KR101659300B1 - Composition of forming mask pack and forming mask pack using the same - Google Patents

Composition of forming mask pack and forming mask pack using the same Download PDF

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KR101659300B1
KR101659300B1 KR1020150175767A KR20150175767A KR101659300B1 KR 101659300 B1 KR101659300 B1 KR 101659300B1 KR 1020150175767 A KR1020150175767 A KR 1020150175767A KR 20150175767 A KR20150175767 A KR 20150175767A KR 101659300 B1 KR101659300 B1 KR 101659300B1
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South Korea
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weight
essence
foam
skin
carbonic acid
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KR1020150175767A
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Korean (ko)
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김종택
황영기
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(주) 제이티
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • A61K8/416Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

Abstract

The present invention relates to a bubble mask pack composition and a bubble mask pack manufactured by using the same. More specifically, the bubble mask pack of the present invention has excellent foaming power and has effects in removing residues and waste in the skin by applying a carbonated mist solution to essence having the specific composition and a composition ratio.

Description

BACKGROUND OF THE INVENTION 1. Field of the Invention [0001] The present invention relates to a foam mask package,

The present invention relates to a foam mask pack composition and a foam mask pack manufactured using the same.

Generally, women use a method to beautify the face, and massage after cleansing in order to nourish the skin when the skin becomes rough or sunburned and tired, and to make the facial skin resilient. At this time, in order to supply nutrition to the damaged skin, natural materials such as Oatana citrus, massage cream, nutrition pack, cleansing pack, bleach pack, etc. can be covered with cosmetic tissue or other auxiliary means have. As described above, the cosmetic application agent directly applied to the skin for skin care is generally referred to as a pack. The pack provides moisture to the stratum corneum of the skin, tightens the skin to give elasticity, and cleans the pores to clean the skin have. Face packs for use on the face and body packs for use on the body are also available, including gel, paste, foam, powder, and mask.

Therefore, a cosmetic mask pack which is widely used for simplicity is made by adding water or lotion to a nonwoven fabric or adding an extract known to have functional properties. Nonwovens, however, are made of synthetic polymers. When added with cosmetic lotions or functional extracts, they become stiff and feel bad. Further, in the case of a formulation in which the nonwoven fabric is soaked in an additive such as a cosmetic liquid to induce absorption of a continuous serum, adhesion to the skin is low and denaturation of the cosmetic ingredients caused by exposure of the serum to air is difficult to avoid, There is a disadvantage that skin irritation is likely to occur due to high-concentration cosmetic ingredients coming into contact with the skin.

In order to solve such a problem, a mask pack using a gelling composition without using a nonwoven fabric has been used to solve the problems of the mask pack made of the nonwoven fabric. However, in the case of applying a mask pack of a hydrocolloid, There is a method for manufacturing a mask pack made of a gel type gel comprising at least one galactomanan, guar gum and at least one gelatinized carbohydrate polymer such as agarose, alginate and xanthan gum, Patent Publication No. 2005-0017556). In addition, there is a method for producing a complex hydrogel mask pack comprising a skin lye aqueous solution, alginic acid salt, cellose and agar (Korean Patent Registration No. 0841742). The above-mentioned patents disclose manufacturing methods for mixing a hydrocolloid, adding glycerin, and adding various electrolytic metal salt materials to make a gel having a strong elasticity in various shapes using a frame along the face, neck, eyes, nose, and the like , And sheet-like form. Such a gelation composition requires much evaluation and examination in terms of biocompatibility and safety by using a hydrogel using a synthetic resin.

However, in the case of the mask pack using the gelling composition as described above, a liquid cosmetic material (essence) is simply present on the surface of the gelled composition, so that the liquid cosmetic material does not sufficiently penetrate into the gelled composition, Can not be prevented from being evaporated and a sufficient amount of cost material can not penetrate into the skin in a state in which the liquid cosmetic material is simply on the surface of the gelled composition. There is a falling problem.

Thus, the inventors of the present invention completed a mask pack having an excellent composition and composition ratio that not only has excellent bubble power but also can smoothly remove waste products and residues deep inside the skin. That is, the present invention provides a novel foam mask pack composition in which foam is generated, and a foam mask pack manufactured using the same.

In order to solve the above problems, the present invention relates to a foam mask pack composition, which comprises an essence which reacts with a carbonic acid mist liquid to generate foam.

Another object of the present invention is to provide a foam mask pack which comprises the foam mask pack composition and is characterized in that an essence for generating foam is applied to a face and then a mist of carbonic acid is sprayed or sprayed on the face- Thereby causing the essence to bubble.

Further, the foam mask pack of the present invention is an essence which reacts with a carbonic acid mist liquid to generate foam; And a carbonic acid mist liquid that reacts with the essence to cause the essence to bubble.

In addition, the foam mask pack of the present invention comprises: a mask sheet on which an essence that generates bubbles by reaction with the carbonic acid mist liquid is carried; And a carbonic acid mist liquid which reacts with the essence to cause the essence to foam.

The present invention has excellent foam-forming ability and is effective for penetrating effective cosmetic ingredients on the skin by using it on the skin, thereby more smoothly removing waste products and residues deep inside the skin, thereby helping to make rough skin smooth and smooth.

Fig. 1 is a photograph of the essence prepared in Preparation Example 1. Fig.
FIGS. 2 to 4 are photographs showing bubbles generated in the foam mask packs manufactured in Examples 2 to 4. FIG.
FIGS. 5 and 6 are photographs of bubbles generated in the foam mask packs manufactured in Examples 1 and 5, respectively.
FIG. 7 shows the results of measurement of the degree of foam generation according to the concentration and amount of the carbonic acid mist liquid in the foam mask pack components.

Hereinafter, the present invention will be described in more detail.

In the present invention, the foam mask pack composition includes an essence and a carbonic acid mist liquid, and the essence reacts with the carbonic acid mist liquid to generate a foam, thereby obtaining the effect of removing waste materials and residues in the skin.

In the foam mask pack composition of the present invention, the essence may include a skin conditioner, a solvent, a pH adjuster, a chelating agent, a moisturizer, a surfactant, and a preservative, and may further include a perfume.

The skin conditioner in the essence component may contain 10 to 15% by weight, preferably 11 to 14% by weight, and more preferably 12 to 13.5% by weight of the total weight of the essence.

The skin conditioner includes C3 to C5 alkylene glycol, glycerin, betaine, sodium hyaluronate, aloe vera leaf extract, cucumber extract, xanthan gum and sodium polyacrylate, preferably C3 to C5 85 to 120 parts by weight of glycerin, 15 to 30 parts by weight of betaine, 1 to 3.5 parts by weight of sodium hyaluronate, 7 to 15 parts by weight of aloe vera leaf extract, 7 to 15 parts by weight of cucumber extract 7 To 15 parts by weight, xanthan gum, 1.2 to 4 parts by weight, and sodium polyacrylate, 2 to 8 parts by weight. More preferably, 95 to 105 parts by weight of glycerin, 18 to 25 parts by weight of betaine, 1.5 to 2.5 parts by weight of sodium hyaluronate, 8 to 13 parts by weight of aloe vera leaf extract 8 to 13 parts by weight of cucumber extract, 2 to 3.5 parts by weight of xanthan gum and 3.5 to 7 parts by weight of sodium polyacrylate.

The solvent of the essence component may be at least one selected from the group consisting of purified water and ethanol. Preferably, the solvent may be a mixture of purified water and ethanol. More preferably, purified water is used in an amount of 3,900 to 4,350 Can be mixed and used. When the content of the solvent is less than 82% by weight, the viscosity of the essence becomes too high, so that the amount of the solvent in the face or sheet There may be a problem that the essence flows when it is applied to the solvent, and when the content of the solvent exceeds 89% by weight, the viscosity becomes too high and the foam forming ability may be deteriorated.

The pH adjusting agent in the essence component may be at least one selected from the group consisting of malic acid, tartaric acid, citric acid, glycolic acid aqueous solution, sodium citrate and triethanolamine, It is possible to use a mixture of two kinds or three kinds selected from among acetic acid, tartaric acid and triethanolamine, more preferably malonic acid, tartaric acid and triethanolamine in a ratio of 1: 0.8 to 1.3: 0.1 to 0.4 Or a mixture of citric acid, sodium citrate and glycolic acid at a concentration of 70% by volume in a weight ratio of 1: 0.5 to 0.7: 0.65 to 0.8. When the amount of the pH adjusting agent is less than 0.2 wt% or more than 3.5 wt%, the amount of the pH adjusting agent is preferably from 0.2 to 3.5 wt%, more preferably from 0.6 to 3.5 wt% It may be difficult to adjust the pH of the pH range from 3.10 to 4.00.

The chelating agent in the essence component serves as a sequestering agent, and may be used alone or in combination of two or more selected from disodium EDTA and citric acid. The content of the chelating agent may be 0.1 to 0.7% by weight, preferably 0.15 to 0.5% by weight, based on the total weight of the essence. If the chelating agent content is less than 0.1% by weight, If it is used in excess of 0.7% by weight, the pH of the essence may be lowered to stimulate the skin.

In addition, the moisturizing agent in the essence component can be used by introducing a general moisturizing component used in the art. Preferably, the moisturizing component is selected from the group consisting of mash extract, mulberry extract, molasses extract, hwanggi extract, jujube extract, More preferably at least one species selected from the group consisting of marigold extract, molasses extract and willow tree extract may be used alone or in combination of two or more species. If the humectant is used in an amount of 0.3 to 2% by weight, preferably 0.3 to 1% by weight, the amount of the moisturizer may be 0.3 to 2% by weight based on the total weight of the essence. If the content of the moisturizing agent exceeds 2% by weight, it may be advantageous in terms of the sustainability of the foam produced by the reaction with the carbonic acid mist liquid, but there may be a problem in that the bubble generation time is delayed It is preferable to use it within the above range.

Surfactants in the essence component have the role of maintaining foam formation and foaming form satisfactorily, and can be used in various cosmetic compositions such as paper-60 hydrogenated castor oil, lauramidopropyl betaine, cocamidopropyl betaine, Betaine laura maid dieh, cocamide miei, and cocamide dieh, and preferably one or more selected from the group consisting of phage-60 hydrogenated castor oil, laamapidopropyl betaine, and coca- And one or two or more selected from the group consisting of undifferentiated betaine can be used. The amount of the surfactant used is preferably 0.1 to 0.5% by weight, more preferably 0.15 to 0.35% by weight based on the total weight of the essence. If the content of the surfactant is less than 0.1% by weight, It may be a cause of separation of formulations due to a problem of mixing of water and oil phase, and when it is used in excess of 0.5 wt%, there may be a problem of drying of skin.

In addition, the above-mentioned preservative in the essence component is intended to enhance the long-term preservation stability of the essence and may be a conventional preservative used in the art. Preferably, one or two selected from methylparaben, phenoxyethanol and propylparaben And more preferably, methyl paraben, phenoxy ethanol and propyl paraben can be mixed in a weight ratio of 1: 0.3 to 0.7: 0.05 to 0.2. The preservative may be used in an amount of 0.05 to 0.3% by weight, preferably 0.08 to 0.2% by weight, based on the total weight of the essence. If the preservative content is less than 0.05% by weight, the long-term preservation stability of the carbonic acid mist liquid may deteriorate, If it is used in an amount exceeding 0.3% by weight, there may be a problem that the commercial property is deteriorated and the foaming ability of fine size is deteriorated because it is interfered with foam formation.

In addition, the essence component may further include conventional perfumes used in the art. Specifically, for example, AQUA HP-AE31847 and LEMON-310343 may be used singly or in combination of two or more. The content of the fragrance is preferably 0.001 to 0.05% by weight based on the total weight of the essence.

As the essence component, a colorant may be further used in addition to the skin conditioner, solvent, pH adjusting agent, chelating agent, moisturizing agent, preservative, and perfume.

The essence of the present invention having such a composition and composition ratio may have a pH of 3.10 to 4.00, preferably 3.10 to 3.80, more preferably 3.10 to 3.40.

Hereinafter, the carbonic acid mist liquid which reacts with the essence to generate bubbles will be described.

In the present invention, the carbonic acid mist liquid includes a skin protecting agent (and / or a foaming agent), a solvent, a skin conditioner and a preservative.

The skin protecting agent may be used as a foaming agent and sodium bicarbonate may be used. The content of the skin protective agent may be 4.5 to 8.7 wt%, preferably 5.0 to 8.5 wt%, based on the total weight of the carbonic acid mist liquid, By weight, more preferably from 7.0 to 8.2% by weight, based on the total weight of the composition. If the content of the skin protecting agent is less than 4.5% by weight, foaming of the essence may be insufficient. If it exceeds 8.7% by weight, the foaming ability is excellent, but warming may be carried out to dissolve the sodium bicarbonate, As a matter of fact, there may be a problem of losing the inherent properties of the raw material.

The solvent of the carbonic acid mist liquid component may contain at least one member selected from the group consisting of purified water and ethanol, preferably 4000-5000 parts by weight of purified water per 100 parts by weight of ethanol, It is advantageous in terms of the viscosity of the mist liquid. The solvent may be used in an amount of 86 to 95% by weight, preferably 90 to 94% by weight, based on the total weight of the carbonic acid mist liquid. If the solvent content is less than 86% by weight, It may be difficult to apply the carbonic acid mist liquid to the essence by spraying and / or spraying the carbonic acid mist liquid. If it is used in excess of 95% by weight, the amount of the sodium bicarbonate used as the skin protective agent may be decreased and the foam- .

The skin conditioner of the carbonic acid mist liquid component serves to moisturize and nourish the skin. The skin conditioner includes lysine, histidine, arginine, aspartic acid, threonine, serine, glutamic acid, proline, , Valine, methionine, isoleucine, leucine, tyrosine, phenylalanine, and cysteine may be used alone or in admixture of two or more. The content of the skin conditioner is preferably 0.005 to 0.5% by weight, and more preferably 0.005 to 0.1% by weight, based on the total weight of the carbonic acid mist liquid.

The above preservative in the carbonic acid mist liquid component is intended to enhance the long-term preservation stability of the carbonic acid mist liquid, and may be a conventional preservative used in the art. Preferably, the preservative is selected from the group consisting of methylparaben, phenoxyethanol and propylparaben Or two or more of them may be used in combination. More preferably, three species of methylparaben, phenoxyethanol and propylparaben can be mixed and used. The preservative may be used in an amount of 0.05 to 1% by weight, preferably 0.08 to 0.5% by weight, based on the total weight of the carbonic acid mist liquid. If the preservative content is less than 0.05% by weight, If it is used in an amount exceeding 1% by weight, there may be a problem that the commercial property is deteriorated and the foaming ability of the fine size is lowered due to interference with the foam formation.

The foam mask pack of the present invention is manufactured using the above-described foam mask pack composition. The essence for generating foam is applied to the face, and then the mist mist applied to the face is applied to the face by spraying or spraying, ≪ / RTI >

The amount of the carbonic acid mist liquid may be 1.5 to 20 parts by weight, preferably 2 to 15 parts by weight, more preferably 2 to 10 parts by weight, based on 100 parts by weight of the essence . If the application amount of the carbonic acid mist liquid is less than 1.5 parts by weight, the foaming ability may be lowered and the fine foaming power may be lowered. If the amount is more than 20 parts by weight, It is good.

In addition, the present invention can be provided in the form of a packaged product of the above-described foam mask pack, for example, an essence which reacts with a carbonic acid mist liquid to generate foam; And a carbonic acid mist liquid which reacts with the essence to cause the essence to foam.

The present invention also relates to a mask sheet on which an essence for generating foam by reacting with a carbonic acid mist liquid is carried; And a carbonic acid mist liquid which reacts with the essence to cause the essence to foam.

Hereinafter, the present invention will be described in more detail with reference to examples. However, the scope of the present invention is not limited by the following examples.

[Example]

Preparation Example 1: Preparation of essence

Then, xanthan gum and sodium polyacrylate were added to purified water (80 DEG C) heated to 80 DEG C and stirred at a speed of about 1,000 rpm for 20 minutes.

Next, the mixture was cooled to 50 ° C, and then butylen glycol, glycerin, citric acid, malic acid, tartaric acid, betaine and disodium were added to the dithia and stirred at a rate of about 950 rpm for 20 minutes.

Next, a paper-60 hydrogenated castor oil, a perfume, ethanol, phenoxyethanol, methylparaben and propylparaben were added to the flask and stirred at a speed of about 1,100 rpm for 10 minutes.

Next, triethanolamine was added at room temperature (24 ° C to 26 ° C), and the mixture was stirred at a speed of about 900 rpm for 5 minutes.

Next, the aloe vera leaf extract, sodium hyaluronate, cucumber extract and horseradish extract were added at room temperature (24 ° C to 26 ° C) and stirred at 900 rpm for 5 minutes to prepare the essence. The pH of the prepared essence Was 3.16.

The above Essenes have the compositions shown in Table 1 below, and the produced essence photographs are shown in Fig.

division weight% CAS. NO menstruum Purified water 83.772 7732-18-5 ethanol 2.000 64-17-5 skin
Conditioning agent
Butylene glycol 5.000 107-88-0
glycerin 5.000 56-81-5 Betaine 1,000 107-43-7 Aloe vera leaf extract 0.500 85507-69-3 Sodium hyaluronate 0.100 9067-32-7 Cucumber extract 0.500 89998-01-6 Xanthan gum 0.150 11138-66-2 Sodium polyacrylate 0.200 9003-04-07 pH adjusting agent Malik Acid 0.270 6915-15-7 Tataric acid 0.270 87-69-4 Triethanolamine 0.050 102-71-6 Moisturizer Marchia extract 0.500 90083-07-1 Surfactants PIGGY-60 Hydrogenated Castor Oil 0.250 61788-85-0 Chelating agent Disodium iodide 0.030 139-33-3 Citric acid 0.270 77-92-9 Preservative Methylparaben 0.080 99-76-3 Phenoxyethanol 0.040 122-99-6 Propylparaben 0.008 94-13-3 Spices AQUA HP-AE31847 0.010 -

Preparation Example 1-2: Preparation of Essence

Essences were prepared in the same manner as in Preparation Example 1 except that the essence having the composition as shown in Table 2 was prepared by varying kinds and compositions of the pH adjusting agent.

division weight% CAS. NO menstruum Purified water 81.062 7732-18-5 ethanol 2.000 64-17-5 skin
Conditioning agent
Butylene glycol 5.000 107-88-0
glycerin 5.000 56-81-5 Betaine 1,000 107-43-7 Aloe vera leaf extract 0.500 85507-69-3 Sodium hyaluronate 0.100 9067-32-7 Cucumber extract 0.500 89998-01-6 Xanthan gum 0.150 11138-66-2 Sodium polyacrylate 0.200 9003-04-07 pH adjusting agent Citric acid 1.4 - Sodium citrate 0.9 - Glycollic acid 1.0 - Moisturizer Marchia extract 0.500 90083-07-1 Surfactants PIGGY-60 Hydrogenated Castor Oil 0.250 61788-85-0 Chelating agent Disodium iodide 0.030 139-33-3 Citric acid 0.270 77-92-9 Preservative Methylparaben 0.080 99-76-3 Phenoxyethanol 0.040 122-99-6 Propylparaben 0.008 94-13-3 Spices AQUA HP-AE31847 0.010 -

Preparation Example 2-1: Preparation of carbonic acid mist liquid

Sodium bicarbonate was added to purified water at room temperature (24 ° C to 26 ° C), and the mixture was stirred at a rate of 950 rpm for 30 minutes.

Next, ethanol, methylparaben, propylparaben and phenoxyethanol were added at room temperature (24 ° C to 26 ° C), and the mixture was stirred at a rate of 950 rpm for 15 minutes.

Subsequently, an amino acid complex (lysine, histidine, arginine, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, methionine, isoleucine, leucine, Tyrosine, phenylalanine, cysteine) was added thereto, and stirred at a rate of about 1,150 to 1,170 rpm for 5 minutes to prepare a carbonic acid mist liquid. The composition of the carbonic acid mist liquid is shown in Table 3 below.

division weight% CAS. NO menstruum Purified water 89.862 7732-18-5 ethanol 2.000 64-17-5 Skin protection Sodium bicarbonate 8.000 144-55-8 Skin Conditioner Lysine 0.010 56-87-1 Histidine 71-00-1 Arginine 74-79-3 Aspartic acid 56-84-8 Threonine 72-19-5 Serine 56-45-1 Glutamic acid 56-86-0 Proline 147-85-3 Glycine 56-40-6 Alanine 56-41-7 Balin 72-18-4 Methionine 59-51-8 Isoleucine 73-32-5 Leucine 61-90-5 Tyrosine 60-18-4 Phenylalanine 63-91-2 Cysteine 52-90-4 Preservative Methylparaben 0.080 99-76-3 Phenoxyethanol 0.040 122-99-6 Propylparaben 0.008 94-13-3

Preparation Example 2-2 ~ Preparation Example 2-5

Using the same compositions and composition ratios as the solvents, skin protectants, skin conditioners and preservatives in the same manner as in Preparation Example 2-1, the content of purified water and skin protecting agent in the solvent in the carbonic acid mist liquid was varied, A carbonic acid mist liquid having the same composition and composition ratio was prepared.

division menstruum Skin protection Skin Conditioner Preservative Preparation Example 2-1 91.862 wt% 8 wt% 0.01 wt% 0.128 wt% Preparation Example 2-2 94.862 wt% 5 wt% 0.01 wt% 0.128 wt% Preparation Example 2-3 93.862 wt% 6 wt% 0.01 wt% 0.128 wt% Preparation Example 2-4 92.862 wt% 7 wt% 0.01 wt% 0.128 wt% Preparation Example 2-5 90.862 wt% 9 wt% 0.01 wt% 0.128 wt%

Example 1

0.6 g of the carbonic acid mist liquid prepared in Preparative Example 2-1 was mixed with 10 g of the essence of Preparation Example 1, the mixture was mixed at 25 캜 and 5 seconds later, Respectively.

Examples 2 to 5

The same procedure as in Example 1 was repeated, except that 0.625 g of each of the carbonic acid mist liquids prepared in Preparation Examples 2-2 to 2-4 was mixed at 25 DEG C per 10 g of the essence, (Example 2), Fig. 3 (Example 3) and Fig. 4 (Example 4).

Further, in the same manner as in Example 1, 0.625 g of each of the carbonic acid mist liquid of Preparation Example 2-5 per 50 g of the essence was mixed at 50 to 52 캜, and then the degree of foaming was measured after 5 seconds. Example 5).

2 to 6, the carbonic acid mist liquid containing 9% by weight of sodium bicarbonate in Example 5 showed the best foaming power, whereas in Example 5, sodium bicarbonate was contained in an amount of 5 to 8% by weight It is difficult to dissolve in the case of Examples 1 to 4, and in the case of sodium bicarbonate, decomposition proceeds at 50 DEG C or higher, 8% by weight of sodium bicarbonate) and Example 4 (7% by weight of sodium bicarbonate) were excellent in foaming amount and fine foam forming ability. On the other hand, in the case of Example 2 and Example 3, it was confirmed that the amount of foam formation was somewhat insufficient and the foam was large in size, as compared with Example 1 and Example 4. As a result, It is found that there is a problem that the degree of microbubble formation is insufficient.

Examples 6 to 25

The same procedure as in Example 1 was carried out except that the amount of each of the carbonic acid mist liquids prepared in Preparation Examples 2-1 to 2-5 per 10 g of the essence was applied as shown in Table 5 below, The results are shown graphically in FIG.

At this time, the measurement of the degree of foaming was performed using DFA 100, a foam physical property measuring instrument of KRUSS, Germany.

Example 26

The degree of foaming was measured in the same manner as in Example 1 except that 0.6 g of the carbonic acid mist liquid prepared in Preparation Example 2-1 was added to 10 g of the essence prepared in Preparation Example 1-2 instead of the essence of Preparation Example 1 The mixture was mixed at 25 ° C and foamed after 5 seconds.

division essence Carbonic acid mist liquid In the fizzy mist liquid
Sodium bicarbonate content
Bubble generation amount
(Unit ml)
Example 1 10 g 0.625 g 8 wt% 7.9 Example 2 5 wt% 0.9 Example 3 6 wt% 2.4 Example 4 7 wt% 4.0 Example 5 9 wt% 8.8 Example 6 10 g 0.125 g 8 wt% 0.8 Example 7 5 wt% 0.1 Example 8 6 wt% 0.2 Example 9 7 wt% 0.3 Example 10 9 wt% 1.3 Example 11 10 g 0.25 g 8 wt% 3.1 Example 12 5 wt% 0.2 Example 13 6 wt% 0.7 Example 14 7 wt% 1.5 Example 15 9 wt% 3.8 Example 16 10 g 0.375 g 8 wt% 4.6 Example 17 5 wt% 0.5 Example 18 6 wt% 1.3 Example 19 7 wt% 2.0 Example 20 9 wt% 5.4 Example 21 10 g 0.5 g 8 wt% 6.7 Example 22 5 wt% 0.7 Example 23 6 wt% 1.8 Example 24 7 wt% 2.7 Example 25 9 wt% 7.7 Example 26 10 g 0.625 g 8 wt% 7.9

Experimental Example 1: Skin irritation, skin exfoliation and wastes removal

Using the same essence and carbonic acid mist liquid as in Examples 1 to 5 and Examples 21 to 25, 10 g of the essence was applied to the face, and then the same amount of the carbonic acid mist liquid was sprayed by the spraying method in each of Examples, The skin irritation was measured by washing after washing. The results are shown in Table 5 below.

In addition to the above Examples 1 to 5 and Examples 21 to 25, 2.3 g of a carbonic acid mist liquid containing 8% by weight of sodium bicarbonate was used to measure skin irritation, exfoliation and waste disposability, Respectively.

In addition, Comparative Example 2 was further carried out by measuring 0.625 g of a carbonic acid mist liquid containing 10% by weight of sodium bicarbonate to measure skin irritation, exfoliation, and waste removal.

Skin irritation was measured in 20 male and female subjects. 3 points were observed for skin erythema and edema, 2 points for slight erythema on skin, 1 point for skin tickle and 1 point for skin. 0 " is given to the case where they are not visible, and they are evaluated by their average points.

Skin exfoliation and wastage removal were evaluated by measuring the volume of pores using a 3D image of Derma Top ™ (Breuckman, Germany, Eotech Company, France) using optical equipment. The measurement criteria are as follows.

No keratin and no waste: ⊚, almost no keratin and no waste: ◯, keratin and waste left: △, keratin and lots of waste left: ×

division Skin irritation Skin exfoliation and wastes removal Example 1 0.1 Example 2 0.6 Example 3 0.2 Example 4 0.1 Example 5 0 Example 21 0 Example 22 0.2 Example 23 0.8 Example 24 0.4 Example 25 0 Comparative Example 1 0 Comparative Example 2 0

As a result of measuring the skin irritancy in Table 6, skin irritation was reduced as the content of sodium bicarbonate in the carbonic acid mist liquid increased or the amount of the carbonic acid mist liquid was increased. This is because the carbonic acid mist liquid The results of pH neutralization performance are shown in Fig.

In the case of Comparative Example 1 and Comparative Example 2, there was no significant difference in terms of skin irritation in Comparative Example 1 and Comparative Example 2 as compared with Example 1. However, in the case of skin exfoliation and wastes removal performance, Compared to the other two.

Claims (17)

And an essence for generating foam by reacting with a carbonic acid mist liquid containing 4.5 to 8.7% by weight of a skin protecting agent, 86 to 95% by weight of a solvent, 0.005 to 0.5% by weight of a skin conditioner and 0.05 to 1%
The essence may be selected from the group consisting of 10 to 15 wt% of skin conditioner, 82 to 89 wt% of solvent, 0.2 to 3.5 wt% of pH adjusting agent, 0.1 to 0.7 wt% of chelating agent, 0.3 to 2 wt% of moisturizer, 0.1 to 0.5 wt% of surfactant, 0.05 to 0.3% by weight based on the total weight of the composition.
delete The skin conditioner according to claim 1, wherein the skin conditioner comprises C3 to C5 alkylene glycol, glycerin, betaine, sodium hyaluronate, aloe vera leaf extract, cucumber extract, xanthan gum and sodium polyacrylate By weight. The skin conditioner according to claim 3, wherein the skin conditioner comprises 85 to 120 parts by weight of glycerin, 15 to 30 parts by weight of betaine, 1 to 3.5 parts by weight of sodium hyaluronate per 100 parts by weight of C3 to C5 alkylene glycol, 7-15 parts by weight of aloe vera leaf extract, 7-15 parts by weight of cucumber extract, 1.2-4 parts by weight of xanthan gum and 2-8 parts by weight of sodium polyacrylate.
The method according to claim 1, wherein the solvent comprises at least one selected from the group consisting of purified water and ethanol,
Wherein the pH adjusting agent comprises at least one selected from the group consisting of malic acid, tartaric acid, citric acid, glycolic acid, sodium citrate and triethanolamine,
Wherein the chelating agent comprises at least one selected from disodium EDTA and citric acid,
Wherein the preservative comprises at least one selected from methylparaben, phenoxyethanol, and propylparaben.
The composition of claim 1, wherein the surfactant is selected from the group consisting of Pigment-60 Hydrogenated Castor Oil, Lauramidopropyl Betaine, Cocamidopropyl Betaine, Babaisamidopropyl Betaine Lauraamide Deiai, Wherein the foam mask pack comprises at least one selected from the group consisting of polyvinyl alcohol and polyvinyl alcohol. 6. The method of claim 5, wherein the pH adjusting agent comprises malic acid, tartaric acid and triethanolamine in a weight ratio of 1: 0.8 to 1.3: 0.1 to 0.4, or a citric acid, sodium citrate and a 70% Colic acid in a weight ratio of 1: 0.5 to 0.7: 0.65 to 0.8,
Wherein the preservative comprises methyl paraben, phenoxy ethanol and propyl paraben in a weight ratio of 1: 0.3 to 0.7: 0.05 to 0.2.
The foam mask pack composition according to claim 1, wherein the essence has a pH of 3.10 to 4.00. delete The method of claim 1, wherein the skin protection agent comprises sodium bicarbonate,
Wherein the solvent comprises at least one selected from the group consisting of purified water and ethanol,
The skin conditioner includes at least one selected from lysine, histidine, arginine, aspartic acid, threonine, serine, glutamic acid, proline, glycine, alanine, valine, methionine, isoleucine, leucine, tyrosine, phenylalanine and cysteine In addition,
Wherein the preservative comprises at least one selected from the group consisting of methylparaben, phenoxyethanol and propylparaben.
The foam mask pack composition according to claim 10, wherein the solvent comprises 4,000 to 5,000 parts by weight of purified water per 100 parts by weight of ethanol. A foam mask pack comprising the foam mask pack composition of any one of claims 1, 3 to 8, and 10. A method of using the foam mask pack of claim 12,
After applying a bubbling essence to the face, apply the carbonic acid mist liquid to the face-applied essence in a spraying or spraying manner to cause the essence to foam,
Wherein 1.5 to 20 parts by weight of the carbonic acid mist liquid is applied to 100 parts by weight of the essence.
delete A method of using the foam mask pack of claim 12,
A method of using a foam mask pack, wherein a mask sheet carrying an essence for generating foam is attached to a face, and a carbonic acid mist liquid is applied to the mask sheet by spraying or spraying to cause the essence to foam.
An essence which reacts with the carbonic acid mist liquid to generate foam; And
And a carbonic acid mist liquid which reacts with the essence to cause the essence to foam,
Wherein the carbonic acid mist liquid comprises 4.5 to 8.7 wt% of a skin protecting agent, 86 to 95 wt% of a solvent, 0.005 to 0.5 wt% of a skin conditioner, and 0.05 to 1 wt% of a preservative,
The essence may be selected from the group consisting of 10 to 15 wt% of skin conditioner, 82 to 89 wt% of solvent, 0.2 to 3.5 wt% of pH adjusting agent, 0.1 to 0.7 wt% of chelating agent, 0.3 to 2 wt% of moisturizer, 0.1 to 0.5 wt% of surfactant, 0.05 to 0.3% by weight.
A mask sheet on which an essence is formed to react with the carbonic acid mist liquid to generate bubbles; And
And a carbonic acid mist liquid which reacts with the essence to cause the essence to foam,
Wherein the carbonic acid mist liquid comprises 4.5 to 8.7 wt% of a skin protecting agent, 86 to 95 wt% of a solvent, 0.005 to 0.5 wt% of a skin conditioner, and 0.05 to 1 wt% of a preservative,
The essence may be selected from the group consisting of 10 to 15 wt% of skin conditioner, 82 to 89 wt% of solvent, 0.2 to 3.5 wt% of pH adjusting agent, 0.1 to 0.7 wt% of chelating agent, 0.3 to 2 wt% of moisturizer, 0.1 to 0.5 wt% of surfactant, 0.05 to 0.3% by weight.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210026888A (en) * 2019-09-02 2021-03-10 코스맥스 주식회사 A Cosmetic composition comprising methyl hydrogenated rosinate

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Publication number Priority date Publication date Assignee Title
KR100878080B1 (en) * 2007-03-02 2009-01-13 최완정 A composite of nutrition pack for skin beauty and making method thereof
JP2014118408A (en) * 2012-12-17 2014-06-30 Viita Kk Cosmetic method and medicine thereof in which foamy carbonic acid pack and skin cream are made into one
KR20150108611A (en) * 2014-03-18 2015-09-30 주식회사 한국화장품제조 Mask sheet cosmetic composition with self foaming function and manufacturing method thereof
KR20150121846A (en) * 2014-04-22 2015-10-30 긴세이 세이시 가부시키가이샤 Cosmetic sheet

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100878080B1 (en) * 2007-03-02 2009-01-13 최완정 A composite of nutrition pack for skin beauty and making method thereof
JP2014118408A (en) * 2012-12-17 2014-06-30 Viita Kk Cosmetic method and medicine thereof in which foamy carbonic acid pack and skin cream are made into one
KR20150108611A (en) * 2014-03-18 2015-09-30 주식회사 한국화장품제조 Mask sheet cosmetic composition with self foaming function and manufacturing method thereof
KR20150121846A (en) * 2014-04-22 2015-10-30 긴세이 세이시 가부시키가이샤 Cosmetic sheet

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210026888A (en) * 2019-09-02 2021-03-10 코스맥스 주식회사 A Cosmetic composition comprising methyl hydrogenated rosinate
KR102297560B1 (en) * 2019-09-02 2021-09-03 코스맥스 주식회사 A Cosmetic composition comprising methyl hydrogenated rosinate

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