KR101286798B1 - A manufacturing the same for composition method and composition of detergent for electrical machines insulation - Google Patents
A manufacturing the same for composition method and composition of detergent for electrical machines insulation Download PDFInfo
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- KR101286798B1 KR101286798B1 KR1020130012769A KR20130012769A KR101286798B1 KR 101286798 B1 KR101286798 B1 KR 101286798B1 KR 1020130012769 A KR1020130012769 A KR 1020130012769A KR 20130012769 A KR20130012769 A KR 20130012769A KR 101286798 B1 KR101286798 B1 KR 101286798B1
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- composition
- dichloroethane
- tetrafluoroethane
- weight
- insulation
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- 239000000203 mixture Substances 0.000 title claims abstract description 41
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 238000009413 insulation Methods 0.000 title claims description 32
- 238000000034 method Methods 0.000 title description 5
- 239000003599 detergent Substances 0.000 title 1
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 31
- 239000011707 mineral Substances 0.000 claims abstract description 31
- 238000004891 communication Methods 0.000 claims abstract description 13
- 235000015096 spirit Nutrition 0.000 claims abstract description 12
- WMIQCCDZARURRI-UHFFFAOYSA-N 1,1-dichloroethane Chemical compound CC(Cl)Cl.CC(Cl)Cl WMIQCCDZARURRI-UHFFFAOYSA-N 0.000 claims description 21
- 238000004140 cleaning Methods 0.000 claims description 15
- CDOGRWFBFCCGDR-UHFFFAOYSA-N 1,1,1,2-tetrafluoroethane Chemical compound FCC(F)(F)F.FCC(F)(F)F CDOGRWFBFCCGDR-UHFFFAOYSA-N 0.000 claims description 14
- 239000012459 cleaning agent Substances 0.000 claims description 12
- 238000010292 electrical insulation Methods 0.000 claims description 3
- LVGUZGTVOIAKKC-UHFFFAOYSA-N 1,1,1,2-tetrafluoroethane Chemical compound FCC(F)(F)F LVGUZGTVOIAKKC-UHFFFAOYSA-N 0.000 abstract description 5
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 1
- 230000035943 smell Effects 0.000 abstract 1
- 230000015556 catabolic process Effects 0.000 description 11
- 238000012360 testing method Methods 0.000 description 11
- 238000003756 stirring Methods 0.000 description 6
- 235000019645 odor Nutrition 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- GGNNRMGTGPKLNB-UHFFFAOYSA-N ClC(C)Cl.FC(CF)(F)F Chemical compound ClC(C)Cl.FC(CF)(F)F GGNNRMGTGPKLNB-UHFFFAOYSA-N 0.000 description 4
- 239000000428 dust Substances 0.000 description 4
- 230000001105 regulatory effect Effects 0.000 description 4
- 241000220259 Raphanus Species 0.000 description 3
- 235000006140 Raphanus sativus var sativus Nutrition 0.000 description 3
- 239000000356 contaminant Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000014509 gene expression Effects 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000003507 refrigerant Substances 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 238000004378 air conditioning Methods 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/50—Solvents
- C11D7/5004—Organic solvents
- C11D7/5018—Halogenated solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/28—Organic compounds containing halogen
- C11D7/30—Halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/14—Hard surfaces
- C11D2111/22—Electronic devices, e.g. PCBs or semiconductors
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/24—Hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
Description
본 발명은 통전기기 절연 세척제용 조성물 및 이의 제조방법에 관한 것으로, 더욱 상세하게는 절연성을 유지한 상태로 통신장비(전기장비설비 및 패널) 내부에 잔존하여 불량요인이 될 수 있는 이물질(먼지, 그리스, 레진 등)을 신속하게 제거함과 동시에 냄새가 없는 통전기기 절연 세척제용 조성물 및 이의 제조방법에 관한 것이다.The present invention relates to a composition for electric insulation cleaner and a method of manufacturing the same, more specifically, foreign matter (dust, Grease, resin, etc.) and the odorless and electrically conductive insulation cleaning composition and a method for producing the same.
종래의 각종 세척제는 무기염류와 계면활성제 등으로 조성한 세척제가 있으나 한정된 기능에 의하여 사용범위가 극히 제한되어 있다. 또한, 반고형 오물세척용 세척제의 경우에 있어서는 대부분이 세척능력을 갖는 성분에 마찰성 물질을 첨가하여 사용시 경도가 큰 마찰성 물질을 배합한 세척제는 그 사용 빈도가 높을 경우 피세척물의 표면이 마모되어 손상을 입게 되고 기계류의 경우에는 정확도를 상실하게 된다. 더 심각한 문제로 대부분의 세척제에는 사용시 유해한 향과 같은 냄새와 전원이 단락된 상태에서 사용되지 못한다는 것이 있다. 따라서 해당 기술분야에서는 이와 같은 문제점을 해결할 수 있는 세척제에 대한 기술 개발이 요구되고 있다.Conventional various cleaning agents include cleaning agents composed of inorganic salts and surfactants, etc., but the use range is extremely limited due to limited functions. In addition, in the case of semi-solid dirt cleaning agent, the most of the cleaning agent is a compound that has the ability to wash, and the compound that has high hardness when used is a cleaning agent that wears and damages the surface of the object. And the accuracy of machinery is lost. A more serious problem is that most cleaners cannot be used in the presence of short circuits and odors such as harmful odors. Therefore, there is a need in the art to develop a technology for a cleaning agent that can solve such problems.
본 발명의 목적은 상기한 바와 같은 종래의 특성을 개선하기 위하여 제안된 것으로서, 절연성을 유지한 상태로 통신장비(전기장비설비 및 패널) 내부에 잔존하여 불량요인이 될 수 있는 이물질(먼지, 그리스, 레진 등)을 신속하게 제거함과 동시에 냄새가 없는 통전기기 절연 세척제용 조성물 및 이의 제조방법을 제공함에 있다.An object of the present invention has been proposed to improve the conventional characteristics as described above, foreign matter (dust, grease) remaining in the interior of the communication equipment (electrical equipment and panels) to maintain the insulation can be a bad factor , Resins, etc.) to quickly remove the odor and at the same time provide a composition for an electrical insulation cleaner for the odor and its manufacturing method.
본 발명은 앞서 본 목적을 달성하기 위하여 다음과 같은 구성을 가진다.The present invention has the following structure in order to achieve the above object.
본 발명의 통전기기 절연 세척제용 조성물은, 1,1-디클로로에탄(1,1-DICHLOROETHANE): 15~20 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3):55~65 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 18~20 중량%로 구성된다.The composition for the electrical insulating machine insulation cleaner of the present invention, 1,1-dichloroethane (1,1-DICHLOROETHANE): 15 to 20% by weight, mineral spirit 66/3 (MINERAL SPIRITS 66/3): 55 to 65% by weight and 1,1,1,2-tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE): 18 to 20% by weight.
그리고 본 발명의 통전기기 절연 세척제용 조성물은, 1,1-디클로로에탄(1,1-DICHLOROETHANE): 20 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3):60 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 20 중량%로 구성되는 것이 바람직하다.In addition, the composition for the electrical insulating machine insulation cleaner of the present invention, 1,1-dichloroethane (1,1-DICHLOROETHANE): 20% by weight, mineral spirit 66/3 (MINERAL SPIRITS 66/3): 60% by weight and 1,1 , 1,2-tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE): It is preferably composed of 20% by weight.
한편 본 발명의 통전기기 절연 세척제용 조성물을 제조하기 위한 방법으로써, 1,1-디클로로에탄(1,1-DICHLOROETHANE), 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3) 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE)을 각각 1:1:3의 중량비가 되도록 혼합하여 제조된다.On the other hand, as a method for producing a composition for the electrical insulating machine insulation cleaning agent of the present invention, 1,1-dichloroethane (1,1-DICHLOROETHANE), mineral spirit 66/3 (MINERAL SPIRITS 66/3) and 1,1,1, 2-Tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE) is prepared by mixing to a weight ratio of 1: 1: 3, respectively.
그리고 본 발명의 통전기기 절연 세척제용 조성물 제조방법은, 1,1-디클로로에탄(1,1-DICHLOROETHANE) 1 중량비, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3) 1 중량비 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE) 3 중량비를 각각 혼합기에 개별적으로 투입하며 5분간 교반하여 제조되는 것이 바람직하며, 20~50℃ 사이에서 이루어지는 것이 바람직하다.And the method for producing a composition for the electrical insulating machine insulation cleaner of the present invention, 1,1-dichloroethane (1,1-DICHLOROETHANE) 1 weight ratio, mineral spirit 66/3 (MINERAL SPIRITS 66/3) 1 weight ratio and 1,1,1 , 2-Tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE) 3 weight ratios are added to the mixer separately, and preferably prepared by stirring for 5 minutes, preferably between 20 and 50 ° C.
본 발명에 따른, 절연성을 유지한 상태로 통신장비(전기장비설비 및 패널) 내부 등에 잔존하여 불량요인이 될 수 있는 이물질(먼지, 그리스, 레진 등)을 신속하게 제거하는 효과가 있다.According to the present invention, there is an effect of quickly removing foreign matter (dust, grease, resin, etc.) remaining in the interior of communication equipment (electrical equipment and panels) in a state of maintaining insulation, which may be a bad factor.
또한, 본 발명에 따르면 사용시 냄새가 나지않으며, 절연 세척제로 사용되면서도 기기에 전기가 통하고 있을 경우에도 사용할 수 있는 효과가 있다.In addition, according to the present invention does not smell when used, there is an effect that can be used even when electricity is applied to the device while being used as an insulation cleaner.
또한 본 발명에 따르면, 통신기기의 세척력은 좋으면서 환경에 유해한 성분을 최소화하여 환경친화적인 세척이 가능한 효과가 있다.In addition, according to the present invention, the cleaning power of the communication device is good and there is an effect that can be environmentally friendly by minimizing harmful components to the environment.
이하, 본 발명의 바람직한 실시 예들을 첨부된 도면을 참고하여 더욱 상세히 설명한다. 본 발명의 실시 예들은 여러 가지 형태로 변형될 수 있으며, 본 발명의 범위가 아래에서 설명하는 실시 예들에 한정되는 것으로 해석되어서는 안 된다. 본 실시 예들은 당해 발명이 속하는 기술 분야에서 통상의 지식을 가진 자에게 본 발명을 더욱 상세하게 설명하기 위해서 제공되는 것이다. 따라서 도면에 나타난 각 요소의 형상은 보다 분명한 설명을 강조하기 위하여 과장될 수 있다.Hereinafter, preferred embodiments of the present invention will be described in more detail with reference to the accompanying drawings. The embodiments of the present invention may be modified in various forms, and the scope of the present invention should not be construed as being limited to the embodiments described below. These embodiments are provided to explain in detail the present invention to those skilled in the art. Accordingly, the shape of each element shown in the drawings may be exaggerated to emphasize a clearer description.
제1, 제2 등의 용어는 다양한 구성요소들을 설명하는데 사용될 수 있지만, 구성요소들은 용어들에 의해 한정되어서는 안 된다. 용어들은 하나의 구성요소를 다른 구성요소로부터 구별하는 목적으로만 사용된다.The terms first, second, etc. may be used to describe various elements, but the elements should not be limited by terms. Terms are used only for the purpose of distinguishing one component from another.
본 출원에서 사용한 용어는 단지 특정한 실시 예를 설명하기 위해 사용된 것으로, 본 발명을 한정하려는 의도가 아니다. 단수의 표현은 문맥상 명백하게 다르게 뜻하지 않는 한, 복수의 표현을 포함한다. 본 출원에서, "포함하다" 또는 "가지다" 등의 용어는 명세서상에 기재된 특징, 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것이 존재함을 지정하려는 것이지, 하나 또는 그 이상의 다른 특징들이나 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것들의 존재 또는 부가 가능성을 미리 배제하지 않는 것으로 이해되어야 한다.The terminology used in this application is used only to describe a specific embodiment and is not intended to limit the invention. Singular expressions include plural expressions unless the context clearly indicates otherwise. In this application, the terms "comprise" or "have" are intended to indicate that there is a feature, number, step, operation, component, part, or combination thereof described in the specification, and one or more other features. It is to be understood that the present invention does not exclude the possibility of the presence or the addition of numbers, steps, operations, components, components, or a combination thereof.
본 발명의 통전기기 절연 세척제용 조성물은, 1,1-디클로로에탄(1,1-DICHLOROETHANE): 15~20 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3):55~65 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 18~20 중량%로 구성되어 있다.The composition for the electrical insulating machine insulation cleaner of the present invention, 1,1-dichloroethane (1,1-DICHLOROETHANE): 15 to 20% by weight, mineral spirit 66/3 (MINERAL SPIRITS 66/3): 55 to 65% by weight and 1,1,1,2-tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE): 18 to 20% by weight.
그리고 본 발명의 통전기기 절연 세척제용 조성물은, 1,1-디클로로에탄(1,1-DICHLOROETHANE): 20 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3):60 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 20 중량%로 구성되는 것이 바람직하다.In addition, the composition for the electrical insulating machine insulation cleaner of the present invention, 1,1-dichloroethane (1,1-DICHLOROETHANE): 20% by weight, mineral spirit 66/3 (MINERAL SPIRITS 66/3): 60% by weight and 1,1 , 1,2-tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE): It is preferably composed of 20% by weight.
이는 아래 실험예들에서 보이듯이 각각의 조성물 성분비가 상기와 같을 경우 산업용 절연파괴전압을 만족하기 때문이다.This is because, as shown in the following experimental examples, each composition component ratio satisfies the industrial breakdown voltage.
한편 본 발명의 통전기기 절연 세척제용 조성물을 제조하기 위한 방법으로써, 1,1-디클로로에탄(1,1-DICHLOROETHANE), 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3) 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE)을 각각 1:1:3의 중량비가 되도록 혼합하여 제조된다.On the other hand, as a method for producing a composition for the electrical insulating machine insulation cleaning agent of the present invention, 1,1-dichloroethane (1,1-DICHLOROETHANE), mineral spirit 66/3 (MINERAL SPIRITS 66/3) and 1,1,1, 2-Tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE) is prepared by mixing to a weight ratio of 1: 1: 3, respectively.
즉, 각각의 성분들을 각각의 중량비에 맞춰 혼합기에 천천히 투입하며 툽입하는 과정에 5분간 교반이 이루어지도록 하며, 이때 상기 각각의 성분들은 모두 혼합력, 절연성 및 세척력을 포함하고 있다.In other words, each component is slowly added to the mixer according to the weight ratio, and stirring is performed for 5 minutes in the process of injecting, wherein each of the components includes mixing power, insulation and cleaning power.
한편 본 발명의 통전기기 절연 세척제용 조성물 제조방법은, 1,1-디클로로에탄(1,1-DICHLOROETHANE) 1 중량비, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3) 1 중량비 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE) 3 중량비를 각각 혼합기에 개별적으로 투입하며 5분간 교반하여 제조되는 것이 바람직하며, 20~55℃ 사이에서 이루어지는 것이 바람직하다.Meanwhile, the method for preparing a composition for an electric insulation cleaner for cleaning the present invention includes 1 weight ratio of 1,1-dichloroethane (1,1-DICHLOROETHANE), 1 weight ratio of mineral spirit 66/3, and 1,1,1. , 2-Tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE) 3 weight ratios are added to the mixer individually, and preferably prepared by stirring for 5 minutes, preferably between 20 and 55 ° C.
즉, 각각의 성분들을 모두 한번에 투입하며 교반할 수 있지만 그러할 경우 각각의 성분들이 균일하게 혼합되지 않을 우려가 있기 때문에 먼저 혼합제의 주된 성분인 1,1-디클로로에탄(1,1-DICHLOROETHANE)을 투입한 후 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3)을 투입하며 5분간 교반하고, 이 후 다시 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE)을 투입하며 5분간 교반하는 방식으로 개별 투입과 교반을 병행하면 각각의 성분들이 균일하게 교반이 이루어질 수 있게 하는 것이 가능하다.In other words, each component can be added and stirred at the same time, but in that case, each component may not be uniformly mixed. Therefore, 1,1-dichloroethane (1,1-DICHLOROETHANE), which is the main component of the mixture, is first added. Then, mineral spirit 66/3 (MINERAL SPIRITS 66/3) was added and stirred for 5 minutes, after which 1,1,1,2-tetrafluoroethane (1,1,1,2-TETRAFLUOROETHANE) was added again. When the mixture is added and stirred in a manner of stirring for 5 minutes, it is possible to uniformly stir each component.
이를 통해 혼합된 조성물은 전압파괴증력이 증가하면서도 세척력이 우수하게 될 수 있을 뿐만 아니라 냄새 및 인체자극을 최소화할 수 있어 환경적 친화적성을 가질 수 있게 된다.Through this, the mixed composition may not only be excellent in washing power while increasing voltage breakdown force, but also may minimize odor and human irritation, thereby enabling environmental friendliness.
한 발명의 제조방법에서는 각각 교반시 온도를 20~50℃ 사이에서 이루어지게 하는 것이 바람직하다. 이는 각각의 성분들의 인화점 중 1,1-디클로로에탄(1,1-DICHLOROETHANE)의 끊는 점이 57.3℃이기 때문에 그 이하 온도에서 교반하여야 하며 일정 온도를 유지할 경우 교반시 각각의 성분들의 혼합이 더 쉽게 이루어지기 때문이다.
In the production method of the invention it is preferable to make the temperature between 20 ~ 50 ℃ each stirring. This is because the break point of 1,1-dichloroethane (1,1-DICHLOROETHANE) of each component is 57.3 ° C, so it must be stirred at a temperature below that. For losing.
이하, 각각의 성분들을 혼합비율을 달리하여 실험한 실험예를 통해 본 발명을 설명하도록 한다.
Hereinafter, the present invention will be described through experimental examples in which each component is mixed at different mixing ratios.
여기서 본 발명의 실험예는 한국석유관리원(Kpetro)을 통해 실험한 것으로 실험방법은 KS C IEC 60156:2003에 의해 이루어졌다. 또한 실험예에서는 성분의 조성비율에 따른 절연파괴전압결과치, ODC규제물질 유/무, 인화점 및 세척력의 변화를 실험하였다.Here, the experimental example of the present invention was conducted through the Korea Petroleum Management Institute (Kpetro), the test method was made by KS C IEC 60156: 2003. In the experimental example, the results of dielectric breakdown voltage, ODC regulatory substance presence / absence, flash point and cleaning power were tested according to the composition ratio of the component.
또한 본 실험예들에서는 1,1-디클로로에탄(1,1-DICHLOROETHANE), 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3) 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE) 각각을 1:1:3의 중량비로 혼합된 것을 기초로 하였다.In addition, in the present experimental examples, 1,1-dichloroethane (1,1-DICHLOROETHANE), mineral spirit 66/3 and 1,1,1,2-tetrafluoroethane (1,1, 1,2-TETRAFLUOROETHANE) were each mixed at a weight ratio of 1: 1: 3.
*주1) 본 실험예에서의 세척력 테스트는 테스트용 배전반을 일정량 오염시킨 후 본 조성물을 분사하였을 때 오염된 표면의 오염원 제거 정도를 나타낸 것으로 세척력의 정도는 우수, 좋음, 낮음, 매우 낮음으로 표시하였으며, 각각의 실험예 사용되는 오염물은 기름 성분을 포함한 미세먼지를 이용하였으며, KS C 2101:2006의 방법을 이용하였다.* 1) The cleaning power test in this Experimental Example shows the degree of removal of contaminants on the contaminated surface when the composition was sprayed after a certain amount of contamination in the test switchboard. In each experiment, contaminants used were fine dust including an oil component, and the method of KS C 2101: 2006 was used.
*주2) 본 실험예에서의 인화점 테스트는 테스트용 배전반이 주로 산업용 고전압에 이용되는 것을 감안하여 테스트하였으며 테스트용 배전반의 온도를 상승시켰을 때의 인화 온도를 표시하였으며, KS M ISO 2719;2003의 방법을 이용하였다.* 2) The flash point test in this test example was conducted in consideration of the fact that the test switchgear is mainly used for industrial high voltage, and displayed the flash temperature when the temperature of the test switchgear was increased, and according to KS M ISO 2719; 2003. Method was used.
한편 본 실험예들에서는 테스트용 배전반은 안전을 위하여 통전된 상태와 통전되지 않은 상태를 구분하였다.
On the other hand, in the test examples, the test switchboard distinguished between the energized state and the non-energized state for safety.
실험예Experimental Example 1 One
1,1-디클로로에탄(1,1-DICHLOROETHANE): 12 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3): 50 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 38 중량%의 비율로 혼합하여 테스트용 배전반에 분사하였을 때 아래와 같은 결과가 도출되었다.1,1-dichloroethane (1,1-DICHLOROETHANE): 12% by weight, mineral spirit 66/3: 50% by weight and 1,1,1,2-tetrafluoroethane (1, 1,1,2-TETRAFLUOROETHANE): The following results were obtained when mixed at a ratio of 38% by weight and spraying the test switchboard.
이하, 미네랄스피릿66/3은 "M"으로, 1,1-디클로로에탄은 "D"로, 1,1,1,2-테트라플루오에테인은 "T"로 표시한다.
Hereinafter, mineral spirit 66/3 is represented by "M", 1,1-dichloroethane is represented by "D", and 1,1,1,2- tetrafluoroethane is represented by "T".
실험예 1에 의해 나타난 표 1의 결과를 보면, M과 T의 함유량은 많고 D의 함유량이 적을 경우 세척력은 우수한 것으로 나타나지만 배전반의 절연파괴전압은 측정 불가로 나타나고 인화점은 대체로 높게 형성됨을 알 수 있다. 이를 볼 때 실험예 1의 조성비를 가질 경우 배전반의 세척에는 유리하나 배전반의 특성상 절연상태를 항상 유지해야 한다는 점 감안할 때에 절연 세척제로써의 이용은 불가능할 것으로 보인다.
In the results of Table 1 shown by Experimental Example 1, when the content of M and T is high and the content of D is low, the cleaning power appears to be excellent, but the breakdown voltage of the switchboard appears to be unmeasurable and the flash point is generally formed high. . In view of this, the composition ratio of Experimental Example 1 is advantageous for cleaning the switchboard, but considering that the insulation state should always be maintained due to the characteristics of the switchboard, it may not be used as an insulation cleaner.
실험예Experimental Example 2 2
1,1-디클로로에탄(1,1-DICHLOROETHANE): 18 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3): 55 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 27 중량%의 비율로 혼합하여 테스트용 배전반에 분사하였을 때 아래와 같은 결과가 도출되었다.1,1-dichloroethane (18) by weight, MINERAL SPIRITS 66/3: 55% by weight and 1,1,1,2-tetrafluoroethane (1,1-dichloroethane) 1,1,2-TETRAFLUOROETHANE): The following results were obtained when the mixture was sprayed to the test switchgear at a ratio of 27% by weight.
실험예 2에 의해 나타난 표 2의 결과를 보면, 전체적으로 만족할 수 있는 수치를 보이고 있음을 알 수 있어 본 발명의 통전기기용 절연 세척제로 이용할 수 있음을 알 수 있다.
Looking at the results of Table 2 shown by Experimental Example 2, it can be seen that the numerical value that can be satisfied as a whole can be seen that it can be used as the insulation cleaning agent for the electric current collector of the present invention.
실험예Experimental Example 3 3
1,1-디클로로에탄(1,1-DICHLOROETHANE): 22 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3): 60 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 18 중량%의 비율로 혼합하여 테스트용 배전반에 분사하였을 때 아래와 같은 결과가 도출되었다.1,1-DICHLOROETHANE: 22% by weight, MINERAL SPIRITS 66/3: 60% by weight and 1,1,1,2-tetrafluoroethane (1,1-dichloroethane) 1,1,2-TETRAFLUOROETHANE): The following results were obtained when the mixture was sprayed in a test switchgear at a ratio of 18% by weight.
실험예 2에 의해 나타난 표 2의 결과를 보면, D의 조성비를 높일 경우 절연파괴전압 수치는 상당히 높게 나오지만 상대적으로 인화점이 낮게 형성되어 배전반의 사용 특성상 실험예 3의 조성물로 세척제를 이용할 경우 세척제에 의해 배전반의 화제 등으로 이어질 수 있어 세척제로써의 이용에는 어려움이 있을 것으로 보인다.
In the results of Table 2 shown by Experimental Example 2, when the composition ratio of D is increased, the dielectric breakdown voltage value is quite high, but the flash point is formed relatively low, so when the cleaning agent is used as the composition of Experimental Example 3 due to the characteristics of the switchboard, This may lead to the topic of the switchboard, so there is a difficulty in use as a cleaning agent.
예컨대 통전기기, 특히 산업용 배전반 등의 경우 사용되는 전압이 매우 높고 이로 인해 발생되는 열 또한 높기 때문에 절연파괴전압 및 인화점 등이 일정 부분 유지되어야 하므로 실험예 1의 경우 세척력은 우수하나 절연파괴전압을 측정할 수 없을 정도로 절연성을 유지할 수 없었고, 실험예 3의 경우 절연파괴전압과 세척력은 우수하나, 인화점이 상대적으로 낮게 형성되어 고전압기 흐르는 경우 화재로 이어질 수 있는 단점이 있어 통전기기용 절연 세척제로 이용하는데에는 어려움이 있고, 실험예 2의 경우 실험예 1과 3에 비하여 상대적으로 낮은 세척력을 보이지만 절연파괴전압 및 인화점이 상대적으로 높게 형성되어 있어 고전압이 흐르는 통전기기용 절연 세척제로서 매우 우수한 것으로 보인다.
For example, in case of an electric machine, especially an industrial switchboard, the voltage used is very high and the heat generated by it is also high. Therefore, the breakdown voltage and the flash point must be kept to a certain degree. Insulation could not be maintained to the extent that it could not, and in the case of Experiment 3, the insulation breakdown voltage and washing power are excellent, but the flash point is formed relatively low, which can lead to fire when flowing high voltage. It is difficult to do this, and Experimental Example 2 shows relatively low cleaning power compared to Experimental Examples 1 and 3, but the insulation breakdown voltage and flash point are formed relatively high, and thus, it appears to be very excellent as an insulation cleaner for an electric current flowing through a high voltage.
또한 본 발명의 조성물은 통전기기 절연 세척제로 이용시 냄새와 환경에 유해한 물질을 생성하지 않아 친환경적 조성물이다.
In addition, the composition of the present invention is an environment-friendly composition does not produce a substance harmful to the smell and the environment when used as an electric insulation cleaner.
한편, 본 발명에 따른 통전기기 절연 세척제는 1) 모든 전기, 전자장비 내부, 통신장비(기지국), 2) 전압조정기, MCC 패널, 스위치 및 축전기, PCB기판, 3) 에어컨 설비 모터 및 장비, 자동판매기, 롤러, 주차미터기, 상하수 처리장 정밀부품, 교통신호기, 화재경보기, 4) 식품가공, 제과, 유가공공장, 음료 산업의 장비, 하수 및 상수처리의 모터, 장착상태의 브레이크 라이닝 등, 5) 특히 다습한 조건의 수배전 설비, 전동기, 선박과 빌딩의 자가 발전기, 등에 사용할 수 있다. 즉, 프레온과 화학 반응이 없으므로 슬로지(기름 성분을 포함한 오염물)로 오염된 냉매를 냉매라인으로부터 제거할 수 있다.On the other hand, the electrical insulation insulating cleaner according to the present invention 1) all electrical and electronic equipment, communication equipment (base station), 2) voltage regulator, MCC panel, switch and capacitor, PCB board, 3) air conditioning equipment motor and equipment, automatic Vending machines, rollers, parking meters, water and sewage treatment plants, precision parts, traffic signals, fire alarms, 4) food processing, confectionery, milk processing plants, equipment for the beverage industry, sewage and water treatment motors, brake linings, etc. It can be used in water distribution facilities, electric motors, self generators of ships and buildings, etc. in humid conditions. That is, since there is no chemical reaction with Freon, the refrigerant contaminated with the sludge (contaminants including oil components) can be removed from the refrigerant line.
이상, 본 발명을 바람직한 실시예를 통해 설명하였으나, 이는 본 발명의 기술적 내용에 대한 이해를 돕고자 하는 것일 뿐 발명의 기술적 범위를 이에 한정하고자 함이 아니다.While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it is to be understood that the invention is not limited to the disclosed exemplary embodiments.
즉, 본 발명의 기술적 요지를 벗어나지 않고도 당해 발명이 속하는 기술 분야에서 통상의 지식을 가진 자라면 다양한 변형이나 개조가 가능함은 물론이고, 그와 같은 변경이나 개조는 청구범위의 해석상 본 발명의 기술적 범위 내에 있음은 말할 나위가 없다.That is, those skilled in the art without departing from the technical gist of the present invention can be variously modified or modified, as well as such changes or modifications, the technical scope of the present invention in the interpretation of the claims. It is hard to say that I am within.
Claims (5)
20~50℃ 사이에서 이루어지는 것을 특징으로 하는 통신기기 절연 세척제용 조성물 제조방법.The method for producing a composition for cleaning communication device insulation according to claim 1 or 2,
Method for producing a composition for cleaning communication equipment insulation, characterized in that made between 20 ~ 50 ℃.
1,1-디클로로에탄(1,1-DICHLOROETHANE): 15~20 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3):55~65 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 18~20 중량%로 조성된 것을 특징으로 하는 통전기기 절연 세척제용 조성물.The composition used in the method for producing a composition for communication device insulation cleaner of claim 3,
1,1-dichloroethane (1,1-DICHLOROETHANE): 15-20% by weight, mineral spirit 66/3: 55-65% by weight and 1,1,1,2-tetrafluoro Ethene (1,1,1,2-TETRAFLUOROETHANE): A composition for an electric insulation cleaner for cleaning, characterized in that composed of 18 to 20% by weight.
1,1-디클로로에탄(1,1-DICHLOROETHANE): 20 중량%, 미네랄 스피릿 66/3(MINERAL SPIRITS 66/3):60 중량% 및 1,1,1,2-테트라플루오로에테인(1,1,1,2-TETRAFLUOROETHANE): 20 중량%로 조성된 것을 특징으로 하는 통전기기 절연 세척제용 조성물.The composition used in the method for producing a composition for communication device insulation cleaner of claim 3,
1,1-dichloroethane (1,1-DICHLOROETHANE): 20% by weight, mineral spirit 66/3: 60% by weight and 1,1,1,2-tetrafluoroethane (1, 1,1,2-TETRAFLUOROETHANE): Composition for an electrical insulation cleaner for the composition, characterized in that composed of 20% by weight.
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| KR1020130012769A KR101286798B1 (en) | 2013-02-05 | 2013-02-05 | A manufacturing the same for composition method and composition of detergent for electrical machines insulation |
| PCT/KR2014/000852 WO2014123324A1 (en) | 2013-02-05 | 2014-01-29 | Detergent composition for insulated electricity-conducting device, and preparation method therefor |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101520648B1 (en) * | 2015-03-25 | 2015-05-15 | 김종오 | Insulating detergent composition |
| KR101956513B1 (en) | 2018-08-23 | 2019-03-08 | 한두희 | Insulation cleaner composition for uninterruptible power supply |
| KR102260232B1 (en) | 2020-07-17 | 2021-06-03 | (주)거산엠텍 | Insulation cleaner composition for communication devices that can be washed in a live state |
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|---|---|---|---|---|
| US20080125342A1 (en) | 2006-11-07 | 2008-05-29 | Advanced Technology Materials, Inc. | Formulations for cleaning memory device structures |
| KR100965430B1 (en) | 2008-10-15 | 2010-06-24 | 베이스코리아아이씨(주) | Insulating detergent for electric machine |
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| JPH08199199A (en) * | 1995-01-27 | 1996-08-06 | Surluster Co | Dust-preventing and lustering detergent for tire |
| US6113708A (en) * | 1998-05-26 | 2000-09-05 | Candescent Technologies Corporation | Cleaning of flat-panel display |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080125342A1 (en) | 2006-11-07 | 2008-05-29 | Advanced Technology Materials, Inc. | Formulations for cleaning memory device structures |
| KR100965430B1 (en) | 2008-10-15 | 2010-06-24 | 베이스코리아아이씨(주) | Insulating detergent for electric machine |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101520648B1 (en) * | 2015-03-25 | 2015-05-15 | 김종오 | Insulating detergent composition |
| KR101956513B1 (en) | 2018-08-23 | 2019-03-08 | 한두희 | Insulation cleaner composition for uninterruptible power supply |
| KR102260232B1 (en) | 2020-07-17 | 2021-06-03 | (주)거산엠텍 | Insulation cleaner composition for communication devices that can be washed in a live state |
| WO2022015097A1 (en) * | 2020-07-17 | 2022-01-20 | 주식회사 거산엠텍 | Insulating cleanser composition for communication device |
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