KR101198854B1 - Side-docking type raw material supply apparatus for continuous growing single crystals - Google Patents
Side-docking type raw material supply apparatus for continuous growing single crystals Download PDFInfo
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- KR101198854B1 KR101198854B1 KR20100063973A KR20100063973A KR101198854B1 KR 101198854 B1 KR101198854 B1 KR 101198854B1 KR 20100063973 A KR20100063973 A KR 20100063973A KR 20100063973 A KR20100063973 A KR 20100063973A KR 101198854 B1 KR101198854 B1 KR 101198854B1
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- raw material
- crystal growth
- material supply
- docking
- pipe
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- Engineering & Computer Science (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
Abstract
The present invention relates to a side docking raw material supply device for continuous crystal growth coupled to the side of the crystal growth apparatus in a detachable docking manner to enable continuous crystal growth by recharging the raw material for crystal growth in the chamber. It is connected to the side of the crystal growth apparatus for growing a single crystal through the raw material filled in the inner crucible, and the raw material at the other end of the transfer pipe installed through the side of the crystal growth apparatus so that one end is located on the crucible As the discharge pipe is discharged is lowered and inserted is characterized in that the raw material loaded on the side hopper is dropped through the transfer pipe to fill the crucible.
Description
The present invention relates to a side docking raw material supply device for continuous crystal growth, and is coupled to the side of the crystal growth apparatus in a detachable docking method to enable continuous crystal growth by recharging the raw material for crystal growth in the chamber. It relates to a side docking raw material feeder for continuous crystal growth.
As is well known, a crystalline material is divided into a single crystal and a polycrystal, and a single crystal refers to a crystal in which the directionality of an atomic arrangement is constant throughout, and a polycrystal refers to a crystal in which crystal grains and grain boundaries exist.
Here, the grains (grsin) refers to each part having the same directionality of the atomic arrangement, and the boundary between the grains and the grains is called a grain boundary (grain boundary). That is, although the basic cells of each grain are the same, the orientation in which the basic cells are arranged is different for each grain. Thus, single crystals do not have grain boundaries. Such single crystals are mainly used as semiconductor materials or optical materials, such as silicon wafers, and are made from polycrystals to single crystals through crystal growth.
Usually, the single crystal growth method includes a Czochralski crystal growth method and a float zone crystal growth method, also referred to as a pulling method.
In the single crystal growth method according to the above-mentioned pulling method, a raw material is charged into a crucible, heated and melted, and then gradually immersed in a melt while seed seed is immersed and rotated to grow crystals from seed crystals to form a large single crystal. To grow. This pulling method has the advantage of being able to grow high quality single crystals in large size in a relatively short time.
In the conventional single crystal growth method, the raw material is injected into the crucible only once when the apparatus is operated. When the growth of the silicon single crystal is completed, the temperature of the crystal growth apparatus is cooled to 500 ° C. or less at which oxidation does not occur. At this time, the method of cooling the crystal growth apparatus is to release the power applied to the internal heater and then to naturally cool until the temperature of the chamber in the crystal growth apparatus is 500 ℃ or less.
However, since the crucible is heated at a temperature higher than 1420 ° C., which is the melting point of silicon, to melt the silicon, the temperature in the center of the chamber is maintained at a temperature higher than 1000 ° C. even when the heater is turned off. In such a high temperature state, cooling the temperature of the chamber to 500 ° C. or less using only a natural cooling method takes a long time, and thus there is a disadvantage in that continuous production of the ingot is impossible.
Furthermore, when the heater is turned off, the silicon solution inside the crucible hardens and is broken, making it impossible to use the device.
An object of the present invention is to solve the problems of the conventional single crystal growth apparatus as described above, it is coupled in a detachable docking method to the side of the crystal growth apparatus to recharge the raw material for crystal growth in the chamber (Recharge) It is to provide a side docking raw material feeder for continuous crystal growth.
The present invention is a means for solving the above problems, is detachably connected to the side of the crystal growth apparatus for growing a single crystal through the raw material filled in the inner crucible, one end of the crystal growth apparatus is located on the crucible The side docking type for continuous crystal growth, characterized in that the discharge pipe is discharged to the other end of the transfer pipe installed through the side is lowered and inserted into the crucible by dropping the raw material loaded in the side hopper through the transfer pipe Provide raw material feeder.
Preferably, the side docking raw material supply apparatus, the raw material filling chamber is moved to the side of the crystal growth apparatus connected; A hopper coupled to the side of the raw material filling chamber to drop the raw material; Raw material supply control unit for adjusting the input amount of the raw material supplied from the hopper; An impurity injecting unit provided in the raw material filling chamber for injecting impurities; A raw material supply pipe that receives and discharges the raw materials and impurities; An elevating unit for elevating the raw material supply pipe; And an opening / closing coupling part configured to open or close the discharge pipe of the raw material supply pipe to insert and detach the discharge pipe.
More preferably, the transfer pipe is a pipe having a hollow shape, one end is located on the crucible and the other end is characterized in that the discharge pipe is formed in a vertical shape from the outside to be inserted.
More preferably, the hopper is characterized in that the raw material injection port for receiving the raw material from the outside is formed.
More preferably, the lower portion of the hopper is characterized in that the weight measuring unit for measuring the weight that changes according to the discharge of the raw material of the hopper is disposed.
More preferably, the raw material supply control unit, the hollow receiving tube of the discharge end of the hopper is accommodated; An opening and closing hole for opening and closing the lower portion of the receiving tube by moving up and down at the lower portion of the receiving tube; A motor unit coupled to the opening and closing hole to vertically move the opening and closing hole; And an adjusting inlet tube accommodating the accommodation tube and the opening and closing inside and discharging the discharged raw material downward. And a control unit.
More preferably, the opening and closing is provided with a hemispherical dish in contact with the receiving tube at the top, characterized in that the dish and the receiving tube is made of a silicon material.
More preferably, the raw material supply pipe has two openings through which raw materials and impurities are supplied, and a discharge pipe is formed at the lower side thereof, so that the lower end of the discharge pipe passes through the ball valve of the open / close coupling portion and is inserted into the transfer pipe when docked. It is characterized by.
More preferably, the elevating unit, the top plate is coupled to the discharge pipe in a penetrating state; A lower plate through which the discharge pipe passes; And a cylinder coupled between the upper plate and the lower plate to raise and lower the upper plate. Including a lowering the discharge pipe when docking.
More preferably, a vacuum port and a gas injection port are formed on one side of the raw material filling chamber to make the interior of the raw material filling chamber into a vacuum state through the vacuum port when the raw material filling chamber is docked, and to separate the raw material filling chamber. Shut off the valve of the vacuum port and injecting gas through the gas injection port is characterized in that the inside of the material filling chamber to the atmospheric pressure state.
The side docking raw material supply device for continuous crystal growth according to the present invention is coupled in a detachable docking manner to the side of the crystal growth apparatus to enable continuous crystal growth by recharging the raw material for crystal growth in the chamber. It works.
In addition, it is possible to accurately measure the amount of raw material input when the raw material is supplied to the user, as well as to precisely control the input amount of the raw material, thereby increasing the production yield.
In addition, when the raw material is added, the raw material falls near the crucible, thereby enabling the stable injection of the raw material.
1 is a side cross-sectional view for explaining the docking state of the side docking raw material supply for continuous crystal growth according to the present invention.
Figure 2 is a side cross-sectional view for explaining a docking state of the side docking raw material supply for continuous crystal growth according to the present invention.
Figure 3 is a side sectional view showing a raw material supply control unit according to the present invention.
4 shows a supply box according to the invention.
Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings.
1 is a side cross-sectional view for explaining a state before docking the side docking raw material supply for continuous crystal growth according to the present invention, Figure 2 is a docking of the side docking raw material supply for continuous crystal growth according to the present invention It is a side sectional view for demonstrating a state.
1 and 2, in the present invention, the raw
First, the basic configuration of the
The
Such
Here, since the
Since the internal structure of the above-described
At this time, the
That is, the
Accordingly, the
At this time, the
The raw
The
In order to load the raw material into the
At this time, the raw
The
The
The
Therefore, when the raw material in the
3 is a side cross-sectional view showing in detail such a raw material
Referring to FIG. 3, the raw material
That is, the raw material falling through the raw
Here, the
Here, the PID (proportional integral derivative control) control is a kind of feedback control to maintain the output voltage of the system based on the error between the control variable and the reference input in the control of the automation system, proportional (Proportional) control And proportional-integral control and proportional-derivative control.
According to the forward / reverse rotation of the
And when the release of the raw material occurs in accordance with the vertical movement of the opening and
Therefore, the input of the raw material as desired can be made by adjusting the vertical movement speed of the opening and
On the other hand, the raw
The raw
At this time, the
The elevating
The open /
Therefore, when the
When the supply of raw materials and impurities is completed, the
Eventually, the
Here, the
In fact, when the growth of the silicon single crystal is completed, the temperature of the
However, since the
In addition, when the power supply of the
Therefore, the raw material must be recharged to the
Meanwhile, the principle of docking the
During side docking, the raw
4 shows one side of the
Referring to FIG. 4, a
On the other hand, when the filling of the raw material is completed to close the valve of the
As described above, an optimal embodiment has been disclosed in the drawings and specification. Although specific terms have been employed herein, they are used for purposes of illustration only and are not intended to limit the scope of the invention as defined in the claims or the claims. Therefore, those skilled in the art will appreciate that various modifications and equivalent embodiments are possible without departing from the scope of the present invention. Therefore, the true technical protection scope of the present invention will be defined by the technical spirit of the appended claims.
100: crystal growth apparatus 110: crucible
120: heater 130: heat insulating member
140: chamber portion 150: gate chamber
200: raw material supply device 210: hopper
211: raw
220: raw material supply control unit 221: receiving pipe
222: opening and
223
224a: inlet tube outlet 230: impurity inlet
240: raw material supply pipe 243: discharge pipe
250: elevating unit 251: upper plate
252: bottom plate 253: cylinder
260: raw material filling chamber 261: supply box
262: vacuum port 263: gas injection port
270: open and close coupling portion 271: ball valve
272: open and close motor 280: transfer pipe
281: inlet 282: outlet
Claims (10)
The side docking raw material supply device,
A raw material filling chamber connected to and moved to the side of the crystal growth apparatus;
A hopper coupled to an upper portion of the raw material filling chamber to drop raw materials;
Raw material supply control unit for adjusting the input amount of the raw material supplied from the hopper;
An impurity injecting unit provided in the raw material filling chamber for injecting impurities;
A raw material supply pipe that receives and discharges the raw materials and impurities;
An elevating unit for elevating the raw material supply pipe; And
Side opening-type docking raw material supply apparatus for continuous crystal growth comprising a; opening and closing the opening and closing of the discharge pipe of the raw material supply pipe to insert into the transfer pipe.
The transport pipe is a pipe having a hollow shape, one end of which is located on the crucible and the other end of the side docking raw material supply for continuous crystal growth, characterized in that the discharge pipe is formed in a vertical shape to be inserted from the outside Device.
Side docking raw material supply apparatus for continuous crystal growth, characterized in that the hopper is formed with a raw material injection port for receiving the raw material from the outside.
The lower side of the hopper is a side docking raw material supply device for continuous crystal growth, characterized in that the weight measuring unit for measuring the weight changes in accordance with the discharge of the raw material of the hopper is disposed.
The raw material supply control unit,
A hollow accommodating tube accommodating an outlet end of the hopper;
An opening and closing hole for opening and closing the lower portion of the receiving tube by moving up and down at the lower portion of the receiving tube;
A motor unit coupled to the opening and closing hole to vertically move the opening and closing hole; And
An adjusting inlet tube accommodating the accommodation tube and the opening and closing portion and discharging the discharged raw material downward; Side docking raw material supply device for continuous crystal growth comprising a.
The opening and closing is provided with a hemispherical dish in contact with the receiving tube on the upper side, the side docking raw material supply apparatus for continuous crystal growth, characterized in that the dish and the receiving tube is made of a silicon material.
The raw material supply pipe is formed with two openings for receiving the raw material and impurities and a discharge pipe formed at the lower side, so that the lower end of the discharge pipe is inserted into the transfer pipe through the ball valve of the opening and closing portion when docking. Side docking feeder for continuous crystal growth.
The ascending /
An upper plate to which the discharge pipe is coupled in a penetrating state;
A lower plate through which the discharge pipe passes; And
A cylinder coupled between the upper plate and the lower plate to raise and lower the upper plate; Side docking raw material supply device for continuous crystal growth, characterized in that to lower the discharge pipe when docking.
A vacuum port and a gas injection port are formed at one side of the raw material filling chamber to make the inside of the raw material filling chamber into a vacuum state through the vacuum port when the raw material filling chamber is docked, and the vacuum port is separated when the raw material filling chamber is separated. Side docking type raw material supply device for continuous crystal growth, characterized in that for closing the valve and injecting gas through the gas injection port to make the inside of the material filling chamber to atmospheric pressure.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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KR20100063973A KR101198854B1 (en) | 2010-07-02 | 2010-07-02 | Side-docking type raw material supply apparatus for continuous growing single crystals |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR20100063973A KR101198854B1 (en) | 2010-07-02 | 2010-07-02 | Side-docking type raw material supply apparatus for continuous growing single crystals |
Publications (2)
Publication Number | Publication Date |
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KR20120003223A KR20120003223A (en) | 2012-01-10 |
KR101198854B1 true KR101198854B1 (en) | 2012-11-07 |
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KR20100063973A KR101198854B1 (en) | 2010-07-02 | 2010-07-02 | Side-docking type raw material supply apparatus for continuous growing single crystals |
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Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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KR101554223B1 (en) * | 2014-04-25 | 2015-09-18 | (주)에스테크 | Continuous supply apparatus of ingot raw material |
KR102493638B1 (en) * | 2021-06-18 | 2023-01-31 | 한화솔루션 주식회사 | Silicon supply control method for pre-melting crucible of ingot grower |
KR102493637B1 (en) * | 2021-06-25 | 2023-01-31 | 한화솔루션 주식회사 | Ingot growing apparatus and control method for perliminary crcible of the same |
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2010
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