KR101584128B1 - Sample aggregate and apparatus for measuring a optical constant using the same - Google Patents
Sample aggregate and apparatus for measuring a optical constant using the same Download PDFInfo
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- KR101584128B1 KR101584128B1 KR1020140025001A KR20140025001A KR101584128B1 KR 101584128 B1 KR101584128 B1 KR 101584128B1 KR 1020140025001 A KR1020140025001 A KR 1020140025001A KR 20140025001 A KR20140025001 A KR 20140025001A KR 101584128 B1 KR101584128 B1 KR 101584128B1
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- South Korea
- Prior art keywords
- electromagnetic wave
- sample
- optical constant
- laser beam
- aggregate
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- 230000003287 optical effect Effects 0.000 title claims abstract description 99
- 238000000034 method Methods 0.000 claims description 14
- 230000005684 electric field Effects 0.000 claims description 8
- 230000008033 biological extinction Effects 0.000 claims description 7
- 238000000605 extraction Methods 0.000 claims description 2
- 239000000523 sample Substances 0.000 description 92
- 239000013074 reference sample Substances 0.000 description 11
- 238000010586 diagram Methods 0.000 description 6
- 238000005259 measurement Methods 0.000 description 5
- 230000005540 biological transmission Effects 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
- 229910052737 gold Inorganic materials 0.000 description 2
- 239000010931 gold Substances 0.000 description 2
- 229910000673 Indium arsenide Inorganic materials 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- RPQDHPTXJYYUPQ-UHFFFAOYSA-N indium arsenide Chemical compound [In]#[As] RPQDHPTXJYYUPQ-UHFFFAOYSA-N 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000001131 transforming effect Effects 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3581—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using far infrared light; using Terahertz radiation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/41—Refractivity; Phase-affecting properties, e.g. optical path length
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Toxicology (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
The present invention relates to a sample aggregate and an optical constant measuring apparatus using the sample aggregate. The sample aggregate of the present invention includes an electromagnetic wave generator for generating a first electromagnetic wave by interacting with a laser beam emitted from a laser beam oscillator and a sample layer on which the sample is stacked, Layer and is oscillated as a second electromagnetic wave. The optical constants measuring device using the sample aggregate of the present invention may further comprise a laser beam oscillator for emitting a laser beam, a sample aggregate for interacting with the laser beam emitted from the laser beam oscillator to oscillate a first electromagnetic wave, And an optical constant calculating unit for receiving the second electromagnetic wave and calculating an optical constant for the sample using the first electromagnetic wave and the second electromagnetic wave. According to the present invention, by stacking a sample layer that transmits or reflects electromagnetic waves to an electromagnetic wave generating portion that interacts with a laser beam to oscillate the electromagnetic wave, an optical constant for the sample can be measured using electromagnetic waves oscillating in multiple paths There is an advantage.
Description
The present invention relates to a sample aggregate and an optical constant measuring apparatus using the sample aggregate.
A device for measuring the optical constant of a sample is used to obtain information about the material. Using such an optical constant measuring device, noninvasive information on the sample or material contained in the sample can be obtained.
Conventional optical constants measuring apparatuses should be used differently depending on whether the sample is transparent or opaque. Such an optical constant measuring device uses a lens or a mirror to measure electromagnetic waves to measure an optical constant.
On the other hand, a reflection type optical constant measuring device for measuring the optical constant of an opaque sample is more complicated than a transmission type optical constant measuring device in terms of characteristics. The complexity of such a device configuration poses technical problems, particularly in the region where the frequency characteristic is in terahertz. That is, when focusing a light using a lens or a mirror, the minimum focusing area increases in proportion to the wavelength (diffraction limit), so that in the case of a terahertz wave having a wavelength of approximately mm, the diameter of the focused beam is approximately several mm Lt; / RTI >
As described above, when the optical constant of an opaque sample is measured, if the sample size of the sample is small, the size of the lens or mirror must be increased accordingly. Therefore, according to the conventional optical constant measuring apparatus, it is difficult to measure a sample having a small size.
The sample aggregate of the present invention aims to oscillate electromagnetic waves in multiple paths by laminating a sample layer that transmits or reflects electromagnetic waves generated by an electromagnetic wave generating unit that interacts with a laser beam to oscillate electromagnetic waves.
In addition, the optical constants measuring apparatus of the present invention using such a sample aggregate aims at measuring optical constants for samples using electromagnetic waves oscillating in multi-paths in a sample aggregate.
The objects of the present invention are not limited to the above-mentioned objects, and other objects and advantages of the present invention which are not mentioned can be understood by the following description and more clearly understood by the embodiments of the present invention. It will also be readily apparent that the objects and advantages of the invention may be realized and attained by means of the instrumentalities and combinations particularly pointed out in the appended claims.
In order to accomplish the above object, the present invention provides a sample assembly comprising an electromagnetic wave generator for generating a first electromagnetic wave by interacting with a laser beam emitted from a laser beam oscillator, and a sample layer on which the sample is stacked, And the first electromagnetic wave is reflected by the sample layer and is oscillated by the second electromagnetic wave.
The optical constants measuring device using the sample aggregate of the present invention may further comprise a laser beam oscillator for emitting a laser beam, a sample aggregate for interacting with the laser beam emitted from the laser beam oscillator to oscillate a first electromagnetic wave, And an optical constant calculating unit for receiving the second electromagnetic wave and calculating an optical constant for the sample using the first electromagnetic wave and the second electromagnetic wave.
According to the present invention as described above, by stacking a sample layer that transmits or reflects electromagnetic waves generated by an electromagnetic wave generating portion that interacts with a laser beam to oscillate electromagnetic waves, electromagnetic waves that oscillate in a multi- There is an advantage that the constant can be measured.
BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a view for explaining a conventional optical constant measuring method for measuring an optical constant for an opaque sample. FIG.
2 is a configuration diagram of a conventional optical constant measuring apparatus for measuring optical constants for opaque samples.
3A is a configuration diagram of a sample aggregate according to an embodiment of the present invention.
FIG. 3B is a perspective view of a sample assembly according to an embodiment of the present invention. FIG.
4 is a configuration diagram of an optical constant measuring apparatus according to an embodiment of the present invention.
5 is a graph for explaining an optical constant calculation process according to an embodiment of the present invention.
6 is a graph showing the results of optical constant measurement for exemplary samples.
The above and other objects, features, and advantages of the present invention will become more apparent by describing in detail exemplary embodiments thereof with reference to the attached drawings, which are not intended to limit the scope of the present invention. In the following description, well-known functions or constructions are not described in detail since they would obscure the invention in unnecessary detail. Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings. In the drawings, the same reference numerals are used to denote the same or similar elements.
1 is a view for explaining a conventional optical constant measuring method for measuring an optical constant for an opaque sample. Referring to FIG. 1, a conventional optical constant measuring method irradiates an electromagnetic wave to each of the
More specifically, the electric field of the light ray incident on the reference sample 102
) Is the electric field reflected by the reference sample 102 ) And the following equation (1).[Equation 1]
here,
Can be expressed as a function of n and k with reflection Fresnel coefficients, where n is the refractive index and k is the extinction coefficient. That is, the reflection Fresnel coefficient is
As a function of refractive index and extinction coefficient. Using the equation (1), the reflection Fresnel coefficient for the
That is, in the conventional optical constant measuring method of FIG. 1, the electromagnetic wave reflected from a reference sample such as air or a reference sample is measured and compared with the electromagnetic wave reflected through the
However, when the optical constants are compared with the measured values of the target sample based on the measured values of the reference samples, the reflectance of the reference sample and the target sample become similar (for example, the reflectance is close to 99% there is a problem that it is difficult to measure the optical constant in the region where the value of k is about 100 or more).
2 is a block diagram of a conventional optical constant measuring apparatus for measuring an optical constant for an opaque sample. 2, a conventional optical constant measuring apparatus includes a
More specifically, the laser beam oscillated in the
That is, in the conventional optical constant measuring apparatus of FIG. 2, the
3A is a configuration diagram of a sample aggregate according to an embodiment of the present invention. Referring to FIG. 3A, the sample aggregate includes an electromagnetic
The
The
More specifically, the laser beam is irradiated to the
In other words, the first electromagnetic wave
) Is an electromagnetic wave that oscillates primarily by interacting with the surface of the electromagnetic3B is a perspective view of a sample aggregate according to an embodiment of the present invention. Referring to FIG. 3B, the
3A and 3B can oscillate the first electromagnetic wave and the second electromagnetic wave having frequency characteristics in the terahertz (10 12 Hz) region. That is, the laser beam can oscillate with an electromagnetic wave having a frequency characteristic of a terahertz region by interacting with the electromagnetic wave generating portion. As described above, the electromagnetic wave generating part of the present invention can be used as a first electromagnetic wave that oscillates primarily by interacting with a laser beam emitted from a laser beam oscillator, and a second electromagnetic wave that is reflected by a sample layer stacked on the electromagnetic wave generating part, have. The first electromagnetic wave and the second electromagnetic wave can be terahertz files having a frequency characteristic of a terahertz region.
According to the sample assembly of the present invention, the
4 is a configuration diagram of an optical constant measuring apparatus according to an embodiment of the present invention. The optical constant measuring apparatus of the present invention includes the sample aggregate of FIG. 3A. 4, the optical constant measuring apparatus includes a
The optical constants measuring apparatus according to the embodiment of the present invention can use the sample aggregates described in FIG. 3A. As described above, the
The
The
The
The optical constant measuring apparatus of the present invention may include a plane mirror, a
The optical
As described above, since the first electromagnetic wave and the second electromagnetic wave have different optical paths, the optical
Preferably, the optical
&Quot; (2) "
here,
The electric field of the first electromagnetic wave, Is a spectrum obtained by Fourier transforming the electric field of the second electromagnetic wave. , The function of Can be defined as a function. The (C is the speed of light and? Is the length of the wavelength). Means a path length difference from the laser beam irradiated to the electromagneticIs defined as a reflection Fresnel coefficient of the
&Quot; (3) "
Equation (3) reflects the electromagnetic wave reflected from the
Is defined as a transmission Fresnel coefficient of the electromagnetic
&Quot; (4) "
In equations (3) and (4)
The refractive index of theangle of incidence
For example, 45 [deg.], Depending on the installation position of the laser oscillator, Is based on Snell's law ( ). ≪ / RTI >Using Equations (2) to (4), the reflection Fresnel coefficients
) Of Can be obtained. Is the optical constant of the sample forming theThe refractive index of the electromagnetic
&Quot; (5) "
The first electromagnetic wave may be reflected from the
As a result, through equations (2) and (5), the optical constant
And Can be obtained at the same time.Optical constant
The As shown in FIG. here, Is a refractive index, Is the extinction coefficient.5 is a graph illustrating an optical constant calculation process according to an embodiment of the present invention. Referring to FIG. 5, the
Referring to the
As described above, the first
In the process of calculating the optical constant, equations (2) to (5) can be used.
The optical constant is the refractive index for the frequency
) And extinction coefficient ( ). ≪ / RTI > On the6 is a graph showing the results of optical constant measurement for exemplary samples. For the n-
Particularly, in the case of measuring the optical constant for a 60
However, according to the optical constant measuring apparatus of the present invention, since the optical constant is measured by comparing the multiple reflected electromagnetic waves from the sample with each other, the optical constant can be measured even for a sample having a reflectance similar to that of the reference sample.
While the present invention has been described in connection with what is presently considered to be practical exemplary embodiments, it is to be understood that the invention is not limited to the disclosed embodiments, but, on the contrary, But the present invention is not limited thereto.
Claims (8)
And a sample layer disposed below the electromagnetic wave generating portion,
Wherein the laser beam interacts with a surface of the electromagnetic wave generating portion to be converted into a first electromagnetic wave,
A part of the first electromagnetic wave is transmitted into the electromagnetic wave generating part, reflected by the sample layer and converted into a second electromagnetic wave,
The optical path of the second electromagnetic wave is longer than the optical path of the first electromagnetic wave,
The optical constant of the sample included in the sample layer is calculated using the electric field of the first electromagnetic wave and the second electromagnetic wave
Sample aggregate.
The first electromagnetic wave and the second electromagnetic wave
When the frequency characteristic is in terahertz (10 12 Hz)
Sample aggregate.
A sample aggregate which interacts with the laser beam to oscillate a first electromagnetic wave and a second electromagnetic wave; And
And an optical constant calculating unit for receiving the first electromagnetic wave and the second electromagnetic wave to calculate an optical constant for a sample included in the sample aggregate,
The sample aggregate
An electromagnetic wave generating unit to which a laser beam is incident; And
And a sample layer disposed below the electromagnetic wave generating portion,
Wherein the laser beam interacts with a surface of the electromagnetic wave generating portion to be converted into a first electromagnetic wave,
A part of the first electromagnetic wave is transmitted into the electromagnetic wave generating part, reflected by the sample layer and converted into a second electromagnetic wave,
The optical path of the second electromagnetic wave is longer than the optical path of the first electromagnetic wave,
Wherein the optical constant is calculated using an electric field of the first electromagnetic wave and the second electromagnetic wave
Optical Constant Measuring Apparatus Using Sample Assembly.
The first electromagnetic wave and the second electromagnetic wave
When the frequency characteristic is in terahertz (10 12 Hz)
Optical Constant Measuring Apparatus Using Sample Assembly.
The optical constant
Including refractive index and extinction coefficient
Optical Constant Measuring Apparatus Using Sample Assembly.
A plane mirror for changing the traveling path of the laser beam;
A parabolic mirror and a convex lens for converging the first electromagnetic wave and the second electromagnetic wave oscillating in the sample aggregate,
And an optical constant measuring device using the sample aggregate.
The optical constant extraction unit
Separating the first electromagnetic wave and the second electromagnetic wave on a time axis,
The first electromagnetic wave and the second electromagnetic wave separated from each other are Fourier transformed
Calculating an optical constant
Optical Constant Measuring Apparatus Using Sample Assembly.
Priority Applications (2)
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KR1020140025001A KR101584128B1 (en) | 2014-03-03 | 2014-03-03 | Sample aggregate and apparatus for measuring a optical constant using the same |
PCT/KR2014/013063 WO2015133715A1 (en) | 2014-03-03 | 2014-12-30 | Sample assembly and optical constant measurement device using same |
Applications Claiming Priority (1)
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KR1020140025001A KR101584128B1 (en) | 2014-03-03 | 2014-03-03 | Sample aggregate and apparatus for measuring a optical constant using the same |
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KR101584128B1 true KR101584128B1 (en) | 2016-01-11 |
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WO (1) | WO2015133715A1 (en) |
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KR101877954B1 (en) * | 2017-12-26 | 2018-07-12 | 주식회사 어니언소프트웨어 | Air conditioning system for server room |
KR102167799B1 (en) * | 2019-07-24 | 2020-10-20 | 한양대학교 산학협력단 | Thickness measuring device |
Citations (3)
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JP2009036693A (en) * | 2007-08-03 | 2009-02-19 | Institute Of Physical & Chemical Research | Near field micro device and spectral image acquisition method |
US20130155410A1 (en) | 2010-07-07 | 2013-06-20 | Melys Diagnostics Ltd | Optical Assembly and Method for Determining Analyte Concentration |
KR101296748B1 (en) * | 2012-03-26 | 2013-08-20 | 한국전기연구원 | Spectroscopy and imaging system of high-speed and high-resolution using electromagnetic wave based on optics |
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KR101395908B1 (en) * | 2006-11-21 | 2014-05-15 | 브라운 유니버시티 | Picosecond ultrasonic system incorporating an optical cavity |
KR101059690B1 (en) * | 2009-09-21 | 2011-08-26 | 부산대학교 산학협력단 | Refractive index measurement system and method for flat media using interference between transmitted and reflected light |
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- 2014-03-03 KR KR1020140025001A patent/KR101584128B1/en active IP Right Grant
- 2014-12-30 WO PCT/KR2014/013063 patent/WO2015133715A1/en active Application Filing
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JP2009036693A (en) * | 2007-08-03 | 2009-02-19 | Institute Of Physical & Chemical Research | Near field micro device and spectral image acquisition method |
US20130155410A1 (en) | 2010-07-07 | 2013-06-20 | Melys Diagnostics Ltd | Optical Assembly and Method for Determining Analyte Concentration |
KR101296748B1 (en) * | 2012-03-26 | 2013-08-20 | 한국전기연구원 | Spectroscopy and imaging system of high-speed and high-resolution using electromagnetic wave based on optics |
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