KR101447483B1 - Cosmetic composition contained horse chestnut extract - Google Patents

Cosmetic composition contained horse chestnut extract Download PDF

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KR101447483B1
KR101447483B1 KR1020130002573A KR20130002573A KR101447483B1 KR 101447483 B1 KR101447483 B1 KR 101447483B1 KR 1020130002573 A KR1020130002573 A KR 1020130002573A KR 20130002573 A KR20130002573 A KR 20130002573A KR 101447483 B1 KR101447483 B1 KR 101447483B1
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cosmetic composition
extract
fruit
organic solvent
extracted
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KR20140090474A (en
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김명화
권정희
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김명화
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    • HELECTRICITY
    • H02GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
    • H02SGENERATION OF ELECTRIC POWER BY CONVERSION OF INFRARED RADIATION, VISIBLE LIGHT OR ULTRAVIOLET LIGHT, e.g. USING PHOTOVOLTAIC [PV] MODULES
    • H02S30/00Structural details of PV modules other than those related to light conversion
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E10/00Energy generation through renewable energy sources
    • Y02E10/50Photovoltaic [PV] energy

Abstract

본 발명은 마로니에 열매 추출물을 함유하는 화장품 조성물에 관한 것으로, 도로변 가로수로 흔히 볼 수 있는 마로니에 열매를 채취하여 충분히 건조한뒤 세척하고 세척된 마로니에 열매에 유기용매를 가하여 용해한 뒤 상온에서 교반하면서 유용성분을 추출하고, 추출된 추출물은 여과하여 가온하면서 가압농축하여 화장품 조성물을 얻도록 함으로서, 저렴한 제조비용으로 켈세틴 등 각종 유용성분을 함유한 화장품 조성물을 얻을 수 있도록 하면서 천연유래물질로서의 안전성과 화장품에 첨가시 제형에 문제가 없는 안정성 및 항산화작용과 피부노화방지 등에 의한 사용성 등을 모두 만족시켜 줄 수가 있는 자연친화적인 화장품 조성물을 제공할 수 있도록 한 것이다.The present invention relates to a cosmetic composition containing a Marrony fruit extract, which is obtained by collecting marrony fruit commonly found on the roadside tree, thoroughly drying it, washing it, adding the organic solvent to the washed marrony, dissolving it, The extract is filtered and concentrated under pressure while heating to obtain a cosmetic composition. Thus, it is possible to obtain a cosmetic composition containing various useful ingredients such as kelecetin at an inexpensive manufacturing cost, The present invention provides a cosmetic composition that is environmentally friendly, which can satisfy both stability and antioxidative action with no problem in time formulation and usability due to prevention of skin aging and the like.

Description

마로니에 열매 추출물을 함유하는 화장품 조성물{COSMETIC COMPOSITION CONTAINED HORSE CHESTNUT EXTRACT}COSMETIC COMPOSITION CONTAINED HORSE CHESTNUT EXTRACT <br> <br> <br> Patents - stay tuned to the technology COSMETIC COMPOSITION CONTAINED HORSE CHESTNUT EXTRACT

본 발명은 마로니에 열매로부터 추출된 인체에 유익한 켈세틴 성분을 다량함유하는 화장품 조성물에 관한 것이다.The present invention relates to a cosmetic composition containing a large amount of a keletiline ingredient useful for human body extracted from horse chestnut fruit.

플라보노이드는 방향족 폴리페놀로서, 플라보놀(flavonol), 플라본(flavone), 안토시아니딘(anthocyanidin), 이소플라본(isoflavone) 등으로 분류된다.Flavonoids are aromatic polyphenols, which are classified as flavonol, flavone, anthocyanidin, isoflavone, and the like.

또한 폴리페놀은 벤젠고리(C6H6)의 수소 중 하나가 수산기(OH)로 치환된 물질을 말하며, 이와 같은 구조를 갖는 화합물은 자연계에 많이 존재한다.Also, polyphenol refers to a substance in which one of the hydrogen atoms of the benzene ring (C6H6) is substituted with a hydroxyl group (OH), and many compounds having such a structure exist in nature.

즉 녹차에 들어있는 카데킨류와 커피에 포함되어 있는 클로로겐산 그리고 딸기, 포도, 검은콩, 팥 등의 붉은색이나 자색의 안토시아닌계 색소 등은 모두 폴리페놀 화합물이다.That is, the reddish or purple anthocyanin pigments such as cadecins contained in green tea, chlorogenic acid contained in coffee, strawberry, grape, black bean, and red bean are all polyphenol compounds.

공개특허 특2000-0009820호 미용식 조성물 및 그 제조방법과 특허등록번호 10-0340763호 남성 생식기능 저하에 대한 예방 및 치료효과를 지닌 천연페놀 및 폴리페놀계 화합물을 포함하는 약제학적 조성물 및 특허등록번호 10-0671460호 폴리페놀을 함유한 기능성 알코올 음료 등은 폴리페놀과 관련한 대표적인 발명들로서, 이처럼 폴리페놀류는 강력한 항산화효과와 항염증 효과를 기대할 수가 있어 화장품과 식품 및 의약품 등의 원료로서 많은 관심과 주목을 받고 있다.Patent Application No. 2000-0009820 A cosmetic composition and method for producing the same, and Patent Registration No. 10-0340763 A pharmaceutical composition comprising a natural phenol and a polyphenol compound having a preventive and therapeutic effect on male reproductive dysfunction and a patent registration number 10-0671460 A functional alcoholic beverage containing polyphenol is a representative invention related to polyphenols. As such, polyphenols can be expected to have a strong antioxidative and anti-inflammatory effect, thus paying a lot of attention and attention as raw materials for cosmetics, foods, and pharmaceuticals .

또한 켈세틴(quercetin)은 일반적으로 당류와 에테르 결합을 한 배당체의 형태로서 양파, 사과, 포도를 비롯한 다양한 채소와 과일에 함유되어 있고, 체외실험에서 켈세틴과 초음파를 조합하여 치료할때 배양피부와 전립선 암세포는 악성이 아닌 세포에 비해 억제되었으며, 화학요법약물로서 대장종양 저항감도를 미소부수체(microsatellite)와 함께 증가시켰다는 연구결과가 보고된바 있다.In addition, quercetin is generally in the form of glycosides with sugar and ether bonds, and is contained in various vegetables and fruits, including onions, apples, grapes. In the in vitro experiment, when quercetin is combined with ultrasound, Prostate cancer cells have been inhibited compared to non-malignant cells, and research has been reported to increase resistance to colorectal tumor resistance as a chemotherapeutic agent with microsatellite.

최근까지도 방광암, 유방암, 결장암, 전립선암, 간암 등에 여러 종류의 암세포에 대하여도 켈세틴의 효능에 관한 연구가 활발히 진행되고 있으며, 그 결과 암세포를 억제하는데 어느 정도 효과가 있는 것으로 알려져 있다.Until recently, studies on the efficacy of keletil have been actively conducted on various types of cancer cells such as bladder cancer, breast cancer, colon cancer, prostate cancer, liver cancer, and the like, and it is known that cancer cells are somewhat effective in suppressing cancer cells.

또한 켈세틴은 비만세포 억제속성의 섬유근육치료 및 고혈압 치료에 효과적이고, 콜레스테롤을 감소시킬 뿐만 아니라 지방세포 생성을 억제한다고 알려져 있으며, 이외에도 면역세포증강과, 항바이러스와, 신경보호작용과, 항염작용 및 항노화에도 효과가 있는 것으로 알려져 있다.In addition, keletiline is known to be effective in the treatment of fibromyalgia and hypertension in mast cell inhibitory properties, and it is known that it not only reduces cholesterol but also inhibits adipocyte formation. In addition, it has immune cell enhancement, antiviral, Action and anti-aging.

한편 우리나라도 경제성장에 따른 일반인들의 생활수준향상으로 미에 대한 관심 및 욕구가 점차 높아짐에 따라 안전성과 안정성 및 사용성 등을 모두 만족하는 자연친화적인 천연화장품에 대한 관심이 높아지고 있는 만큼 화장품원료산업이 뒷받침되어야 하나, 현재 앞서 언급한 바와같이 인체에 매우 유익하고 또화장품 원료로서 주목받고 있는 켈세틴을 저렴한 비용으로 추출하기 위한 추출방법이 제공된바 없어 값싸고 간단한 방법으로 켈세틴을 추출할 수 있는 방법에 대한 연구가 절실히 요구되고 있는 것이 현실이다.Meanwhile, as Korea's economic growth has raised the level of living standards of the general public, interest and desire for beauty has gradually increased. Therefore, interest in nature-friendly natural cosmetics that satisfy both safety, stability and usability is increasing, However, as mentioned above, there is no extraction method for extracting keletil, which is very beneficial to the human body and is attracting attention as a cosmetic raw material, at a low cost as described above. Thus, a method of extracting keletil Research is urgently required.

본 발명의 목적은 주위에서 가로수로 흔히 찾아볼 수 있는 마로니에 열매로부터 천연기능성 화장품 원료로 이용할 수 있는 켈세틴을 추출하여 농축하는 기술을 확립하기 위한 마로니에 열매 추출물을 함유하는 화장품 조성물을 제공하는데 있다.It is an object of the present invention to provide a cosmetic composition containing a Marrony fruit extract for establishing a technique for extracting and concentrating keletil, which can be used as a raw material for natural functional cosmetics, from a marrony fruit commonly found as a row of trees around.

상기한 목적달성을 위한 본 발명 마로니에 열매 추출물을 함유하는 화장품 조성물은 세척 및 건조된 마로니에 열매에 유기용매를 가하여 용해한 상태에서 상온에서 교반하면서 유용성분을 추출하여 여과하고, 여과된 추출물은 가온하면서 가압, 농축하여 구성함을 특징으로 한다.In order to achieve the above object, the cosmetic composition of the present invention contains extracts of active ingredients in a washed and dried marrony with addition of an organic solvent and dissolving while stirring at room temperature, filtering the extracted extract, , And concentrated.

본 발명은 주위에서 가로수로서 흔히 찾아볼 수 있는 마로니에 열매로부터 켈세틴등 유용성분을 추출하여 농축한 화장품 조성물을 얻을 수 있도록 함으로서, 현저히 낮은 제조원가로 가격경쟁력을 높여줄 수가 있고 또 자연친화적인 천연화장품에 대한 관심이 고조되고 있는 현시점에서 안전성과 안정성 및 사용성 등을 모두 만족하는 화장품 원료를 제공할 수가 있게 됨은 물론 이러한 원료를 이용한 화장품의 제조, 사용 시 부작용이 전혀없이 항산화작용과 항염증작용 및 피부노화방지 등으로 사용자의 피부미용과 건강에 큰 도움을 줄 수가 있게 되는 등의 효과가 있는 것이다.The present invention enables a cosmetic composition to be obtained by extracting a useful ingredient such as kelecetin from a marrony fruit commonly found in the vicinity of a tree as a tree, thereby making it possible to enhance price competitiveness at a remarkably low production cost and to provide a natural- It is possible to provide cosmetic raw materials satisfying safety, stability, and usability at the current point where interest is increasingly high. In addition, there is no side effect when manufacturing and using cosmetic products using such a raw material, It is possible to provide a great benefit to the skin beauty and health of the user through anti-aging and the like.

이하 본 발명을 실시하기 위한 형태에 대하여 설명하기로 한다. 다만 본 발명의 실시예는 여러가지 형태로 변형될 수 있으므로 권리범위는 아래에서 상세히 설명되는 실시예로 한정되는 것으로 해석되어서는 아니되며, 본 발명의 요지를 불필요하게 흐릴 수 있다고 판단되는 공지기능 및 구성에 대한 상세한 기술은 생략하기로 한다.Hereinafter, embodiments for carrying out the present invention will be described. It is to be understood that both the foregoing general description and the following detailed description are exemplary and explanatory and are not to be construed as limiting the present invention. The present invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Will not be described in detail.

본 발명의 마로니에 열매 추출물을 함유하는 화장품 조성물은 마로니에 열매로부터 켈세틴(quercetin) 등 각종 유용성분을 포함하는 추출물을 함유하도록 하는 것을 특징으로 한다.The cosmetic composition containing the fruit extract of horse chestnut of the present invention is characterized in that an extract containing various useful components such as quercetin is contained in the horse chestnut fruit.

마로니에는 도로변의 가로수로 널리 이용되고 있는 것으로서, 10월 하순경에 채취한 열매를 10~20일간 통풍이 용이한 곳에서 자연건조한다.Marroni is widely used as the roadside tree of the roadside, and the fruit collected in the bottom of October is naturally dried for 10 ~ 20 days where ventilation is easy.

이때 마로니에 열매의 채취시기는 열매가 충분히 성숙된 시기를 말하며, 채취한 열매의 건조 또한 밀폐된 건조실 내에서 인공건조가 이루어지도록 할 수도 있으나, 추출하고자 하는 유효성분의 유지 및 극대화를 위하여는 자연건조해 주는 것이 바람직하다.At this time, the harvesting time of the marronies refers to the time when the fruit is fully matured, and the harvested fruit can be dried or artificially dried in the closed drying chamber. However, in order to maintain and maximize the active ingredient to be extracted, It is desirable to do it.

건조된 마로니에 열매는 정제수로 깨끗이 세척한 뒤 유기용매를 가하여 용해한 상태에서 상온에서 교반하면서 켈세틴 등 유용성분을 추출토록 한다.Dried horse chestnut fruit is cleaned with purified water, then dissolved with organic solvent, and stirred at room temperature to extract useful components such as keletil.

이때 이용되는 유기용매는 에탄올과 해양심층수를 6:4 ~ 8:2로 혼합하여서 된 것으로서, 마로니에 열매 1㎏에 유기용매 4~6리터를 투입하여 용해시켜 주도록 하고 또 용해된 용해물은 상온에서 80~120rpm의 속도로 교반되게 하면서 유효성분을 추출토록 하여 유용성분의 추출과정에서 유용성분의 파괴를 방지하면서 최적의 온도 및 원심력하에서 유용성분의 추출을 극대화할 수 있도록 한다.The organic solvent used is a mixture of ethanol and deep sea water at a ratio of 6: 4 to 8: 2. 4 to 6 liters of an organic solvent is added to 1 kg of horse chestnut fruit, and the dissolved lysate is dissolved at room temperature The active ingredient is extracted while being stirred at a speed of 80 to 120 rpm so as to maximize the extraction of the useful ingredient under optimal temperature and centrifugal force while preventing destruction of the useful ingredient in the extraction process of the useful ingredient.

그리고 교반을 통하여 추출된 추출물은 여과지로 여과하고 또 여과된 추출물은 가온하면서 가압, 농축하여 화장품 조성물을 얻도록 구성된다.Then, the extract extracted through agitation is filtered with a filter paper, and the filtered extract is pressurized and concentrated while being warmed to obtain a cosmetic composition.

이러한 추출물을 여과하여 가온하면서 가압농축하여 화장품 조성물을 얻도록 할시 반복된 실험결과에 의하면, 유용성분들 중 켈세틴의 효과적인 분리를 위하여는 No2에 해당하는 공극을 가진 여과지를 사용하는 것이며, 여과후 농축시에도 40~60℃로 가온한 상태에서 280~320㎜Hg의 기압으로 가압해 주어야만 추출물에 남아있는 용매를 단시간에 증발시켜 줄 수가 있게 된다.According to the results of repeated experiments conducted to obtain a cosmetic composition by filtering and heating the extract while heating, a filter paper having pores corresponding to No. 2 is used for effective separation of keletiline among the oil soluble components, It is necessary to pressurize at a pressure of 280 ~ 320 mmHg in a state of being warmed to 40 ~ 60 ° C, so that the solvent remaining in the extract can be evaporated in a short time.

따라서 본 발명은 도로변의 가로수로 식재되는 마로니에 열매로부터 켈세틴 등 유용성분을 추출하여 켈세틴을 함유한 화장품 조성물을 얻도록 하고 또 채취한 마로니에 열매를 건조하여 유기용매를 가한후 상온에서 교반하여 유용성분을 추출하고 또 추출된 유용성분을 여과하여 가온상태에서 가압, 농축하여 화장품 조성물을 얻기까지의 과정이 큰 어려움 없이 저렴한 비용부담으로 이루어질 수가 있게 된다.Accordingly, the present invention provides a cosmetic composition containing keletil, which is obtained by extracting useful components such as keletil from a marrony fruit cultivated on the roadside of a roadside tree, drying the fruit on the marrow harvested, adding an organic solvent, The components are extracted and the extracted useful components are filtered to obtain a cosmetic composition by pressurization and concentration under heating. The process can be performed at a low cost without any difficulty.

또한 본 발명을 통하여 얻게 되는 화장품 조성물은 천연유래물질로서 안전성을 보장해 줄 수가 있고 또 화장품의 제조시 원료로 첨가하여도 제형에 문제가 없어 안정성을 보장해 줄 수가 있으며, 켈세틴의 대표적인 효능인 항산화효과와 피부노화방지 등으로 사용성을 만족시켜 줄 수가 있게 된다.In addition, the cosmetic composition obtained through the present invention can guarantee safety as a naturally derived material, and even when it is added as a raw material in the production of cosmetics, there is no problem in formulation and stability can be ensured, and the antioxidant effect And anti-aging of the skin.

더 나아가 본 발명 화장품 조성물을 원료로 한 화장품의 제조사용시 켈세틴은 체내독소배출에 뛰어난 작용을 하고, 강력한 항산화작용을 하고, 수은이나 카드뮴등 각종 유해물질들을 포획하여 사멸시키고, 항바이러스와, 항암작용과, 항염증과, 비만억제 및 대사증후군에 대한 효과 등 사용자의 피부미용과 건강에 큰 도움을 줄 수가 있게 되는 것이다.Furthermore, in the manufacture of cosmetics using the cosmetic composition of the present invention, keletiline exerts an excellent effect on toxin release in the body, has a strong antioxidative effect, captures and kills various harmful substances such as mercury and cadmium, And anti-inflammatory, anti-obesity, and metabolic syndrome effects on the user's skin beauty and health can be greatly helped.

Claims (6)

채취한 마로니에 열매를 건조하여 정제수로 세척하고, 세척된 마로니에 열매에 유기용매를 가하여 용해하고, 용해된 용해물은 상온에서 교반하여 유용성분을 추출하며, 추출된 추출물은 여과하여 가온하면서 가압, 농축하여서된 마로니에 열매 추출물을 함유하는 화장품 조성물에 있어서, 상기 유기용매는 에탄올 60~80중량부에 대하여 해양심층수 20~40중량부를 혼합하여 얻은 다음 마로니에열매 1㎏에 유기용매 4~6리터를 투입하여 용해가 이루어지도록 하고, 유기용매가 가해진 마로니에 열매를 상온에서 교반하여 유용성분을 추출할시 80~120rpm의 속도로 교반이 이루어지도록 하고, 추출된 추출물의 여과는 No2에 해당하는 공극의 와트만여과지에 의해 여과가 이루어지도록 하고, 추출물의 가온시에는 40~60℃의 온도가 주어지도록 하며, 여과된 추출물을 가온하면서 가압하여 농축할시에는 280~320㎜Hg의 기압력을 가해 주도록 함을 특징으로 하는 마로니에 열매 추출물을 함유하는 화장품 조성물.The extracted marrow is dried, washed with purified water, dissolved in an organic solvent to the washed marrow, and the dissolved lysate is stirred at room temperature to extract a useful ingredient. The extracted extract is filtered, Wherein the organic solvent is obtained by mixing 20 to 40 parts by weight of deep sea water with respect to 60 to 80 parts by weight of ethanol and then adding 4 to 6 liters of an organic solvent to 1 kg of fruit in a marronier to prepare a cosmetic composition, When the active ingredient is extracted by stirring the fruit at the room temperature with the organic solvent-applied marrow, stirring is carried out at a speed of 80 to 120 rpm. Filtration of the extracted extract is carried out by using Wattmann filter paper And the extract is heated at a temperature of 40 to 60 DEG C, and the filtered extract And a pressure of 280 to 320 mmHg is applied when the composition is pressurized and concentrated while warmed. 삭제delete 삭제delete 삭제delete 삭제delete 삭제delete
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