KR100868579B1 - Method for preparing fermented rice wine using spice and fruit - Google Patents

Method for preparing fermented rice wine using spice and fruit Download PDF

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KR100868579B1
KR100868579B1 KR1020080026058A KR20080026058A KR100868579B1 KR 100868579 B1 KR100868579 B1 KR 100868579B1 KR 1020080026058 A KR1020080026058 A KR 1020080026058A KR 20080026058 A KR20080026058 A KR 20080026058A KR 100868579 B1 KR100868579 B1 KR 100868579B1
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liquor
glutinous rice
yeast
water
prepared
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조성오
송성헌
문선희
설관수
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/05Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides
    • C12G3/055Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides extracted from plants
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/02Preparation of other alcoholic beverages by fermentation
    • C12G3/021Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn
    • C12G3/022Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn of botanical genus Oryza, e.g. rice
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/06Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients

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Abstract

A manufacturing method of the fermentation grain wine using spice and fruit is provided to have a high yield, an excellent taste, flavor and liquor characteristic by improving a traditional manufacturing method of Ojong-liquor. Glutinous rice is dipped. The yeast filter liquor is prepared by adding water in yeast powder and filtering and leaching the yeast powder. Water is added in the increased glutinous rice and the yeast filter liquor, and fermented and saccharified. Piperis nigri Fructus, cinnamomi Cortex, zingiberis Rhizoma crudus, pine-nuts, zizyphi Fructus, immersion, the glutinous rice, capital-increased the liquefying agent, and the converting agent and distilled liquor soju are added and fermented in the first manufactured crude liquor. The manufactured second rude liquor is filter and water is added. An alcoholic content of the filtered liquor is standardized.

Description

향신료와 과실을 이용한 발효곡주의 제조방법 {Method for Preparing Fermented Rice Wine Using Spice and Fruit}Method for Preparing Fermented Rice Wine Using Spice and Fruit {Method for Preparing Fermented Rice Wine Using Spice and Fruit}

본 발명은 문헌에서 전래되는 오종주의 전통적인 제조방법을 개량하여 정량화함으로서, 고수율과 우수한 맛, 향미와 주질을 갖는 발효곡주의 제조방법에 관한 것이다.The present invention relates to a method for producing fermented grain wine having a high yield, excellent taste, flavor and quality by improving and quantifying the traditional production method of Ohjongju, which is introduced in the literature.

오종주(五種酒)에 관한 문헌은 규합총서(閨閤叢書)에 유일하게 전해지고 있다. 규합총서 중의 오종주방문(五種酒方文)을 보면,‘한 제 하려면 찹쌀 한 말, 누룩가루 한 되, 후추(胡椒) 한 돈, 계피(桂皮) 한 돈, 잣(松實) 한 돈, 생강(生薑) 한 돈, 대추(棗) 한 되, 소주 사십오 복자 및 물 두 사발이 재료로 필요하고 이 중 후추 및 계피는 가루로 만들어 베 조각으로 주머니를 지어 넣고, 생강은 두드려 그저 넣고, 잣은 가루로 만들어 그저 넣고, 대추는 깨끗이 씻어 그저 넣는다. 그 주조방법으로, 찹쌀을 쓸어 담그는 날 누룩을 물에 담근 후, 찰밥을 지어 서늘하게 식혀 누룩 담근 물을 체에 걸러 찰밥에 버무려 넣어둔 다음, 사흘(삼일째)이 되어 달콤한 맛이 들거든 소주 사십오 복자(기름같은 것을 되는 기구)를 부어 한이레(7일)쯤 두면 밥알이 끓어오른다. 한이레(7일)고 두이레(14일)고 맛이 어우러지면 떠 먹으면 된다. 여름이라도 소주를 부어 더운데 덮어 두어야 쉬이 된다.’라고 기재되어 있다 (정랑완 저, 규합총서, 보진제, 1980). The literature on Ojongju is said to be the only one in the rally. If you look at Ohjongju's visit in the book, you can say, 'If you want to make Korean cold, you have one word of glutinous rice, one yeast powder, one pepper, one cinnamon, and one pine nut. You will need a piece of ginger, a jujube, a bowl of shochu forty-five bokbok, and two bowls of water. Put pine nuts into powder, just put in, and wash jujube. With the casting method, soak the glutinous rice in the day of soaking the yeast in water, and make the glutinous rice, cool it down, sift the yeast soaked water, and soak it in the rice. After 3 days (3rd), it is sweet taste. Forty-five blessing boxes (oil-like utensils) are poured and left for about seven days (7 days). Hanire (7 days) and Duire (14 days) and when the taste goes well you can eat. Even in summer, it is easy to pour soju and cover it in the hot place. '(Jang Rang-Wan, Kyu-Kyu , Bo Jin-je, 1980).

후추(Piper nigrum)는 인도 남부 원산으로 열대지방에서 향신료로 가꾼다. 속명의 piper는 고대 라틴 이름이며, 종명의 nigrum는 ‘검은 빛’을 뜻한다. 유효성분으로는 피페린 5~9%, 차비신 6% 및 정유 1~2.5%를 함유하고 있다. 구풍제, 건위제 등으로 사용하며, 식품의 향신료로도 이용된다. 한국, 인도, 인도네시아, 말레이반도, 서인도제도 등지에서 재배한다.Pepper (Piper nigrum ) is native to southern India and goes from the tropics to spices. The generic piper is the ancient Latin name, and the nigrum of the species means 'black light'. The active ingredient contains 5 to 9% of piperine, 6% of chabicin and 1 to 2.5% of essential oils. It is used as antiperspirant, dry matter, and also as a food spice. It is grown in Korea, India, Indonesia, Malay Peninsula and West Indies.

계피(Cinnamomum cassia Blume)는 육계나무 또는 기타 동속 근연식물의 어린가지를 사용해 만든 약재로서, 특이한 향기를 가지는데, 껍질부분은 색이 더욱 진하며, 약성은 맵고 따뜻하다. 초기 감기에 피부의 땀구멍을 열어 땀을 내며, 어깨와 등의 통증, 사지관절의 동통을 완화시켜주며, 기혈의 순환을 촉진시키고 양기부족을 치료한다. 약리작용으로는 대장균, 고초간균, 황색포도균, 폐렴쌍구균 등의 발육 억제, 유행성감기바이러스의 억제, 이뇨작용 등이 알려져 있다. Cinnamomum cassia Blume ) is a medicinal herb made from young twigs of broiler trees or other related plants. It has a distinctive scent, with a darker bark and a weaker hot. Opening the pores of the skin during the early cold to sweat, relieve pain in the shoulders and back, pain in the extremities joints, promote circulation of blood and treat lack of yang. The pharmacological action is known to inhibit the development of Escherichia coli, Bacillus subtilis, Staphylococcus aureus, pneumococcus pneumoniae, inhibition of influenza virus, and diuretic effect.

생강(Zingiber officinale)은 새양 또는 새앙이라고도 하는데, <고려사>에 있는 생강에 대한 기록으로 보아 한국에서는 고려시대 이전부터 재배했으리라 추정하고, 고려시대 문헌인 <향약구급방>에는 약용 식물로 기록되어 있다. 1996년 한국의 생강 생산량은 2만 7,890톤으로, 전라북도, 충청남도에서 총 생산량의 92%를 생산하고 있다. 뿌리 줄기는 말려 갈아서 빵, 과자, 카레, 소스, 피클 등 향신료로 사용하고, 껍질을 벗기고 끓인 후 시럽에 넣어 절이기도 하며, 생강차와 생강주 등을 만들기도 한다. 한방에서는 뿌리 말린 것을 건강(乾薑)이라는 약재로 쓰는데, 소화불량, 구토, 설사에 효과가 있고, 혈액 순환을 촉진하며, 항염증, 진통 효과가 있다.Ginger ( Zingiber (officinale ), also known as Saeyang or Saeang, is considered to have been cultivated in Korea before the Goryeo Dynasty. In 1996, ginger production in Korea was 27,890 tons, producing 92% of total production in North Jeolla Province and South Chungcheong Province. The rhizome is dried and used as a spice such as bread, sweets, curry, sauce, and pickles. Peel, boil, and then marinated in syrup. Ginger tea and ginger are also made. In oriental medicine, the root is used as a medicine called health (乾薑), which is effective for indigestion, vomiting and diarrhea, promotes blood circulation, and has anti-inflammatory and analgesic effects.

대추는 대추나무의 열매로서, 조(棗) 또는 목밀(木蜜)이라고도 한다. 과실은 생식할 뿐만 아니라 채취한 후 푹 말려 건과(乾果)로서 과자, 요리 및 약용으로 쓰인다. 생활 속에서 가공하여 대추술, 대추차, 대추식초, 대추죽 등으로도 활용한다. 한방에서는 이뇨, 강장, 완화제(緩和劑)로 쓰인다.Jujube is a fruit of the jujube tree, also known as crude (목) or wood wheat (木 蜜). Fruits are not only raw, but also dried after being harvested and used as sweets, dishes, and medicinal herbs. Processed in everyday life, jujube wine, jujube tea, jujube vinegar, jujube porridge. In oriental medicine, it is used as a diuretic, tonic, palliative (緩和 劑).

잣은 잣나무의 열매로서, 해송자(海松子), 백자(柏子), 송자(松子), 실백(實柏)이라고도 한다. 솔방울처럼 생긴 구과(毬果)에 들어 있으며, 속에 있는 흰 배젖(胚乳)은 향기와 맛이 좋으므로 식용하거나 약용한다. 유효성분으로 지방유(脂肪油) 74%, 단백질 15%를 함유하며, 자양강장의 효과가 있다. 각종 요리에 고명으로 쓰이며, 죽을 끓여 먹기도 한다.Pine nuts are the fruits of pine trees, also known as Haesongja (海松 子), white porcelain (柏 子), songja (松子), and silver white (實 柏). Condensation-like conifers (毬果) is contained in, and the white belly milk (胚乳) in the scent and taste good, so edible or medicinal. It contains 74% fatty oil and 15% protein as an active ingredient and has the effect of nourishing tonic. It is used as a garnish in various dishes, and also boiled porridge.

이에, 본 발명자들은 문헌에서 전래되는 전통적인 제조방법에 의해 제조된 오종주의 수득율이 낮고 주질이 농후하여 음용이 어려운 단점을 참고하여 수득율이 높고 주질이 개선된 발효곡주의 제조방법을 개발하고자 예의 노력한 결과, 급수비율만을 증량하는 방법 또는 급수비율을 증량하고 발효시간을 늘려서 완전 발효시킨 후, 액화제 및 당화제를 첨가하는 방법으로 제조된 제성주가 높은 수득율을 가지고 개선된 주질을 나타냄을 확인하고 본 발명을 완성하게 되었다.Accordingly, the present inventors have made diligent efforts to develop a method of producing fermented grain wine with high yield and improved quality, referring to the disadvantages of low yield and poor quality of alcoholic beverages prepared by the conventional manufacturing methods introduced in the literature. After the fermentation was completed by increasing only the water feed rate or increasing the water feed rate and increasing the fermentation time, and adding the liquefaction agent and saccharifying agent, it was confirmed that the sake liquor produced improved quality with high yield. The invention was completed.

본 발명의 주된 목적은 문헌에서 전래되는 오종주의 전통적인 제조방법을 개량하여 정량화함으로서, 고수율과 우수한 맛, 향미 및 주질을 갖는 발효곡주의 제조방법을 제공하는 데 있다. The main object of the present invention is to provide a method for producing fermented grain wine having high yield, excellent taste, flavor and quality by improving and quantifying the traditional production method of five kinds of liquor derived from the literature.

상기 목적을 달성하기 위하여, 본 발명은 (a) 찹쌀을 침지, 증자하는 단계; (b) 누룩가루에 물을 첨가하고 침출 및 여과시켜 누룩 여과액을 준비하는 단계; (c) 상기 (a) 단계에서 증자된 찹쌀과 상기 (b) 단계에서 준비된 누룩 여과액에 물을 첨가하고 당화 및 발효시켜 1단 담금의 술덧을 제조하는 단계; (d) 상기 제조된 1단 담금의 술덧에 후추, 계피, 생강, 잣, 대추 및 증류식 소주를 첨가하고 발효시켜 2단 담금의 술덧을 제조하는 단계; 및 (e) 상기 제조된 2단 담금의 술덧을 여과하고 물을 첨가하여 여과주의 알코올분을 규격화하는 단계를 포함하는 향신료와 과실을 이용한 발효곡주의 제조방법을 제공한다.In order to achieve the above object, the present invention comprises the steps of (a) dipping, increasing the glutinous rice; (b) adding water to the yeast powder, leaching and filtering to prepare a yeast filtrate; (c) adding water to the glutinous rice cooked in step (a) and the yeast filtrate prepared in step (b), saccharifying and fermenting to prepare a drunk of one step immersion; (d) adding the fermentation of pepper, cinnamon, ginger, pine nuts, jujube and distilled soju to the sourdough of the first stage soak to prepare the sourdough of the two-stage dip; And (e) provides a method of producing fermented grain wine using spices and fruits comprising the step of filtering the sultry of the prepared two-stage immersion and adding water to standardize the alcohol content of the filtered strain.

본 발명은 또한, (a) 찹쌀을 침지, 증자하는 단계; (b) 누룩가루에 물을 첨가하고 침출 및 여과시켜 누룩 여과액을 준비하는 단계; (c) 상기 (a) 단계에서 증자된 찹쌀과 상기 (b) 단계에서 준비된 누룩 여과액에 물을 첨가하고 당화 및 발효시켜 1단 담금의 술덧을 제조하는 단계; (d) 상기 제조된 1단 담금의 술덧에 후추, 계피, 생강, 잣, 대추, 침지, 증자시킨 찹쌀, 액화제, 당화제 및 증류식 소주를 첨 가하고 발효시켜 2단 담금의 술덧을 제조하는 단계; 및 (e) 상기 제조된 2단 담금의 술덧을 여과하고 물을 첨가하여 여과주의 알코올분을 규격화하는 단계를 포함하는 향신료와 과실을 이용한 발효곡주의 제조방법을 제공한다.The present invention also comprises: (a) immersing and increasing the glutinous rice; (b) adding water to the yeast powder, leaching and filtering to prepare a yeast filtrate; (c) adding water to the glutinous rice cooked in step (a) and the yeast filtrate prepared in step (b), saccharifying and fermenting to prepare a drunk of one step immersion; (d) adding the fermentation of pepper, cinnamon, ginger, pine nuts, jujube, dipping, increased glutinous rice, liquefaction agent, saccharifying agent, and distilled shochu to fermentation of the prepared one-stage immersion, and fermentation of two-stage immersion step; And (e) provides a method of producing fermented grain wine using spices and fruits comprising the step of filtering the sultry of the prepared two-stage immersion and adding water to standardize the alcohol content of the filtered strain.

본 발명은 문헌에서 전래되는 오종주의 전통적인 제조방법을 개량하여 정량화함으로서, 급수비율만을 증량하는 방법 또는 급수비율을 증량하고 발효시간을 늘려서 완전 발효시킨 후, 액화제 및 당화제를 첨가하는 방법으로 제조되고, 고수율과 우수한 맛, 향미 및 주질을 갖는 것을 특징으로 하는 발효곡주의 제조방법을 제공하는 효과가 있다.The present invention is produced by the method of increasing the water supply ratio only or by increasing the fermentation time and fully fermenting by increasing the fermentation rate by quantifying by improving the conventional manufacturing method of Ohjongju, which is introduced in the literature. It is effective in providing a method for producing fermented grain wine, which has a high yield and excellent taste, flavor and quality.

본 발명은 일 관점에서, (a) 찹쌀을 침지, 증자하는 단계; (b) 누룩가루에 물을 첨가하고 침출 및 여과시켜 누룩 여과액을 준비하는 단계; (c) 상기 (a) 단계에서 증자된 찹쌀과 상기 (b) 단계에서 준비된 누룩 여과액에 물을 첨가하고 당화 및 발효시켜 1단 담금의 술덧을 제조하는 단계; (d) 상기 제조된 1단 담금의 술덧에 후추, 계피, 생강, 잣, 대추 및 증류식 소주를 첨가하고 발효시켜 2단 담금의 술덧을 제조하는 단계; 및 (e) 상기 제조된 2단 담금의 술덧을 여과하고 물을 첨가하여 여과주의 알코올분을 규격화하는 단계를 포함하는 향신료와 과실을 이용한 발효곡주의 제조방법에 관한 것이다.The present invention in one aspect, (a) immersing, increasing the glutinous rice; (b) adding water to the yeast powder, leaching and filtering to prepare a yeast filtrate; (c) adding water to the glutinous rice cooked in step (a) and the yeast filtrate prepared in step (b), saccharifying and fermenting to prepare a drunk of one step immersion; (d) adding the fermentation of pepper, cinnamon, ginger, pine nuts, jujube and distilled soju to the sourdough of the first stage soak to prepare the sourdough of the two-stage dip; And (e) relates to a method of producing fermented grain wine using spices and fruit comprising the step of filtering the sultry of the prepared two-stage immersion and adding water to standardize the alcohol content of the filtered liquor.

본 발명에 있어서, 상기 (b) 단계를 거친 1단 담금의 술덧의 급수량은 찹쌀과 누룩가루 합계중량의 120~200%인 것을 특징으로 할 수 있다.In the present invention, the water supply amount of the drunk of the first stage immersion passed through the step (b) may be characterized in that 120 ~ 200% of the total weight of glutinous rice and yeast powder.

본 발명은 다른 관점에서, (a) 찹쌀을 침지, 증자하는 단계; (b) 누룩가루에 물을 첨가하고 침출 및 여과시켜 누룩 여과액을 준비하는 단계; (c) 상기 (a) 단계에서 증자된 찹쌀과 상기 (b) 단계에서 준비된 누룩 여과액에 물을 첨가하고 당화 및 발효시켜 1단 담금의 술덧을 제조하는 단계; (d) 상기 제조된 1단 담금의 술덧에 후추, 계피, 생강, 잣, 대추, 침지, 증자시킨 찹쌀, 액화제, 당화제 및 증류식 소주를 첨가하고 발효시켜 2단 담금의 술덧을 제조하는 단계; 및 (e) 상기 제조된 2단 담금의 술덧을 여과하고 물을 첨가하여 여과주의 알코올분을 규격화하는 단계를 포함하는 향신료와 과실을 이용한 발효곡주의 제조방법에 관한 것이다.The present invention in another aspect, (a) immersing, increasing the glutinous rice; (b) adding water to the yeast powder, leaching and filtering to prepare a yeast filtrate; (c) adding water to the glutinous rice cooked in step (a) and the yeast filtrate prepared in step (b), saccharifying and fermenting to prepare a drunk of one step immersion; (d) adding the fermentation of pepper, cinnamon, ginger, pine nuts, jujube, dipping, increased glutinous rice, liquefaction agent, saccharifying agent, and distilled shochu to fermentation of the prepared single-stage immersion to prepare the two-stage immersion step; And (e) relates to a method of producing fermented grain wine using spices and fruit comprising the step of filtering the sultry of the prepared two-stage immersion and adding water to standardize the alcohol content of the filtered liquor.

본 발명에 있어서, 상기 (b) 단계를 거친 1단 담금의 술덧의 급수량은 찹쌀과 누룩가루 합계중량의 120~200%인 것을 특징으로 할 수 있다.In the present invention, the water supply amount of the drunk of the first stage immersion passed through the step (b) may be characterized in that 120 ~ 200% of the total weight of glutinous rice and yeast powder.

본 발명에 있어서, 상기 당화 및 발효는 약 25℃에서 약 6일간 수행하는 것을 특징으로 할 수 있다.In the present invention, the saccharification and fermentation may be performed for about 6 days at about 25 ℃.

본 발명에 있어서, 상기 액화제는 α-아밀라아제이고, 당화제는 β-아밀라아제인 것을 특징으로 할 수 있다.In the present invention, the liquefying agent is α-amylase, the glycating agent may be characterized in that the β-amylase.

본 발명에서 급수비율(%)은 전체급수량(㎖)/(찹쌀+누룩가루 합계중량(g))× 100으로 계산하였다.In the present invention, the water supply ratio (%) was calculated as the total water supply amount (ml) / (total weight (g) of glutinous rice + yeast powder) x 100.

규합총서에서 곡류의 양은 말(斗)과 되를 단위로 하여 사용하고 있으나 대두 혹은 소두의 정확한 표현이 없으므로 본 발명에서는 소두를 기준으로 하였고, 한 말은 9ℓ로 쌀 한 말의 중량은 실측에 의하여 약 8㎏이며, 또한, 한 되는 0.9ℓ로 곡류 한 되의 중량은 실측에 의하여 약 0.5㎏이고, 대추 한 되의 중량은 실측에 의하여 약 0.3㎏이다. 소주를 첨가하는 단위로는 복자를 사용하고 있는데 복자에 관한 양은 적선소주(謫仙燒酒)(정동효 저, 우리 술 사전, p455, 중앙대학교 출판부, 1995)에서 한 되가 네 복자 되는 것 같다고 기술하고 있으므로 한 복자는 미터법으로 225㎖가 된다. 누룩을 물에 담그는 데 사용한 사발은 요즘 사용되고 있는 국그릇으로, 한 사발의 양은 0.6ℓ가 된다. 상기의 내용은 척관법을 미터법으로 계량화한 것으로 정리하자면 다음과 같다.The amount of grains in the rally is used as a unit of horse and soybean, but since there is no accurate expression of soybean or soybean, in the present invention, it is based on soybean, and one horse is 9 liters. It is about 8 kg, and the weight of the grain which has been grained to 0.9 liter is about 0.5 kg by actual measurement, and the weight of the jujube is about 0.3 kg by actual measurement. Bokja is used as a unit for adding soju, and the amount of fuchu is described as one of the four lucky ones in the red wine shochu (Jeong Dong-hyo), Korean Liquor Dictionary , p455, Chung-Ang University Press, 1995). Therefore, one futon becomes 225 ml in metric system. The bowl used to soak the malt in water is a soup bowl that is used nowadays, and the amount of one bowl is 0.6ℓ. The above is a quantification of the duct method as follows.

소두(한 말) : 9ℓ, 소두(한 되) : 0.9ℓSoybean (s): 9ℓ, Soybeans (Han): 0.9ℓ

소두(한 되): 0.9ℓ를 기준으로 미터법으로 계량화하였을 경우,Soybean (Han): When metrically measured at 0.9 liters,

: 쌀 0.9ℓ = 800g / 대추 0.9ℓ = 300g / 누룩 0.9ℓ = 500g: Rice 0.9ℓ = 800g / Jujube 0.9ℓ = 300g / Yeast 0.9ℓ = 500g

소두(한 되) : 0.9ℓ = 네 복자(∴ 한 복자 = 225㎖)Soybean paste (Han): 0.9ℓ = Four futons (∴ One futon = 225ml)

한 사발 = 0.6ℓ One bowl = 0.6ℓ

본 발명에서는 규합총서 문헌상의 내용대로 종래의 척관법(尺貫法)을 현대의 미터(meter)법으로 계량화하여 시험 양조함으로써 전통적인 오종주를 재현하였고, 이를 바탕으로 급수비율만을 증량하는 방법 또는 급수비율을 증량하고 발효시간을 늘려서 완전 발효시킨 후, 액화제 및 당화제를 첨가하는 방법으로 제조된 발효곡주를 대상으로 제성비율측정, 향미성분분석 및 관능평가를 실시하여 본 발명에 따른 발효곡주가 높은 수득율을 가지고 개선된 주질을 나타냄을 확인하였다. In the present invention, conventional jongju was reproduced by quantifying and brewing a conventional duct method using a modern meter method as described in the document of the rally, and based on this, a method of increasing only the watering rate or increasing the watering rate. The fermented grain liquor according to the present invention can be obtained by measuring the ratio of fermentation grains, flavor component analysis and sensory evaluation of fermented grain liquor prepared by adding fermentation agent and saccharifying agent. It has been confirmed that it shows improved quality.

발효곡주의 제조에 있어서, 전래방법과 같이 전체급수량이 찹쌀과 누룩가루 합계중량의 약 18%에 해당할 경우에는 원료인 찹쌀사용량을 기준으로 계산한 알코올분 18% 제성주의 제성비율이 260%로 수득율이 낮으므로, 본 발명에서는 1단 담금 술덧제조단계에서 전체급수량이 찹쌀과 누룩가루 합계중량의 160%가 되도록 하기 위하여 급수만을 증량하는 방법 및 1단 담금 술덧제조단계에서 전체급수량이 찹쌀과 누룩가루 합계중량의 160%가 되도록 하기 위하여 급수를 증량하고 알코올 발효비율이 70% 이상 이루어질 수 있도록 발효기간을 문헌상에 기재된 3일보다 늘려서 5~7일로 하여 완전발효시킨 후, 2단 담금 술덧제조단계에서 원하는 양의 일정한 당분을 잔존시킬 수 있도록 원료의 전처리 단계에서와 동일한 방법으로 침지, 증자시킨 찹쌀을 첨가하고, 제조수율을 높이기 위하여 α-아밀라아제, β-아밀라아제를 첨가하여 당화발효를 진행시킴으로써, 원료인 찹쌀사용량을 기준으로 계산한 알코올분 18% 제성주의 제성비율을 약 400~460% 수준으로 수득량을 높였다.In the production of fermented grain wine, if the total water supply amount is about 18% of the total weight of glutinous rice and yeast powder as in the conventional method, the alcohol content calculated based on the amount of glutinous rice used as raw material is 18%. As the yield is low, in the present invention, a method of increasing only the water supply in order to make the total water supply amount to 160% of the total weight of glutinous rice and yeast powder in the first-stage dipped sake manufacturing step and the total water supply in the one-stage dipped sake manufacturing step In order to make 160% of the total weight of yeast powder, increase the water supply, and fermentation period is increased to 5 ~ 7 days than 3 days described in the literature so that alcohol fermentation ratio can be 70% or more. In order to retain the desired amount of sugar in the step, add soaked and increased glutinous rice in the same manner as in the pretreatment step of the raw material, In order to increase the yield, α-amylase and β-amylase were added to the saccharification fermentation to increase the yield to about 400-460% of alcohol content calculated based on the amount of glutinous rice used as raw material. .

이하, 비교예와 실시예를 통하여 본 발명을 더욱 상세히 설명하고자 한다. 이들 실시예는 오로지 본 발명을 예시하기 위한 것으로, 본 발명의 범위가 이들 실시예에 의해 제한되는 것으로 해석되지 않는 것은 당업계에서 통상의 지식을 가진 자에게 있어서 자명할 것이다.Hereinafter, the present invention will be described in more detail with reference to comparative examples and examples. These examples are only for illustrating the present invention, and it will be apparent to those skilled in the art that the scope of the present invention is not to be construed as being limited by these examples.

특히, 하기 실시예에서는 찹쌀을 사용한 경우만을 예시하였으나, 통상의 주류 제조에 사용되는 옥수수, 조 등의 곡물을 사용할 수 있는 것은 당업계의 통상의 지식을 가진 자에게 있어서 자명할 것이다.In particular, the following examples illustrate only the case of using glutinous rice, it will be apparent to those skilled in the art that the grains such as corn, crude, etc. that are used in the general liquor production can be used.

비교예 1Comparative Example 1

1-1. 원료의 전처리1-1. Pretreatment of raw materials

수세한 찹쌀 800g을 물에 3시간 동안 침지하고 1시간 동안 물빼기를 하여 증자기로 1.2㎏/㎠, 120℃에서 50분간 증자하고 15분간 뜸들이기를 하여 30℃로 냉각시켰다. 파쇄한 누룩가루 50g에 물 150㎖를 첨가하고 5~10℃의 냉장고에서 1일간 침출시킨 다음, 25 메쉬(mesh)체로 여과하여 찌꺼기가 제거된 누룩 여과액 150㎖를 제조하였다.800 g of washed glutinous rice was immersed in water for 3 hours, drained for 1 hour, and steamed at 1.2 kg / cm 2 and 120 ° C. for 50 minutes with steam, and then steamed for 15 minutes and cooled to 30 ° C. 150 ml of water was added to 50 g of crushed Nuruk powder, and leached in a refrigerator at 5 to 10 ° C. for 1 day, and filtered through a 25 mesh sieve to prepare 150 ml of Nuruk filtrate from which debris was removed.

1-2. 1단 담금의 술덧제조1-2. Preparation of drunk of one step immersion

상기 1-1에서 전처리된 찹쌀 800g과 누룩 여과액 150㎖를 혼합하여 25℃의 항온기에서 3일간 당화 및 알코올 발효시켜 1단 담금의 술덧을 제조하였다.800 g of glutinous rice pretreated in 1-1 and 150 ml of yeast filtrate were mixed, and saccharification and alcohol fermentation were performed for 3 days in a thermostat at 25 ° C. to prepare a single-dip immersion.

1-3. 2단 담금의 술덧제조1-3. Production of drunk of two steps of soaking

상기 1-2에서 제조된 1단 담금의 술덧에 후추 및 계피 각각 0.375g을 분말화하여 베주머니에 담아 넣고, 생강 및 잣 각각 0.375g을 빻아서 넣고, 대추 30g은 깨끗이 씻어 넣고, 45% 증류식 소주 1,012.5㎖를 첨가한 후, 25℃의 항온기에서 14일간 발효시켜 2단 담금의 알코올분 26.4% 숙성술덧 2,180㎖를 제조하였다.Powdered pepper and cinnamon 0.375g each into a bag, add 0.375g of ginger and pine nuts, respectively, and add 30g of jujube to wash, and distill 45% After adding 1,012.5 ml of food soju, fermentation was carried out for 14 days in a thermostat at 25 ° C. to prepare 2,180 ml of alcohol content of 26.4% aging.

1-4. 여과 및 제성1-4. Filtration and Detergent

상기 1-3에서 제조된 2단 담금의 숙성술덧 2,180㎖를 여과포로 압착하여 술지게미 730g을 걸러내어 알코올분 26.4% 여과주 1,420㎖를 얻었고, 알코올분 18%로 규격화하기 위하여 물 662㎖를 첨가하여 알코올분 18% 원주 2,082㎖를 제조하였으며, 0℃ 이하에서 1㎛ 이하의 막으로 냉동 여과하여 제성주를 제조하였다.2,180 ml of the two-stage immersion prepared in 1-3 were pressed with a filter cloth to filter out 730 g of sake lees to obtain 1,420 ml of alcohol content 26.4%, and 662 ml of water was added to standardize alcohol content 18%. 2,082 ml of 18% alcohol content was prepared, and the brew was prepared by freezing filtration with a membrane of 1 μm or less at 0 ° C.

실시예Example 1  One

1-1. 원료의 전처리1-1. Pretreatment of raw materials

수세한 찹쌀 800g을 물에 3시간 동안 침지하고 1시간 동안 물빼기를 하여 증자기로 1.2㎏/㎠, 120℃에서 50분간 증자하고 15분간 뜸들이기를 하여 30℃로 냉각시켰다. 파쇄한 누룩가루 50g에 물 150㎖를 첨가하고 5~10℃의 냉장고에서 1일간 침출시킨 다음, 25 메쉬(mesh)체로 여과하여 찌꺼기가 제거된 누룩 여과액 150㎖를 제조하였다.800 g of washed glutinous rice was immersed in water for 3 hours, drained for 1 hour, and steamed at 1.2 kg / cm 2 and 120 ° C. for 50 minutes with steam, and then steamed for 15 minutes and cooled to 30 ° C. 150 ml of water was added to 50 g of crushed Nuruk powder, and leached in a refrigerator at 5 to 10 ° C. for 1 day, and filtered through a 25 mesh sieve to prepare 150 ml of Nuruk filtrate from which debris was removed.

1-2. 1단 담금의 1-2. 1-stage immersion 술덧제조Drunk manufacturing

상기 1-1에서 전처리된 찹쌀 800g과 누룩 여과액 150㎖를 혼합하고 전체급수량이 찹쌀과 누룩가루 합계중량의 160%가 되도록 하기 위하여 물 1,210㎖를 첨가하여 25℃의 항온기에서 3일간 당화 및 알코올 발효시켜 1단 담금의 술덧을 제조하였다.800 g of glutinous rice pretreated in 1-1 and 150 ml of yeast filtrate were mixed and 1,210 ml of water was added to make the total water supply amount 160% of the total weight of glutinous rice and yeast powder. Fermentation was performed to prepare the sour syrup of the first stage immersion.

1-3. 2단 담금의 1-3. Two-stage immersion 술덧제조Drunk manufacturing

상기 1-2에서 제조된 1단 담금의 술덧에 후추 및 계피 각각 0.375g을 분말화하여 베주머니에 담아 넣고, 생강 및 잣 각각 0.375g을 빻아서 넣고, 대추 30g은 깨끗이 씻어 넣고, 45% 증류식 소주 1,012.5㎖를 첨가한 후, 25℃의 항온기에서 14일간 발효시켜 2단 담금의 알코올분 19.3% 숙성술덧 3,360㎖를 제조하였다. Powdered pepper and cinnamon 0.375g each into a bag, add 0.375g of ginger and pine nuts, respectively, and add 30g of jujube to wash, and distill 45% After adding 1,012.5 ml of dietary liquor, fermentation was carried out for 14 days in a thermostat at 25 ° C. to prepare 3,360 ml of aged 19.3% alcohol fraction in two stages.

1-4. 여과 및 1-4. Filtration and 제성Castle

상기 1-3에서 제조된 2단 담금의 숙성술덧 3,360㎖를 여과포로 압착하여 술지게미 346g을 걸러내어 알코올분 19.3% 여과주 3,000㎖를 얻었고, 알코올분 18%로 규격화하기위하여 물 216㎖를 첨가하여 알코올분 18% 원주 3,216㎖를 제조하였으며, 0℃ 이하에서 1㎛ 이하의 막으로 냉동 여과하여 제성주를 제조하였다.3,360 ml of the two-stage immersion prepared in 1-3 were pressed with a filter cloth to filter out 346 g of sake lees to obtain 3,000 ml of alcohol content in 19.3% alcohol, and 216 ml of water to be standardized to 18% alcohol content. 3,216 ml of alcohol content of 18% alcohol was prepared, and a sacrificial liquor was prepared by freezing filtration with a membrane of 1 μm or less at 0 ° C. or less.

실시예Example 2  2

2-1. 원료의 전처리2-1. Pretreatment of raw materials

수세한 찹쌀 601g을 물에 3시간 동안 침지하고 1시간 동안 물빼기를 하여 증자기로 1.2㎏/㎠, 120℃에서 50분간 증자하고 15분간 뜸들이기를 하여 30℃로 냉각시켰다. 파쇄한 누룩가루 50g에 물 150㎖를 첨가하고 5~10℃의 냉장고에서 1일간 침출시킨 다음, 25 메쉬(mesh)체로 여과하여 찌꺼기가 제거된 누룩 여과액 150㎖를 제조하였다.601 g of washed glutinous rice was immersed in water for 3 hours, drained for 1 hour, and then steamed at 1.2 kg / cm 2 and 120 ° C. for 50 minutes using a steam cooker, and cooled to 30 ° C. by steaming for 15 minutes. 150 ml of water was added to 50 g of crushed Nuruk powder, and leached in a refrigerator at 5 to 10 ° C. for 1 day, and filtered through a 25 mesh sieve to prepare 150 ml of Nuruk filtrate from which debris was removed.

2-2. 1단 담금의 2-2. 1-stage immersion 술덧제조Drunk manufacturing

상기 2-1에서 전처리된 찹쌀 601g과 누룩 여과액 150㎖를 혼합하고 전체급수량이 찹쌀과 누룩가루 합계중량의 160%가 되도록 하기 위하여 물 1,210㎖를 첨가하였고, 알코올 발효비율 70% 이상이 되도록 25℃의 항온기에서 6일간 당화 및 알코올 발효시켜 1단 담금의 술덧을 제조하였다.601 g of glutinous rice pretreated in 2-1 and 150 ml of yeast filtrate were mixed and 1,210 ml of water was added so that the total water supply amount was 160% of the total weight of glutinous rice and yeast powder, and the alcohol fermentation ratio was 25% or more. Saccharification and alcohol fermentation were performed for 6 days in a thermostat at 0 ° C. to prepare a dipped soak.

2-3. 2단 담금의 2-3. Two-stage immersion 술덧제조Drunk manufacturing

상기 2-2에서 제조된 1단 담금의 술덧에 후추 및 계피 각각 0.375g을 분말화 하여 베주머니에 담아 넣고, 생강 및 잣 각각 0.375g을 빻아서 넣고, 대추 30g은 깨끗이 씻어 넣고, 수세한 찹쌀 199g을 물에 3시간 동안 침지하고 1시간 동안 물빼기를 하여 증자기로 1.2㎏/㎠, 120℃에서 50분간 증자하고 15분간 뜸들이기를 하여 30℃로 냉각시킨 다음, 첨가하고 α-아밀라아제 및 β-아밀라아제 각각 0.02g 및 45% 증류식 소주 1,012.5㎖를 첨가한 후, 25℃의 항온기에서 14일간 발효시켜 2단 담금의 알코올분 21.5% 숙성 술덧 3,360㎖를 제조하였다. Powdered pepper and cinnamon 0.375g each into a bag, and add 0.375g of ginger and pine nuts, respectively, and wash 30g of jujube, and wash with glutinous rice. 199 g Submerged in water for 3 hours, drained for 1 hour, steamed at 1.2 kg / cm 2, at 50 ° C. for 50 minutes, steamed at 15 ° C. for 15 minutes, cooled to 30 ° C., and added to α-amylase and β-amylase. After adding 0.02 g and 45% distilled shochu 1,012.5 ml, respectively, fermentation was carried out in a thermostat at 25 ° C. for 14 days to prepare 3360 ml of 21.5% aged alcohol powder.

2-4. 여과 및 2-4. Filtration and 제성Castle

상기 2-3에서 제조된 2단 담금의 숙성술덧 3,360㎖를 여과포로 압착하여 술지게미 255g을 걸러내어 알코올분 21.5% 여과주 3,040㎖를 얻었고, 알코올분 18%로 규격화하기 위하여 물 591㎖를 첨가하여 알코올분 18% 원주 3,631㎖를 제조하였으며, 0℃ 이하에서 1㎛ 이하의 막으로 냉동 여과하여 제성주를 제조하였다 (도 1 참조).3,360 ml of the two-stage immersion prepared in 2-3 was pressed with a filter cloth to filter out 255 g of sake lees to obtain 3,040 ml of alcohol content 21.5%, and 591 ml of water was added to standardize alcohol content 18%. 3,631 ml of alcohol content of 18% alcohol was prepared, and a sacrificial liquor was prepared by freezing filtration with a membrane of 1 μm or less at 0 ° C. or less (see FIG. 1).

실시예Example 3 3

3-1. 원료의 전처리3-1. Pretreatment of raw materials

수세한 찹쌀 601g을 물에 3시간 동안 침지하고 1시간 동안 물빼기를 하여 증자기로 1.2㎏/㎠, 120℃에서 50분간 증자하고 15분간 뜸들이기를 하여 30℃로 냉각시켰다. 파쇄한 누룩가루 50g에 물 150㎖를 첨가하고 5~10℃의 냉장고에서 1일간 침출시킨 다음, 25 메쉬(mesh)체로 여과하여 찌꺼기가 제거된 누룩 여과액 150㎖를 제조하였다.601 g of washed glutinous rice was immersed in water for 3 hours, drained for 1 hour, and then steamed at 1.2 kg / cm 2 and 120 ° C. for 50 minutes using a steam cooker, and cooled to 30 ° C. by steaming for 15 minutes. 150 ml of water was added to 50 g of crushed Nuruk powder, and leached in a refrigerator at 5 to 10 ° C. for 1 day, and filtered through a 25 mesh sieve to prepare 150 ml of Nuruk filtrate from which debris was removed.

3-2. 1단 담금의 3-2. 1-stage immersion 술덧제조Drunk manufacturing

상기 3-1에서 전처리된 찹쌀 601g과 누룩 여과액 150㎖를 혼합하고 전체급수량이 찹쌀과 누룩가루 합계중량의 160%가 되도록 하기 위하여 물 1,210㎖를 첨가하였고, 알코올 발효비율 70% 이상이 되도록 25℃의 항온기에서 6일간 당화 및 알코올 발효시켜 1단 담금의 술덧을 제조하였다.601 g of glutinous rice pretreated in 3-1 and 150 ml of yeast filtrate were mixed and 1,210 ml of water was added so that the total water supply amount was 160% of the total weight of glutinous rice and yeast powder, and the alcohol fermentation ratio was 25% or more. Saccharification and alcohol fermentation were performed for 6 days in a thermostat at 0 ° C. to prepare a dipped soak.

3-3. 2단 담금의 3-3. Two-stage immersion 술덧제조Drunk manufacturing

상기 3-2에서 제조된 1단 담금의 술덧에 후추 및 계피 각각 0.375g을 분말화하여 베주머니에 담아 넣고, 생강 및 잣 각각 0.375g을 빻아서 넣고, 대추 30g은 깨끗이 씻어 넣고, 수세한 찹쌀 199g을 물에 3시간 동안 침지하고 1시간 동안 물빼기를 하여 증자기로 1.2㎏/㎠, 120℃에서 50분간 증자하고 15분간 뜸들이기를 하여 30℃로 냉각시킨 다음, 첨가하고 45% 증류식 소주 1,012.5㎖를 첨가한 후, 25℃의 항온기에서 14일간 발효시켜 2단 담금의 알코올분 21.5% 숙성술덧 3,360㎖를 제조하였다. Powdered pepper and cinnamon 0.375g each into a bag, add 0.375g of ginger and pine nuts, and wash 30g of jujube. 199 g Submerged in water for 3 hours, drained for 1 hour, steamed at 1.2㎏ / ㎠, steamer at 120 ℃ for 50 minutes, steamed for 15 minutes, cooled to 30 ℃, then added and 45% distilled shochu 1,012.5ml After the addition, fermentation was carried out in a thermostat at 25 ° C. for 14 days to prepare 3,360 ml of alcohol in 2 stages of immersion 21.5%.

3-4. 여과 및 3-4. Filtration and 제성Castle

상기 3-3에서 제조된 2단 담금의 숙성술덧 3,360㎖를 여과포로 압착하여 술지게미 542g을 걸러내어 알코올분 21.5% 여과주 2,800㎖를 얻었고, 알코올분 18%로 규격화하기위하여 물 544㎖를 첨가하여 알코올분 18% 원주 3,344㎖를 제조하였으며, 0℃ 이하에서 1㎛ 이하의 막으로 냉동 여과하여 제성주를 제조하였다.3,360 ml of the two-stage immersion prepared in 3-3 was compressed with a filter cloth to filter out 542 g of sake lees to obtain 2,800 ml of alcohol content in 21.5% alcohol, and 544 ml of water was added to normalize to 18% alcohol content. 3,344 ml of alcohol content of 18% alcohol was prepared, and a sacrificial liquor was prepared by freezing filtration with a membrane of 1 μm or less at 0 ° C. or less.

각 실험구별로는 전통적인 오종주 제조방법을 재현한 비교예 1, 급수비율만을 160%로 증량한 실시예 1, 급수비율을 160%로 증량하고 발효시간을 6일로 늘려서 알코올 발효비율이 70% 이상이 되도록 1단 담금 술덧을 제조하고, 침지, 증자시킨 찹쌀, α-아밀라아제, β-아밀라아제를 첨가하여 2단 담금 술덧을 제조한 실시예 2 및 α-아밀라아제와 β-아밀라아제의 첨가를 제외하고는 실시예 2와 동일한 방법으로 제조한 실시예 3(아밀라아제류 미사용)로 나누어 실험하였다 (표 1 참조).For each experimental section, Comparative Example 1, which reproduced the traditional method of producing five kinds of liquor, Example 1, which increased only the water supply ratio to 160%, increased the water supply ratio to 160%, and increased the fermentation time to 6 days. Except for preparing a two-stage immersion prepared by the first step soaked, and added, soaked, cooked glutinous rice, α-amylase, β-amylase and the addition of α-amylase and β-amylase Experiment was carried out by dividing into Example 3 (not using amylases) prepared in the same manner as in Example 2 (see Table 1).

담금배합표Immersion Table 구 분division 원 료 명Raw material name 비교예 1Comparative Example 1 실시예 1Example 1 실시예 2 Example 2 실시예 3Example 3 1단 담금1st stage immersion 누룩가루(g)Yeast Powder (g) 5050 5050 5050 5050 찹쌀(g)Glutinous rice (g) 800800 800800 601601 601601 급수(㎖)Water supply (ml) 150150 1,3601,360 1,3601,360 1,3601,360 2단 담금2-stage immersion 찹쌀(g)Glutinous rice (g) -- -- 199199 199199 α-아밀라아제(g)α-amylase (g) -- -- 0.020.02 -- β-아밀라아제(g)β-amylase (g) -- -- 0.020.02 -- 45% 증류식소주(㎖)45% distilled shochu (mL) 1,012.51,012.5 1,012.51,012.5 1,012.51,012.5 1,012.51,012.5 약제(g)Drug (g) 31.531.5 31.531.5 31.531.5 31.531.5 비 고Remarks 시험구분Test 원방 Far 급수160%Water supply 160% 증양법 Augmentation Act 증양법 Augmentation Act

1단 담금술덧의 각종 비율Various ratios of single stage immersion 구 분division 비교예 1Comparative Example 1 실시예 1Example 1 실시예 2Example 2 실시예 3Example 3 숙성술덧량 (㎖)  Aging amount (ml) 950950 2,1602,160 1,9611,961 1,9611,961 숙성술덧의 알코올분 (%)  Alcohol content of aged wine (%) 6.26.2 7.47.4 12.612.6 12.612.6 숙성술덧의 알코올량 (㎖) (주1)  Alcohol content of aged wine (ml) (Note 1) 58.958.9 159.84159.84 247.1247.1 247.1247.1 이론 알코올생성량 (㎖) (주2)  Theoretical alcohol production (ml) 423.28423.28 423.28423.28 317.99317.99 317.99317.99 발 효 비 율 (%)(주3)Fermentation rate (%) (Note 3) 13.913.9 37.837.8 77.777.7 77.777.7 (주 1) 숙성술덧의 알코올량 = 숙성술덧량 × 숙성술덧의 알코올분 (주 2) 이론 알코올생성량 = 쌀 사용량 × 쌀의 전분가(0.74) × 전분의 알코올 환산계수(0.715) (주 3) 발효비율 = (숙성술덧의 알코올량 / 이론 알코올생성량)× 100  (Note 1) Alcohol content of fermented liquor = Alcohol content of fermented liquor × Alcohol content of fermented liquor (Note 2) Theoretical alcohol production amount = Rice consumption × Starch value of rice (0.74) × Alcohol conversion factor of starch (0.715) (Note 3) Fermentation Proportion = (Alcohol Amount / Theoretical Alcohol Production) × 100

1단 담금술덧의 알코올분 측정 결과, 표 2에 나타난 바와 같이, 비교예 1의 경우는 급수량이 적어 액체가 거의 없는 관계로 시료채취가 곤란하여 알코올분을 측정할 수없었고, 이에 대용으로 탄산가스 발생량을 측정하여 수치를 환산하였다. 탄산가스 발생량 측정결과, 45g의 탄산가스가 발생하였고, 알코올로 비례 환산할 경우 47g이며, 용량으로 비례 환산할 경우 59㎖가 되어 숙성술덧 알코올분은 6.2%로 나타났다. 실시예 1은 7.4%, 실시예 2는 12.6%로 나타났다. 한편, 1단 담금술덧의 발효비율의 산출결과, 비교예 1은 13.9%, 실시예 1은 37.8%, 실시예 2는 77.7%이였므로 알코올 발효향취는 발효 비율이 가장 높은 실시예 2가 가장 많았으며 다음으로 실시예 1, 비교예 1의 순서인 것을 알 수 있었다.As a result of measuring the alcohol content of the first stage immersion, as shown in Table 2, in the case of Comparative Example 1, the sample was difficult to collect due to the small amount of water and there was little liquid, and thus the alcohol content could not be measured. The amount generated was measured and converted to a numerical value. As a result of measuring the amount of carbon dioxide generated, 45g of carbon dioxide was generated, and it was 47g when proportionally converted to alcohol, and 59ml when proportionally converted to capacity, and the amount of alcohol content was 6.2%. Example 1 was found to be 7.4%, and Example 2 was found to be 12.6%. On the other hand, as a result of calculating the fermentation ratio of the first stage immersion, Comparative Example 1 was 13.9%, Example 1 was 37.8%, Example 2 was 77.7%, so alcohol fermentation fragrance was the highest in Example 2 with the highest fermentation ratio. Next, it was found that the order of Example 1, Comparative Example 1.

2단 담금술덧의 여과주(㎖)와 술지게미(g)의 수량 및 제성비율Yield and Determination Ratio of Filtered Wine (ml) and Sake Flavor (g) 구 분division 비교예 1Comparative Example 1 실시예 1Example 1 실시예 2Example 2 실시예 3 (아밀라아제류 미사용)Example 3 (not using amylases) 숙성술덧량(㎖)Aging liquor amount (ml) 2,1802,180 3,3603,360 3,3603,360 3,3603,360 숙성술덧의 여과주량(㎖)Filtration stock of aged wine (ml) 1,4201,420 3,0003,000 3,0403,040 2,8002,800 여과주 알코올분(%)Filter alcohol content (%) 26.426.4 19.319.3 21.521.5 21.521.5 알코올분 18% 제성주량(㎖)Alcohol content 18% Detergent liquor (ml) 2,0822,082 3,2163,216 3,6313,631 3,3443,344 찹쌀사용량의 18% 제성주비율(%)18% ratio of glutinous rice consumption (%) 260260 402402 454454 418418 술지게미량(g)Alcohol content (g) 730730 346346 255255 542542 찹쌀사용량의 술지게미비율(%)Alcohol consumption ratio of glutinous rice consumption (%) 91.2591.25 43.2543.25 31.8831.88 67.7567.75

2단 담금의 숙성술덧의 여과주량(ml), 술지게미량(g) 및 제성비율 측정결과, 표 3에 나타난 바와 같이, α-아밀라아제와 β-아밀라아제를 첨가한 실시예 2의 경우, α-아밀라아제와 β-아밀라아제의 첨가를 제외하고는 실시예 2와 동일한 방법으로 제조한 실시예 3의 경우보다 제성비율이 높은 것을 알 수 있었다. 반면에, 전통적인 오종주 제조방법을 재현한 비교예 1은 실시예 1 및 실시예 2에 비하여 제성주 비율이 약 1.5~1.8배 적으므로 원가면에서 실시예 1 및 실시예 2를 상품화하는 것이 유리함을 알 수 있었다.As shown in Table 3, as shown in Table 3, in Example 2 to which α-amylase and β-amylase were added, α-amylase was measured. Except for the addition of and β-amylase it was found that the formulation ratio is higher than in the case of Example 3 prepared in the same manner as in Example 2. On the other hand, Comparative Example 1, which reproduces the traditional method of producing five kinds of liquor, has a ratio of about 1.5 to 1.8 times less than the ratio of Example 1 and Example 2, so it is advantageous to commercialize Examples 1 and 2 in terms of cost. And it was found.

상기에서 비교예 1에 비하여 실시예 1에서는 술지게미 발생이 감소하였으며, 실시예 2에서는 45%의 증류식 소주와 같이 찹쌀을 첨가하는 관계로 찹쌀의 경화에 의한 술지게미가 과다 발생하는 원인을 α-아밀라아제와 β-아밀라아제의 첨가로 감소시켰음을 알 수 있었다.In Example 1 compared to Comparative Example 1, the generation of sake lees was reduced, and in Example 2, due to the addition of glutinous rice, such as 45% distilled shochu, the cause of excessive sake lees due to the hardening of the glutinous rice α-amylase And β-amylase was found to reduce.

여과주의 주요성분 함량Main Components of Filtered Wine 구 분division 비교예 1Comparative Example 1 실시예 1Example 1 실시예 2Example 2 비중importance 1.0491.049 1.0251.025 1.0111.011 에틸알코올(v/v%)Ethyl alcohol (v / v%) 26.426.4 19.319.3 21.521.5 산도 Acidity 4.44.4 6.86.8 6.86.8 아미노산도 Amino acid degree 2.92.9 1.71.7 1.91.9 직당(%)Per share (%) 20.1420.14 7.57.5 6.16.1 불휘발분(g/100㎖)Nonvolatile matter (g / 100mL) 22.722.7 12.812.8 9.69.6 Acetaldehyde(ppm)Acetaldehyde (ppm) 4040 2424 3030 Ethylacetate(ppm) Ethylacetate (ppm) 180180 105105 103103 Methanol(ppm) Methanol (ppm) 1212 88 77 n-Propanol(ppm)n-Propanol (ppm) 105105 7373 7474 i-Butanol(ppm)i-Butanol (ppm) 196196 145145 149149 n-Butanol(ppm) n-Butanol (ppm) 3.33.3 1.91.9 1.91.9 i-Amylalcohol(ppm)i-Amylalcohol (ppm) 396396 316316 310310 Fusel Oil(ppm) Fusel Oil (ppm) 700.3700.3 535.9535.9 534.9534.9

※ G.C 분석조건※ G.C analysis condition

- 기기 : GC6890 system   Instrument: GC6890 system

- Detector Temperature : 220℃(F.I.D)   -Detector Temperature: 220 ℃ (F.I.D)

- Injector Temperature : 200℃   -Injector Temperature: 200 ℃

- Column Temperature : 40℃ - (10℃/min) - 120℃   -Column Temperature: 40 ℃-(10 ℃ / min)-120 ℃

- Column : HP - inowax(Crosslinked polyethylene glycol 1 × 0.53 × 30)   -Column: HP-inowax (Crosslinked polyethylene glycol 1 × 0.53 × 30)

- Carrier gas : N2(30㎖/min)Carrier gas: N 2 (30mL / min)

여과주의 주요성분 함량측정결과, 표 4에 나타난 바와 같이, 비교예 1은 직당이 약 20%로 음용하기에는 당분이 과다한 편이고, 실시예 1 및 실시예 2는 6.1~7.5%로 알코올분 18% 제성주로 환산하면 약 5~7%이므로 현대인이 음용하기에 적합한 직당량임을 알 수 있었다. 한편, 향기성분인 퓨젤유의 생산은 원료의 종류, 국, 효모, 발효시의 온도 경과 등에 따라 영향을 받는데, 본 발명에서는 45%의 증류식 소주를 첨가하는 관계로 증류식 소주의 영향을 많이 받아서 급수비율이 낮은 비교예 1이 급수비율이 높은 실시예 1 및 실시예 2보다 아세트알데히드, 에틸아세테이트, 퓨젤유(노르말 프로판올, 이소 부탄올, 노르말 부탄올, 이소 아밀알코올) 함량이 높게 나타났다. 이와 같이, 향기성분은 증류식 소주의 영향을 많이 받지만 발효의 향취는 비교예 1보다 실시예 1 및 실시예 2가 풍부한 것으로 나타났다.As a result of the measurement of the content of the main components of the filter strain, as shown in Table 4, Comparative Example 1 is too much sugar to drink about 20% of the sugar content, Example 1 and Example 2 is 6.1 to 7.5% alcohol content 18% When converted to Sungju, it is about 5 ~ 7%, so it can be seen that it is a suitable equivalent weight for modern people to drink. On the other hand, the production of the fragrance fusel oil is affected by the type of raw material, soup, yeast, temperature during fermentation, etc. In the present invention, 45% of distilled shochu is added, so it is affected by distilled shochu Comparative Example 1 having a low water supply ratio showed higher acetaldehyde, ethyl acetate, and fusel oil (normal propanol, iso butanol, normal butanol, and iso amyl alcohol) than Examples 1 and 2 having a high water feed rate. As described above, the fragrance component was greatly affected by the distilled shochu, but the aroma of fermentation was found to be richer in Examples 1 and 2 than in Comparative Example 1.

관능검사 및 종합적인 주질 평가표 (※ 배점기준 : 상 3점, 중 2점, 하 1점)Sensory test and comprehensive quality evaluation table (※ scoring criteria: 3 points on the top, 2 points on the middle, 1 point on the bottom) 주질 평가 항목Main quality evaluation item 비교예 1Comparative Example 1 실시예 1Example 1 실시예 2Example 2 flavor Prize +++ (9)+++ (9) ++++ (12)++++ (12) +++++ (15)+++++ (15) medium ++++ (8)++++ (8) +++ (6)+++ (6) ++ (4)++ (4) Ha -- -- -- 소 계sub Total 1717 1818 1919 향기Scent Prize ++++ (12)++++ (12) +++++ (15)+++++ (15) +++++ (15)+++++ (15) medium +++ (6)+++ (6) ++ (4)++ (4) ++ (4)++ (4) Ha -- -- -    - 소 계sub Total 1818 1919 1919 종합 평가 점수A comprehensive evaluation score 3535 3737 3838

평가의 재현성을 높이기 위하여 숙련된 주류 분석전문가 성인 7명을 선정하여 20℃, 관계습도 60%로 공기조절된 관능검사실에서 알코올분 18%로 제성한 제성주를 대상으로 관능검사 및 종합적인 주질평가를 실시하였다.In order to improve the reproducibility of the evaluation, the sensory test and comprehensive quality assessment were conducted on the adult sake made with 18% alcohol in the sensory laboratory, which had been selected by 7 experienced liquor analysts at 20 ℃ and 60% relative humidity. Was carried out.

관능검사 결과, 표 5에 나타난 바와 같이, 비교예 1은 전통적인 방법으로 제조한 제성주로서 당분이 너무 많고 주질이 농후하여 현대인의 기호에는 조금 부적합한 듯하였고, 실시예 1 및 실시예 2는 당분의 양이 알맞고 비교예 1보다 주질이 가벼워서 맛이 좋게 평가되었고, 향기 면에서는 원료인 찹쌀, 향신료와 과실, 증류식 소주의 향과 발효향의 산뜻한 향이 잘 조화되며, 전체적인 주질은 중후하면서도 부드러워 음용하기에 적합한 것으로 나타났다.As a result of the sensory test, as shown in Table 5, Comparative Example 1 is a sake prepared by the traditional method, too much sugar and rich in quality seemed to be a little unsuitable for the taste of modern people, Example 1 and Example 2 The amount was moderate and the quality was lighter than the comparative example 1, and the taste was evaluated well. Appeared to be suitable for.

이상으로 본 발명 내용의 특정한 부분을 상세히 기술하였는바, 당업계의 통상의 지식을 가진 자에게 있어서, 이러한 구체적 기술은 단지 바람직한 실시양태일 뿐이며, 이에 의해 본 발명의 범위가 제한되는 것이 아닌 점은 명백할 것이다. 따라서 본 발명의 실질적인 범위는 첨부된 청구항들과 그것들의 등가물에 의하여 정의된다고 할 것이다.The specific parts of the present invention have been described in detail above, and it is apparent to those skilled in the art that such specific descriptions are merely preferred embodiments, and thus the scope of the present invention is not limited thereto. something to do. Thus, the substantial scope of the present invention will be defined by the appended claims and their equivalents.

도 1은 본 발명에 따른 향신료와 과실을 이용한 발효곡주의 제조공정도이다.1 is a manufacturing process chart of fermented grain wine using spices and fruits according to the present invention.

Claims (5)

삭제delete 다음의 단계를 포함하는 향신료와 과실을 이용한 발효곡주의 제조방법:Method for preparing fermented grain wine using spices and fruits, comprising the following steps: (a) 찹쌀을 침지, 증자하는 단계;(a) dipping and increasing the glutinous rice; (b) 누룩가루에 물을 첨가하고 침출 및 여과시켜 누룩 여과액을 준비하는 단계;(b) adding water to the yeast powder, leaching and filtering to prepare a yeast filtrate; (c) 상기 (a) 단계에서 증자된 찹쌀과 상기 (b) 단계에서 준비된 누룩 여과액에 물을 첨가하고 당화 및 발효시켜 1단 담금의 술덧을 제조하는 단계;(c) adding water to the glutinous rice cooked in step (a) and the yeast filtrate prepared in step (b), saccharifying and fermenting to prepare a drunk of one step immersion; (d) 상기 제조된 1단 담금의 술덧에 후추, 계피, 생강, 잣, 대추, 침지, 증 자시킨 찹쌀, 액화제, 당화제 및 증류식 소주를 첨가하고 발효시켜 2단 담금의 술덧을 제조하는 단계; 및(d) To prepare the sourdough of the two-stage soaked by adding the fermented pepper, cinnamon, ginger, pine nuts, jujube, dipping, glutinous rice, liquefied, saccharifying agent and distilled shochu to the prepared soybean paste Doing; And (e) 상기 제조된 2단 담금의 술덧을 여과하고 물을 첨가하여 여과주의 알코올분을 규격화하는 단계.(e) standardizing the alcohol content of the filtered liquor by filtering the drunk of the prepared two-stage dip and adding water. 삭제delete 제2항에 있어서, 상기 당화 및 발효는 20~30℃에서 5~7일간 수행하는 것을 특징으로 하는 발효곡주의 제조방법.The method of claim 2, wherein the saccharification and fermentation is performed for 5 to 7 days at 20 ~ 30 ℃. 제2항에 있어서, 상기 액화제는 α-아밀라아제이고, 당화제는 β-아밀라아제인 것을 특징으로 하는 발효곡주의 제조방법.The method of claim 2, wherein the liquefaction agent is α-amylase, and the saccharifying agent is β-amylase.
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104087478A (en) * 2014-07-21 2014-10-08 安徽古井贡酒股份有限公司 Method for culturing bacterial solution used for inoculation of pit mud
KR101790414B1 (en) * 2015-11-19 2017-11-30 장정수 Method for Preparing of Vinegar Using Balsam Pear or Vinegar using Balsam Pear Prepared by the Method
KR101806812B1 (en) 2016-12-29 2017-12-08 재단법인 장흥군버섯산업연구원 Method for producing water-clear Makgeolli using shiitake, cinnamon, plum and ginger
CN114480053A (en) * 2022-03-02 2022-05-13 潘叶平 Brewing method of rice-flavor glutinous grain white spirit

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JP2003284541A (en) 2002-03-28 2003-10-07 Aomori Prefecture Method for producing alcoholic beverage, unrefined sake and alcoholic beverage
KR20040056205A (en) * 2002-12-23 2004-06-30 우희열 Manufacturing method of mild rice wine
KR20060082488A (en) * 2005-01-12 2006-07-18 최금조 Brew method of korea rice wine

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Publication number Priority date Publication date Assignee Title
JP2003284541A (en) 2002-03-28 2003-10-07 Aomori Prefecture Method for producing alcoholic beverage, unrefined sake and alcoholic beverage
KR20040056205A (en) * 2002-12-23 2004-06-30 우희열 Manufacturing method of mild rice wine
KR20060082488A (en) * 2005-01-12 2006-07-18 최금조 Brew method of korea rice wine

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104087478A (en) * 2014-07-21 2014-10-08 安徽古井贡酒股份有限公司 Method for culturing bacterial solution used for inoculation of pit mud
KR101790414B1 (en) * 2015-11-19 2017-11-30 장정수 Method for Preparing of Vinegar Using Balsam Pear or Vinegar using Balsam Pear Prepared by the Method
KR101806812B1 (en) 2016-12-29 2017-12-08 재단법인 장흥군버섯산업연구원 Method for producing water-clear Makgeolli using shiitake, cinnamon, plum and ginger
CN114480053A (en) * 2022-03-02 2022-05-13 潘叶平 Brewing method of rice-flavor glutinous grain white spirit

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