KR101378361B1 - Coagulating agent - Google Patents
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- KR101378361B1 KR101378361B1 KR1020080027045A KR20080027045A KR101378361B1 KR 101378361 B1 KR101378361 B1 KR 101378361B1 KR 1020080027045 A KR1020080027045 A KR 1020080027045A KR 20080027045 A KR20080027045 A KR 20080027045A KR 101378361 B1 KR101378361 B1 KR 101378361B1
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
- C02F1/5245—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents using basic salts, e.g. of aluminium and iron
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
- C02F1/56—Macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/32—Nature of the water, waste water, sewage or sludge to be treated from the food or foodstuff industry, e.g. brewery waste waters
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- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Abstract
(과제) 이 발명은 응집제의 사용량이 시판품보다 적고, 게다가 응집 후의 침전물이 음식물 쓰레기 처리 가능한 화학 물질인 것을 특징으로 하고, 처리 후의 배수에 대해서도 환경 기준 (BOD 및 COD) 을 따른 응집제를 개발하는 것에 있다. (Problem) The present invention is characterized in that the amount of flocculant used is less than that of commercially available products, and the precipitate after flocculation is a chemical substance that can treat food waste. have.
(해결 수단) 천연 유기산이 1 ∼ 3 중량퍼센트, 황산암모늄알루미늄이 40 ∼ 55 중량퍼센트, 황산나트륨알루미늄이 7 ∼ 10 중량퍼센트, 평균 분자량이 900 만 ∼ 1000 만인 아크릴아미드·폴리머가 8 ∼ 15 중량퍼센트, 탄산나트륨이 20 ∼ 25 중량퍼센트 (pH 조정값으로서, 6.5 ∼ 7.5 부근으로 설정) 를 함유하는 것을 특징으로 하는 응집제이며, 천연 유기산이 시트르산, 락트산, 락트산철에서 선택된 것이다. (Solution) 1 to 3 weight percent of natural organic acid, 40 to 55 weight percent of aluminum ammonium sulfate, 7 to 10 weight percent of sodium aluminum sulfate, and 8 to 15 weight percent of acrylamide polymer having an average molecular weight of 9 million to 10 million. Sodium carbonate contains 20 to 25% by weight (a pH adjustment value, set at around 6.5 to 7.5), and a coagulant is selected from citric acid, lactic acid and iron lactate.
Description
이 발명은 공사 현장으로부터의 배수, 식품 소재를 사용한 공장이나 가정으로부터의 생활 배수 물질을 소량으로 응집 침전을 발생시키고, 처리 후의 배수에 대해서도 환경 기준 (BOD 및 COD) 을 따른 응집제에 관한 것이다. This invention relates to the flocculation agent which conforms to environmental standards (BOD and COD) about the wastewater from a construction site, the coagulation sedimentation | generation of a small amount of the domestic wastewater material from a factory or a home using a food material, and the wastewater after processing.
종래, 공사 현장으로부터의 배수, 식품 소재를 사용한 공장이나 가정으로부터의 생활 배수의 처리에 대해서는, 환경 규제법이 있음에도 불구하고, 하수 등으로 방류하여 공공 기관에서의 처리에 의지하고 있는 것이 현상황이다. Background Art Conventionally, the present situation is about the wastewater from a construction site, the processing of the domestic wastewater from a factory and a home using a food material, although there is an environmental regulation law, it is discharged to sewage or the like and resorted to processing in public institutions.
특히, 공사 현장으로부터는 토양 오니를 함유하는 배수, 식품 소재를 사용한 생활 배수로서는, 소면 공장 등의 공장으로부터의 배수, 가정으로부터의 쌀 씻은 물, 감자전분을 함유하는 배수 등이 존재한다. In particular, from the construction site, there are drainages containing soil sludge, and drainages from factories such as a noodle factory, rice-washed water from homes, drainages containing potato starch, and the like.
그 때문에, 여러 가지 응집제가 시판되고 있지만, 배수의 종류에 따라서는 그 효과가 충분히 활용되지 않아 문제가 남아 있다. 예를 들어, 특허 문헌 1 과 같이. Therefore, although various flocculants are commercially available, the effect is not fully utilized depending on the kind of wastewater, and a problem remains. For example, as in Patent Document 1.
특허 문헌 1 : 일본 공개특허공보 2005-118675호Patent Document 1: Japanese Unexamined Patent Publication No. 2005-118675
그래서 이 발명은, 응집제의 사용량이 시판품보다 적고, 게다가 응집 후의 침전물이 음식물 쓰레기 처리 가능한 화학 물질이며, 처리 후의 배수에 대해서는 환경 기준을 따른 지구 환경의 보호를 기도할 수 있는 응집제를 개발하는 것에 있다. Therefore, the present invention is to develop a flocculant that uses less flocculant than commercially available products, and the precipitate after flocculation is a chemical substance capable of treating food waste, and which can pray for the protection of the global environment according to environmental standards for the wastewater after treatment. .
이 발명, 상기의 목적을 달성하기 위해서, 이하의 수단을 채용하는 것이다. In order to achieve this invention and the above object, the following means are employed.
이 발명의 응집제는, 천연 유기산이 1 ∼ 3 중량퍼센트, 황산암모늄알루미늄이 40 ∼ 55 중량퍼센트, 황산나트륨알루미늄이 7 ∼ 10 중량퍼센트, 평균 분자량이 900 만 ∼ 1000 만인 아크릴아미드·폴리머가 8 ∼ 15 중량퍼센트, 탄산나트륨이 20 ∼ 25 중량퍼센트 (pH 조정치로서, 6.5 ∼ 7.5 부근으로 설정) 를 함유하는 것을 특징으로 하는 것이다. The coagulant of this invention is 1-15 weight% of natural organic acids, 40-55 weight% of aluminum ammonium sulfate, 7-10 weight% of sodium aluminum sulfate, and 8-15 of acrylamide polymers whose average molecular weights are 9 million-10 million. The weight percent and sodium carbonate contain 20 to 25 weight percent (set to 6.5 to 7.5 as the pH adjustment value).
그리고, 이 발명에 사용하는 천연 유기산은, 시트르산, 락트산, 락트산철에서 선택된 것이다. The natural organic acid used in the present invention is selected from citric acid, lactic acid and iron lactate.
이 발명의 응집제에 의하면, 다방면에 걸쳐서의 배수에 대해 사용한 결과, 응집제의 사용료가 종래품보다 적고, 응집 후의 침전물이 음식물 쓰레기 처리 가능한 화학 물질이며, 처리 후의 배수에 대해서도 환경 기준 (BOD 및 COD) 을 따른 것으로 우수한 효과를 나타낸다. According to the flocculant of this invention, as a result of using it for drainage over various aspects, the fee for use of the flocculant is less than that of the conventional products, and the precipitate after flocculation is a chemical substance capable of treating food waste, and environmental standards (BOD and COD) are also used for the drainage after treatment. By following it shows excellent effect.
이하, 이 발명의 바람직한 실시형태에 대해서 상세하게 설명하면, 천연 유기산이 1 ∼ 3 중량퍼센트, 황산암모늄알루미늄이 40 ∼ 55 중량퍼센트, 황산나트륨알루미늄이 7 ∼ 10 중량퍼센트, 평균 분자량이 900 만 ∼ 1000 만인 아크릴아미드·폴리머가 8 ∼ 15 중량퍼센트, 탄산나트륨이 20 ∼ 25 중량퍼센트 (pH 조정값으로서, 6.5 ∼ 7.5 부근으로 설정) 를 함유하는 것을 특징으로 하는 응집제로 구성되는 것이다. EMBODIMENT OF THE INVENTION Hereinafter, if it demonstrates in detail about preferred embodiment of this invention, 1 to 3 weight% of natural organic acid, 40 to 55 weight% of aluminum ammonium sulfate, 7 to 10 weight% of sodium aluminum sulfate, and 9-10 million weight average molecular weight It consists of a coagulant characterized by containing 8-15 weight% of full acrylamide polymers, and 20-25 weight% of sodium carbonate (set to 6.5-7.5 vicinity as pH adjustment value).
다음으로, 이 발명의 하나의 실시예 (응집제 A) 에 대해 상세히 서술하면, Next, one Example (coagulant A) of this invention is described in detail,
으로 구성되는 것이다. 〔단위는, 중량퍼센트〕. [Unit is weight percent]
또한, 이 발명의 다른 실시예 (응집제 B) 에 대해 상세히 서술하면,Moreover, if another Example (coagulant B) of this invention is described in detail,
으로 구성되는 것이다. 〔단위는, 중량퍼센트〕. [Unit is weight percent]
다음으로, 토양 오니 처리에 대한 결과를 설명하면, Next, explaining the results of the treatment of soil sludge,
유사의 토양 오니 배수 200 밀리리터 (이하, ㎖) 에, 본 발명의 응집제 (A), 본 발명의 응집제 (B), 그리고, 시판품을 사용하여 그 효과를 비교 검토하였다.The effect was compared and examined using the flocculant (A) of this invention, the flocculant (B) of this invention, and a commercial item in 200 milliliters (hereinafter, ml) of similar soil sludge drainage.
그 결과, 시판품에서는, 800㎎ 을 필요로 했지만, 본 발명의 응집제 (A) 에 서는 200㎎, 본 발명의 응집제 (B) 에서는 300㎎ 정도 투입하여 교반하면, 응집 침전이 발생하는데, 상청 수용액의 투과도는 본 발명의 응집제 (A) 쪽이 양호한 투과 결과가 얻어졌다. As a result, although 800 mg was required for a commercial item, in the flocculant (A) of this invention, about 200 mg and about 300 mg in the flocculant (B) of this invention were added and stirred, agglomeration precipitation generate | occur | produced, The permeability | permeability obtained the permeation | transmission result favorable for the coagulant (A) of this invention.
다음으로, 감자전분을 함유하는 배수 처리에 대한 결과를 설명하면, Next, the results of the drainage treatment containing potato starch,
유사 처리제인 본 발명의 응집제 (A) 의 효력 시험으로서, 감자전분 10g/l 및 20g/l 의 배수를 시작 (試作) 하여, 각각 200㎖ 에 대하여 본 발명의 응집제 (A) 200㎎ 및 300㎎ 을 첨가하여 응집 상태를 관찰하였다. As the potency test of the flocculant (A) of the present invention which is a similar treatment agent, drainage of 10 g / l and 20 g / l potato starch was started, and 200 mg and 300 mg of the flocculant (A) of the present invention were added to 200 ml, respectively. Was added to observe the aggregation state.
그 결과, 어느 조건 하에 있어서도 양호한 응집 침전이 확인되었다. As a result, good coagulation precipitation was confirmed under all conditions.
그래서, 본 발명의 응집제 (A) 의 능력 시험으로서, 감자전분 배수 10g/l 에 대한 첨가량을 구한 결과, 최소 첨가량으로서 40㎎ 인 것을 알 수 있었다. Therefore, as a capability test of the flocculant (A) of this invention, when the addition amount with respect to 10 g / l of potato starch drainage was calculated | required, it turned out that it is 40 mg as a minimum addition amount.
다음으로, 쌀 씻은 물 배수 처리에 대한 결과를 설명하면, Next, describing the results for the treatment of rice-washed water drainage,
쌀 4 합에 대하여 통상적인 씻기 방법을 행하여, 처음에는 두번째로 씻은 배수를 합친 것을 20O㎖ 사용하였다. A conventional washing method was performed for 4 rice mixtures, and 20OmL of the sum of the first washed drainage waters was used.
응집제로서는, 본 발명의 응집제 (A) 와 시판품을 첨가하여 그 효력을 비교하였다. As a flocculant, the flocculant (A) of this invention and a commercial item were added, and the effect was compared.
그 결과, 본 발명의 응집제 (A) 에서는 170㎎ 을 첨가한 시점에서 응집이 시작되어, 25O㎎ 에서 거의 응집이 완결되는 것을 알 수 있었다. As a result, in the coagulant (A) of the present invention, aggregation was started when 170 mg was added, and it was found that aggregation was almost completed at 250 mg.
최종적으로는 500㎎ 이 필요하다고 생각된다. 또, 플록의 응집은 시간의 경과와 함께 상부에 집합되는 것이 관찰되었다. Finally, 500 mg is considered necessary. In addition, flocculation was observed to be gathered at the top with the passage of time.
한편, 시판품에서는 800㎎ 을 첨가해도, 전혀 응집은 발생되지 않고, 백색 현탁 상태이었다. On the other hand, even if it added 800 mg, in the commercial item, aggregation did not occur at all and was in a white suspended state.
또한, 우동의 뜨거운 국물 배수 처리에 대한 결과를 설명하면, In addition, the results of the hot broth drainage treatment of udon,
시판되는 우동 20 개를 3ℓ 의 뜨거운 물 (90℃ 이상) 중에서 푼 뜨거운 국물을 실험에 사용하였다. 뜨거운 국물을 8 배 희석, 4 배 희석 및 2 배 희석시킨 200㎖ 의 용액에 응집제로서, 본 발명의 응집제 (A) 를 사용하고, 8 배 희석에서는 135㎎, 4 배 희석에서는 195㎎, 2 배 희석에서는 350㎎ 을 첨가하였다. 발생된 플록은 전분을 응집하고 있기 때문에, 용액 중에 부유한 상태가 되어 응집되는 모습이 관찰되었다. The hot broth extracted from 3 commercially available udon noodles in 3 liter of hot water (90 degreeC or more) was used for the experiment. In a 200 ml solution in which hot broth was diluted 8-fold, 4-fold and 2-fold, the flocculant (A) of the present invention was used, and at 8-fold dilution, 135 mg, 1-95 mg, 2-fold In dilution 350 mg was added. Since the generated floc aggregated starch, the floc which became floating in the solution and was aggregated was observed.
그리고, 이 발명의 응집제 (A) 와 응집제 (B) 를 사용하여, 토양 오니, 감자전분, 우유를 각각 용해시킨 배수 및 쌀 씻은 물 등을 처리한 배수에 대한 pH 를, 하기의 표 1 에 나타낸다. And using the flocculant (A) and the flocculant (B) of this invention, the pH with respect to the wastewater which processed soil sludge, potato starch, the milk which melt | dissolved respectively, rice wash water, etc. is shown in Table 1 below. .
이 표 1 로부터도 알 수 있는 바와 같이, 이 발명의 응집제 (A), 응집제 (B) 모두, 중성영역에 있는 것으로, 바람직한 배수 기준을 클리어하고 있는 것을 알 수 있다. 따라서, 종래품의 응집제와 비교해도 손색이 없는 것이 판명되었다. As can be seen from Table 1, it can be seen that both the coagulant (A) and the coagulant (B) of the present invention are in the neutral region, thereby clearing a preferable drainage standard. Therefore, it turned out that there is no inferiority even compared with the conventional flocculant.
다음으로, 시판품의 우유의 배수 처리에 대한 결과를 설명하면, Next, when the result about the drainage treatment of the milk of a commercial item is demonstrated,
우유 10㎖ 에 20 배량 ∼ 100 배량의 물을 첨가하여 희석시킨 후, 이 발명의 응집제 (A) 140㎎ ∼ 660㎎ 을 첨가하여, 응집 상태를 관찰하였다. 그 결과, 양호한 우유 배수 처리 조건으로는, 30 배량 ∼ 70 배량의 물을 첨가하여 희석시킨 후, 이 발명의 응집제 (A) 240㎎ ∼ 600㎎ 을 첨가함으로써, 플록의 응집이 확인되었다. 그 중에서도, 가장 양호한 처리 조건으로서는, 50 배량의 물로 희석시켜, 응집제 (A) 240㎎ 을 첨가한 조건으로, 플록의 응집은 시간의 경과와 함께 진행되어, 용액 중에 부유한 후, 플록의 성장이 진행되어 침전되는 것이 관찰되었다. 〔표 2 참조〕After diluting by adding 20 times-100 times the amount of water to 10 ml of milk, 140 mg-660 mg of flocculants (A) of this invention were added, and the aggregation state was observed. As a result, as favorable milk drainage treatment conditions, floc flocculation was confirmed by adding 240 mg-600 mg of the flocculant (A) of this invention after adding and diluting 30 times-70 times of water. Among them, as the best treatment conditions, flocculation of flocs proceeds with the passage of time under the condition of dilution with 50 times the amount of water and the addition of 240 mg of the flocculant (A). Progression and precipitation were observed. [See Table 2]
이 표 2 로부터도 알 수 있는 바와 같이, 이 발명의 응집제 (A) 는, 어느 응집제를 첨가한 경우에도, 중성영역에 있는 것으로, 바람직한 배수 기준을 클리어하고 있는 것을 알 수 있다. 따라서, 종래품의 응집제와 비교해도 손색이 없는 것이 판명되었다. As can be seen from Table 2, even when any flocculant is added, the flocculant (A) of the present invention is in the neutral region, and it can be seen that the desired drainage standard is cleared. Therefore, it turned out that there is no inferiority even compared with the conventional flocculant.
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| Application Number | Priority Date | Filing Date | Title |
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| JPJP-P-2008-00016666 | 2008-01-28 | ||
| JP2008016666A JP5216338B2 (en) | 2008-01-28 | 2008-01-28 | Flocculant |
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| Publication Number | Publication Date |
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| KR20090082840A KR20090082840A (en) | 2009-07-31 |
| KR101378361B1 true KR101378361B1 (en) | 2014-03-27 |
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| JP (1) | JP5216338B2 (en) |
| KR (1) | KR101378361B1 (en) |
| CN (1) | CN101497468A (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR101298125B1 (en) | 2012-01-26 | 2013-08-21 | (주) 에코솔루텍 | Manufacture method of high functional cohesive agent for water-treatment |
| CN102745787B (en) * | 2012-06-29 | 2014-01-01 | 武汉钢铁(集团)公司 | Fast flocculating agent and its preparation method |
| CN102976466A (en) * | 2012-12-11 | 2013-03-20 | 常州大学 | Compound barium remover for treating baric wastewater |
| KR102021502B1 (en) * | 2015-12-04 | 2019-09-16 | 주식회사 엘지화학 | Coagulum of abs resin and mehtod of preparation of abs resin using the same |
| CN106517465A (en) * | 2016-12-10 | 2017-03-22 | 钦州学院 | Compound type flocculating agent and preparation method thereof |
| CN106517466A (en) * | 2016-12-10 | 2017-03-22 | 钦州学院 | Quick flocculant and preparing method thereof |
| CN110386651B (en) * | 2018-04-20 | 2022-06-28 | 上海四奥化工有限公司 | Polyacrylamide flocculant for tailings and preparation method thereof |
| CN109608020A (en) * | 2018-12-18 | 2019-04-12 | 安徽建筑大学 | A kind of composite flocculation agent and preparation method thereof for Treatment of Sludge |
| CN109607727A (en) * | 2018-12-18 | 2019-04-12 | 安徽建筑大学 | A kind of mixed flocculation agent and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR19980081423A (en) * | 1997-04-16 | 1998-11-25 | 이데이노부유끼 | Polymer flocculant, the manufacturing method of this flocculant, and the water treatment method using this flocculant |
| KR20010033053A (en) * | 1997-12-15 | 2001-04-25 | 쯔쇼산교쇼 고교기쥬쯔인쵸가 다이효스루 니혼고꾸 | Method of removing harmful ions and remover for use in the same |
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| JP4552287B2 (en) * | 2000-08-07 | 2010-09-29 | 関西電力株式会社 | Jellyfish processing apparatus and processing method |
| JP3925123B2 (en) * | 2001-07-26 | 2007-06-06 | 関西電力株式会社 | Jellyfish processing apparatus and processing method |
| JP2003236562A (en) * | 2002-02-20 | 2003-08-26 | Mitsubishi Paper Mills Ltd | Method for treating boron-containing waste water |
| JP2004074001A (en) * | 2002-08-16 | 2004-03-11 | Awa Reiji Co Ltd | Cleaning agent for organic pollution drainage |
| JP4549962B2 (en) * | 2005-11-22 | 2010-09-22 | 株式会社トクヤマ | Foamable solid flocculant for water treatment |
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2008
- 2008-01-28 JP JP2008016666A patent/JP5216338B2/en not_active Expired - Fee Related
- 2008-03-24 KR KR1020080027045A patent/KR101378361B1/en active IP Right Grant
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR19980081423A (en) * | 1997-04-16 | 1998-11-25 | 이데이노부유끼 | Polymer flocculant, the manufacturing method of this flocculant, and the water treatment method using this flocculant |
| KR20010033053A (en) * | 1997-12-15 | 2001-04-25 | 쯔쇼산교쇼 고교기쥬쯔인쵸가 다이효스루 니혼고꾸 | Method of removing harmful ions and remover for use in the same |
Also Published As
| Publication number | Publication date |
|---|---|
| JP5216338B2 (en) | 2013-06-19 |
| CN101497468A (en) | 2009-08-05 |
| JP2009172555A (en) | 2009-08-06 |
| KR20090082840A (en) | 2009-07-31 |
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