KR101866161B1 - heat treatment method of low alloy steel - Google Patents

heat treatment method of low alloy steel Download PDF

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KR101866161B1
KR101866161B1 KR1020180021835A KR20180021835A KR101866161B1 KR 101866161 B1 KR101866161 B1 KR 101866161B1 KR 1020180021835 A KR1020180021835 A KR 1020180021835A KR 20180021835 A KR20180021835 A KR 20180021835A KR 101866161 B1 KR101866161 B1 KR 101866161B1
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cooling
alloy steel
low alloy
water
storage tank
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KR1020180021835A
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Korean (ko)
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백태식
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백태식
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/18Hardening; Quenching with or without subsequent tempering
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/62Quenching devices
    • C21D1/63Quenching devices for bath quenching
    • C21D1/64Quenching devices for bath quenching with circulating liquids
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D10/00Modifying the physical properties by methods other than heat treatment or deformation
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0062Heat-treating apparatus with a cooling or quenching zone

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Heat Treatments In General, Especially Conveying And Cooling (AREA)

Abstract

The present invention relates to a heat treatment method of a low alloy steel with a new structure which is able to improve impact toughness of the low alloy steel. According to the heat treatment method of a low alloy steel of the present invention, the low alloy steel is heated at 890-910°C and has maintained the temperature for two hours in a homogenizing step, is cooled down to 595-605°C in a cooling step, and is heated at 620-640°C and has maintained the temperature for two hours in a tampering step such that the low alloy steel with improved impact toughness can be obtained.

Description

TECHNICAL FIELD [0001] The present invention relates to a low-

The present invention relates to a new low alloy steel heat treatment method capable of improving impact toughness of a low alloy steel.

In recent years, various types of low alloy steels having various kinds of small amounts or small amounts of third elements added to carbon steel have been developed and widely used in EPC, shipbuilding, offshore plant and construction fields.

Such a low alloy steel is produced by heating an intermediate material such as a vulcanized slab or a slab produced by a performance method at 1300 ° C, subjecting it to gogging and upsetting, and then performing a tip hole machining, heat treatment, It is manufactured in finished product form.

At this time, the heat treatment process for heat-treating the low alloy steel includes a homogenization step of heating the low alloy steel to a predetermined temperature, a cooling step of cooling the low alloy steel which has passed the homogenization step, a step of heating the cooled low alloy steel to a predetermined temperature And a tempering step.

At this time, the homogenization step is a step of homogenizing the structure of the low alloy steel by heating the low alloy steel to 900 ° C. or higher.

Wherein the cooling step comprises abruptly cooling the low alloy steel that has passed through the homogenization step to prevent internal structural changes caused by cooling of the heated low alloy steel and includes a cooling method for cooling the heated low alloy steel in the air, Cooling the low alloy steel by rapidly immersing the low alloy steel in the cooling water stored in the cooling water tank.

The tempering step is a step of increasing the viscosity of the low alloy steel by reheating the cooled low alloy steel through the cooling step to a temperature lower than the temperature of the homogenizing step.

Fig. 1 is an electron micrograph of a structure of a low alloy steel obtained through such a heat treatment step. The structure is composed of ferrite and pearlite, and has appropriate strength and viscosity.

On the other hand, recently, such a low alloy steel is required to have a high impact toughness of 90 J or more. However, impact toughness of the low alloy steel after the conventional heat treatment has been 20 to 60 J, which means that it is difficult to satisfy the required impact toughness.

Therefore, there is a need for a new method to solve such a problem.

10-1719560,

SUMMARY OF THE INVENTION The present invention has been made to solve the above-mentioned problems, and it is an object of the present invention to provide a novel low alloy steel heat treatment method capable of improving impact toughness of a low alloy steel.

The present invention for achieving the deadline includes a homogenizing step of heating a low alloy steel to a predetermined temperature, a cooling step of cooling the low alloy steel that has passed through the homogenizing step, a step of heating the cooled low alloy steel to a predetermined temperature, Wherein the homogenizing step comprises heating the low alloy steel to 890 to 910 占 폚 to maintain the temperature for 2 hours and the tempering step heating the low alloy steel to 670 to 690 占 폚 for 2 hours Is maintained for a long period of time.

According to another aspect of the present invention, in the cooling step, the low alloy steel which has been heated through the homogenization step is rapidly cooled using a water cooling method in which the low alloy steel is immersed in the cooling water stored in the water storage tank (A) An alloy steel heat treatment method is provided.

According to still another aspect of the present invention, there is provided a low alloy steel heat treatment method characterized in that the cooling step is to cool the heated low alloy steel to 595 to 605 占 폚.

According to still another aspect of the present invention, the low alloy steel comprises 96.13 to 99.89 wt% of Fe, 1 to 1.5 wt% of Mn, 0 to 0.6 wt% of Ni, 0.15 to 0.4 wt% of Si, 0 to 0.25 weight%, C0 to 0.22 weight%, V of 0.0 to 0.1 weight%, Al of 0.0 to 0.06 weight%, Ti of 0 to 0,05 weight% 0 to 0.04% by weight of Nb, 0 to 0.03% by weight of P, and 0 to 0.1% by weight of Si.

According to another aspect of the present invention, in the cooling step, the low alloy steel heated through the homogenization step is air-cooled to a target temperature of 670 to 690 ° C, which is the tempering step, and then the low alloy steel cooled at 670 to 690 ° C is introduced into the water storage tank A ), And water cooling is performed at 595 to 605 占 폚.

According to another aspect of the present invention, the low alloy steel is conveyed by the hoist 1 to be immersed in the cooling water stored in the water storage tank (A), and the water storage tank (A) And a space inside the water storage tank A is partitioned into an upper cooling portion 12 and a lower discharge portion 13 in the middle portion of the water storage tank A and a plurality of communication holes 11a are formed in the upper and lower surfaces A water supply port 14 connected to the cooling unit 12 and a drain port 15 connected to the discharge port 13 are formed on a circumferential surface of the water storage tank A, A water purification unit 20 connected to the water discharge port 15 for filtering foreign substances contained in the cooling water discharged to the water discharge port 15 and a circulation pipe 18 for connecting the water purification unit 20 and the water supply port 14, (30), and a cooling water passage (30) provided at a middle portion of the circulation pipe (30) A circulation pump 40 for circulating the cooling water through the water supply port 14 to the cooling part 12 of the water storage tank A and a circulation pump 40 provided at the middle part of the circulation pipe 30, (60) for measuring the surface temperature of the low alloy steel conveyed by the hoist (1) to be cooled and then lifted for a predetermined period of time, the cooling means (50) And control means (70) for receiving signals from the noncontact temperature measuring means (60) and controlling the operation of the circulating pump (40) and the cooling means (50), wherein the diaphragm (11) And a plurality of metal plates extending in the left-right direction and having a height in the up-and-down direction higher than the thickness in the lateral direction are coupled to each other in a lattice form. The noncontact temperature measuring means (60) , And the control means (70) Characterized in that the cooling means (50) is driven to cool the cooling water stored in the water storage tank (A) when the temperature of the low alloy steel measured by the hot water temperature measuring means (60) An alloy steel heat treatment method is provided.

According to another aspect of the present invention, the drain port 15 is formed at the lower end of the inner front surface of the water storage tank A and is provided in the water storage tank A so that foreign matter, which sinks to the bottom of the water storage tank A, And the foreign matter discharging means 80 includes a pair of guide rails 81 extending in both forward and backward directions on both sides of the inside of the water storage tank A, A slide bar 82 having both ends slidably coupled to the guide rail 81 and having a shape extending in a lateral direction and having an upper end connected to the slide bar 82, A scrapper 83 having an upper portion formed with an extension bar 83a extending upwardly from an upper end of the scrapper 83, And the front and rear directions A piston rod 84a fixed to the outer surface of the water storage tank A and extending forward extends through the through hole 19 formed in the side surface of the water storage tank A to extend the scrap pipe 83 When the cylinder mechanism 84 is extended, the scrapper 83 is rotated downward so that the lower surface of the scrapper 83 contacts the inner bottom surface of the water tank A, The scrapper 83 and the slide bar 82 are advanced toward the drain port 15 and the foreign substances sinking on the bottom surface of the water tank A are pushed toward the drain port 15. [ A low alloy steel heat treatment method is provided.

According to another aspect of the present invention, a lower partition 17 for forming a water supply chamber 18 is formed below the discharge unit 13 in the lower portion of the water storage tank A, The lower partition plate 17 is formed to extend downward from the center of the lower partition plate 17 to the lower side of the water storage tank A and the upper surface of the lower partition plate 17 is inclined downward toward the drain port 15, A plurality of water supply holes 17a for connecting the upper discharge port 13 and the lower water supply chamber 18 are formed and the end of the circulation pipe 30 is connected to the water supply port 14, The control means 70 branches the branch pipe 31 to a second branch pipe 32 connected to the water supply chamber 18 and is provided in each of the first and second branch pipes 31 and 32, Further comprising first and second solenoid valves (33, 34) operatively controlled by the non-contact temperature measuring means (60), wherein the control means (70) When the measured temperature of the low alloy steel is 600 ° C or less, the circulation pump 40 is driven at the first operation speed in a state in which the first solenoid valve 33 is closed and the second solenoid valve 34 is opened, The cooling water discharged to the drain 15 is supplied to the water supply chamber 18 through the second branch pipe 32 and then supplied to the lower side of the discharge portion 13 through the water supply hole 17a to be supplied to the lower partition 17 And the temperature of the low alloy steel measured by the noncontact temperature measuring means 60 is 600 ° C. or higher, the foreign matter deposited on the lower side of the lower partition plate 17 is moved toward the drain port 15 along the slope of the lower partition plate 17, The first solenoid valve 33 is closed and the second solenoid valve 34 is closed and the circulation pump 40 is driven at a second operation speed which is faster than the first operation speed and the cooling means 50 is operated, And the cooling water cooled by the cooling means (50) The low alloy heat treatment method characterized in that that group supplied to the first branch pipe 31 cooling unit 12 through is provided.

According to the heat treatment method for a low alloy steel according to the present invention, in the homogenization step, the low alloy steel is heated to 890 to 910 캜 for 2 hours, the low alloy steel is cooled to 595 to 605 캜 in the cooling step, The low alloy steel can be obtained by heating the low alloy steel at 620 ~ 640 ℃ for 2 hours during the tempering step.

FIG. 1 is a photograph of a structure of a low alloy steel obtained through a conventional heat treatment step, taken by an electron microscope,
FIG. 2 is a flowchart showing a low-alloy steel heat treatment method according to the present invention,
FIG. 3 is a photograph of a microstructure of a low alloy steel obtained through a low alloy steel heat treatment method according to the present invention,
4 is a side cross-sectional view showing a water tank of a low alloy steel heat treatment method according to the present invention,
5 is a plan view showing a partition plate of a water storage tank of a low alloy steel heat treatment method according to the present invention,
6 is a circuit diagram of a water tank of a low alloy steel heat treatment method according to the present invention,
FIG. 7 and FIG. 8 are reference views showing the operation of the water tank of the low alloy steel heat treatment method according to the present invention,
FIG. 9 is a side sectional view showing a water tank according to a second embodiment of the low alloy steel heat treatment method according to the present invention. FIG.
10 is a circuit diagram of a water storage tank according to a second embodiment of the low alloy steel heat treatment method according to the present invention.
11 and 12 are reference views showing the operation of the water storage tank according to the second embodiment of the low alloy steel heat treatment method according to the present invention.

Hereinafter, the present invention will be described in detail with reference to the accompanying drawings.

FIGS. 2 to 8 illustrate a low alloy steel heat treatment method according to the present invention, which comprises a homogenization step of heating a low alloy steel to a predetermined temperature, a cooling step of cooling the low alloy steel that has passed through the homogenization step, Is tempered by heating to a predetermined temperature.

According to the present invention, the low alloy steel is composed of 96.13 to 99.89 wt% of Fe, 1 to 1.5 wt% of Mn, 0 to 0.6 wt% of Ni, 0.15 to 0.4 wt% of Si, 0 to 0.35 wt% of Cu % Of Cr, 0 to 0.3 wt% of Cr, 0 to 0.25 wt% of Mo, 0 to 0.22 wt% of C, 0.0 to 0.1 wt% of V, 0.0 to 0.06 wt% of Al, 0 to 0.05 wt% of Ti, 0 to 0.04 wt% of Nb, 0 to 0.03 wt% of P, and 0 to 0.1 wt% of S.

According to the present invention, in the homogenization step, a low alloy steel is charged into the furnace and heated to 890 to 910 캜, followed by maintaining the temperature for 2 hours.

In the cooling step, the low-alloyed steel heated through the homogenization step is cooled to 595 to 605 ° C.

At this time, as a means of cooling the low alloy steel, a water cooling method of rapidly cooling the low alloy steel by immersing the heated low alloy steel in the cooling water stored in the water storage tank A is used.

In the tempering step, the cooled low-alloy steel which has passed through the cooling step is heated to 670 to 690 ° C., maintained for 2 hours, and then cooled.

FIG. 3 is an electron micrograph of the structure of the low alloy steel obtained through such a heat treatment process, showing that the structure is made of ferrite and bainite, and the homogeneity of the structure is improved.

Impact toughness of the low alloy steel subjected to such a heat treatment process is 160 J, and the impact toughness (90 J) required for the low alloy steel can be obtained.

FIG. 4 shows a water tank A used for cooling the low alloy steel in the cooling step, and the low alloy steel heated through the homogenization step is transferred by the hoist 1, ). ≪ / RTI >

In the middle of the water storage tank A, a space inside the water storage tank A is divided into a cooling part 12 on the upper side and a cooling part 12 on the lower side in the middle part of the water storage tank A, And a diaphragm 11 partitioned by the discharge part 13 and formed so as to penetrate the upper and lower surfaces of the plurality of communication holes 11a.

As shown in FIGS. 4 and 5, the diaphragm 11 is composed of a plurality of metal plates extending in the front-rear direction and the left-right direction and having a height in the up-and-down direction higher than the thickness in the lateral direction, , And a plurality of quadrangular communication holes 11a are formed.

A water supply port 14 connected to the cooling unit 12 and a drain port 15 connected to the discharge port 13 are formed on the circumference of the water storage tank A and connected to the drain port 15 A circulation pipe 30 for connecting the water purification unit 20 and the water supply port 14 and a circulation pipe 30 for connecting the water purification unit 20 and the circulation pipe 30, A circulation pump 40 provided in an intermediate portion of the water purification unit 30 for circulating the cooling water having passed through the water purification unit 20 to the cooling unit 12 of the water storage tank A through the water supply port 14, A cooling means 50 provided at a middle portion of the pipe 30 for cooling the cooling water circulated through the circulation pipe 30 and cooled by the hoist 1 for a predetermined period of time, Contact type temperature measuring means (60) for measuring the surface temperature of the low alloy steel which is raised after the temperature of the non-contact type temperature measuring means (60) And control means 70 for controlling the operation of the circulation pump 40 and the cooling means 50.

The water supply port 14 is formed at the upper end of the side wall of the water storage tank A and the drain hole 15 is formed at the lower end of the inner front surface of the water storage tank A.

The water purifier unit 20 includes a case 21 connected to the drain port 15 through a drain pipe 23 and a filter body 22 disposed inside the case 21, So that only the clean cooling water from which foreign substances have been removed is circulated to the water storage tank A through the circulation pipe 30.

The circulation pump 40 is continuously operated so that the cooling water stored in the water storage tank A continuously passes through the water purification unit 20 and then flows along the circulation pipe 30 Circulated to the water storage tank (A).

The cooling means 50 includes a heat exchanger 51 provided at an intermediate portion of the circulation pipe 30 and a cooling device 50 which is operated by the control means 70 to supply cold refrigerant to the heat exchanger 51. [ (52). When the cooling device (52) is driven, the coolant supplied to the heat exchanger (51) is supplied, and the supplied coolant is heat-exchanged with the cooling water passing through the circulation pipe Cool the temperature of the cooling water.

The noncontact temperature measuring means 60 uses a laser temperature measuring device for measuring the temperature of the low alloy steel by irradiating a laser on the surface of the object. The noncontact temperature measuring means 60 is provided on the support bar 16 provided at the upper circumference of the water storage tank A do.

Therefore, when the low alloy steel is transported by the hoist 1, is cooled by the cooling water stored in the water storage tank A, and is lifted, the surface of the low alloy steel which is lifted is irradiated with laser, The temperature of the low alloy steel can be measured.

The control means (70) stops the cooling means (50) when the temperature of the low alloy steel measured by the noncontact type temperature measuring means (60) is 600 DEG C or lower, When the temperature of the low alloy steel is raised to 600 ° C or more, the cooling means (50) is driven to cool the cooling water stored in the water storage tank (A) so that the low alloy steel passing through the cooling process can be cooled to 595 to 605 ° C The temperature of the cooling water is adjusted.

In addition, the water storage tank A is provided with a foreign matter discharging means 80 for discharging a foreign matter sinking to the bottom of the water storage tank A to the drain hole 15.

The foreign matter discharging means 80 includes a pair of guide rails 81 extending in both forward and backward directions on both sides of the inside of the water storage tank A and a pair of guide rails 81 A slide bar 82 slidably coupled to the slide bar 82 and having a panel shape extending in the lateral direction and having an upper end rotatably coupled to the front surface of the slide bar 82 in a vertical direction, A scrapper 83 provided with a bar 83a and an operation control unit 80 connected to the upper end of the extension of the scrapper 83 arranged to extend in the front and rear direction on the outer surface of the water tank, And a cylinder mechanism (84).

The front side of the slide bar 82 is provided with a forwardly extending hinge bracket 82a.

The scrapper 83 is vertically coupled to the hinge bracket 82a by a hinge shaft 83C extending laterally from the rear of the upper end of the hinge bracket 82a so as to be vertically rotatable in a forward angle range of 45 degrees.

At this time, the scrapper 83 is provided at its lower end with a rubber member 83b, and when the scrapper 83 is rotated downward, the contact member 83b is closely attached to the inner bottom surface of the water storage tank A vertically .

The cylinder mechanism 84 uses a pneumatic cylinder that is expanded and contracted under the control of the control means 70. A piston rod 84a fixed to the outer surface of the water reservoir A and extending forward is inserted into the water reservoir A And is hinged to the upper end of the extended portion.

Therefore, as shown in Fig. 4, in a state in which the slide bar 82 and the scrapper 83 are retracted and the scrapper 83 is rotated upward, as shown in Fig. 7, The lower end of the scrapper 83 is pivoted downward by pushing the extension bar 83a of the scrapper 83 forward so that the lower end of the scrapper 83 is pivoted downward, Make sure it is in close contact with the inner bottom surface.

When the cylinder mechanism 84 is further elongated, the scrapper 83 and the slide bar 82 are pushed forward as shown by the dotted line in Fig. 7, The foreign matter sinking on the inner bottom surface of the air bag A is pushed toward the front, that is, toward the drain 15.

8, in a state in which the scrapper 83 and the slide bar 82 are advanced, when the cylinder mechanism 84 is contracted, the extension bar 83a is pulled backward, When the lower end of the scrapper 83 is spaced upward from the inner bottom surface of the water storage tank A and the cylinder mechanism 84 is further reduced as shown in Fig. 4, The scrapper 83 and the slide bar 82 are retracted and returned to their original positions.

Therefore, by extensively expanding and contracting the cylinder mechanism 84 at the pre-input period of the control means 70, the foreign matter sinking to the inner bottom surface of the water storage tank A is pushed toward the drain port 15, So that it can be smoothly discharged to the drain hole (15).

According to the low alloy steel heat treatment method thus configured, the low alloy steel is heated to 890 to 910 占 폚 and maintained at the temperature for 2 hours in the homogenizing step, and the low alloy steel is cooled to 595 to 605 占 폚 in the cooling step, The low alloy steel is heated to 620 to 640 DEG C for 2 hours to obtain a low alloy steel having improved impact toughness.

Particularly, in the cooling step, the low alloy steel heated by using the water cooling method in which the low alloy steel heated through the homogenization step is immersed in the cooling water stored in the water storage tank A is rapidly cooled to obtain the low alloy steel in which the structure is uniformized more effectively There are advantages to be able to.

The low alloy steel is fed by the hoist 1 and is immersed in the cooling water stored in the water storage tank A. The water storage tank A is formed in a tubular shape having an upper surface opened and a cooling water stored therein, A space inside the water storage tank A is partitioned by an upper cooling portion 12 and a lower discharge portion 13 in the middle portion of the water storage tank A and a plurality of communication holes 11a are formed in the intermediate portion of the water storage tank A, .

Therefore, when the low alloy steel heated in the cooling water is immersed in the low alloy steel to cool the low alloy steel, foreign matter or other foreign matter generated by the separation from the low alloy steel flows through the communication hole 11a of the diaphragm 11 to the lower discharge portion 13 And then deposited on the bottom surface of the water storage tank A.

A water supply port 14 connected to the cooling unit 12 and a drain port 15 connected to the discharge port 13 are formed on the circumference of the water storage tank A and connected to the drain port 15 A circulation pipe 30 for connecting the water purification unit 20 and the water supply port 14 and a circulation pipe 30 for connecting the water purification unit 20 and the circulation pipe 30, A circulation pump 40 provided in an intermediate portion of the water purification unit 30 for circulating the cooling water having passed through the water purification unit 20 to the cooling unit 12 of the water storage tank A through the water supply port 14, A cooling means 50 provided at a middle portion of the pipe 30 for cooling the cooling water circulated through the circulation pipe 30 and cooled by the hoist 1 for a predetermined period of time, Contact type temperature measuring means (60) for measuring the surface temperature of the low alloy steel which is raised after the temperature of the non-contact type temperature measuring means (60) And control means 70 for controlling the operation of the circulation pump 40 and the cooling means 50.

Therefore, when the circulation pump 40 is driven, the cooling water stored in the discharge unit 15 of the water storage tank A passes through the water purification unit 20, and foreign substances contained in the cooling water are purified by the water purification unit 20 And only clean cooling water is supplied to the cooling unit 12 of the water storage tank A.

Therefore, there is an advantage that when the low alloy steel is cooled, the surface of the low alloy steel can be prevented from being contaminated by the foreign substances contained in the cooling water.

Particularly, the diaphragm 11 is composed of a plurality of metal plates extending in the front-rear direction and the left-right direction and having a height in the up-and-down direction higher than the thickness in the lateral direction, The flow of cooling water generated when the low alloy steel is immersed or taken out is blocked by the partition plate 11 and is not transmitted to the discharge unit 13 on the lower side so that once the foreign substances accumulated on the bottom surface of the water storage tank A are heated It is possible to prevent the low alloy steel from being floated upward due to the vibration generated when the low alloy steel is immersed in or taken out of the cooling part 12, and thus it is possible to more effectively prevent the low alloy steel from being contaminated by the contaminants.

The temperature of the low alloy steel measured by the non-contact temperature measuring means (60) is set to 600 deg. C (60 deg. C) when the temperature of the low alloy steel measured by the noncontact temperature measuring means (60) , The cooling means (50) is driven to cool the cooling water stored in the water storage tank (A).

Accordingly, there is an advantage that the low alloy steel cooled by being immersed in the cooling water can be effectively controlled to be cooled to the target temperature of 595 to 605 DEG C, which is the cooling step.

That is, in the cooling step, the low alloy steel is immersed in the cooling water stored in the water tank A using the hoist 1 to rapidly freeze the low alloy steel, and the low alloy steel is immersed in the cooling water for a predetermined time.

In this case, the degree of cooling of the low alloy steel held in the cooling water for a predetermined time is influenced by various variables such as the temperature of the cooling water and the ambient temperature. Therefore, only by keeping the temperature of the cooling water constant, The alloy steel can not be precisely controlled to be cooled to 595 to 605 ° C.

However, in the case of the present invention, the control means 70 receives the signal of the noncontact temperature measuring means 60, and is cooled by being cooled for a predetermined period of time in the cooling water stored in the water storage tank (A) And when the temperature of the low alloy steel rises to 600 DEG C or more, which is the middle of the target temperature of 595 to 605 DEG C, it is determined that the temperature of the cooling water is low and the cooling means 50 is driven By controlling the temperature of the cooling water stored in the water storage tank (A), the low alloy steel which is cooled by being immersed in the cooling water next time is adjusted so as to be cooled to exactly 595 ~ 605 ° C.

On the other hand, when the temperature of the low alloy steel is lowered to 600 占 폚 or less, the control means 70 stops the cooling means 50 to prevent the low alloy steel from being cooled below the target temperature.

Therefore, there is an advantage that the low alloy steel that has passed through the cooling process can be accurately controlled to be cooled to 595 to 605 ° C.

The drain port 15 is formed at the lower end of the inner front surface of the water storage tank A and is provided in the water storage tank A so as to discharge a foreign substance, which has settled to the bottom of the water storage tank A, The foreign matter discharging means 80 includes a pair of guide rails 81 extending in both forward and backward directions on both sides of the interior of the water storage tank A, A slide bar 82 slidably coupled to the guide rail 81 at both ends thereof and a laterally extending panel shape so that an upper end of the slide bar 82 is vertically rotatable A scrapper 83 having an upper portion formed with an extension bar 83a extending upward and an upper portion extending from the lower portion of the scrapper 83, And A piston rod 84a fixed to the outer surface of the water tray A and extending forward extends through a through hole 19 formed in a side surface of the water storage tank A and is connected to an upper end of an extension of the scrapper 83. [ And a mechanism 84.

Therefore, when the cylinder mechanism 84 is extended, the scrapper 83 is rotated downward, and the scrapper 83 is brought into contact with the inner bottom surface of the water storage tank A, The slide bar 82 is advanced toward the drain port 15 and the foreign substances sinking on the bottom surface of the water tank A are pushed toward the drain port 15 so that the foreign matter sinking to the bottom of the water tank A effectively flows into the drain port 15, When the cylinder mechanism 84 is contracted, the scrapper 83 is rotated upward to be spaced upward from the inner bottom surface of the water storage tank A, By moving back to the original position, it is possible to prevent foreign matter that has settled on the floor from being pushed backward by the scrapper 83 when the scrapper 83 is returned to its original position, There .

In the cooling step, the low-alloyed steel heated through the homogenization step is directly cooled in the cooling water. However, in the cooling step, the low-alloyed steel heated through the homogenization step is cooled to a temperature of 670 - The low alloy steel cooled to 670 to 690 DEG C is immersed in the cooling water stored in the water storage tank A and water-cooled to 595 to 605 DEG C.

As described above, when the low alloy steel is cooled in two stages, the temperature of the cooling water is minimized when the low alloy steel is immersed in the cooling water and water-cooled while maintaining the same structure of the low alloy steel as that of the above- And the energy consumed to cool the cooling water by the cooling means 50 can be reduced.

9 to 12 illustrate another embodiment of the present invention in which the water storage tank A is provided with a diaphragm 11 therein and a water supply port 14 connected to the cooling unit 12 at its periphery, And a drain port (15) connected to the discharge port (13), a water purification unit (20) connected to the drain port (15) to filter out foreign substances contained in the cooling water discharged to the drain port (15) A circulation pipe 30 connecting the unit 20 and the water supply port 14 and cooling water passing through the water purification unit 20 provided at a middle portion of the circulation pipe 30 to the water supply port 14, A circulation pump 40 for circulating the cooling water circulated through the circulation pipe 30 to the cooling unit 12 of the water storage tank A through the circulation pipe 30, (50), a low alloy steel which is conveyed by the hoist (1) to be cooled in the cooling water for a predetermined period of time after being cooled (70) for receiving signals from the non-contact temperature measuring means (60) and controlling the operation of the circulating pump (40) and the cooling means (50) Which is the same as the conventional one.

According to the present embodiment, a lower partition plate 17 for forming a water supply chamber 18 below the discharge unit 13 is further provided inside the water storage tank A.

At this time, the drain port 15 is formed to extend from the center of the lower partition plate 17 to the lower side of the water storage tank A, and the upper surface of the lower partition plate 17 is inclined downward toward the drain port 15 .

The lower partition plate 17 is formed with a plurality of water supply holes 17a connecting the upper discharge unit 13 and the lower water supply chamber 18.

The end of the circulation pipe 30 is branched into a first branch pipe 31 connected to the water supply port 14 and a second branch pipe 32 connected to the water supply chamber 18, The first and second branch pipes (31, 32) are provided with first and second solenoid valves (33, 34) controlled by the control means (70), respectively.

When the temperature of the low alloy steel measured by the noncontact temperature measuring means 60 is 600 DEG C or lower, the control means 70 closes the first solenoid valve 33 as shown in FIG. 11 The circulation pump 40 is driven at a first operation speed in a state in which the second solenoid valve 34 is opened so that the cooling water discharged to the drain 15 flows through the second branch pipe 32 to the water supply chamber 18 And then supplied to the lower side of the discharge unit 13 through the water supply hole 17a.

When the cooling water is supplied to the lower side of the discharge portion 13 through the water supply hole 17a, the foreign matter sinking to the inner bottom surface of the water storage tank A, that is, the upper surface of the lower partition plate 17, The water is pushed upward by the cooling water supplied to the discharge unit 13 through the hole 17a and then moved to the drain port 15 along the inclined surface of the lower partition plate 17 and then flows through the drain port 15 to the water purification unit 20).

At this time, the first operation speed represents a speed at which the cooling water is slowly supplied to the discharge portion 13 through the water supply hole 17a.

When the temperature of the low alloy steel measured by the noncontact temperature measuring means 60 is 600 DEG C or higher, the control means 70 controls the first solenoid valve 33 to open The second solenoid valve 34 is closed and the circulation pump 40 is driven at a second operation speed which is faster than the first operation speed and the cooling means 50 is driven, 50 to be supplied to the cooling unit 12 through the first branch pipe 31. [

At this time, the second operation speed is set to such a degree that the cooling water stored in the water storage tank A is circulated through the circulation pipe 30 at a high speed and the temperature of the cooling water stored in the cooling unit 12 can be cooled.

When the cooling water is supplied to the cooling unit 12, the supplied cooling water is lowered to lower the temperature of the cooling water in the cooling unit 12 so that the low-alloy steel immersed in the cooling water is cooled to 620 to 640 ° C. can do.

According to the low alloy steel heat treatment method as described above, unlike the above-described first embodiment in which the foreign substances that have settled on the bottom surface of the water storage tank A are pushed toward the drain port 15 by using the foreign substance discharging means 80, The foreign matter is moved toward the drain port 15 by using the cooling water supplied to the upper side of the lower partition plate 17 through the through holes 17a. Thus, the structure is simpler and the operation reliability is high.

A. Water tank 20. Water purification unit
30. Circulation tube 40. Circulation pump
50. Cooling means 60. Temperature measuring means
70. Control means 80. Foreign matter discharging means

Claims (3)

A homogenizing step of heating the low alloy steel to a predetermined temperature,
A cooling step of cooling the low alloy steel which has passed through the homogenization step,
A low alloy steel heat treatment method comprising a tempering step of tempering a cooled low alloy steel at a predetermined temperature,
In the homogenization step, the low alloy steel is heated to 890 to 910 DEG C, the temperature is maintained for 2 hours,
Wherein the tempering step is characterized in that the low alloy steel is heated to 670 to 690 DEG C and maintained for 2 hours,
The cooling step is characterized in that the low alloy steel heated by the water cooling method in which the low alloy steel heated through the homogenization step is immersed in the cooling water stored in the water storage tank A is rapidly cooled,
The cooling step is characterized by cooling the heated low alloy steel to 595 to 605 DEG C,
Wherein the low alloy steel comprises 96.13 to 99.89 wt% of Fe, 1 to 1.5 wt% of Mn, 0 to 0.6 wt% of Ni, 0.15 to 0.4 wt% of Si, 0 to 0.35 wt% of Cu, 0 to 0.3 wt% 0 to 0.25 wt% of Mo, 0 to 0.22 wt% of C, 0.0 to 0.1 wt% of V, 0.0 to 0.06 wt% of Al, 0 to 0 wt% of Ti, 0 to 0.04 wt% of Nb, To 0.03% by weight, and S 0 to 0.1% by weight,
In the cooling step, the low-alloy steel heated through the homogenization step is air-cooled to a target temperature of 670 to 690 ° C. of the tempering step, and then the low alloy steel cooled to 670 to 690 ° C. is immersed in the cooling water stored in the water storage tank A, Lt; 0 > C,
The low alloy steel is conveyed by the hoist 1 to be immersed in the cooling water stored in the water storage tank A,
The water storage tank (A) has a tubular shape in which an upper surface is opened and cooling water is stored therein,
A space inside the water storage tank A is partitioned into an upper cooling portion 12 and a lower discharge portion 13 at the middle portion of the water storage tank A and a plurality of communication holes 11a are formed in the partition plate 11,
A water supply port 14 connected to the cooling unit 12 and a drain port 15 connected to the discharge unit 13 are formed on the circumference of the water storage tank A,
A water purifier unit 20 connected to the drain port 15 to filter out foreign substances contained in the cooling water discharged to the drain port 15,
A circulation pipe 30 connecting the water purification unit 20 and the water supply port 14,
A circulation pump 40 provided in the middle of the circulation pipe 30 for circulating the cooling water having passed through the water purification unit 20 to the cooling unit 12 of the water storage tank A through the water supply port 14, Wow,
A cooling means 50 provided at a middle portion of the circulation pipe 30 for cooling the cooling water circulated through the circulation pipe 30,
A non-contact temperature measuring means (60) for measuring the surface temperature of the low alloy steel which is conveyed by the hoist (1) and cooled and then cooled by being immersed in the cooling water for a predetermined time,
Further comprising control means (70) for receiving signals of said non-contact temperature measuring means (60) and for controlling the operation of said circulating pump (40) and cooling means (50)
The diaphragm 11 is composed of a plurality of metal plates extending in the front-rear direction and the lateral direction and having a height in the up-and-down direction higher than the thickness in the lateral direction,
The noncontact temperature measuring means 60 is provided at the upper end of the water storage tank A,
When the temperature of the low alloy steel measured by the noncontact temperature measuring means 60 rises to 600 ° C or higher, the control means 70 drives the cooling means 50 to cool the cooling water stored in the water storage tank A Wherein the heat treatment is performed at a temperature higher than the melting point of the low alloy steel.
The method according to claim 1,
The drain port (15) is formed at the lower end of the inner front surface of the water storage tank (A)
Further comprising a foreign matter discharging means (80) provided in the water storage tank (A) for discharging foreign matter sinking to the bottom of the water storage tank (A) to the drain hole (15)
The foreign matter discharging means (80)
A pair of guide rails 81 extending in the front-rear direction on both inner sides of the water storage tank A,
A slide bar 82 having a bar shape extending sideways and having both ends slidably coupled to the guide rail 81,
The upper end of the slide bar 82 is rotatably coupled to the front surface of the slide bar 82 in a vertical direction so that the lower surface of the slide bar 82 is closely contacted with the inner bottom surface of the water reservoir A A scrapper 83 provided with an extension bar 83a extending upward,
A piston rod 84a fixed to the outer side surface of the water storage tank A and extending forward extends through the through hole 19 formed in the side surface of the water storage tank A, And a cylinder mechanism (84) connected to the upper end of the extension of the cylinder,
When the cylinder mechanism 84 is extended, the scrapper 83 is rotated downward and the scrapper 83 and the slide bar 83 are brought into close contact with the inner bottom surface of the water storage tank A, (82) is advanced toward the drain port (15) so as to push foreign substances sinking on the bottom surface of the water storage tank (A) toward the drain port (15).
The method according to claim 1,
A lower partition 17 for forming a water supply chamber 18 below the discharge unit 13 is further provided inside the water storage tank A,
The drain port 15 is formed to extend from the center of the lower partition plate 17 to the lower side of the water storage tank A,
The upper surface of the lower partition plate 17 is inclined downward toward the drain port 15,
The lower partition plate 17 is provided with a plurality of water supply holes 17a connecting the upper discharge unit 13 and the lower water supply chamber 18,
The end of the circulation pipe 30 branches into a first branch pipe 31 connected to the water supply port 14 and a second branch pipe 32 connected to the water supply chamber 18,
Further comprising first and second solenoid valves (33, 34) respectively provided in the first and second branch pipes (31, 32) and controlled by the control means (70)
The control means (70)
When the temperature of the low alloy steel measured by the noncontact temperature measuring means 60 is 600 캜 or less, the first solenoid valve 33 is closed and the second solenoid valve 34 is opened, Is driven at a first operating speed so that the cooling water discharged to the drain 15 is supplied to the water supply chamber 18 through the second branch pipe 32 and then discharged through the water supply hole 17a to the discharge portion 13 So that the foreign matter sinking to the lower side of the lower partition plate 17 is moved toward the drain port 15 along the inclined surface of the lower partition plate 17,
When the temperature of the low alloy steel measured by the noncontact temperature measuring means 60 is 600 ° C or higher, the first solenoid valve 33 is opened, the second solenoid valve 34 is closed, and the circulation pump 40) at a second operation speed that is faster than the first operation speed and drives the cooling means (50) so that the cooling water cooled by the cooling means (50) flows through the first branch pipe Cooling section (12).
KR1020180021835A 2018-02-23 2018-02-23 heat treatment method of low alloy steel KR101866161B1 (en)

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Cited By (1)

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Publication number Priority date Publication date Assignee Title
CN113999956A (en) * 2021-11-03 2022-02-01 临西县军华机械配件有限公司 Temperature-stable continuous spheroidizing furnace

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KR101220273B1 (en) * 2011-07-11 2013-01-09 주식회사 포스코 Opening/closing apparatus of lid and the method thereof
KR101628175B1 (en) * 2014-10-22 2016-06-08 주식회사 메타즈 Heat treatment process of boron alloy steel for track link of construction vehicles
KR101719560B1 (en) 2017-01-16 2017-04-05 케이제이에프 주식회사 Heat treatment method for surface hardened alloy steel

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Publication number Priority date Publication date Assignee Title
KR101220273B1 (en) * 2011-07-11 2013-01-09 주식회사 포스코 Opening/closing apparatus of lid and the method thereof
KR101628175B1 (en) * 2014-10-22 2016-06-08 주식회사 메타즈 Heat treatment process of boron alloy steel for track link of construction vehicles
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113999956A (en) * 2021-11-03 2022-02-01 临西县军华机械配件有限公司 Temperature-stable continuous spheroidizing furnace

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