KR101178104B1 - Kapok-fiber Finshing Method For Improving Spinning Property - Google Patents
Kapok-fiber Finshing Method For Improving Spinning Property Download PDFInfo
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- KR101178104B1 KR101178104B1 KR1020090132987A KR20090132987A KR101178104B1 KR 101178104 B1 KR101178104 B1 KR 101178104B1 KR 1020090132987 A KR1020090132987 A KR 1020090132987A KR 20090132987 A KR20090132987 A KR 20090132987A KR 101178104 B1 KR101178104 B1 KR 101178104B1
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/84—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
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- D—TEXTILES; PAPER
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- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
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Abstract
본 발명은 초경량성이고 천연중공섬유인 케이폭(kapok)섬유의 무게를 크게 증가시켜 방적성을 향상시키기 위한 케이폭섬유의 가공방법에 관한 것이다.The present invention relates to a processing method of kapok fiber for improving the spinning property by greatly increasing the weight of kapok fiber, which is a super lightweight and natural hollow fiber.
구체적으로 케이폭섬유를 증량가공제로 처리한 후 건조시키는 것을 포함하여 이루어지는 것을 특징으로 하는 방적성을 향상시키기 위한 케이폭섬유의 가공방법에 관한 것이다.Specifically, the present invention relates to a processing method of kapok fibers for improving the spinning property, comprising drying and then treating the kapok fibers with an extender.
케이폭, 증량가공, 방적 K-Pop, Increased Processing, Spinning
Description
본 발명은 초경량성이고 천연중공섬유인 케이폭(kapok)섬유의 무게를 크게 증가시켜 방적성을 향상시키기 위한 케이폭섬유의 가공방법에 관한 것이다.The present invention relates to a processing method of kapok fiber for improving the spinning property by greatly increasing the weight of kapok fiber, which is a super lightweight and natural hollow fiber.
케이폭(Kapok) 섬유는 높이 10~15m에 달하는 교목의 다래에서 채취한 섬유이다. 다래의 모양은 면화와 다르며 길이는 10~15cm이며, 중앙부의 최대 직경은 4~6cm의 방사형이다. 이 다래는 성숙하면 저절로 벌어져서 속으로부터 섬유가 자라난다. 면화는 자란 것 그 자체가 밑으로 늘어지지만, 케이폭은 자란 것이 바람이 불면 씨앗이 부착된 채로 날아가 버리기 때문에 다래가 벌어지기 전에 수확한다. 씨앗은 면 씨앗보다 상당히 작고 붉은 색을 띄며, 씨앗과 섬유와는 가볍게 치기만 해도 쉽게 분리가 되므로 면화의 조면과 같은 번거로운 작업은 필요 없다.Kapok fibers are obtained from the arboretum of 10-15 m in height. Its shape is different from that of cotton and its length is 10 ~ 15cm, and its central diameter is 4 ~ 6cm radial. When the stalk matures, it spontaneously opens up, and fibers grow from the inside. Cotton grows by itself, but kapok grows when the wind blows, with seeds attached, when the wind blows. Seeds are considerably smaller and more red than cotton seeds, and can be easily separated from the seeds and fibers simply by tapping them, eliminating the hassle of cotton.
케이폭섬유의 길이는 일반적으로 18~27㎜, 직경은 약 0.02㎜ 정도이며 섬유내부는 완전한 중공으로 되어있다.The length of kapok fiber is generally 18 ~ 27mm, the diameter is about 0.02mm and the inside of the fiber is completely hollow.
물의 침투에 견디는 힘이 강하고 부연성이 풍부하며 자체 중량의 35배 정도를 띄울 수 있는 힘이 있다. 침수 후 1개월 후에도 26배량의 무게를 띄울 수 있는 힘이 있는 성질을 이용하여 구명용구의 충진재료로도 사용되기도 한다. 또한 가볍고 탄력 및 보온성이 풍부한 성질을 이용하여 베게나 이불면 대신에 사용되고 있다.It is strong enough to withstand the penetration of water, rich in flammability, and capable of floating about 35 times its own weight. It is also used as a filling material for life-saving equipments because of its ability to lift 26 times the weight even after one month of immersion. In addition, it is used instead of pillow or duvet cotton because of its light, elasticity and warmth.
이러한 특성을 이용하여 초경량, 보온성을 가지는 케이폭 섬유제품화에 대한 요구가 대두되고 있으나, 케이폭섬유는 면섬유와 비교해서 표면이 엉키는 성질이 없는데다 강력도 비교적 약하기 때문에 이것만으로는 방적할 수 없으며, 케이폭 섬유만으로 장시간 사용하는 경우에는 섬유의 이어짐이 끊어져서 평면 상태를 상실하고 단단하게 엉켜붙는 문제가 발생하여 혼합방적사를 만드는 경우에도 균일한 강력 및 균제도의 달성이 어려운 문제점이 있었다.By using these characteristics, there is a demand for the commercialization of ultra-light and heat-retaining kapok fiber. However, kapok fiber has no property of tangling compared to cotton fiber and its strength is relatively weak, so it cannot be spun alone. In the case of use, the fiber is broken and the plane state is lost and the problem of being firmly entangled occurs. Thus, even when a mixed yarn is made, it is difficult to achieve uniform strength and uniformity.
특히 케이폭 섬유를 방적사로 제조할 때, 일반 면섬유에 비해 비중이 낮아 방적공정 중 비산되어 방적성이 좋지 못하고 작업환경을 해하는 문제점이 있다.In particular, when the kapok fiber is manufactured with a yarn, the specific gravity is lower than that of the general cotton fiber is scattered during the spinning process, there is a problem that the spinning property is not good and harm the working environment.
이와 같은 종래의 문제점을 해결하기 위한 본 발명은 케이폭섬유의 무게를 증가시켜 방적시 케이폭섬유가 비산되는 것을 방지하여 방적성 및 작업환경을 크게 향상시킬 수 있는 케이폭섬유의 가공방법을 제공하는 것을 목적으로 한다.The present invention for solving the above problems is to provide a processing method of the kapok fiber that can increase the weight of the kapok fiber to prevent the kapok fiber is scattered during spinning to greatly improve the spinning properties and working environment It is done.
상기와 같은 목적을 달성하기 위한 본 발명은, The present invention for achieving the above object,
증량가공제인 4차 암모늄 화합물이 2~5 중량%로 포함된 물에 케이폭섬유를 처리한 후 건조시키는 것을 포함하여 이루어지는 것을 특징으로 하는 방적성을 향상시키기 위한 케이폭섬유의 가공방법을 제공한다.It provides a processing method of kapok fiber for improving the spinning property, comprising the step of treating the kapok fiber in water containing 2 to 5% by weight of the quaternary ammonium compound as an extender.
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또한 상기 증량가공제가 처리된 케이폭섬유를 40~60℃온도로 2~4시간동안 건조시키는 것이 바람직하다.In addition, it is preferable to dry the kapok fiber treated with the extender for 2 to 4 hours at a temperature of 40 ~ 60 ℃.
이하, 본 발명의 방적성을 향상시키기 위한 케이폭섬유의 가공방법을 상세히 설명한다.Hereinafter, the processing method of the kapok fiber for improving the spinning property of the present invention will be described in detail.
본 발명의 케이폭섬유의 가공방법은 케이폭섬유를 증량가공제로 처리한 후 건조시키는 공정을 포함하여 이루어진다.The processing method of the kapok fiber of the present invention comprises a step of treating the kapok fiber with an extender and then drying.
증량가공제는 케이폭섬유의 중량을 증가시키기 위한 것으로서, 4차 암모늄 화합물을 사용한다.The extender is intended to increase the weight of kapok fibers, using quaternary ammonium compounds.
상기 증량가공제는 물에 혼합(용해)시켜 상기 케이폭섬유를 처리한다. 이때 상기 증량가공제는 물에 2~5중량% 혼합하는 것이 바람직하다. 2중량% 미만으로 혼합할 경우 케이폭 섬유의 중량의 증가가 미비하여 방적시 비산되고, 5중량% 초과로 혼합되는 경우 섬유내 축적되어 황변현상을 발생시키는 등의 문제가 있다.The extender is mixed (dissolved) in water to treat the kapok fibers. At this time, the extender is preferably mixed with 2 to 5% by weight in water. When mixing less than 2% by weight, the increase in the weight of the kapok fiber is insufficient to scatter when spun, when mixed with more than 5% by weight accumulates in the fiber to cause a yellowing phenomenon.
그리고 상기 증량가공제에 처리된 케이폭섬유를 건조시킨다. 가공처리된 케이폭 섬유의 증량효과를 극대화하기 위하여 상기 증량가공제처리 후 40~60℃온도로 건조시키는 것이 바람직하다.And the kapok fiber treated to the extender is dried. In order to maximize the increasing effect of the processed kapok fiber, it is preferable to dry at 40 to 60 ° C. after the increase processing agent treatment.
증량가공한 케이폭 섬유를 건조할 때 가능한 낮은 온도에서 건조하는 것이 바람직하며, 건조온도가 증가할수록 케이폭 섬유의 황변현상이 발생할 가능성이 높아진다. 또한 건조시간이 길어 질수록 온도에 의해 케이폭 섬유가 손상될 확률이 높아지고, 증량가공의 효과 또한 줄어들기 때문에 가능한 낮은 온도와 적은 건조시간으로 처리하는 것이 바람직하다. 건조온도는 상온보다 약간 높은 40~60℃가 바람직하며, 진공건조기를 사용하는 것이 건조효과를 향상시킬 수 있다. 건조시간은 2시간에서 4시간 정도가 바람직하며, 건조할 케이폭 섬유의 양에 따라 시간을 조절하는 것이 바람직하다. It is preferable to dry the increased kapok fiber at the lowest possible temperature, and the increase in the drying temperature increases the possibility of yellowing of the kapok fiber. In addition, the longer the drying time, the higher the probability of damaging the kapok fiber due to the temperature, and the effect of the increase processing is also reduced, so it is desirable to treat it at the lowest possible temperature and drying time. The drying temperature is preferably 40 ~ 60 ℃ slightly higher than the room temperature, using a vacuum dryer can improve the drying effect. The drying time is preferably about 2 hours to 4 hours, and the time is preferably adjusted according to the amount of kapok fibers to be dried.
본 발명의 케이폭섬유의 가공방법은 케이폭섬유의 무게를 크게 증가시킬 수 있어 방적시 케이폭섬유가 비산되는 것을 방지할 수 있는 등 방적성을 크게 향상시킬 수 있는 효과가 있다.The processing method of the kapok fiber of the present invention can greatly increase the weight of the kapok fiber, it is possible to prevent the kapok fiber from scattering during spinning, such as to greatly improve the spinning properties.
이하 본 발명의 방적성을 향상시키기 위한 케이폭섬유의 가공방법을 실시예를 들어 더욱 상세히 설명하면 다음과 같고, 본 발명의 권리범위는 하기의 실시예에 한정되는 것은 아니다.Hereinafter, the processing method of the kapok fiber for improving the spinning property of the present invention will be described in more detail with reference to the following Examples, the scope of the present invention is not limited to the following examples.
[실시예 1]Example 1
증량가공제 2중량%가 혼합된 물 50㎖에 케이폭섬유 10g을 침지시켜 처리한 후 진공오븐을 이용하여 50℃로 3시간 동안 건조시켜 실시예 1인 중량가공된 케이폭섬유를 얻었다. 이때 증량가공제로서는 4급암모늄계를 사용하였고, 케이폭섬유는 섬유장이 25mm이고, 평균섬유직경이 0.026mm이었다.10 g of kapok fiber was immersed in 50 ml of water mixed with 2% by weight of the extender, and dried at 50 ° C. for 3 hours using a vacuum oven to obtain the weight-treated kapok fiber of Example 1. At this time, quaternary ammonium was used as the extender, and the kapok fiber had a fiber length of 25 mm and an average fiber diameter of 0.026 mm.
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[실시예 2~5]EXAMPLES 2-5
실시예 1과 달리 증량가공제 1중량%, 3중량%, 5중량% 및 7중량%가 각각 혼합된 물 50㎖에 케이폭섬유를 침지시켜 처리 및 건조시켜 실시예 2~5의 중량가공된 케이폭섬유를 얻었다.Unlike Example 1, the processed kapok fibers of Examples 2 to 5 were treated and dried by immersing the kapok fibers in 50 ml of water containing 1% by weight, 3% by weight, 5% by weight, and 7% by weight of the extender. Got.
[실시예 6~9][Examples 6 to 9]
실시예 1과 달리 증량가공제처리된 케이폭섬유를 30℃, 40℃, 60℃ 및 70℃의 각 온도로 조절된 진공오븐을 이용하여 3시간 동안 건조시켜 실시예 6~9의 중량가공된 케이폭섬유를 얻었다.Unlike Example 1, the kapok fiber treated with the increased weight was dried for 3 hours using a vacuum oven adjusted to 30 ° C, 40 ° C, 60 ° C and 70 ° C for 3 hours, and then the weighted kapok fiber of Examples 6-9. Got.
[실시예 10~13][Examples 10-13]
실시예 1과 달리 증량가공제처리된 케이폭 섬유를 50℃로 1시간, 2시간, 4시간 및 5시간 동안 각각 진공오븐을 이용하여 건조시켜 실시예 10~13의 중량가공된 케이폭섬유를 얻었다.Unlike Example 1, the kapok fiber treated with the extender was dried at 50 ° C. for 1 hour, 2 hours, 4 hours, and 5 hours using a vacuum oven to obtain the weight processed kapok fibers of Examples 10 to 13.
이와 같이 제조된 실시예 1~13의 중량가공된 케이폭섬유의 중량 및 섬유상태를 측정 및 확인하였고, 그 결과는 하기의 표 1과 같다.The weight and fiber condition of the kapok fiber processed by the weight of Examples 1 to 13 thus prepared and measured, and the results are shown in Table 1 below.
[표 1] 중량가공된 케이폭섬유의 증량비율 및 섬유상태 Table 1 Expansion rate and fiber state of weight processed kapok fiber
중량(g)After treatment
Weight (g)
비율Increase
ratio
상태fiber
condition
표 1의 중량가공된 케이폭섬유의 증량비율 및 섬유상태에서 확인되는 바와 같이 실시예 1 내지 13 모두 8% 이상의 증량이 되었고, 섬유상태가 모두 양호하였다. 특히 증량가공제가 1중량% 혼합된 실시예 2의 경우 증량비율이 8%로 미비한 반면 증량가공제가 2~5중량% 혼합된 실시예 1,3~13의 경우 증량비율이 12.0% 이상으로 높아 효과적으로 방적성이 향상되는 이점이 있다. 실시예 5의 경우 증량비율이 14.2%로 높았으나 황변이 부분적으로 발생하였다.As can be seen from the increase ratio and fiber state of the weight processed kapok fiber of Table 1, all of Examples 1 to 13 were increased by 8% or more, and the fiber state was all good. In particular, in the case of Example 2 in which 1% by weight of the extender was mixed, the increase ratio was insignificant to 8%, while in Examples 1 and 3 to 13, in which 2 to 5% by weight of the extender was mixed, the increase ratio was 12.0% or more. There is an advantage that the spinning property is improved. In Example 5, the increase ratio was high as 14.2%, but yellowing partially occurred.
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CN103938430A (en) * | 2014-04-14 | 2014-07-23 | 东华大学 | Textile post-processing method for restoring hollowness of kawo kawo fiber |
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CN104404762A (en) * | 2014-11-06 | 2015-03-11 | 赵正兴 | Kapok fiber processing technology |
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