heat energy from a microwave oven, and it can be used as a loess fomentation device And can be used for cold-warming by putting it in a freezer room if necessary.

The method for producing the loess fomentation apparatus includes the step of preparing the loess base (S100), the body preparation step (S200), and the injection step (S300), thereby producing the loess feminine goods having the above-mentioned effects.

First, the clay base manufacturing step (S100) is a process for manufacturing an alfalfa base containing yellow soil, charcoal powder and calcium phosphate as active ingredients. The loess base is produced by mixing 65 to 80% by weight of loess, 10 to 25% by weight of charcoal powder and 5 to 20% by weight of calcium phosphate based on the total weight of the loess base. At this time, the charcoal powder has a deodorizing effect and an electromagnetic wave shielding effect, and the calcium phosphate has an antibacterial property and effectively absorbs moisture and has an effect of preventing condensation.

Here, the shape of the loess base may be a ball, a gel, a powder, a sponge, and the like. There is no limitation in the shape of the loess base, and the loess base may be manufactured by further adding a solvent according to the shape of the loess base . For example, the loess balls may be manufactured by molding the loess dough into a spherical shape and then subjecting it to a sintering process. The loess sponge may be produced by mixing yellow loess with a yellow sponge in the general sponge manufacturing process.

Next, the main body preparation step S200 is a step of preparing a main body having a space for injecting a yellow clay base (a detailed description thereof will be described later). Here, the main body may be made of a material such as plastic, cloth, sponge, etc., and a power source for providing thermal energy to the loess base included in the main body may be provided. Further, an inlet through which the loess base can be inserted and removed can be provided, so that the loess base can be further injected or withdrawn.

Finally, in the step of completing the loess fomentation apparatus, the above-described loess base is injected into the above-mentioned main body to complete the loess fomentation apparatus.

In the above-described clay base preparation step (S100), it is possible to produce an ocher base by additionally containing apatite hydroxide. Since apatite hydroxide is excellent in mold resistance and antibacterial property, it effectively prevents the propagation of fungi and bacteria inside the ocher base .

The method for producing the loess base includes mixing 60 to 80% by weight of loess, 10 to 20% by weight of charcoal powder, 5 to 15% by weight of calcium phosphate and 5 to 15% by weight of hydroxyapatite based on the whole loess base weight, A loess base added as an active ingredient can be prepared.

The loess fomentation produced by the above method is more effective for human health than the conventional fomentation owing to the far-infrared radiation effect of the loess, and the far-infrared effect of the loess can be maximized by adding the adjuvant to the loess base described above. 2 together with the following.

4 is a flow chart showing a process for producing the adjuvant of the present invention.

Referring to FIG. 4, the adjuvant contains alumina as an active ingredient and maximizes the far-infrared effect of the loess.

Here, alumina is an oxide of aluminum and is the most important material of ceramics together with silica. It is generally used for spark plugs, grinding abrasives, and grinders in automobiles.

The auxiliary agent may be added in an amount of 0.1 to 10% by weight based on the total weight of the loess base. The step of preparing the auxiliary material may include a first material preparation step (S110), a second material preparation step (S111) , And an auxiliary agent completion step (S113).

First, in the first material preparation step (S110), 20 to 40% by weight of alumina (Al ₂ O ₃ ) and 60 to 80% by weight of carbon are mixed with respect to the weight of all the primary materials, While stirring at 800 to 1200 rpm to prepare a primary material.

In this case, alumina and carbon are in the form of fine powder. It is important to consider the particle size of alumina and carbon in the production of the primary material. Specifically, in order to maximize the mechanical properties of the primary material, (Preferably 1.2 mu m), and it is preferable that carbon has a particle size of 20 to 70 nm (preferably 50 nm) for coating the surface of alumina.

Here, in order to maximize the yield of the auxiliary agent to be produced through the steps described later, it is preferable to mix the alumina with less than carbon to prepare the primary material.

Then, the secondary material production step (S111) is a process for producing a secondary material by flowing nitrogen gas into the primary material at 1500 to 1800 DEG C for 30 minutes to 4 hours while maintaining a pressure of 0.12 MPa.

At this time, the secondary material production step (S111) is a process in which a primary material is charged into a graphite crucible and a nitrogen gas is supplied to cause a reduction reaction to generate aluminum nitride. Here, the graphite crucible is made of graphite Which means a crucible, is an environment suitable for producing a secondary material through a reduction reaction after melting a primary material which is a metal material.

In addition, carbon monoxide gas is generated in the process of producing the secondary material to lower the partial pressure of the nitrogen gas flowing into the graphite crucible. The carbon monoxide gas is discharged through a gas discharging unit provided separately in the graphite crucible to control the partial pressure of nitrogen Secondary materials can be prepared under optimal conditions.

Next, the third material preparation step (S112) comprises mixing 10 to 40% by weight of the secondary material, 1 to 10% by weight of yttrium oxide, and 50 to 80% by weight of ethanol with respect to the weight of all the tertiary materials, .

At this time, yttrium oxide is used as a sintering agent, and it plays a role of preventing deterioration of the far-infrared radiation rate of the adjuvant to be produced through the step described later by oxygen and other impurities remaining in the tertiary material. Specifically, a secondary material containing aluminum nitride, yttrium oxide and ethanol (wherein ethanol is used as a solvent to prevent hydration reaction of aluminum nitride contained in the secondary material with water due to wet mixing). ) Is mixed to produce a tertiary material which is a liquid mixture. In this process, oxygen and impurities in the tertiary material can suppress the molecular motion in the crystal grains and improve the far-infrared radiation rate of the loess. At this time, oxygen is a factor having a great influence on the emissivity of aluminum nitride, and is influenced by the far infrared emissivity of the yellow loess due to the presence of oxygen.

Finally, the auxiliary agent finishing step (S113) is a step of drying the auxiliary material at 70 to 95 ° C for 12 to 30 hours while stirring to prevent the precipitation of the tertiary material, followed by pulverization to complete the auxiliary agent.

Here, the third material may be dried while stirring the magnetic material so that the third material is not precipitated, and the third material may be dried and pulverized to complete the powder-like auxiliary agent and mix well with the batter.

The auxiliary agent manufactured through such a process performs the function of radiating the far-infrared ray irradiated from the yellow soil so that the far-infrared ray can be more easily reached to the body of the user using the yellow soil fumigator of the present invention.

Here, an alumina composite modified with alumina, which is an active ingredient of the auxiliary agent, can be prepared to produce an auxiliary agent having high mechanical strength and being robust at high temperature of the fumaceator, and having excellent heat resistance and oxidation resistance.

The process for producing such an alumina composite may include an aluminum aqueous solution production step, a first mixed solution production step, a second mixed solution production step, an intermediate powder production step, and an alumina composite finishing step.

First, the aluminum aqueous solution preparation step is a step of preparing an aluminum aqueous solution by mixing 80 to 99% by weight of water and 1 to 20% by weight of aluminum precursor with respect to the weight of the entire aluminum aqueous solution, and stirring at 60 to 90 ° C for 10 minutes to 2 hours It is preferable to proceed. Here, the aluminum precursor can be aluminum isopropoxide and provides aluminum ions in the alumina complex.

Next, the first mixed solution is prepared by mixing 70 to 99% by weight of the aluminum aqueous solution, 0.1 to 15% by weight of the copper nitrate solution and 0.1 to 15% by weight of the zinc nitrate solution with respect to the total weight of the first mixed solution, It is preferable to proceed with stirring for 30 minutes to 5 hours as a production process. At this time, the copper nitrate solution and the zinc nitrate solution provide copper ion and zinc ion to the alumina complex.

Hereinafter, the second mixed solution is prepared by mixing 95 to 99.9 wt% of the first mixed solution and 0.1 to 5 wt% of the nitric acid with respect to the total weight of the second mixed solution, For 1 minute to 2 hours, and serves as a silver nitrate silver oxide catalyst.

Next, in the intermediate powder preparation step, the second mixed solution is dried and pulverized to prepare an intermediate powder. The drying process is preferably performed at 100 to 200 ° C for 36 to 60 hours, and the moisture in the second mixed solution It is to dry completely.

Finally, the step of finishing the alumina composite is a step of finishing the alumina composite after heat-treating the intermediate powder at 500 to 1500 ° C. Here, the alumina composite is an alumina-copper oxide-zinc oxide composite in detail, and has characteristics that the mechanical strength and melting point are higher than those of conventional alumina, and the heat resistance and oxidation resistance are improved.

By using the alumina composite thus prepared as an active ingredient of the auxiliary agent instead of the conventional alumina, it is possible to maximize the far-infrared effect of the yellow loam, and at the same time to manufacture the loam base having high mechanical strength and good durability.

5 is a flow chart showing a process for producing the antibacterial agent of the present invention.

Horticulture is excellent for antibacterial and insecticidal effects, but the antimicrobial effect of loess can be improved by adding an antimicrobial agent containing an effective ingredient of tetraethylorthosilicate (TEOS) and silane-based organics to the loess base. The antimicrobial agent may be contained in an amount of 0.1 to 10% by weight based on the total weight of the loess base.

Methods for producing such an antimicrobial agent may include an intermediate solution preparation step (S130), an intermediate material preparation step (S131), and an antibacterial agent completion step (S132).

First, in the intermediate solution preparation step (S130), 10 to 30 wt% of TEOS, 10 to 30 wt% of silane-based organic material, 25 to 50 wt% of water, 25 to 50 wt% of ethanol, 0.1 to 5 wt% of ethanol, % By weight of water to prepare an intermediate solution.

Here, TEOS is a precursor of an antimicrobial agent, and ammonia water (NH ₄ OH) can be used as a catalyst. Methacryloxypropyl trimethoxysilane may be used as the silane-based organic material, and it acts as a low-energy organic material for realizing the super-water repellency of the antimicrobial agent. When the antimicrobial agent becomes water-repellent, It is possible to prevent corrosion and damage of the loess base.

Next, the intermediate material preparation step (S131) is a process of preparing an intermediate material by ultrasonication of the intermediate solution for 30 to 120 minutes, wherein the surface modification of TEOS, which is a precursor of the antimicrobial agent in the intermediate solution, and the production of the antimicrobial agent are proceeded. Through this process, the water and the ethanol in the intermediate solution preparation step (S130) are dried, so that the intermediate solution is dried to become a gel-type intermediate material.

Finally, the antimicrobial agent completion step (S132) is a step of drying the intermediate material at 100 to 200 DEG C for 30 minutes to 5 hours to complete the antimicrobial agent.

The antimicrobial agent produced through this process is positively charged and diffuses into the cell membrane of the bacterial cell using the electrostatic attraction with the negatively charged bacterial cells, thereby inactivating the energy metabolism and ion exchange of the bacteria and performing the antibacterial action .

In addition, the silane-based organic material, which is a reactant in the production process of the antimicrobial agent, can be further uniformly dispersed in the loess base so that the antimicrobial action can be performed. The friction coefficient is reduced to reduce the friction frequency between the antimicrobial agent and the loess base, .

The method of modifying the silane-based organic material may include a first solution producing step, a second solution producing step, a third solution producing step, a fourth solution producing step, and a silane based organic material finishing step.

First, a first solution is prepared by mixing 5 to 20% by weight of a silane coupling agent, 60 to 80% by weight of isopropyl alcohol and 10 to 20% by weight of water with respect to the weight of the entire first solution .

The silane coupling agent may be 3-glycidoxypropyl trimethoxysilane (GPTMS) or 3-aminopropyl trimethoxysilane (APTMS), and isopropyl alcohol and water may be used as the silane coupling agent. It is used as a solvent.

Next, the second solution preparation step is a step of preparing a second solution by mixing 95 to 99% by weight of the first solution and 1 to 5% by weight of nitric acid with respect to the weight of the total second solution, And hydrolyzing the coupling agent.

Thereafter, the third solution preparing step is a step of preparing a third solution by mixing 99 to 99.9% by weight of the second solution and 0.1 to 1% by weight of the silica powder with respect to the weight of the total third solution, It's a process I'm combining. In this process, stirring at 50 to 90 DEG C for 4 to 10 hours is preferable.

Next, in the fourth solution preparing step, the fourth solution is prepared by mixing 85 to 95% by weight of the third solution, 1 to 10% by weight of the SF coating, and 0.1 to 5% by weight of the curing agent with respect to the total weight of the fourth solution, It is preferable to stir at 1000 to 2000 rpm for 30 seconds to 30 minutes. Here, the SF-paint is a material for coating the silica powder of the third solution, which can improve the durability of the silica powder, and the hardener can use polyamide and provide a function of increasing the hardness of the silica powder.

Finally, in the step of completing the silane-based organic material, the fourth solution is dried in an IR lamp for 20 to 40 seconds and then dried at 70 to 90 ° C for 2 to 5 hours to complete the silane-based organic material. And then heat-curing the film by drying.

Since the silane-based organic material produced through this process does not aggregate more than the conventional silane-based organic material, when used in the manufacturing process of the antimicrobial agent, the antimicrobial agent is uniformly dispersed in the loess base to help antimicrobial action. By reducing the frequency of friction between the antimicrobial agent and the loess base, the damage due to friction can be reduced.

S100: Yellow clay base manufacturing step S200: Body preparing step
S300: injection step S210: primary material production step
S211: Secondary material manufacturing step S212: Third material manufacturing step
S213: auxiliary agent preparation step S220: primary solution preparation step
S221: Secondary solution preparation step S222: Step of obtaining residue
S223: maintenance completion step

Claims (3)

A method for producing an environmentally friendly loess body warmer containing a loess base,
An ocher base manufacturing step for producing an ocher base containing ocher, charcoal powder and calcium phosphate;
A body preparing step of preparing a body provided with an inner space into which the loess base is injected;
And injecting the loess base into the inner space to complete the loess body warmer,
The clay-
0.1 to 10% by weight of an antibacterial agent containing 60 to 80% by weight of loess, 10 to 20% by weight of charcoal powder, 5 to 15% by weight of calcium phosphate, TEOS (tetraethylorthosilicate, tetraethylorthosilicate) Wherein the step of preparing the green loess fomentation apparatus comprises the steps of: The method according to claim 1,
The anti-
10 to 30% by weight of TEOS, 10 to 30% by weight of silane-based organic substances, 25 to 50% by weight of water, 25 to 50% by weight of ethanol and 0.1 to 5% by weight of catalyst are mixed with each other to prepare an intermediate solution , An intermediate solution preparation step;
The intermediate solution is sonicated for 30 to 120 minutes to produce an intermediate;
And drying the intermediate material at 100 to 200 DEG C for 30 minutes to 5 hours to complete an antimicrobial agent. The method of manufacturing an eco-friendly loess fomentation apparatus containing the clayey base. 3. The method of claim 2,
The silane-
Preparing a first solution by mixing 5 to 20% by weight of a silane coupling agent, 60 to 80% by weight of isopropyl alcohol and 10 to 20% by weight of water with respect to the weight of the entire first solution;
Preparing a second solution by mixing 95 to 99 wt% of the first solution and 1 to 5 wt% of nitric acid with respect to the total weight of the second solution;
A third solution preparation step in which 99 to 99.9% by weight of the second solution and 0.1 to 1% by weight of silica powder are mixed with respect to the total weight of the third solution to prepare a third solution;
Preparing a fourth solution by mixing 85 to 95% by weight of the third solution, 1 to 10% by weight of SF coating, and 0.1 to 5% by weight of a curing agent with respect to the weight of the total fourth solution;
Wherein the fourth solution is dried in an IR lamp for 20 to 40 seconds and then dried at 70 to 90 DEG C for 2 to 5 hours to complete the silane-based organic material. Containing ocher poultice.

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