KR101223809B1 - the boild functional salt manufacture method - Google Patents

the boild functional salt manufacture method Download PDF

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KR101223809B1
KR101223809B1 KR1020100087791A KR20100087791A KR101223809B1 KR 101223809 B1 KR101223809 B1 KR 101223809B1 KR 1020100087791 A KR1020100087791 A KR 1020100087791A KR 20100087791 A KR20100087791 A KR 20100087791A KR 101223809 B1 KR101223809 B1 KR 101223809B1
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leaves
water
salt
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/40Table salts; Dietetic salt substitutes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2300/00Processes
    • A23V2300/14Extraction
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2300/00Processes
    • A23V2300/50Concentrating, enriching or enhancing in functional factors

Abstract

본 발명은 기능성 자염의 제조방법에 관한 것으로, 생리활성물질로 조릿대줄기와 잎,연잎,녹차,갈대잎과 줄기,뽕잎,울금,홍삼은 잘게 썰어 청정수에 세척하는 재료준비단계(S1)와;청정지역에서 취수한 해수 83중량부에 대하여, 조릿대줄기와 잎17중량부, 연잎 17중량부, 녹차 10 중량부 ,갈대잎·줄기 및 뿌리 17중량부, 뽕잎 17중량부, 울금 17중량부, 홍삼 10중량부를 넣고 70∼110℃로 4∼24시간 가열해 염도 2.4∼3.2도의 함수로 열수추출하는 단계(S2)와;농축된 함수를 고체불순물을 필터로 1차 여과후 액체의 밀도차를 이용한 원심분리로 여과하는 정제단계(S3)와;정제단계에의 함수를 가마솥에 넣고 80∼150℃로 10시간 동안 거품을 거두어내면서 1차가열농축단계(S4)와;가열농축된 함수를 분류탑에서 침전된 20부피% 잔량은 버리고 상등수만 수득하는 분별증류단계(S5)와;분별증류된 함수만을 가마솥에 넣고 80∼150℃에서 거품을 거두어내면서 2차가열농축하여 자염(煮鹽)을 석출하는 최종단계(S6)를 거쳐 해수나 천일염에 포함된 잔류중금속의 농도를 최소로 하면서도 건강기능식 소금으로서 각종 생리활성물질을 갖는 기능성 자염 제조방법을 제공하도록 한 것이다.The present invention relates to a method for preparing functional suicide, comprising a material preparation step (S1) for slicing stems and leaves, lotus leaf, green tea, reed leaves and stems, mulberry leaves, turmeric, red ginseng and finely rinsing in clean water as a bioactive substance; 83 parts by weight of seawater taken from clean areas, 17 parts by weight of stalks and leaves, 17 parts by weight of lotus leaves, 10 parts by weight of green tea, 17 parts by weight of reed leaves and stems, roots, 17 parts by weight of mulberry leaves, 17 parts by weight of turmeric, 10 parts by weight of red ginseng and heated to 70 to 110 ℃ for 4 to 24 hours to extract hot water as a function of salinity of 2.4 to 3.2 degrees (S2); Purification step (S3) and filtration by centrifugation using; Put the function of the purification step into the cauldron and remove the foam for 10 hours at 80 ~ 150 ℃ primary heating concentration step (S4) and; heat concentrated function classification Fractional distillation stage that yields only supernatant water, discarding 20% by volume remaining in the tower (S5); and the remaining heavy metals contained in seawater or sun salt through the final step (S6) by depositing only the fractionated distilled water in the cauldron, and the second heating concentrated to remove the bubbles at 80 ~ 150 ℃ It is to provide a functional suicide manufacturing method having various bioactive substances as a health functional salt while minimizing the concentration of.

Description

기능성 자염 제조방법{ the boild functional salt manufacture method }The boild functional salt manufacture method

본 발명은 기능성 자염의 제조방법에 관한 것으로, 특히 대나무와 연,녹차,갈대,뽕,울금,홍삼을 해수로 열수 추출시켜, 기능성 자염을 제조하는 방법에 관한 것이다.The present invention relates to a method for producing functional suicide, and more particularly to a method for producing functional suicide by hot water extraction of bamboo and lotus, green tea, reed, mulberry, turmeric, red ginseng with sea water.

관련기술로 국내등록특허 제535229호 소금제조장치에 따르면, 갯벌에 마련한 해수유입부와 유입된 해수를 농축해 채집하는 함수채수부와,함수에서 수분을 증발시켜소금을 석출하는 증발부로 이루어진 소금제조장치의 경우에, 함수로 갯벌토층이나,황토층을 이용하는 방법과,또 다른 국내 등록특허 제436222호 자염간수의 제조장치에 따르면,조금 전후 7∼8일간 해수가 들어오지 않는 갯벌에서 염분이 농축된 갯벌 함토(鹹土)를 염분추출조와 염분침전조가 다단으로 이루어진 염류추출공정에 의해서,해수정의 해수를 추출용제로하여 염도 17-20도의 함수를 만들어,이를 보일러시스템으로 염도 24-15로 1차 농축하여, 1차 불순물을 제거하고, 2차농축공정을 통해 자염을 석출침전하고, 3차농축공정을 통해 간수를 제조하는 방법과 같은 선행기술의 경우에 있어는 주로 갯벌토층을 이용해 만든 함토를 가열하여 자염을 추출하는 방법과 같은 자염을 제조하는 방법이나 수단이 제시되고 있는 실정이다.According to the Korean Patent No. 533229 salt manufacturing apparatus for related technology, salt production consists of a seawater inflow portion provided on the tidal flat, a water collection portion for concentrating and collecting the incoming seawater, and an evaporation portion for depositing salt by evaporating water from the function. In the case of the apparatus, according to the method using a tidal flat soil layer, or a loess layer as a function, and another manufacturing device of Korean Patent No. 436222 self-preserved salt water, a tidal flat in which salt is concentrated in a tidal flat where seawater does not enter for about 7-8 days before and after The salt extraction process consists of a multi-stage salt extraction tank and a salt precipitating tank. The seawater of the seawater is used as an extraction solvent to produce a function of salinity of 17 to 20 degrees, which is first concentrated to a salinity of 24 to 15 by a boiler system. In the case of the prior art, such as the method of removing the primary impurities, precipitating the salt salt through the secondary concentration process, and preparing the water from the tertiary concentration process. The present situation is proposed a method or a means for preparing the salt, such as a method of extracting the salt by heating the soil made mainly by the mud flat soil layer.

또, 다른 국내의 많은 기능성 소금에 대한 관련기술중 국내등록특허 제10-0383389호에서는 각종 유용 미네랄을 글루콘산염의 형태로 함유하는 기능성 소금으로 원료소금 50∼90%(w/w)에 5∼25%(w/w)의 글루콘산나트륨, 2∼12.5%(w/w)의 염화칼륨,2∼12.5%(w/w)의 염화칼슘,0.1∼2%(w/w)의 염화마그네슘,0.1∼2%(w/w)의 황산아연 및 0.1∼1%(w/w)의 황산망간으로 구성된 원료물을 20∼30%(w/v)의 농도로 60∼80℃의 온도범위에서 가열 용해하여, 활성탄을 0.02∼0.05%(w/v)가하고 교반 여과후, 600∼700mmHg 감압하에 가열농축하여 재결정 핵을 생성하여, 결정을 탈수시키고 수분함량을 0.5%(w/w)이하로 건조함을 특징으로 한다.In addition, among the related technologies for many domestic functional salts in Korea Patent No. 10-0383389 is a functional salt containing a variety of useful minerals in the form of gluconate salt of raw salt 50 to 90% (w / w) 5 -25% (w / w) sodium gluconate, 2-12.5% (w / w) potassium chloride, 2-12.5% (w / w) calcium chloride, 0.1-2% (w / w) magnesium chloride, A raw material composed of 0.1 to 2% (w / w) zinc sulfate and 0.1 to 1% (w / w) manganese sulfate at a temperature range of 60 to 80 ° C. at a concentration of 20 to 30% (w / v). After heating and dissolving, activated carbon was added to 0.02% to 0.05% (w / v), and after stirring and filtration, the mixture was heated and concentrated under a reduced pressure of 600 to 700 mmHg to form recrystallized nuclei. The crystals were dehydrated and the water content was 0.5% (w / w) or less. It is characterized by dryness.

또 다른 기능성 소금으로 등록특허 제10-0466579호에서는 국산천일염과 0.1∼5%의 키토산을 결합후 재결정하여 얻은 소금 및 기타 국산천일염에 녹차의 유효성분을 포함하여 결합후 재결정하는 소금, 백련초나 버섯, 마늘,다시마나 미역, 톳 성분을 천일염에 결합후 재결정하여 얻은 소금이나, 천일염에 국화,장미,진달래,쑥,깻잎,갓,시금치,생강,솔잎,양파,고추씨,홍고추,청고추,포도,자두,체리,산머루,석류,레몬,치자 등의 식물성분을 코팅한 기능성 칼라소금 등이 기술되고 있다. As another functional salt, Patent No. 10-0466579 discloses salts obtained by combining domestic natural salts with chitosan of 0.1 to 5% and recrystallized salts and other domestic natural salts, including the active ingredient of green tea, salt, white lotus or mushroom Salt obtained by combining garlic, seaweed, seaweed and seaweed ingredients with sun salt, or chrysanthemum, rose, rhododendron, mugwort, sesame leaf, fresh, spinach, ginger, pine needle, onion, red pepper seed, red pepper, blue pepper, grape Functional color salts coated with plant ingredients such as plums, cherries, wild grapes, pomegranate, lemon and gardenia are described.

상기와 같은 갯벌토층을 이용해 만든 함토를 가열하여 제조하는 자염이나, 천일염에 각종 생리활성물질을 가하여 코팅하거나 가열농축하여 재결정해 제조하는 각종 기능성 소금들에 있어서도 최근의 해양오염상태나 많은 환경유해물질이 유입 퇴적되어,오염되어가는 연안갯벌에 누적된 중금속으로부터 온전할 수 없는 실정이다.The current state of marine pollution and many environmentally harmful substances also exist in various functional salts prepared by heating various types of salts prepared using the above-mentioned tidal flat soil layer, or coating and heating and recrystallization by adding various bioactive substances to sun salt. This inflow is not able to be intact from the heavy metal accumulated in the coastal tidal flats that are being deposited and polluted.

참고로 국내 연안지역의 해수 중금속 함유량은 0.003ppm 카드륨,0.012ppm의 구리,0.001ppm의 납,0.02ppm의 아연, 0.0004ppm의 수은이 검출된 국립환경연구소 조사연구결과 각각의 값은 자연상태보다 더 높은 실정임을 알 수 있는 실정이고,자원환경지질확회에서 최근 조사보고된 국내 특정 연안지역의 갯벌 중금속함량조사결과 망간 32∼53㎎/kg,아연 14∼32㎎/kg,구리 2.5∼17.0㎎/kg,납2.4∼6.8㎎/kg,카드륨0.5 ∼0.7㎎/kg순으로 검출되고 있어 인위적인 금속오염원에 의하여 누적오염이 진행되고 있음을 시사한바 있다.For reference, seawater heavy metals in coastal areas of Korea are 0.003ppm cadmium, 0.012ppm copper, 0.001ppm lead, 0.02ppm zinc, and 0.0004ppm mercury. It was found that the situation was higher, and the result of the survey of heavy metal content in a specific coastal area of Korea, which was recently reported by the resource environmental geological survey, manganese 32-53mg / kg, zinc 14-32mg / kg, copper 2.5-17.0mg / kg, lead 2.4 ~ 6.8mg / kg, cadmium 0.5 ~ 0.7mg / kg in order to detect the cumulative contamination by the artificial source of metal suggests that.

이에 최근 식약청은 천일염의 규격이 염화나트륨70.0%이상,총염소40.0%이상, 수분15.0%이하,불용분0.15%이하,황산이온5.0%이하,사분0.2%이하,비소0.5㎎/㎏이하,납2.0㎎/㎏이하,카드륨0.5㎎/㎏이하,수은0.1㎎/㎏이하,페로시안화이온 불검출이 식품으로 사용할 수 있는 소금의 위생규격으로 정하고,가공소금도 원료소금 함량을 종전 95%이상에서 50%이상으로 완화하여 다양한 가공소금이 생산될 수 있도록 하였다.In recent years, KFDA's standards of natural salt are more than 70.0% of sodium chloride, more than 40.0% of total chlorine, less than 15.0% of moisture, less than 0.15% of insoluble matter, less than 5.0% of sulfate ion, less than 0.2%, less than 0.5mg / kg of arsenic, and lead 2.0. ㎎ / kg or less, cadmium 0.5mg / kg or less, mercury 0.1mg / kg or less, ferrocyanide non-detection is defined as the hygienic standard of salt that can be used as food. It has been relaxed to more than% so that various processed salts can be produced.

[문헌1] KR 10-0535229호 B1 2005.12.02[Document 1] KR 10-0535229 B1 2005.12.02 [문헌2] KR 10-0436222호 B1 2004.06.04[Document 2] KR 10-0436222 B1 2004.06.04 [문헌3] KR 10-0383389호 B1 2003.04.25[Reference 3] KR 10-0383389 B1 2003.04.25 [문헌4] KR 10-0466579호 B1 2005.01.06[Document 4] KR 10-0466579 B1 2005.01.06 [문헌5] KR 10-0698899호 B1 2007.03.16[Document 5] KR 10-0698899 B1 2007.03.16 [문헌6] KR 10-0858030호 B1 2008.09.04[Document 6] KR 10-0858030 B1 2008.09.04 [문헌7] KR 10-0528963호 B1 2005.11.09[Document 7] KR 10-0528963 B1 2005.11.09 [문헌8] KR 10-0448672호 B1 2004.09.03[Document 8] KR 10-0448672 B1 2004.09.03 [문헌9] KR 2001-0054209 A 2001.07.02Document 9 KR 2001-0054209 A 2001.07.02

본 발명은 상기와 같이 최근의 해양오염상태나 많은 환경유해물질이 유입 퇴적되어,오염되어가는 연안갯벌에 누적된 중금속으로부터 온전할 수 없는 실정을 감안하여,조릿대,연,녹차,갈대,뽕,울금,홍삼과 같은 각종 생리활성물질을 해수로 열수 추출한 다음 가마솥에서 재결정시켜 완성하는 해수나 천일염에 포함된 잔류중금속의 농도를 최소로 하는 기능성 자염 제조방법을 제공함을 목적으로 한다. The present invention in view of the current situation of marine pollution or inflow and accumulation of many environmentally harmful substances, and intact from heavy metals accumulated in the coastal tidal flat that is polluted, stalk, lead, green tea, reed, mulberry, It is an object of the present invention to provide a method for producing functional suicide which minimizes the concentration of residual heavy metals contained in seawater or sun salt, which is completed by hot water extraction of various biologically active substances such as turmeric and red ginseng into seawater and then recrystallized in a cauldron.

상기와 같은 점을 감안하여, 본 발명에 따른 기능성 자염 제조방법은 생리활성물질로 조릿대줄기와 잎,연잎,녹차,갈대잎과 줄기,뽕잎,울금,홍삼은 잘게 썰어 청정수에 세척하는 재료준비단계(S1)와;In view of the above points, the method for preparing functional suicide according to the present invention is a biologically active material preparing step for slicing finely chopped stems and leaves, lotus leaf, green tea, reed leaves and stems, mulberry leaves, turmeric, red ginseng and washing them in clean water. (S1);

청정지역에서 취수한 해수 83중량부에 대하여, 조릿대줄기와 잎17중량부, 연잎 17중량부, 녹차 10 중량부 ,갈대잎·줄기 및 뿌리 17중량부, 뽕잎 17중량부, 울금 17중량부, 홍삼 10중량부를 넣고 70∼110℃로 4∼24시간 가열해 염도 2.4∼3.2도의 함수로 열수추출하는 단계(S2)와;83 parts by weight of seawater taken from clean areas, 17 parts by weight of stalks and leaves, 17 parts by weight of lotus leaves, 10 parts by weight of green tea, 17 parts by weight of reed leaves and stems, roots, 17 parts by weight of mulberry leaves, 17 parts by weight of turmeric, Adding 10 parts by weight of red ginseng and heating it at 70-110 ° C. for 4 to 24 hours to extract hot water as a function of salinity of 2.4 to 3.2 degrees (S2);

농축된 함수를 고체불순물을 필터로 1차 여과후 액체의 밀도차를 이용한 원심분리로 여과하는 정제단계(S3)와;Purifying step (S3) for filtering the concentrated water by centrifugation using the difference in density of the liquid after the primary filtration of the solid impurities with a filter;

정제단계에의 함수를 가마솥에 넣고 80∼150℃로 10시간 동안 거품을 거두어내면서 1차가열농축단계(S4)와;Put the water in the purification step in the cauldron to remove the foam for 10 hours at 80 ~ 150 ℃ primary heating concentration step (S4) and;

가열농축된 함수를 분류탑에서 침전된 20부피% 잔량은 버리고 상등수만 수득하는 분별증류단계(S5)와;A fractional distillation step (S5) of discarding the 20% by volume remaining in the concentrated fraction of the heated concentrated water and obtaining only the supernatant;

분별증류된 함수만을 가마솥에 넣고 80∼150℃에서 거품을 거두어내면서 2차가열농축하여 자염(煮鹽)을 석출하는 최종단계(S6)를 거치는 기능성 자염 제조방법을 제공하도록 한 것이다.Only fractionated distillation function in the cauldron to remove the foam at 80 ~ 150 ℃ while heating the secondary heating concentration to provide a method for producing a functional suicide through the final step (S6) to precipitate suicide (염).

본 발명 기능성 자염 제조방법의 제조공정에 따른 자염은 해수나 천일염에 포함된 잔류중금속의 농도를 최소로 하면서도 건강기능식 소금으로서 각종 생리활성물질을 갖는 기능성 자염 제조방법으로 매우 유용하다 할 것이다. The suicide according to the manufacturing process of the functional suicide salt production method of the present invention will be very useful as a functional suicide salt production method having various bioactive substances as a health functional salt while minimizing the concentration of residual heavy metals contained in seawater or sun salt.

본 발명에 따른 자염과 일반 천일염에 대해 성인 남여 각 5명으로부터 5점 척도법에 따른 관능검사결과는 다음 표1과 같다.Sensory test results according to the 5-point scale method from each of five adult men and women for the self-inflammatory and general sun salt according to the present invention are shown in Table 1.

검사요원 Inspector 1One 22 33 44 55 66 77 88 99 1010 합계Sum
flavor
자염Suicide 4.54.5 4.34.3 4.64.6 4.14.1 4.34.3 4.04.0 4.24.2 4.84.8 4.24.2 4.54.5 43.543.5
일반Normal 4.04.0 3.83.8 4.14.1 3.73.7 3.63.6 3.53.5 3.83.8 4.24.2 3.73.7 4.04.0 38.438.4 색상
color
자염Suicide 4.34.3 4.04.0 4.24.2 4.54.5 4.04.0 4.04.0 3.93.9 4.34.3 4.04.0 4.34.3 45.545.5
일반Normal 3.83.8 3.63.6 3.83.8 4.14.1 3.73.7 3.63.6 3.83.8 4.14.1 3.73.7 3.83.8 38.038.0 전반적기호성Overall sign 자염Suicide 4.34.3 4.54.5 4.64.6 4.34.3 4.24.2 4.04.0 4.14.1 4.54.5 4.14.1 4.34.3 42.942.9 일반Normal 3.93.9 3.53.5 3.83.8 3.73.7 3.63.6 3.43.4 3.83.8 4.04.0 3.63.6 3.93.9 37.237.2

상기와 같은 관능조사결과와 같이 본 발명에 따른 자염의 관능도는 일반 천일염에 비해 불순물이 많이 제거된 상태로 색상면에 있어 높은 기호도를 나타냈고, 맛에 있어서도 각종 생리활성물질을 열수 추출해 재결정시킨 자염으로 맛이나 전반적인 기호도면에 있어서 천일염에 비해 기호도가 좋게 나타난 유용한 발명인 것이다.As shown in the above sensory evaluation results, the functionality of suicide according to the present invention showed a high degree of preference in terms of color with much impurities removed, compared to general sun salt, and also recrystallized by hot water extraction of various physiologically active substances in taste. It is a useful invention in which taste is better than sun salt in taste or overall preference drawing.

도 1은 본 발명에 따른 제조공정도1 is a manufacturing process diagram according to the present invention

상기와 같은 점을 감안하여, 이하 첨부된 도면에 따라 본 발명의 일실시 구성을 상세히 알아보면 다음과 같다.In view of the foregoing, one embodiment of the present invention according to the accompanying drawings in detail as follows.

도 1은 본 발명 기능성 자염 제조방법의 제조공정으로서, 1 is a manufacturing process of the functional suicide printing method of the present invention,

생리활성물질로 조릿대줄기와 잎,연잎,녹차,갈대잎과 줄기,뽕잎,울금,홍삼은 잘게 썰어 청정수에 세척하는 재료준비단계(S1)와;As a bioactive substance, stalk stem and leaves, lotus leaf, green tea, reed leaves and stems, mulberry leaves, turmeric, red ginseng finely chopped and washed in clean water (S1) and;

청정지역에서 취수한 해수 83중량부에 대하여, 조릿대줄기와 잎17중량부, 연잎 17중량부, 녹차 10 중량부 ,갈대잎·줄기 및 뿌리 17중량부, 뽕잎 17중량부, 울금 17중량부, 홍삼 10중량부를 넣고 70∼110℃로 4∼24시간 가열해 염도 2.4∼3.2도의 함수로 열수추출하는 단계(S2)와;83 parts by weight of seawater taken from clean areas, 17 parts by weight of stalks and leaves, 17 parts by weight of lotus leaves, 10 parts by weight of green tea, 17 parts by weight of reed leaves and stems, roots, 17 parts by weight of mulberry leaves, 17 parts by weight of turmeric, Adding 10 parts by weight of red ginseng and heating it at 70-110 ° C. for 4 to 24 hours to extract hot water as a function of salinity of 2.4 to 3.2 degrees (S2);

농축된 함수를 고체불순물을 필터로 1차 여과후 액체의 밀도차를 이용한 원심분리로 여과하는 정제단계(S3)와;Purifying step (S3) for filtering the concentrated water by centrifugation using the difference in density of the liquid after the primary filtration of the solid impurities with a filter;

정제단계에의 함수를 가마솥에 넣고 80∼150℃로 10시간 동안 거품을 거두어내면서 1차가열농축단계(S4)와;Put the water in the purification step in the cauldron to remove the foam for 10 hours at 80 ~ 150 ℃ primary heating concentration step (S4) and;

가열농축된 함수를 분류탑에서 침전된 20부피% 잔량은 버리고 상등수만 수득하는 분별증류단계(S5)와;A fractional distillation step (S5) of discarding the 20% by volume remaining in the concentrated fraction of the heated concentrated water and obtaining only the supernatant;

분별증류된 함수만을 가마솥에 넣고 80∼150℃에서 거품을 거두어내면서 2차가열농축하여 자염(煮鹽)을 석출하는 최종단계(S6)로 이루어진다.Only the fractionated distilled water is put into the cauldron and the final step (S6) to precipitate suicide (2) by concentrating secondary heating while removing the foam at 80 ~ 150 ℃.

참고로 1차가열농축단계의 함수 2,000㎏에서 수득된 자염은 800㎏로 각종 기능성 활성물질과 미네랄이 풍부하고, 2차례에 걸쳐 가열농축하면서 불순물을 걸러내면서 분류탑에서 상등수만 수득하는 분별증류단계를 거쳐 미세중금속의 잔류농도를 더욱 떨어뜨린 자염으로서, 식약청이 규정한 천일염의 식품안전규격품의 국내천일염으로부터 잔류중금속의 잔류농도가 더욱 최소로 된 기능성 자염 제조방법을 제공하게 된 것이다. For reference, the suicide obtained from the function of 2,000 kg of the primary heating concentration step is 800 kg, which is rich in various functional active substances and minerals, and the fractionation distillation step of obtaining only the supernatant water from the fractionation tower while filtering impurities while heating and heating two times. As a suicide which further reduced the residual concentration of the fine heavy metals through, the natural salt of the food safety standard of the Japan Food Salt standard provided by the Korea Food and Drug Administration to provide a method for producing a functional suicide with a minimum residual concentration of residual heavy metals.

또, 본 발명에 따른 해수 83 중량부에 각종 기능성 활성물질을 10∼17중량부로 한정한 것은 식약청에서 규정한 가공소금으로서 원료소금 함량의 제한 범위내에서 이루어지도록 한 것이며,각 기능성 활성물질들의 첨가량은 20중량부 이상이면 소금으로서 역할이 미약하며, 사전처리된 해수 2,000㎏에서 최종 수득된 기능성자염 800㎏을 생산하는 효율 면에서 산출한 것이다.In addition, the limit of 10 to 17 parts by weight of various functional active substances in 83 parts by weight of seawater according to the present invention is to be made within the limit of the raw salt content as a processed salt prescribed by the KFDA, the amount of each functional active substance added Silver is not more than 20 parts by weight of the role as a salt, calculated in terms of the efficiency of producing 800 kg of the final obtained functional salt salt from 2,000 kg of pretreated seawater.

참고로 본 발명 기능성자염중에 포함된 생리활성물질중 특히 조릿대는 동의보감, 본초강목, 신농 본초경에도 “인삼을 능가할 만큼 놀라운 약성을 지닌 약초”이며, 제주대의 이남호 교수팀이 분리한 신물질 ESQ10은 염증현상을 야기하는 프로스타글란딘(Prostaglandin)과 나이트릭 옥사이드(Nitric Oxide) 및 인터루킨-6(IL-6)의 생성을 억제할 뿐만 아니라 인체세포에서도 독성이 없는 것으로 규명된 것이며,특히 자염의 산도와 가까운 알칼리성이 강해 산성체질을 알칼리성체질로 개선하는데도 유용하다.For reference, among the physiologically active substances included in the functional neuritis of the present invention, the stalks are the herbs of Donggibogam, herbaceous wood, and Sinnon herbaceous plants. In addition to inhibiting the production of prostaglandin, nitrous oxide and interleukin-6 (IL-6), which cause symptoms, they have been shown to be nontoxic in human cells, especially alkalis close to the acidity of suicide. It is also useful for improving this strong acidic constitution to alkaline constitution.

또, 연잎은 차로도 시판중에 있는 만큼 HIV와 고혈압 억제효과,활성산소를 억제시키는데 유효한 성분이 있다는 전남보건환경연구소의 연구조사결과나, 동의 보감에 따른 오장을 보하고 갈증과 설사를 다스리는데 유용하다.In addition, lotus leaf is commercially available in the market as it is effective in inhibiting HIV, hypertension, and free radicals. Do.

한편, 녹차는 콜레스테롤을 줄여주고 인슐린의 합성을 촉진하는 다당류가 풍부해 당뇨에도 좋고 중금속과 니코틴 해독작용에도 유효하다.Green tea, on the other hand, is rich in polysaccharides that reduce cholesterol and promote the synthesis of insulin, which is good for diabetes and is effective for detoxifying heavy metals and nicotine.

그리고, 갈대잎·줄기 및 뿌리는 동의보감 탕액편에 맛은 달고 성질이 차며, 열을 내리며, 갈증해소와 복어독 해소에 유용하다는 유용성이 감안한 것이다.In addition, reed leaves, stems and roots are considered to be useful for the taste of the Dongbogam Tanggeumtang, sweet and cold, to reduce heat, to quench thirst, and to relieve blowfish poison.

뽕잎은 가바(GAVA)성분이 풍부해 혈압을 내리며,루틴성분으로 모세혈관강화와 칼슘과 식이섬유 및 각종 미네랄이 풍부하는 등 뽕잎의 풍부한 영양성분이 과학적으로 입증이 되면서,전통의서에 명기된 각종 약효 성분도 속속 밝혀지고 있어 채택한 유용한 성분이다.Mulberry leaves are rich in GAVA ingredients to lower blood pressure, and the rich nutritional ingredients of mulberry leaves are scientifically proven, including capillary strengthening, calcium, dietary fiber and various minerals. Various active ingredients are also revealed one after another and are useful ingredients.

한편, 네이버지식에 따르면 울금 역시 성미(性味)는 심장,폐,간에 응용되며,모든 혈증 치료에 쓰이고 카레의 원료로도 사용되고 최근에는 암치료의 보조제, 간장염, 담석증, 요혈 비만, 지방간, 노화, 항암, 만성피로, 숙취에 좋다는 유용성을 감안한 것이다.On the other hand, according to Naver's knowledge, turmeric is also applied to the heart, lungs, liver, and is used to treat all bloodemia, and is also used as a raw material of curry. Considering the usefulness of aging, anti-cancer, chronic fatigue, hangover.

기타, 홍삼은 한의학적으로 가장 오랜 약용 역사를 가지고 있으며, 가장 광범위하게 임상적으로 응용되어온 것으로 임상학적 효능은 현대과학적 연구결과에 의해서도 홍삼의 진정한 약용 가치가 실증되고 있으며, 특히 건강 보조식품으로 현대의료에 사용되는 의약품으로도 세계적으로 활용되고 있는데 따른 유용성을 감안하였다.In addition, red ginseng has the longest medicinal history in Korean medicine and has been widely applied clinically. The clinical efficacy of the red ginseng demonstrates the true medicinal value of modern red ginseng. In consideration of its usefulness, it is being used worldwide as a medicine used in medical treatment.

위와 같이 본 발명에 기능성 자염 제조방법에 따른 자염은 해수나 천일염에 포함된 잔류중금속의 농도를 최소로 하면서도 건강기능식 소금으로서 각종 생리활성물질을 갖는 기능성 자염 제조방법으로 매우 유용한 것이다. As described above, the suicide according to the functional suicide production method is very useful as a functional suicide production method having various bioactive substances as health functional salts while minimizing the concentration of residual heavy metals contained in seawater or sun salt.

S1:재료준비단계 S2:열수 추출단계
S3:정제단계 S4:1차가열농축단계
S5:분별증류단계 S6:2가열농축하여 자염 석출하는 최종단계
S1: Material preparation step S2: Hot water extraction step
S3: Purification stage S4: 1st heating concentration stage
S5: fractional distillation stage S6: final stage of precipitation precipitation by heating concentration

Claims (1)

생리활성물질로 조릿대줄기와 잎,연잎,녹차,갈대잎과 줄기,뽕잎,울금,홍삼은 잘게 썰어 청정수에 세척하는 재료준비단계(S1)와;
청정지역에서 취수한 해수 83중량부에 대하여, 조릿대줄기와 잎17중량부, 연잎 17중량부, 녹차 10 중량부 ,갈대잎·줄기 및 뿌리 17중량부, 뽕잎 17중량부, 울금 17중량부, 홍삼 10중량부를 넣고 70∼110℃로 4∼24시간 가열해 염도 2.4∼3.2도의 함수로 열수추출하는 단계(S2)와;
농축된 함수를 고체불순물을 필터로 1차 여과후 액체의 밀도차를 이용한 원심분리로 여과하는 정제단계(S3)와;
정제단계에의 함수를 가마솥에 넣고 80∼150℃로 10시간 동안 거품을 거두어내면서 1차가열농축단계(S4)와;
가열농축된 함수를 분류탑에서 침전된 20부피% 잔량은 버리고 상등수만 수득하는 분별증류단계(S5)와;
분별증류된 함수만을 가마솥에 넣고 80∼150℃에서 거품을 거두어내면서 2차가열농축하여 자염(煮鹽)을 석출하는 최종단계(S6)로 이루어짐을 특징으로 하는 기능성 자염 제조방법.
As a bioactive substance, stalk stem and leaves, lotus leaf, green tea, reed leaves and stems, mulberry leaves, turmeric, red ginseng finely chopped and washed in clean water (S1) and;
83 parts by weight of seawater taken from clean areas, 17 parts by weight of stalks and leaves, 17 parts by weight of lotus leaves, 10 parts by weight of green tea, 17 parts by weight of reed leaves and stems, roots, 17 parts by weight of mulberry leaves, 17 parts by weight of turmeric, Adding 10 parts by weight of red ginseng and heating it at 70-110 ° C. for 4 to 24 hours to extract hot water as a function of salinity of 2.4 to 3.2 degrees (S2);
Purifying step (S3) for filtering the concentrated water by centrifugation using the difference in density of the liquid after the primary filtration of the solid impurities with a filter;
Put the water in the purification step in the cauldron to remove the foam for 10 hours at 80 ~ 150 ℃ primary heating concentration step (S4) and;
A fractional distillation step (S5) of discarding the 20% by volume remaining in the concentrated fraction of the heated concentrated water and obtaining only the supernatant;
Functional fractionation production method characterized in that the final step (S6) of depositing the saline (煮 鹽) by the second heating concentrated while removing the foam at 80 ~ 150 ℃ only fractional distillation in the cauldron.
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