KR101727028B1 - Composition for powder typed make up cosmetics for eye containing amorphous silica and its manufacturing method - Google Patents

Abstract

The present invention relates to a powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient and a method for producing the same. More specifically, the present invention relates to a powder type eye makeup cosmetic composition comprising amorphous silica, And is a powder type eye makeup containing an amorphous silica as an active ingredient which improves the adhesion and adhesion of the skin by mixing the aqueous component in the amorphous silica with the external powder and converting it into a liquid or gel form upon application to the skin, To a cosmetic composition and a process for producing the same.
The present invention relates to a silica base, which comprises an amorphous silica or an amorphous silica-based derivative, or a mixture of amorphous silica and amorphous silica-based derivative, wherein the amorphous silica base has a silica base in which an aqueous phase component is collected and a powder is adsorbed to the outside of the amorphous silica base, Or an amorphous silica-based derivative or a mixture of amorphous silica and amorphous silica-based derivative is contained in an amount of 1 to 20% by weight, the aqueous phase component comprises a silica base containing 80 to 99% by weight, By weight, and the powder is 30 to 70% by weight.
In the present invention, a water-soluble moisturizing component is added to a stirrer and a mixture of amorphous silica or an amorphous silica-based derivative or amorphous silica and an amorphous silica-based derivative is added while stirring, and stirred at 1,000 to 3,000 rpm for 3 to 6 hours to prepare a silica base (Pearl and extender pigment) is added to the silica base produced in the step (S10), and stirring is performed at a speed of 100 to 300 rpm for 10 to 30 minutes (S20) do.

Description

TECHNICAL FIELD The present invention relates to a powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient and a method for producing the same.

The present invention relates to a powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient and a method for producing the same. More specifically, the present invention relates to a powder type eye makeup cosmetic composition comprising amorphous silica, The present invention relates to a powder type eye makeup cosmetic composition containing amorphous silica serving as a carrier of the present invention as an active ingredient and a method for producing the same.

In addition, the present invention relates to a powder type eye makeup cosmetic composition comprising amorphous silica as an active ingredient, which improves adhesion and adhesion of the skin by mixing an aqueous phase component in the amorphous silica with an external powder and converting into a liquid phase or a gel phase, To compositions and methods of making the same.

Colored cosmetics are used to change the appearance beautifully and to make the skin look beautiful. It is divided into base make-up used to uniformize the skin color of the whole face, cover of defects, and point make-up to partially enhance the three-dimensional feeling such as lips, eyes and nails. Base make-up consists of make-up base, foundation and powder. Point make-up consists of lips cosmetics and eye make-up cosmetics.

Eye make-up cosmetics include mascara, eyeliner, eye shadow, and eyebrow pencil. Eye make-up cosmetics are applied around the eyes to emphasize the outline of the eyes and to give beauty to the eyes.

In general, eye-make cosmetics should be free of irritation to the eyes because they are applied around eyes, and should not be buried immediately after application due to rapid drying speed, and should not be spread easily on sweat, tears and oil, There is no feeling of burden when using it, there is little possibility of contamination with microorganisms, and it should be easily cleared when cleansing.

For example, Korean Patent Registration No. 10-1163180 discloses an eye makeup cosmetic composition, which relates to a method for preparing a dome shaped powder eye shadow cosmetic composition, A calcium silicate-oil binder mixing step in which the calcium silicate-oil binder is uniformly mixed with calcium silicate, which is an inorganic thickening agent, and a pearl powder phase containing a carnauba wax-treated mica while stirring the mixed calcium silicate- And an additive including at least one selected from the group consisting of an antiseptic agent and an antiseptic agent, and pulverizing the resultant into a dome shape. The present invention also relates to a method for producing a dome shaped powder eye shadow cosmetic composition.

Since the conventional drying process is not carried out in the conventional art, the decrease in the coloring power due to drying can be reduced.

However, there is a problem that the pearl is poured into the extender pigment and the pearl is lowered by proceeding the papermaking process in the molding step. Since the product of the prior art is made of powder, There are disadvantages.

In order to solve the above-mentioned conventional problems, Korean Patent Registration No. 10-1140092 discloses a conventional art for improving pearl feeling, which is related to an eye makeup cosmetic composition with improved pearl feeling and a method for producing the same. , The pearl was improved by containing at least 65 wt% of pearl based on the total weight of the composition and the pearl feeling was improved by containing at least 20 wt% of the oil binder. Compositions and methods of making the same.

The above-mentioned prior art has solved the problems of lowering the pearlness and the dusting of the powder, but it has a problem that the adhesive force is decreased when applying the skin because of the state of the dry powder not containing water.

In addition, the prior art has a disadvantage in that it contains a small amount of extender pigment and thus can not stabilize the pearl with a large particle size, thereby giving a feeling of being scratched when applying the skin.

In addition, pigments such as pearls and extender pigments have a property of being settled by gravity and have an effect on the interface depending on the surface properties of the pigment. For this reason, when the content of pearl and extender pigment in the formulation exceeds 50%, the dispersing power of pearl drops sharply and the pearl precipitates in the product. In addition to not only deteriorating the stereoscopic effect upon eye creaming due to the above-mentioned problems, but also in terms of feeling of use, the pearl is sinking in a large amount, so that the color development and gloss effect of pearl can not be obtained.

SUMMARY OF THE INVENTION The present invention has been conceived to solve the problems as described above, and it is an object of the present invention to provide a method for manufacturing a toner, which comprises capturing an aqueous phase component in amorphous silica and adsorbing the powder to the outside of the amorphous silica, It is an object of the present invention to provide a powder type eye makeup cosmetic composition and a process for producing the same.

In addition, the present invention relates to a powder type eye makeup cosmetic composition comprising amorphous silica as an active ingredient, which improves adhesion and adhesion of the skin by mixing an aqueous phase component in the amorphous silica with an external powder and converting into a liquid phase or a gel phase, And to provide a method for preparing the same.

It is another object of the present invention to provide amorphous silica, which is an amorphous silica whose active ingredient is amorphous silica in which the pearl and sieving pigment are prevented from settling due to the adsorption force of amorphous silica, whereby the pearl is uniformly present in the cosmetic composition, It is an object of the present invention to provide a powder type eye makeup cosmetic composition and a process for producing the same.

The present invention is characterized in that a silica base in which an amorphous silica or an amorphous silica-based derivative or a mixture of an amorphous silica and an amorphous silica-based derivative is selected to collect an aqueous phase component and a powder is adsorbed to the outside of the silica base.

In the present invention, the amorphous silica or amorphous silica-based derivative or a mixture of amorphous silica and amorphous silica-based derivative is contained in an amount of 1 to 20% by weight, and the aqueous phase component is contained in a silica base in an amount of 80 to 99% by weight .

In the present invention, the silica base is contained in an amount of 30 to 70% by weight, and the powder is contained in an amount of 30 to 70% by weight.

In addition, a water-soluble moisturizing component is added to a stirrer and a mixture of amorphous silica or an amorphous silica-based derivative or amorphous silica and an amorphous silica-based derivative is added while stirring, and stirred at 1,000 to 3,000 rpm for 3 to 6 hours to prepare a silica base (Step S10); and adding powder (pearl and extender pigment) to the silica base produced in step S10 and stirring the mixture at a speed of 100 to 300 rpm for 10 to 30 minutes (step S20) .

As described above, the powder type eye makeup cosmetic composition comprising the amorphous silica as an active ingredient according to the present invention and the method for producing the same, collects the aqueous phase components in the amorphous silica and adsorbs the powder to the outside of the amorphous silica, The present invention provides an effect of providing a powder type eye makeup cosmetic composition and a process for producing the same.

Also, the present invention provides a powder type eye makeup cosmetic composition and a method for manufacturing the same, which improves adhesion and adhesion of skin by converting an aqueous component in amorphous silica and an external powder into a liquid or gel form upon application to skin .

In addition, the present invention provides a powder type eye makeup cosmetic composition in which the pearl and the extender pigment are prevented from being settled by the adsorption force of the amorphous silica, whereby the pearl is uniformly present in the cosmetic composition and the light scattering effect of the pearl and pearl is improved. There is an effect of providing a manufacturing method thereof.

BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a schematic diagram of an amorphous silica, an aqueous phase component, and a powder according to the present invention. FIG.
2 is a schematic diagram of an amorphous silica-based derivative, an aqueous phase component, and a powder according to the present invention.
3 is a schematic diagram of a mixture of an amorphous silica and an amorphous silica-based derivative, an aqueous phase component, and a powder according to the present invention.
4 is a schematic diagram showing that the aqueous phase component according to the present invention is passed between amorphous silicas.
FIG. 5 is a schematic view showing the amorphous silica according to the present invention mixed with a water phase component to change into a liquid phase or a gel phase.
6 is a flowchart of a method of manufacturing a powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient according to the present invention.

Disclosure of the Invention As a result of intensive research to achieve the above object, the present invention has developed a method for manufacturing a powder eye makeup cosmetic composition containing amorphous silica as an active ingredient, A powder type eye makeup cosmetic composition comprising silica as an active ingredient is characterized in that an aqueous phase component is collected inside amorphous silica and the powder is adsorbed to the outside of the amorphous silica and an aqueous phase component in the amorphous silica and an external powder are mixed, Or gel-like form, thereby improving the adhesion and adhesion of the skin, thereby completing the present invention.

A powder type eye makeup cosmetic composition comprising amorphous silica as an active ingredient according to the present invention will be described with reference to the accompanying drawings.

Fig. 1 is a schematic view of a powder eye makeup cosmetic composition containing amorphous silica as an active ingredient according to the present invention, Fig. 2 is a schematic diagram of an amorphous silica-based derivative, an aqueous phase component and a powder according to the present invention, FIG. 4 is a schematic view showing that a water component according to the present invention is passed through amorphous silica, and FIG. 5 is a schematic view showing an amorphous silica and an aqueous phase component according to the present invention. Mixed into a liquid or gel form.

The present invention relates to a silica base 10 in which any one of amorphous silica 11 or an amorphous silica-based derivative 12 or a mixture 13 of an amorphous silica and an amorphous silica-based derivative is selected to collect an aqueous phase component 14, And the powder 20 is adsorbed to the outside of the silica base 10.

The amorphous silica-based derivative 11, the amorphous silica-based derivative 12 and the mixture 13 of the amorphous silica and the amorphous silica-based derivative serve as a carrier for the water-based component 14 and the powder 20, And the solid powder 20 coexist.

The amorphous silica-based derivative 12 and the mixture 13 of the amorphous silica and the amorphous silica-based derivative serve as a semi-permeable membrane to freely move the aqueous phase component 14, (11), amorphous silica-based derivatives (12), and mixtures of amorphous silica and amorphous silica-based derivatives (13).

In addition, since the powder 20 is adsorbed to the outside of the amorphous silica 11, the amorphous silica-based derivative 12, and the mixture 13 of the amorphous silica and the amorphous silica-based derivative, the pearl contained in the powder 20, It prevents the sedimentation of the pigment, improves the color development of pearl and light scattering effect, and gives the pearl luster stability.

As shown in FIG. 1, when the amorphous silica 11 and the aqueous phase component 14 are mixed, the aqueous phase component 14 is impregnated into the amorphous silica 11. The amorphous silica 11 and the aqueous phase component 14 are bonded to each other by the intermolecular attraction so that the aqueous phase component 14 is trapped in the amorphous silica 11 to be present as the silica base 10, Is adsorbed to the outside of the amorphous silica (11) to form a powder type eye makeup cosmetic composition.

As shown in FIGS. 2 and 3, an amorphous silica-based derivative 12 or a mixture 13 of an amorphous silica 11 and an amorphous silica-based derivative 12 can be used in place of the amorphous silica 11, It is preferable to use a mixture (13) of amorphous silica (11) and amorphous silica-based derivative (12).

4 and 5, the water component 14 is passed through the amorphous silica 11 and the water component 14 and the powder 20 outside the amorphous silica 11 are mixed to form a liquid or a gel .

As a result, the cosmetic composition can be converted into a liquid or a gel to significantly reduce dusting, and the adhesion and adhesion of the skin can be improved.

The amorphous silica (11) and the amorphous silica-based derivative (12) have an average particle size of 6.0 to 10 탆 and an oil absorption of 5 to 10 ml / g.

If the average particle size of the amorphous silica 11 and the amorphous silica-based derivative 12 is less than 6.0 μm, the attractive force between the water component 14 and the molecule is weak and the water component 14 can not be captured, If the average particle size exceeds 10 μm, the gap between the amorphous silica 11 and the amorphous silica-based derivative 12 becomes narrow, so that the water component 14 can not pass through the gap and the powder 20 ). ≪ / RTI >

If the amount of oil absorption of the amorphous silica 11 and the amorphous silica-based derivative 12 is less than 5 ml / g, the particle size of the amorphous silica 11 and the amorphous silica-based derivative 12 becomes large, If the amount of oil absorption is more than 10 ml / g, the amorphous silica 11 and the amorphous silica-based derivative 12 have a small particle size. Therefore, the adsorption force of the amorphous silica-based derivative 12 and the powder 20 is low, There is a problem that the pearl and extender pigment are settled.

The amount of oil absorption refers to the amount (cc / 100 g) of amiin oil required to form a paste having a certain degree of fluidity when the pigment is added to refined linseed oil. Oil absorption is inversely proportional to the particle size of the pigment, so the smaller the particle size of the pigment, the greater the oil absorption.

It is preferable that the amorphous silica-based derivative (12) is composed of one kind or a mixture of two or more kinds selected from the group consisting of silica dimethicone silylate, silica dimethyl silylate and silica silylate.

The water phase component (14) is a water-soluble moisturizing component and is a water-soluble moisturizing component which is one kind selected from the group consisting of glycerin, diglycerin, propylene glycol, butyleneglycol, polyethylene glycol, sorbitol, trehalose, raffinose, hyaluronic acid, Or a mixture of two or more.

In the silica base 10, a conventional cosmetic composition may be added to the skin cosmetic composition as required. Examples include, but are not limited to, preservatives, thickeners, ethanol, sodium chloride, and salts such as sodium-PCA.

The powder 20 is composed mainly of a pearl and an extender pigment, and is a mixture of one or more selected from the group consisting of mica / titanium dioxide, borosilicate / titanium dioxide, and synthetic fluorofluorophosphate / titanium dioxide .

The silica base 10 contains 1 to 20% by weight of a mixture (13) of amorphous silica (11) or amorphous silica-based derivative (12) or amorphous silica (11) and amorphous silica-based derivative (12) (14) 80 to 99% by weight.

 If the content of the amorphous silica (11) or the amorphous silica-based derivative (12) or the mixture (13) of the amorphous silica-based derivative (12) and amorphous silica-based derivative (12) is less than 1% by weight based on the total weight of the silica base The water component 14 can not be sufficiently collected and a moisturizing effect can not be obtained. When it exceeds 20% by weight, the feeling of use becomes stiff and the feeling of dryness is felt.

If the content of the water-based component (14) is less than 80% by weight with respect to the total weight of the silica base (10), there is a problem that the water- And the like.

In the powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient according to the present invention, the silica base (10) is contained in an amount of 30 to 70% by weight based on the total weight of the cosmetic composition, and the powder (20) And 30 to 70% by weight.

If the amount of the silica base 10 is less than 30% by weight based on the total weight of the cosmetic composition, there is a problem in that the adsorption force of the silica base 10 with the powder 20 is low and sedimentation of pearl and extender pigment contained in the powder 20 occurs. If the amount is more than 70% by weight based on the total weight, the content of the pearl is relatively reduced, the color development of the pear is lowered, and the phenomenon of aggregation with the powder 20 occurs, and the stability of the formulation is lowered.

If the amount of the powder 20 is less than 30% by weight based on the total weight of the cosmetic composition, there is a problem that the content of pearl contained in the powder 20 is so small that the pearl feeling is lowered and the light scattering effect of pearl is also lowered. If the content is more than 70% by weight, a problem of dusting on the occasion of makeup occurs, and a heavy feeling is generated around the eye, resulting in a problem of poor feeling of use.

A method for producing a powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient according to the present invention will be described with reference to the accompanying drawings.

6 is a flowchart of a method of manufacturing a powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient according to the present invention.

Hereinafter, preferred embodiments of the present invention will be described with reference to the accompanying drawings, and it is to be understood that the present invention is not limited thereto.

The present invention relates to a method for preparing a mixture (13) of amorphous silica (11) or amorphous silica-based derivative (12) or amorphous silica (11) and amorphous silica-based derivative (12) (S10) of preparing a silica base (10) by stirring the mixture at a speed of 1,000 to 3,000 rpm for 3 to 6 hours; and a step (S10) of adding a powder (20) to the silica base (10) And stirring the mixture at a rate of 100 to 300 rpm for 10 to 30 minutes (S20).

The manufacturing method of the present invention will be described separately for each step.

A water-based moisturizing component (14) is added to the agitator and the mixture (13) of amorphous silica (11) or amorphous silica-based derivative (12) or amorphous silica (11) and amorphous silica- Followed by stirring at a rate of 1,000 to 3,000 rpm for 3 to 6 hours to prepare a silica base 10 (S10).

The step (S10) of producing the silica base 10 is preferably carried out by mixing the aqueous component ((C)) in the mixture 13 of amorphous silica 11 or amorphous silica-based derivative 12 or amorphous silica 11 and amorphous silica- 14). ≪ / RTI >

The mixture 13 of the amorphous silica 11 or the amorphous silica-based derivative 12 or the amorphous silica 11 and the amorphous silica-based derivative 12 is added to the silica base 10 in an amount of 1 to 20 wt% , And the aqueous phase component (14) is added in an amount of 80 to 99% by weight.

It is necessary to perform the above speed range so that the aqueous phase component 14 is impregnated into the amorphous silica 11 or the amorphous silica-based derivative 12 or the mixture 13 of the amorphous silica-based derivative 11 and the amorphous silica- 10) can be produced.

If the stirring speed is less than 1,000 rpm, the water component 14 may take a long time to be collected. When the stirring speed is more than 3,000 rpm, the water component 14 may be amorphous silica 11 or amorphous silica- 11) and the amorphous silica-based derivative (12) in the mixture (13), thereby deteriorating the moisturizing effect.

If the agitation time is less than 3 hours, the amount of impregnation of the water phase component (14) is insufficient to obtain a moisturizing effect. If the agitation time exceeds 6 hours, the water phase component (14) and the amorphous silica (11) There is a problem that the mixture (13) of the amorphous silica (11) and the amorphous silica-based derivative (12) is aggregated and becomes creamy.

The powder 20 is put into the silica base 10 manufactured in the step S10 and stirred at a speed of 100 to 300 rpm for 10 to 30 minutes.

The step (20) is a step in which the powder is adsorbed to the outside of the amorphous silica (11) or the amorphous silica-based derivative (12) or the mixture (13) of the amorphous silica (11) and the amorphous silica- To prepare a composition.

The powder 20 contains a pearl and an extender pigment as main components and is a mixture of one or more selected from the group consisting of mica / titanium dioxide, borosilicate / titanium dioxide, and synthetic fluorofluorophosphate / titanium dioxide It is preferable to further comprise

 In step 20, the silica base 10 prepared in step 10 is added to the cosmetic composition in an amount of 30 to 70% by weight based on the total weight of the cosmetic composition. The powder 20 is added to the cosmetic composition in an amount of 30 to 70 wt% %.

The silica base 10 and the powder 20 are stirred at a speed of 100 to 300 rpm so that the powder 20 is mixed with the amorphous silica 11 or the amorphous silica derivative 12 or the amorphous silica 11 and the amorphous silica- (13) of the mixture (12).

When the agitation speed is less than 100 rpm, the powder 20 is not uniformly adsorbed, so that the settling phenomenon of the powder 20 occurs. As a result, the color development and gloss effect of the pearl contained in the powder 20 is lowered. If the amount is more than 300 rpm, the amount of the powder 20 to be removed is larger than the amount of the powder 20 to be adsorbed, thereby deteriorating the stability of the powder formulation.

If the agitation time is less than 10 minutes, the powder 20 can not be adsorbed evenly and can not be manufactured into a powder type formulation. If the agitation time is less than 30 minutes, the appearance of the product is not uniform and a rough appearance is shown.

Hereinafter, examples, comparative examples and test examples of the present invention will be described in detail.

The following examples, comparative examples and test examples are illustrative of the present invention, and the present invention is not limited to the following examples, comparative examples and test examples.

< Example  1 > A process for preparing a powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient Example  One

Example 1 of the preparation of a powder type eye makeup cosmetic composition containing the amorphous silica of the present invention as an active ingredient was prepared by the following production steps in terms of the content of the composition shown in Table 1.

(S10): 1 to 8 of the raw materials listed in Table 1 were added to a stirrer at the blending ratios shown in Table 1 and mixed to prepare an aqueous phase. Then, the raw material 15 shown in Table 1 was added to the agitator in the mixing ratio shown in Table 1, and the mixture was stirred at 2,000 rpm for 4 hours to prepare a silica base in which the aqueous phase components were collected.

(S20): 22-23 of the raw materials listed in Table 1 were added to the silica base prepared in the step (10) at the compounding ratios shown in Table 1 and stirred at 100 rpm for 20 minutes to prepare a cosmetic composition.

At this time, a powder type eye makeup cosmetic composition comprising an amorphous silica having an outer layer of amorphous silica and an outer layer of amorphous silica having an outer appearance of a powdery appearance as an active ingredient was prepared.

< Example  2 > The preparation of a powder type eye makeup cosmetic composition containing amorphous silica as an active ingredient Example  One

Example 2 of the preparation of a powder type eye makeup cosmetic composition containing the amorphous silica of the present invention as an active ingredient was prepared through the following production steps with the contents of the compositions shown in Table 1 below.

(S10): 1 to 8 of the raw materials listed in Table 1 were added to a stirrer at the blending ratios shown in Table 1 and mixed to prepare an aqueous phase. Then, the raw material 16 described in Table 1 was added to the agitator in the mixing ratio shown in Table 1, and the mixture was stirred at 2,000 rpm for 4 hours to prepare a silica base in which the aqueous phase components were collected.

(S20): 22-23 of the raw materials listed in Table 1 were added to the silica base prepared in the step (10) at the compounding ratios shown in Table 1 and stirred at 100 rpm for 20 minutes to prepare a cosmetic composition.

In this case, the cosmetic composition contains a powdery eye (amorphous silica) having amorphous silica having an outer appearance of powdery appearance and an outer layer of amorphous silica-based derivative in the form of an amorphous silica-based derivative A makeup cosmetic composition was prepared.

< Example  3> Manufacturing of powder-type eye makeup cosmetic composition containing amorphous silica as an active ingredient Example  3

Example 3 of the preparation of a powder type eye makeup cosmetic composition containing the amorphous silica of the present invention as an active ingredient was prepared through the following production steps with the contents of the compositions shown in Table 1 below.

(S10): 1 to 8 of the raw materials listed in Table 1 were added to a stirrer at the blending ratios shown in Table 1 and mixed to prepare an aqueous phase. Then, the raw material 17 described in Table 1 was added to the agitator at the blending ratio shown in Table 1, and the mixture was stirred at 2,000 rpm for 4 hours to prepare a silica base in which the aqueous phase components were collected.

(S20): 22-23 of the raw materials listed in Table 1 were added to the silica base prepared in the step (10) at the compounding ratios shown in Table 1 and stirred at 100 rpm for 20 minutes to prepare a cosmetic composition.

At this time, the cosmetic composition contains amorphous silica, which is a mixture of amorphous silica and an amorphous silica-based derivative, and amorphous silica having a powder-like appearance apparently surrounded by a powder outside the mixture of amorphous silica and amorphous silica-based derivative To prepare a powder type eye makeup cosmetic composition.

< Comparative Example  1 > for the preparation of a pimple eye makeup cosmetic composition Comparative Example  One

Comparative Example 1 of the preparation of the tabular eye makeup cosmetic composition of the present invention was prepared through the following production steps with the contents of the compositions shown in Table 1 below.

Nine to twelve components of the raw materials listed in Table 1 were uniformly mixed at the compounding ratios shown in Table 1 to prepare an oil phase.

18 to 23 components in the raw materials listed in Table 1 were uniformly mixed at the compounding ratios shown in Table 1 to prepare powder phases.

Thereafter, the oil phase was gradually added to the mixture while stirring the powder phase, mixed, and the mixed cosmetics were placed in an aluminum dish to prepare a tabular eye makeup cosmetic composition Comparative Example 1.

< Comparative Example  2> Normal Powder Eye Make-up Cosmetics  Of the preparation of the composition Comparative Example  2

Comparative Example 2 of the general powder type eye makeup cosmetic composition of the present invention was prepared through the following production steps with the composition shown in Table 1 below.

Twelve to seventeenth components in the raw materials listed in Table 1 were uniformly mixed at the compounding ratios shown in Table 1 to prepare oil phases.

22 to 23 components in the raw materials listed in Table 1 were uniformly mixed at the compounding ratios shown in Table 1 to prepare powder phases.

Thereafter, while stirring the powder phase, the oil phase was gradually added and mixed to prepare a general powder type eye makeup cosmetic composition Comparative Example 2.

< Comparative Example  3> Powder type eye makeup containing an excess of a mixture of amorphous silica and amorphous silica-based derivative as an active ingredient Cosmetics  Of the preparation of the composition Comparative Example  3

In the present invention, Comparative Example 3 for the preparation of a powder type eye makeup cosmetic composition containing a mixture of an amorphous silica and an amorphous silica-based derivative as an active ingredient was prepared by the following production steps in terms of the content of the composition shown in Table 1.

(S10): 1 to 8 of the raw materials listed in Table 1 were added to a stirrer at the blending ratios shown in Table 1 and mixed to prepare an aqueous phase. Then, the raw material 17 described in Table 1 was added to the agitator at the blending ratio shown in Table 1, and the mixture was stirred at 2,000 rpm for 4 hours to prepare a silica base in which the aqueous phase components were collected.

(S20): 22-23 of the raw materials listed in Table 1 were added to the silica base prepared in the step (10) at the compounding ratios shown in Table 1 and stirred at 100 rpm for 20 minutes to prepare a cosmetic composition.

Unit: wt% ingredient Example
One Example
2 Example
3 Comparative Example
One Comparative Example
2 Comparative Example
3 One Purified water to 100 to 100 to 100 - to 100 2 glycerin 3 3 3 - 3 3 Propylene glycol 4 4 4 - 4 4 Butylene glycol One One One - One 5 Polyethylene glycol 2 2 2 - 2 6 Sorbitol One One One - One 7 Trehalose One One One - One 8 Hyaluronic acid 0.5 0.5 0.5 - 0.5 9 Caprylic / capric triglyceride - - - 3 3 - 10 Cetyl hexanoate - - - 4 4 - 11 Diisostearyl malate - - - 6 6 - 12 Hydrogenated polyisobutene - - - 2 2 - 13 Dimethicone - - - - 2 - 14 Phenyl trimecicone - - - - 2 - 15 Amorphous silica 10 - - - - - 16 Silica dimethicone silylate - 10 - - - - 17 Amorphous silica + silica dimethicone silylate - - 10 - - 30 18 Talc - - - 20 20 - 19 Mica - - - to 100 to 100 - 20 Boron nitride - - - 3 3 - 21 nylon - - - 3 3 - 22 Mica / Titanium Dioxide 20 20 20 20 20 20 23 Borosilicate / titanium dioxide 30 30 30 30 30 30

< Test Example  >

The compositions of Examples 1 to 3 and Comparative Examples 1 to 3 were used for 50 to 20, 30 years old female for 7 to 10 days, and the results of use were compared and evaluated. The sensory evaluations were as follows: 1 (very unsatisfactory) to 10 (very satisfied), and the results are shown in Table 2.

Evaluation items Example
One Example
2 Example
3 Comparative Example
One Comparative Example
2 Comparative Example
3 Pearl 9.1 9.6 9.7 6.8 7.1 7.8 Feeling 8.9 9.3 9.8 7.1 7.9 7.6 Moisturizing property 9.3 9.4 9.6 6.7 7.5 7.1 Adhesion 9.3 9.3 9.6 6.3 6.9 7.5 Persistence 8.8 9.3 9.8 6.5 7.3 7.3

Examples 1 to 3: Powder type eye makeup cosmetic composition using the silica base of the present invention

Comparative Example 1: Tabular eye makeup cosmetic composition

Comparative Example 2: General powder type eye makeup cosmetic composition

Comparative Example 3: Powder type eye makeup cosmetic composition using a mixture of excessive amorphous silica and amorphous silica-based derivative

In Comparative Example 1, the tableting process was introduced. When the cosmetic composition was tableted, it was confirmed that the pearl was poured into the extender pigment to reduce the pearl feeling, thereby lowering the feeling of use. In addition, Comparative Example 1 did not contain an aqueous phase component, and it was found that dusting on application to the skin was increased.

Comparative Example 2 is composed of an oil component and an extender pigment, so that the skin is dried when applied to the skin. In addition, when the content ratio of pearl and extender pigment exceeds 50% by weight, the dispersing power of pearl drops sharply, resulting in sedimentation of the pearl product. As a result of the above problems, it has been found that not only the three-dimensional feeling is deteriorated in eye make-up, but also the pearl feeling is lowered as the pearl sinks in a large amount in terms of feeling of use.

In Comparative Example 3, use of a mixture of an amorphous silica and an amorphous silica-based derivative in an excessively large amount makes the feeling and durability worse than those of Examples 1 to 3, and the moisturizing property upon application to the skin is reduced. Also, it was confirmed that the stability of the formulation was lowered due to occurrence of powder and aggregation phenomenon.

Therefore, the compositions of Examples 1 to 3 were satisfactory through sensory evaluation, and in particular, the feeling of feeling on the composition of Example 3 (a powder type eye makeup cosmetic composition containing a mixture of amorphous silica and amorphous silica-based derivative as an active ingredient) .

This is because the mixture of amorphous silica, amorphous silica-based derivative, amorphous silica and amorphous silica-based derivative uniformly adsorbs the water phase components and is uniformly adsorbed to the powder, so that pearlness, usability, moisturizing property, adhesion strength and persistence are superior to those of Comparative Examples 1 to 3 Could know.

It is to be understood that the present invention is not limited to the powder eye makeup cosmetic composition containing amorphous silica as an active ingredient and the method for producing the same, and the present invention is not limited to the above-described embodiments, It is to be understood that the present invention is not limited to the disclosed embodiments, but, on the contrary, is intended to cover various modifications and equivalent arrangements included within the spirit and scope of the appended claims and their equivalents. Lt; / RTI &gt;

10: silica base
11: amorphous silica
12: amorphous silica-based derivative
13: Mixture of amorphous silica and amorphous silica-based derivative
14: Water component
20: Powder

Claims (7)

The silica base 10 (10) in which the aqueous component (14) is collected by selecting any one of amorphous silica (11) or amorphous silica-based derivative (12) or amixture of amorphous silica (11) and amorphous silica- )Wow;
The powder 20 is adsorbed to the outside of the silica base 10,
The amorphous silica (11) and the amorphous silica-based derivative (12) have an average particle size of 6.0 to 10 탆, an oil absorption of 5 to 10 ml / g,
The silica base 10 is prepared by mixing the amorphous silica 11 or the amorphous silica-based derivative 12 or the mixture 13 of the amorphous silica 11 and the amorphous silica-based derivative 12 in an amount of 1 to 20 wt% %, And an aqueous phase component is contained in an amount of 80 to 99% by weight,
The silica base 10 is contained in an amount of 30 to 70% by weight based on the total weight of the powder type eye makeup cosmetic composition and the powder 20 is contained in an amount of 30 to 70% by weight based on the total weight of the powder type eye makeup cosmetic composition By weight of an amorphous silica as an active ingredient.
delete The method according to claim 1,
Wherein the amorphous silica-based derivative (12) is composed of a mixture of at least one member selected from the group consisting of silica dimethiconyl silicate, silica dimethyl silylate, and silica silylate, Type eye makeup cosmetic composition.
The method according to claim 1,
Wherein the water phase component (14) is at least one selected from the group consisting of glycerin, diglycerin, propylene glycol, butyleneglycol, polyethylene glycol, sorbitol, trehalose, raffinose, hyaluronic acid, Wherein the amorphous silica is used as an active ingredient.
delete The method according to claim 1,
The powder (20) is made of amorphous silica, which is a mixture of at least one member selected from the group consisting of mica / titanium dioxide, borosilicate / titanium dioxide, and synthetic fluorofluorophosphate / titanium dioxide as an active ingredient Which is a powder type eye makeup cosmetic composition.
A water-soluble moisturizing component (14) as a water-soluble moisturizing component is added to a stirrer and a mixture (13) of amorphous silica (11) or amorphous silica-based derivative (12) or amorphous silica (11) and amorphous silica- And stirring the mixture at a speed of 1,000 to 3,000 rpm for 3 to 6 hours to prepare a silica base 10 (S10);
The powder 20 is put into the silica base 10 manufactured in the step S10 and stirred at a speed of 100 to 300 rpm for 10 to 30 minutes,
The amorphous silica 11 or the amorphous silica-based derivative 12 or the mixture 13 of the amorphous silica 11 and the amorphous silica-based derivative 12 with respect to the total weight of the silica base 10 in the step (S10) 20% by weight of the water phase component, 80% by weight to 99% by weight of the water phase component,
In the step (S20), the silica base (10) is added in an amount of 30 to 70% by weight based on the total weight of the powder eye makeup cosmetic composition, and the powder (20) is added in an amount of 30 to 70% As an active ingredient, a powder type eye makeup cosmetic composition.

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