KR101684242B1 - Method of manufacturing for disoersing a room temperature of oil dispersion eye liners - Google Patents

Abstract

The present invention relates to a method for producing an oil-dispersed eyeliner at room temperature, and more particularly, to a method for producing an oil-dispersed eyeliner by dispersing volatile oil including isododecane and an agglomerating agent at a high temperature to form an agglomerate base, By maintaining the dispersion temperature at 40 ° C in the dispersion operation of the remaining raw materials, the volatility of isododecane volatilizing at 50 ° C is reduced to less than 5%, so that the content viscosity deviation does not occur, and due to the high temperature operation, The present invention relates to a method for producing a dispersion of an oil-dispersed eyeliner at room temperature by minimizing the volatilization of volatile oil such as dodecane, thereby enhancing the stability of the product.
In order to reduce volatilization of volatile oil such as isododecane due to the opening and closing of the raw material dispersion tank lid, the raw materials are integrally dispersed in the thickener base at one time to prevent the accumulation of powder during the dispersion of the raw material of the eyeliner, The present invention relates to a method for producing a dispersion of an oil-dispersed eyeliner at room temperature.
The present invention is characterized by comprising a step (S1) of dispersing an agglomerating agent and a volatile oil to obtain an increment base, and a step (S2) of collectively adding oil, powder and film forming agent to the agglomerate base and mixing .
In the present invention, it is preferable that the volatile oil in the step (S1) is at least one selected from the group consisting of isododecane, dimethylpolysiloxane, cyclomethicone, C10 to I10 isoparaffin, and isohexadecane .
In the present invention, it is preferable that the dispersion rotation speed is in the range of 2,000 to 5,000 rpm in the step (S1), the dispersion temperature is 70 to 100 ° C, and the dispersion time is 5 to 15 minutes.
Further, in the present invention, the step (S2) may be carried out at a temperature of 25 to 45 ° C., and the duration of the step is preferably 25 to 50 minutes.

Description

BACKGROUND OF THE INVENTION 1. Field of the Invention [0001] The present invention relates to a method for manufacturing a room-temperature dispersed eyeliner,

The present invention relates to a method for producing an oil-dispersed eyeliner at room temperature, and more particularly, to a method for producing an oil-dispersed eyeliner by dispersing volatile oil including isododecane and an agglomerating agent at a high temperature to form an agglomerate base, By maintaining the dispersion temperature at 40 ° C in the dispersion operation of the remaining raw materials, the volatility of isododecane volatilizing at 50 ° C is reduced to less than 5%, so that the content viscosity deviation does not occur, and due to the high temperature operation, The present invention relates to a method for producing a dispersion of an oil-dispersed eyeliner at room temperature by minimizing the volatilization of volatile oil such as dodecane, thereby enhancing the stability of the product.

In order to reduce volatilization of volatile oil such as isododecane due to the opening and closing of the raw material dispersion tank lid, the raw materials are integrally dispersed in the thickener base at one time to prevent the accumulation of powder during the dispersion of the raw material of the eyeliner, The present invention relates to a method for producing a dispersion of an oil-dispersed eyeliner at room temperature.

In general, Oriental women with relatively low eyelashes and relatively small eyes compared to western women have a greater desire to express their eyes more clearly, clearly and clearly by making eye cosmetics.

The eye cosmetics consist of an eyeliner and mascara. The function of the eyeliner is to more effectively emphasize the eyebrows by drawing a line to the eyes to make the eyes more clearly. The function of the mascara is to curl the eyelashes long, It is in emphasizing eyes.

Recently, as the social activities and outdoor activities of women have increased, the desire for persistence of makeup has been greatly increased. Therefore, a lot of products which are not erased even after a certain period of time after eye creams are applied, Many types of water-based eye cosmetics are on the market.

However, the above-mentioned water-in-oil type eye make-up product has a good waterproof effect but lacks oil resistance, and there is a problem that the eye make-up product is worn by sebum over time.

In order to solve the above-mentioned problems, Korean Patent Laid-Open No. 10-2011-0088179 discloses a method for producing an aqueous dispersion of an aqueous emulsion containing an aqueous solution of a hydrogenated rosinate based ester gum, wax, volatile oil, The present applicant's Korean Patent Publication No. 10-2013-0060570 discloses a cosmetic composition for eye-makeup for a water-in-oil type in which a water-dispersed water-in-oil type cosmetic composition is dispersed in a water- The composition of the present invention stably exists at the interface between the water phase and the oil phase with the cosmetic composition so that both the water and the sebum have excellent durability.

In the case of the conventional art, volatile oil such as isododecane is used as a solvent for dissolving the thickener.

However, in the conventional processes shown in the above-described conventional examples, the opening and closing of the lid of the raw material dispersion tank is repeated in the course of the raw material input during the high temperature operation, so that the volatile oil is volatilized and the volatile oil is volatilized, There is a problem that the powder is agglomerated in the course of the dispersion process, and there is a problem that powder suspended in the powder is not dispersed when the dispersion is completed.

Disclosure of Invention Technical Problem [8] Accordingly, the present invention has been made to solve the above-mentioned problems, and it is an object of the present invention to provide a process for preparing a thickener base by dispersing volatile oil including an isododecane and a thickener at high temperature, By maintaining the dispersion temperature at 40 ° C at the time of shaking, the volatility of isododecane volatilizing at 50 ° C is reduced to less than 5%, so that the content viscosity deviation does not occur, and volatile oils such as isododecane Dispersible eyeliner to minimize the volatilization of the product, thereby enhancing the stability of the product.

In addition, the present invention provides a method for manufacturing a room-temperature dispersed eyeliner for dispersing raw materials in a stepwise manner so as to prevent volatilization of volatile oil generated by repeating opening and closing of a lid of a raw material dispersion tank A method is provided.

The present invention is characterized by comprising a step (S1) of dispersing an agglomerating agent and a volatile oil to obtain an increment base, and a step (S2) of collectively adding oil, powder and film forming agent to the agglomerate base and mixing .

In the present invention, it is preferable that the volatile oil in the step (S1) is at least one selected from the group consisting of isododecane, dimethylpolysiloxane, cyclomethicone, C10 to I10 isoparaffin, and isohexadecane .

In the present invention, it is preferable that the dispersion rotation speed is in the range of 2,000 to 5,000 rpm in the step (S1), the dispersion temperature is 70 to 100 ° C, and the dispersion time is 5 to 15 minutes.

In addition, in the present invention, the rotation speed for mixing the thickener base, the oil, the powder and the film forming agent in the step (S2) is 1,000 to 5,000 rpm, the execution temperature is 25 to 45 ° C, and the execution time is 25 to 50 minutes desirable.

As described above, the method for producing the oil-dispersed eyeliner according to the present invention comprises dispersing the volatile oil including isododecane and the thickening agent at a high temperature to form a thickening base, and allowing the thickening base to stand at room temperature, By maintaining the dispersion temperature at 40 ° C during the dispersion operation, the volatility of isododecane volatilizing at 50 ° C is reduced to less than 5%, so that the viscosity of the content does not fluctuate, and isododecane Thereby minimizing volatilization of the volatile oil, thereby enhancing the stability of the product.

In order to prevent volatilization of volatile oil such as isododecane caused by repeating the opening and closing of the lid of the raw material dispersion tank at the time of dispersing the raw materials in stages, the raw materials are integrally dispersed in the base at the same time, Thereby minimizing the volatility of volatile oils such as isododecane, thereby preventing the accumulation of powder during the course of dispersing eye cosmetics, and preventing the suspension of powder from being left upon completion of dispersion.

BRIEF DESCRIPTION OF THE DRAWINGS Fig. 1 is a flow chart showing a method of producing a room-temperature dispersion of a oil-dispersed eyeliner according to an embodiment of the present invention.

An embodiment of a method of manufacturing a room-temperature dispersion of an oil-dispersed eyeliner according to the present invention will be described with reference to the accompanying drawings.

FIG. 1 is a flow chart showing a method of manufacturing a room-temperature dispersion of a oil-dispersed eyeliner according to an embodiment of the present invention.

Hereinafter, the present invention will be described in detail.

The present invention is characterized by comprising the steps of (S1) obtaining an incrementer base by dispersing an agitator and a volatile oil, and (S2) collectively adding oil, powder and film former to the agitator base and mixing them.

The manufacturing method of the present invention will be described separately in each step.

(S1) of dispersing the thickener and the volatile oil to obtain an increment base.

The thickener enhances the viscosity of the cosmetic product to maintain the shape of the cosmetic product stably. The enhancer is selected from the group consisting of high-branched olefin polymers, behenic and behenic derivatives, and polysaccharides It is preferable to use at least one of them.

The above-mentioned thickening agent effectively retains moisture, improves the dispersion stability of the eyeliner cosmetic, and minimizes the change with time. In addition, it has the effect of eliminating the problem of stickiness and dirtiness under eyes, which is a problem that occurs when using conventional natural wax, and improving eyeliner makeup persistence.

The volatile oil is preferably at least one selected from the group consisting of isododecane, dimethylpolysiloxane, cyclomethicone, C10 to I10 isoparaffin, and isohexadecane.

Since the raw material of the volatile oil includes the characteristics of the volatile oil and the characteristic of forming a thin film after volatilization, it is possible to improve the water resistance by forming a soft film film thinly at the time of eye make-up.

In addition, when an incrementer base is dispersed to prepare an incrementer base, there is an effect of delaying the aged change, which is a phenomenon in which the content solidifies with time.

In the step (S1), the dispersion rotation speed is 2,000 to 5,000 rpm, the dispersion temperature is 70 to 100 ° C, and the dispersion time is 5 to 15 minutes.

If the rotation speed, temperature, and time are less than 2,000 rpm, 70 ° C, and less than 5 minutes, there is a problem that the thickening agent does not completely dissolve and the thickener of the thickening agent remains. At 5,000 rpm, 100 ° C, The volatile oil is rapidly evaporated due to an increase in volatility, and the viscosity of the eyeliner formulation is lowered.

A step S2 of charging the oil, the powder and the film-forming agent into the thickener base in a batch manner and mixing them.

In order to reduce the volatilization of the volatile oil due to the opening and closing of the lid of the raw material dispersion tank, the raw materials are mixed at once in the thickener base so that the powder, And prevent the suspension of the powder from remaining when the dispersion is completed.

The oil serves to evenly blend the thickener base, the powder and the film-forming agent and may also be used as an emulsifying agent in the form of liquid paraffin, squalane, palm oil, avocado oil, jojoba oil, sesami oil, olive oil, castor oil, butyl myristate, Polybutene, polyisobutene, hydrogenated polyisobutene, various polyols, tri-2-ethylhexyl glycerin, triglyceride oil, myristyl lactate, octyl It is preferable to use at least one selected from the group consisting of dodecanol, diisostearyl malate and silicone oil.

Wherein the powder is selected from the group consisting of black iron oxide, yellow iron oxide, red iron oxide, ultramarine, ferric ferrocyanide, ferric ammonium ferrosyanide, chromium oxide green, chromium hydroxide green, titanium dioxide, zinc oxide, mica, carbon black, manganese violet , Aluminum powder, and carmine is preferably used.

The addition of the film forming agent eliminates the stickiness of the film former and serves to form a uniform film film. The film forming agent may be at least one selected from the group consisting of polyvinyl alcohol, polyvinyl acetate, polyvinyl pyrrolidone, ammonium acrylate copolymer, acrylate-ammonium methacrylate copolymer, polyvinyl acetate / acrylic acid copolymer, acrylic- Acrylate copolymer, an alkyl acrylate copolymer emulsion, and polyquaternium-4 are preferably used.

In step S2, the rotational speed for mixing the thickener base, the oil, the powder and the film forming agent is 1,000 to 5,000 rpm, the running temperature is 25 to 45 ° C, and the running time is 25 to 50 minutes.

If the rotational speed is less than 1,000 rpm and less than 25 minutes, the thickener base, oil, powder, and film forming agent are not mixed evenly and the powder remains in suspension. When the rotational speed is 5,000 rpm, Bubbles are generated in the thickener base, the oil, and the film forming agent due to the long rotation time, thereby lowering the viscosity of the eyeliner formulation and raising a problem that the defective rate of the eyeliner increases.

In addition, when the temperature is lower than 25 ° C., a part of the thickener base is hardened and oil, powder, and film forming agent are not mixed uniformly and powder agglomeration occurs. When the temperature is higher than 45 ° C., There is a problem that a deviation occurs.

Hereinafter, production examples, examples, comparative examples and test examples of the present invention will be described in detail.

The following Production Examples, Examples, Comparative Examples and Test Examples are merely illustrative of the present invention, and the present invention is not limited to the following Production Examples, Examples, Comparative Examples and Test Examples.

< Manufacturing example  > Incrementer  Dictionary of bass Manufacturing example

Prior to preparation of the oil-dispersed eyeliner room temperature dispersion of the present invention, the thickener was pre-prepared with an incremental base since high temperature dispersion was required.

The following Preparative Examples 1 to 4 are summarized in Table 1, and the hardener bases prepared according to Preparation Example 1 are excellent in hardness and thus used as an optimal thickener base in the present invention.

Advance manufacture of incremental base Base hardness Manufacturing method Discharge method Production Example 1 80 占 폚, 3000 rpm, 15 minutes dispersion After discharging at 80 캜, gradually cool to 30 캜 180 Production Example 2 80 占 폚, 3000 rpm, 15 minutes dispersion Instantaneous quench at 30 ℃ after discharge at 80 ℃ 157 Production Example 3 80 占 폚, 3000 rpm, 15 minutes dispersion Slowly cooling to 30 캜 138 Production Example 4 80 占 폚, 3000 rpm, 15 minutes dispersion Emitted while quenching momentarily at 30 ° C 125

< Example  > Oil dispersion Eyeliner  Of the room temperature dispersion producing method Example

An embodiment of the oil-dispersed eyeliner room temperature dispersion producing method of the present invention is characterized in that an oil, a powder, and a film forming agent are put into a batch of the thickener base prepared in Production Example 1, and the mixture is stirred at a rotational speed of 3000 rpm, To prepare an oil-dispersed eyeliner formulation.

< Comparative Example  > Oil dispersion Eyeliner  Of the room temperature dispersion producing method Comparative Example

In the comparative example of the oil-dispersed eyeliner room temperature dispersion producing method of the present invention, the film-forming agent is added to and dispersed in the thickener base prepared in Production Example 1, the powder is charged and dispersed, the oil is charged and dispersed, The oil dispersed eyeliner formulations were prepared at a speed of 3000 rpm, a temperature of 40 캜, and a time of 40 minutes.

< Test Example  > In the embodiment  Manufactured by Oil dispersion Eyeliner  Formulation In Comparative Example  Manufactured by Eyeliner  Formulation Test Example

In the eyeliner formulation prepared according to the comparative example, even when dispersed for 40 minutes, the dispersing power of the powder is lowered and the agglomerating agent and the powder are clustered. Since the raw material dispersion tank must be closed when each raw material is put in, The volatility increased from 40 to 50%, significantly reducing the amount of isododecane, which lowered the viscosity of the formulation to 124,500 cps.

In the eyeliner formulations prepared according to the examples, the dispersibility of the respective ingredients was improved, the agglomerating agent and the powder aggregation were eliminated, and the volatility of isododecane was lowered to less than 5%, and the viscosity of the formulation was increased to 209,000 cps. (Based on the viscosity of the eyeliner formulation: 150,000 cps)

Thus, it has been confirmed that the manufacturing method according to the embodiment is a method for suppressing the volatilization of isododecane to the utmost, and further, the viscosity of the formulation is improved and an excellent eyeliner product can be produced.

But the present invention is not limited to the above-described embodiments, but is merely an embodiment for the method of producing a room-temperature dispersion of oil-dispersed eyeliner. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined in the appended claims. will be.

Claims (6)

Olefin polymer, behenic acid and behenic acid derivatives, and polysaccharides, and a group consisting of isododecane, dimethylpolysiloxane, cyclomethicone, C10 to 11 isoparaffins and isohexadecane Dispersing volatile oil to select one or more to obtain an incremental base (Sl); And
(S2) the oil, the powder, and the film forming agent in a batch, and mixing the same,
In the step (S2), the rotational speed for mixing the thickener base, the oil, the powder and the film forming agent is 1,000 to 5,000 rpm, the running temperature is 25 to 45 ° C, and the running time is 25 to 50 minutes. A method for producing a dispersion eyeliner at room temperature.
The method according to claim 1,
In step S2, the oil is selected from the group consisting of liquid paraffin, squalane, palm oil, avocado oil, jojoba oil, sesame oil, olive oil, castor oil, butyl myristate, isopropyl myristate, cetyl myristate, isopropyl palmitate, Stearate, stearate, polybutene, polyisobutene, hydrogenated polyisobutene, various polyols, tri-2-ethylhexyl glycerin, triglyceride oil, myristyl lactate, octyldodecanol, diisostearyl malate and silicone oil Wherein the oil-dispersed eyeliner comprises at least one selected from the group consisting of the following.
The method according to claim 1,
In the step (S2), the powder is selected from the group consisting of black iron oxide, yellow iron oxide, red iron oxide, ultramarine, ferric ferrocyanide, ferric ammonium peroxide, chromium oxide green, chromium hydroxide green, titanium dioxide, zinc oxide, Wherein the oil-dispersed eyeliner comprises at least one selected from the group consisting of black, manganese violet, aluminum powder, and carmine.
The method according to claim 1,
In the step (S2), the film forming agent may be at least one selected from the group consisting of polyvinyl alcohol, polyvinyl acetate, polyvinyl pyrinolidone, ammonium acrylate copolymer, acrylate-ammonium methacrylate copolymer, Acrylate copolymer, an acrylate copolymer, an alkyl acrylate copolymer emulsion, and a polyquaternium-4 in an amount of at least 50% by weight based on the weight of the oil-dispersed eyeliner.
The method according to claim 1,
Wherein the dispersing rotational speed is from 2,000 to 5,000 rpm, the dispersing temperature is from 70 to 100 ° C, and the dispersing time is from 5 to 15 minutes in the step (S1).
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