KR101729859B1 - Pyrolysis oil production unit using waste plastics - Google Patents
Pyrolysis oil production unit using waste plastics Download PDFInfo
- Publication number
- KR101729859B1 KR101729859B1 KR1020150151220A KR20150151220A KR101729859B1 KR 101729859 B1 KR101729859 B1 KR 101729859B1 KR 1020150151220 A KR1020150151220 A KR 1020150151220A KR 20150151220 A KR20150151220 A KR 20150151220A KR 101729859 B1 KR101729859 B1 KR 101729859B1
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- South Korea
- Prior art keywords
- tank
- pipe
- gas
- water
- coupled
- Prior art date
Links
- 238000000197 pyrolysis Methods 0.000 title claims abstract description 75
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 239000002699 waste material Substances 0.000 title abstract description 45
- 239000004033 plastic Substances 0.000 title abstract description 7
- 229920003023 plastic Polymers 0.000 title abstract description 7
- 238000001816 cooling Methods 0.000 claims abstract description 62
- 238000010438 heat treatment Methods 0.000 claims abstract description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- 238000002485 combustion reaction Methods 0.000 claims abstract description 13
- 230000002265 prevention Effects 0.000 claims abstract description 10
- 238000003860 storage Methods 0.000 claims abstract description 8
- 239000012535 impurity Substances 0.000 claims abstract description 5
- 239000000498 cooling water Substances 0.000 claims description 44
- 238000000034 method Methods 0.000 claims description 12
- 238000002347 injection Methods 0.000 claims description 11
- 239000007924 injection Substances 0.000 claims description 11
- 239000003054 catalyst Substances 0.000 claims description 9
- 239000002184 metal Substances 0.000 claims description 9
- 229910052751 metal Inorganic materials 0.000 claims description 9
- 239000003638 chemical reducing agent Substances 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 3
- 229920003002 synthetic resin Polymers 0.000 abstract description 37
- 239000000057 synthetic resin Substances 0.000 abstract description 37
- -1 polyethylene terephthalate Polymers 0.000 abstract description 3
- 235000013361 beverage Nutrition 0.000 abstract description 2
- 238000004891 communication Methods 0.000 abstract description 2
- 239000002826 coolant Substances 0.000 abstract 2
- 229920000139 polyethylene terephthalate Polymers 0.000 abstract 1
- 239000005020 polyethylene terephthalate Substances 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 78
- 239000003921 oil Substances 0.000 description 23
- 239000007788 liquid Substances 0.000 description 13
- 238000005979 thermal decomposition reaction Methods 0.000 description 7
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- 239000004743 Polypropylene Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 229920001155 polypropylene Polymers 0.000 description 2
- 238000004227 thermal cracking Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 235000012206 bottled water Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000002440 industrial waste Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000010893 paper waste Substances 0.000 description 1
- 239000004417 polycarbonate Substances 0.000 description 1
- 229920000515 polycarbonate Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D35/00—Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
- B01D35/02—Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D47/00—Separating dispersed particles from gases, air or vapours by liquid as separating agent
- B01D47/06—Spray cleaning
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/77—Liquid phase processes
- B01D53/78—Liquid phase processes with gas-liquid contact
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/10—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal from rubber or rubber waste
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
- F23G5/00—Incineration of waste; Incinerator constructions; Details, accessories or control therefor
- F23G5/02—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment
- F23G5/027—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment pyrolising or gasifying stage
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
- F23G7/00—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals
- F23G7/06—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals of waste gases or noxious gases, e.g. exhaust gases
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
- F23G7/00—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals
- F23G7/12—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals of plastics, e.g. rubber
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/10—Feedstock materials
- C10G2300/1003—Waste materials
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
- F23G2209/00—Specific waste
- F23G2209/28—Plastics or rubber like materials
Abstract
Description
The present invention relates to a pyrolysis oil production apparatus using waste synthetic resin, and more particularly, to a pyrolysis oil production apparatus using waste synthetic resin, and more particularly, to a pyrolysis oil production apparatus using waste synthetic resin, It was developed to extract and recycle pyrolysis oil by burning using incineration heat of waste such as outer covering which acts as pollution source.
Conventional pyrolysis emulsification technology is a technology for producing alternative fuel oil by pyrolyzing polymer waste such as waste synthetic resin in a reactor without oxygen or lean state. Here, the low-molecular-weight gas that is pyrolyzed passes through the condensation system and becomes pyrolysis oil.
As described above, the present invention relates to a waste synthetic resin product, a synthetic resin residue used in various industries, and a waste synthetic resin, which are used in our daily living, and collect waste synthetic resin to extract and recycle the oil contained in the waste synthetic resin to save resources It is.
The present invention relates to a method for producing pyrolyzed oil using waste synthetic resin, which comprises thermally decomposing various kinds of waste synthetic resins such as waste paper made of synthetic resins used in residential living environments and beverage bottles or waste synthetic resins generated throughout the production industry, And it is an object of the present invention to prevent contamination of the surrounding environment by combusting combustible gas generated during pyrolysis.
The pyrolysis process is generally divided into a raw material input process, a pyrolysis reaction process, a condensation process, a residue treatment process, and a non-condensable gas treatment process. Here, the condensation process is reinforced by the same distillation system as the petrochemical process in order to obtain good quality pyrolysis oil.
The most important process in pyrolysis is the calking phenomenon when the waste synthetic resin is pyrolyzed. The coking phenomenon occurs when the pyrolyzed hydrocarbon comes into contact with the inner wall of the reactor containing the heated iron or nickel to separate the hydrogen and the carbon is separated from the inner wall of the pyrolysis tank If the coating is cured by coating, the thickness of the caulking is continuously increased, which causes the cracking tank to rupture. Therefore, most of the pyrolysis reactors have a mechanical structure capable of suppressing or controlling the caulking so that the generation of caulking does not occur.
In the present invention, a rotary shaft is coupled to a lower end of a rotary shaft and a rotary shaft is coupled to an upper end of a rotary shaft at a central portion of the rotary shaft, and a deceleration heating tank having an input shaft and a reducer combined with a small chain gear A primary cooling tank connected to a communicating pipe connected to an upper end of the pyrolysis heating tank; a cooling water discharge pipe fixed to the lower end of the primary cooling tank in multiple stages; a secondary cooling tank provided on the side of the cooling water discharge pipe; A storage tank for storing thermal cracking oil supplied from an uncompacted gas backflow prevention discharge pipe coupled to a side surface of the secondary cooling tank, a gas combustion chamber connected to a gas discharge pipe coupled to the upper end of the secondary cooling tank, A filter device installed at the lower end of the tank for filtering impurities contained in the discharged water and a water pump for circulating water, By constructing a water cooler that cools the primary cooling, and cooling pipe for connecting the water supply pipes are connected to the thermal decomposition of waste plastic intended to extract the pyrolysis oil.
The present invention as described above can be applied to the production of pyrolysis oil by pyrolyzing waste synthetic resin generated in various kinds of waste household articles recovered by separate collection, such as synthetic resin container, case made of synthetic resin, various kinds of plastic bottles and industrial waste, And waste incinerator waste is completely incinerated, toxic gas is not generated, so it is possible to contribute to the natural environment by reducing pollution.
1 is a block diagram of the present invention
2 is an enlarged view of the cooling discharge pipe of the present invention
The present invention collects various waste synthetic resins such as daily necessities used in daily life and bottled water bottles and completely combusts the combustible gas generated during pyrolysis by heating at high temperature and extracts pyrolysis oil and pyrolysis oil, To a minimum, which will be described in detail as follows.
The present invention relates to a pyrolysis heating tank (10) having a rotary shaft (1) at the lower end and a rotary shaft (2) at the upper end coupled with an alternative gear (3)
A speed reducer 6 which combines a small chain gear 4 for operating the
A
A cooling water
A
A
A
A
The cooling water discharge pipe (30) includes a primary gas inlet pipe (31) having a primary spiral injection port (21) fixed to inject a cooling water on a horizontal line,
A secondary
A tertiary
A fourth
And a fifth-order gas inflow pipe (35) in which a fifth-order helical injection port (25) for vertically coupling with the fourth gas inflow pipe (34) and injecting cooling water on a horizontal line is fixed, 21, the secondary spiral jet opening 22, the tertiary spiral jet opening 23, the fourth helical jet opening 24 and the fifth
The extraction of pyrolysis oil from the waste synthetic resin by the apparatus of the present invention will be described in more detail as follows.
First, the cooling water is supplied to the
Then, the
When the operation ready state is completed, the
When the thermal power through the
When the
The
At this time, the supplied cooling water is supplied to the cooling tank
As the
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The combustible gas thus generated flows into the
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When the
As described above, the combustible gas flowing into the
The combustible gas passing through the multistage cooling
As described above, the combustible gas passing through the primary
The combustible gas that has passed through the third
The reason why the cooling water is injected in multiple stages as described above is that in order to cool the combustible gas, the cooling water is brought into contact with the area of contact with the combustible gas within a maximum range to gradually condense the heat and to condense the pyrolysis gas. to be.
As described above, when the temperature of the combustible gas passing through the fifth
In this case, the cooling water and the changed thermal cracking oil passing through the cooling
The residual uncompacted combustible gas, which has not undergone the pyrolysis flow path change, is discharged through the
The reason why the U-shaped
As described above, the cooling water collected in the
In the present invention as described above, in the thermal decomposition of the waste synthetic resin, heat is directly applied to the thermal
The amount of the lead (Pb) used as the metal catalyst in the
For example, the
When the thermal
The above-mentioned caulking phenomenon does not cause 100% caulking phenomenon at the bottom of the
The use of about 1,500 kg of lead in the
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1: rotary blade 2: rotary shaft
10: Pyrolysis heating tank 12: Communicating tube
20: primary cooling tank 21: primary spiral nozzle
22: Second spiral nozzle 23: Third spiral nozzle
24: 4th spiral nozzle 25: 5th spiral nozzle
30: Cooling water outlet pipe 31: Primary gas inlet pipe
32: secondary gas inlet pipe 33: tertiary gas inlet pipe
34: fourth gas inlet pipe 34: fifth gas inlet pipe
40: Secondary cooling tank 41: Non-condensing gas backflow prevention pipe
42: gas discharge pipe 43: U-shaped bent portion
50: Storage tank 60: Gas combustion chamber
70: Filter device 80: Water cooler
Claims (5)
A speed reducer 6 which combines a small chain gear 4 for operating the alternate gear 3 as a chain 5,
A primary cooling tank 20 connected to the communicating pipe 12 connected to the upper end of the pyrolysis heating tank 10,
A primary gas inflow pipe 31 in which a primary helical injection port 21 is fixed so as to inject cooling water on a horizontal line,
A secondary gas inflow pipe 32 which is fixed to a secondary spiral jet opening 22 which horizontally joins the primary gas inflow pipe 31 and injects cooling water on a vertical line,
A tertiary gas inflow pipe 33 which is fixed to the secondary gas inflow pipe 32 and fixes a tertiary helical jet opening 23 for injecting cooling water on a horizontal line,
A fourth gas inflow pipe 34 having a fourth helical injection port 24 fixed horizontally to the third gas inflow pipe 33 and injecting cooling water on a vertical line,
A cooling water discharge pipe 30 having a multi-stage structure constituted by a fifth-order gas inflow pipe 35 having a fifth-order helical injection port 25 fixed vertically to the fourth gas inflow pipe 34 and injecting cooling water on a horizontal line,
A secondary cooling tank 40 provided with the cooling water discharge pipe 30 on the side,
A storage tank 50 for storing pyrolysis oil supplied from a non-condensing gas backflow prevention discharge pipe 41 connected to a side surface of the secondary cooling tank 40,
A gas combustion chamber 60 connected to the gas discharge pipe 42 coupled to the upper end of the secondary cooling tank 40 and a filter installed at the lower end of the secondary cooling tank 40 for filtering impurities contained in the discharged water A device 70 and a water pump 71 for circulating water,
And a water cooler (80) for cooling the cooling pipe (81) for connecting the primary water supply pipe (72) connected to the amphibious pump (71) Manufacturing apparatus.
When the U-shaped bent portion 43 of the uncompacted gas backflow prevention discharge pipe 41 is placed and the water level of the pyrolysis oil collected in the secondary cooling tank 40 falls below the non-condensed gas backflow prevention discharge pipe 41, So that it is prevented from flowing back into the storage tank (50).
(Pb) used as a metal catalyst is further charged into the pyrolysis heating tank (10).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020150151220A KR101729859B1 (en) | 2015-10-28 | 2015-10-28 | Pyrolysis oil production unit using waste plastics |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020150151220A KR101729859B1 (en) | 2015-10-28 | 2015-10-28 | Pyrolysis oil production unit using waste plastics |
Publications (1)
Publication Number | Publication Date |
---|---|
KR101729859B1 true KR101729859B1 (en) | 2017-04-25 |
Family
ID=58703481
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1020150151220A KR101729859B1 (en) | 2015-10-28 | 2015-10-28 | Pyrolysis oil production unit using waste plastics |
Country Status (1)
Country | Link |
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KR (1) | KR101729859B1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR102322943B1 (en) * | 2020-09-04 | 2021-11-09 | 정용훈 | Equipment to produce oil energy by incinerating flammable waste |
-
2015
- 2015-10-28 KR KR1020150151220A patent/KR101729859B1/en active IP Right Grant
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR102322943B1 (en) * | 2020-09-04 | 2021-11-09 | 정용훈 | Equipment to produce oil energy by incinerating flammable waste |
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