JP2006129821A - Rice wine containing rosa rugosa component and method for producing the same - Google Patents

Rice wine containing rosa rugosa component and method for producing the same Download PDF

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JP2006129821A
JP2006129821A JP2004324764A JP2004324764A JP2006129821A JP 2006129821 A JP2006129821 A JP 2006129821A JP 2004324764 A JP2004324764 A JP 2004324764A JP 2004324764 A JP2004324764 A JP 2004324764A JP 2006129821 A JP2006129821 A JP 2006129821A
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hermanus
liquor
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rice
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Fukutoki Ujita
福時 宇治田
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TAMANOHIKARI SHUZO KK
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TAMANOHIKARI SHUZO KK
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Abstract

<P>PROBLEM TO BE SOLVED: To obtain new rice wine containing a Rosa rugosa component, which makes the best use of extraction and aging effect so as to make the rice wine suitable for drinking, enhances the flavor of Rosa rugosa, is mellow and pleasant to the taste and to provide a method for producing the same. <P>SOLUTION: The rice wine containing a Rosa rugosa component, which has a component balance suitable for drinking and a flavor fit for preference and is mellow and pleasant to the taste is obtained by extracting Rosa rugosa in the presence of an alcohol-containing liquid, for example, distilled liquor such as gin, vodka, etc., or fermented liquor such as refined rice wine, wine, etc., and a rice saccharified liquid and aging the extracted liquid by an enzyme contained in Rosa rugosa and/or an added enzyme. <P>COPYRIGHT: (C)2006,JPO&NCIPI

Description

本発明は、ビタミンC及びビタミンA等生理的効果を有するハマナス成分が含有された酒類及びその製造方法に係り、特に香味に優れた健康酒としてのハマナス成分含有酒及びその製造方法に関する。   TECHNICAL FIELD The present invention relates to alcoholic beverages containing a hamanas component having a physiological effect such as vitamin C and vitamin A, and a method for producing the same, and more particularly, to a liquor-containing liquor as a health liquor with excellent flavor and a method for producing the same.

近年、家庭においてホームメイドの果実酒が作られるようになり、種々の果実を利用した果実酒が楽しまれている。これらの果実酒は、酒税法上リキュールに分類され、このリキュールは素材の種類によって、五つに分類される。すなわち、(1)薬草・ハーブ系、(2)種子系、(3)果実系、(4)果皮系、(5)クリーム系(糖分の多いクリーム状のもの)がある。また製法の面からは、(1)ベースの酒に素材を漬け込みエキスを抽出する浸漬法、(2)素材を酒に漬け、さらに蒸留して造る蒸留法、(3)素材のエッセンス(天然と人工の両者がある)を加えるエッセンス法の3類型がある〔秋本栄司、秋本由紀子、砂糖を使わない手作り果実酒・ハーブ・健康酒、14頁、雄鶏社、東京、1996年〕。   In recent years, home-made fruit wine has been made at home, and fruit wine using various fruits has been enjoyed. These fruit wines are classified as liqueurs under the Liquor Tax Law, and these liqueurs are classified into five types according to the type of material. That is, there are (1) medicinal herbs and herbs, (2) seeds, (3) fruits, (4) pericarps, and (5) creams (creams with a high sugar content). In terms of manufacturing methods, (1) a soaking method in which the material is soaked in base liquor and the extract is extracted, (2) a distillation method in which the material is soaked in sake and further distilled, and (3) the essence of the material (natural and natural) There are three types of essence methods that add both (artificial both) (Eiji Akimoto, Yukiko Akimoto, handmade fruit liquor / herb / health liquor without sugar, 14 pages, Rooster, Tokyo, 1996).

ホームメイドで作る果実酒は果実を焼酎又はアルコール(エチルアルコール)と水、時には砂糖を併用して常温で長時間抽出、数週間以上漬ける浸漬法が広く用いられており、その抽出液を飲用に供している。この方法ではアルコールや砂糖が防腐をしつつ抽出を行っている。果実には果実酒に多用されるものがあるが、これらの方法では、長時間抽出で果肉以外の種子成分の抽出成分が多くなり、香味のバランスの崩れが無視できない。良好な抽出と香味が得られず、果実酒原料として使用しにくいものもある。また、濃醇感や香味のバランスも調塾しても調和せず、飲用として必ずしも嗜好に適さない場合がある。   For home-made fruit sake, shochu or alcohol (ethyl alcohol) and water, sometimes with sugar, are extracted for a long time at room temperature, and soaked for several weeks or more. I am serving. In this method, alcohol and sugar are extracted while being preserved. Some fruits are often used in fruit sake, but in these methods, the extraction components of seed components other than the flesh increase by long-time extraction, and the balance of flavor cannot be ignored. There are some that cannot be used as a raw material for fruit sake, because good extraction and flavor cannot be obtained. In addition, the dark blue sensation and flavor balance are not harmonized even if they are prepared, and may not necessarily be suitable for drinking.

ハマナスの果実は熟すと甘酸っぱい味で、別名ハマナシとも呼ばれている。この果実はビタミンCやビタミンAも多く食用になる。このハマナスの果実酒の製品が望まれているが、従来の果実を焼酎又はアルコール(エチルアルコール)と水、時には砂糖を併用して常温で長時間抽出、数週間以上漬ける浸漬法では、熟成感と濃醇感を備えかつ目的にかなう健康酒は得られていない。   The fruit of Hermanus has a sweet and sour taste when ripened, also known as Hamanashi. This fruit is also edible with a lot of vitamin C and vitamin A. This hamanas fruit liquor product is desired, but the conventional fruit is extracted with shochu or alcohol (ethyl alcohol) and water, sometimes with sugar, at room temperature for a long time, soaked for more than a few weeks. There is no healthy liquor that has a dark blue feeling and meets its purpose.

本件出願に関する技術分野に関しては先行する特許文献は発見されていないが、果実を含めて植物エキスを抽出した酒類に関する特許文献としては下記記載のものがある。
特開平10−99069号 特開2002−171957号 上記特許文献のうち、特許文献1は果実の中に鳳仙花エキスを加えるものであり、特許文献2は果実ではなくアガリスク茸のエキスを抽出するものであり、何れも本願発明と目的を異にし、かつ当然のことながらその構成も異なるものである。
Although no prior patent documents have been found in the technical field related to the present application, patent documents relating to alcoholic beverages from which plant extracts including fruits have been extracted include those described below.
JP 10-99069 A Japanese Patent Laid-Open No. 2002-171957 Among the above-mentioned patent documents, Patent Document 1 is to add a bud flower extract to the fruit, and Patent Document 2 is to extract an extract of Agarisk bud instead of the fruit, both of which are the invention of the present application. The purpose is different, and of course, the configuration is also different.

本発明の目的は、ハマナス本来の香味成分を豊富に含有した酒で、ハマナス成分が米糖化液成分と混合調熟して、さらに飲用に適するよう抽出と調熟に工夫がなされ、熟成された新規なハマナス成分含有酒及びその製造方法を提供することにある。   The purpose of the present invention is a liquor rich in the original flavor components of Hermanus, the Hermanus component is mixed and ripened with the rice saccharified solution component, and further devised for extraction and ripening so that it is suitable for drinking Another object of the present invention is to provide a liquor containing a humanus component and a method for producing the same.

本発明者らは、前記従来技術の問題点を解決するために鋭意検討を重ねた結果、ハマナス成分、例えばハマナスの香味成分が豊富で、ハマナスの熟成感と濃醇感の両方を兼ね備え、口当たりの良いハマナス成分含有酒を開発するに至った。   As a result of intensive investigations to solve the problems of the prior art, the present inventors have abundant hermanus ingredients, for example, the flavor ingredient of hermanus, which has both the ripening and dark blue feeling of hermanus, Has led to the development of a good liquor-containing liquor.

本発明を概説すれば、本願発明における発明の第1は、抽出処理したハマナス成分及び米糖化液成分を含有することを特徴とするハマナス成分含有酒に関する。当該第1の発明において、抽出としてはアルコール及び米糖化液が例示される。本発明の第1の態様としては、アルコール7.0〜18.0%v/v、エキス分9.0〜25%w/v、フォルモール態窒素20〜50mgw/v、エキス分(%w/v)に対するフォルモール態窒素(mgw/v)の比率0.8〜5.0であるハマナス成分含有酒であり、抽出されたハマナスの香味がアルコールと米糖液の成分とで熟成し、ハマナスの香味を引き立たせた熟成感と濃醇感のあるハマナス成分含有酒である。   Briefly describing the present invention, the first of the inventions in the present invention relates to a liquor containing a humanus component, characterized in that it contains an extracted hermanus component and a rice saccharified solution component. In the first invention, alcohol and rice saccharified solution are exemplified as the extraction. As the first aspect of the present invention, alcohol 7.0 to 18.0% v / v, extract 9.0 to 25% w / v, formol nitrogen 20 to 50 mgw / v, extract (% w Is a liquor containing a Hamanus component in a ratio of formol nitrogen (mgw / v) to v / v) of 0.8 to 5.0, and the flavor of the extracted Hamanus is aged with alcohol and a component of rice sugar solution, It is a liquor containing a humana component with a ripening and dark blue feel that enhances the flavor of hermanus.

本願発明の第2の発明は、ハマナスをアルコール及び米糖化液存在下で40〜50℃でハマナスが含有する酵素及び/又は添加酵素により処理する工程を包含することを特徴とするハマナス成分含有酒の製造方法に関する。   A second invention of the present invention includes a step of treating hermanus with an enzyme and / or an additional enzyme contained in hermanus at 40 to 50 ° C. in the presence of alcohol and rice saccharified solution. It relates to the manufacturing method.

本願発明の第1〜5の発明において、原料となるハマナスは、別名ハマナシ(学名: Rosa rugosa Thunb.)、近縁種マイカイ(学名:Rosa maikai Hara.)及びこれらの自然交雑種や栽培種が挙げられる。これらをそれぞれ、単独又は組み合わせて併用して用いることができる。   In the first to fifth inventions of the present invention, as a raw material, the genus Hermanus is also known as Hamanashi (scientific name: Rosa rugosa Thunb.), Related species Maikai (scientific name: Rosa maikai Hara.) And their natural hybrids and cultivated species. Can be mentioned. These can be used alone or in combination.

本発明により、ハマナス本来の香味成分を豊富に含有し、熟成感と口当たりのよい濃醇な新規な酒質で、かつハマナス成分が飲用に適合するよう抽出が工夫されており、調塾効果によって口当たりのよいハマナス成分含有酒で従来にない良好なハマナス果実酒類を得ることができる。   According to the present invention, the natural flavor component of Hermanus is contained abundantly, and it has been devised so that it can be used for drinking with a mellow feeling and a rich, fresh and rich liquor, and the Hermanus component is suitable for drinking. It is possible to obtain an unprecedented good hermanus fruit liquor with a liquor-containing liquor-containing liquor.

また、本発明方法を実施することにより上記良質なハマナス成分含有酒を複雑な生産施設を設けることなく得ることが可能となる。   Moreover, by implementing the method of the present invention, it is possible to obtain the above-mentioned high-quality hermanus component-containing liquor without providing a complicated production facility.

抽出用の液としては、アルコール(エチルアルコール)を含有しているものであれば特に限定はなく、95%又は99%v/vアルコールを適宜使用に適する所定のアルコール濃度に設定する。使用対象の酒類としては、例えば蒸留酒である甲類焼酎、果実用焼酎、本格焼酎、ウィスキー、ジン、ウオッカ、ブランディー、ラム、白酒(パイチュウ)等、醸造酒である清酒、ワイン、老酒、みりん、赤酒、濁酒及びそれらのモロミ等を用いる。   The extraction liquid is not particularly limited as long as it contains alcohol (ethyl alcohol), and 95% or 99% v / v alcohol is appropriately set to a predetermined alcohol concentration suitable for use. Examples of alcoholic beverages to be used include distilled spirits such as shellfish shochu, fruit shochu, authentic shochu, whiskey, gin, vodka, brandy, rum, white sake (paichu), etc., sake brewed sake, wine, old sake, Use mirin, red liquor, muddy liquor and their moromi.

以下本発明を具体的に説明し、後述の実施例に及ぶ。
本発明により、ハマナス成分、例えば香味成分が豊富で、ハマナス成分の香味と米糖化液成分がバランスよく熟成され、香味の熟成感と濃醇感の両方を兼ね備えた新規ハマナス成分含有酒が提供される。
Hereinafter, the present invention will be described in detail, and will be described in the following examples.
According to the present invention, there is provided a novel hermanus component-containing liquor that is rich in hermanus components, for example, flavor components, is matured in a well-balanced manner with the flavor of the hermanus component and the rice saccharified solution component, and has both a sense of ripening and a dark sensation of flavor. The

上記における、香味の熟成感と濃醇感の両方を兼ね備えたとは、ハマナス果実の抽出時に、果肉からの成分と種子成分の抽出も平行して行われる。そこで、果実の持つ特性を生かし、果肉及び種子からの成分がバランス良いものとなし、なおかつ米糖化液の成分とアルコール存在下で抽出したハマナスの香味を適切な温度で熟成し、味馴れを達成し、さらに調塾効果でハマナスの香味を引き立たせ、濃醇感のある口当たりのよい酒質に変化させ、嗜好性の高いハマナス成分含有酒にすることを意味する。   In the above, having both the ripening feeling of the flavor and the feeling of dark blue means that the extraction of the component from the flesh and the seed component are also performed in parallel with the extraction of the Hermanus fruit. Therefore, taking advantage of the characteristics of the fruit, the ingredients from the pulp and seeds are balanced, and the flavor of the rice saccharified solution and the scented hamanas extracted in the presence of alcohol are aged at an appropriate temperature to achieve a familiar taste. Furthermore, it means to enhance the flavor of hamanas through the training effect, to change the liquor quality with a rich taste and to make it a highly liquor-containing liquor-containing liquor.

本発明でのハマナスの使用にあっては、少なくともハマナスの果実を用い、花、花弁、根は併用しなくてもよい。これらハマナスの果実、花、花弁、根は生及び/又はそれぞれの加工品を使用してもよい。また、これらのハマナスの果実、花、花弁、根の形状は特に限定はなく、例えばそのまま、細断状、ピューレ状、ペースト状、及び粉末状であってもよい。   In the use of Hermanus in the present invention, at least the fruit of Hermanus is used, and the flowers, petals and roots may not be used in combination. The fruit, flowers, petals and roots of these genus may be used raw and / or processed products thereof. Further, the shape of the fruits, flowers, petals, and roots of these genus are not particularly limited, and may be, for example, chopped, pureed, pasty, and powdered as they are.

本発明において、ハマナスとして生ハマナスまたは加工ハマナスの加工品を例示したが、加工されたハマナスであれば特に限定はないが、加工の処理方法として加熱処理、冷凍処理、電磁処理、放射熱処理、超音波処理、乾燥処理、酵素処理等が挙げられる。加熱処理としては、例えば煮る、蒸す、焼く、炒める、揚げる等が例示される。冷凍処理としては、例えば凍結等があげられる。電磁処理としては、例えはマイクロウエェーブ照射等が挙げられる。放射熱処理としては、例えば近赤外線、遠赤外線処理等が挙げられる。乾燥処理としては、例えば風乾、温風乾燥、凍結乾燥等が挙げられる。酵素処理としては、例えばアミラーゼ、イソメラーゼ、トランスグルコシダーゼ、プロテアーゼ、カルボキシペプチダーゼ、セルラーゼ、ヘミセルラーゼ、リパーゼ、エステラーゼ、及びペクチナーゼからなる群より選ばれた少なくとも一つ以上の酵素による処理等が例示される。また、ハマナスを自然放置することでハマナス自身が含有する酵素により追塾されたハマナスも本発明の加工ハマナスに包含される。これらの処理は目的に応じて組み合わせてもよい。加工ハマナスの形状は特に限定はなく、例えばそのまま、細断状、ピューレ状、ペースト状、及び粉末状であってもよい。また、処理後固液分離をした液部分及び/または固体部分であってもよく、そのまま、濃縮、希釈されたものであってもよい。   In the present invention, raw herbs or processed products of processed herbs are exemplified as hermanus, but there is no particular limitation as long as it is processed hermanus, but the processing method of heat treatment, freezing treatment, electromagnetic treatment, radiant heat treatment, super Examples include sonication, drying, and enzyme treatment. Examples of the heat treatment include boiling, steaming, baking, frying, frying and the like. An example of the freezing process is freezing. Examples of electromagnetic treatment include microwave irradiation. Examples of the radiant heat treatment include near infrared and far infrared treatment. Examples of the drying process include air drying, warm air drying, and freeze drying. Examples of the enzyme treatment include treatment with at least one enzyme selected from the group consisting of amylase, isomerase, transglucosidase, protease, carboxypeptidase, cellulase, hemicellulase, lipase, esterase, and pectinase. Further, the processed humanus of the present invention also includes a hermanus supplemented by an enzyme contained in the hermanus itself by leaving it naturally. These processes may be combined according to the purpose. There is no particular limitation on the shape of the processed humanus, and it may be, for example, a chopped shape, a puree shape, a paste shape, or a powder shape. Further, it may be a liquid part and / or a solid part subjected to solid-liquid separation after treatment, or may be concentrated and diluted as it is.

本発明における抽出用の液としては、アルコールを含有しているものであれば特に限定はなく、95%又は99%v/vアルコールを、適宜使用に適する所定のアルコール濃度に設定できる。なお、ここでいうアルコールとはエチルアルコールのことをいう。酒類使用としては、例えば蒸留酒である甲類焼酎、果実用焼酎、本格焼酎、ウィスキー、ジン、ウオッカ、ブランディー、ラム、白酒(パイチュウ)等、醸造酒である清酒、ワイン、老酒、みりん、赤酒、濁酒及びそれらのモロミ等が挙げられる。   The extraction liquid in the present invention is not particularly limited as long as it contains alcohol, and 95% or 99% v / v alcohol can be appropriately set to a predetermined alcohol concentration suitable for use. In addition, alcohol here means ethyl alcohol. Examples of the use of liquor include distilled spirits such as shell shochu, fruit shochu, authentic shochu, whiskey, gin, vodka, brandy, rum, white liquor (paichu), brewed sake, wine, old sake, mirin, Examples include red sake, muddy sake, and their moromi.

本発明の抽出及び調塾用の液は、米を糖化した液であれば、特に限定はなく、ここでいう糖化は液化及び/又は糖化のことをいう。用いる米は搗精の有無、形状に限定はなく、粒状、粉状、造粒物のいずれであってもよい。米の糖化は、米麹及び/又は酵素で処理して得られる。酵素処理の酵素は、例えばアミラーゼ、イソメラーゼ、トランスグルコシダーゼ、プロテアーゼ、カルボキシペプチダーゼ、セルラーゼ、ヘミセルラーゼ、リパーゼ、エステラーゼ、及びペクチナーゼからなる群より選ばれた少なくとも一つ以上の酵素を用いることができる。これらの酵素は非耐熱性又は耐熱性酵素であってもよい。   The extraction and preparation liquid of the present invention is not particularly limited as long as it is a liquid obtained by saccharification of rice, and saccharification here refers to liquefaction and / or saccharification. The rice to be used is not limited in the presence or absence and shape of semen and may be granular, powdery or granulated. Rice saccharification is obtained by treating with rice bran and / or enzymes. As the enzyme for the enzyme treatment, for example, at least one enzyme selected from the group consisting of amylase, isomerase, transglucosidase, protease, carboxypeptidase, cellulase, hemicellulase, lipase, esterase, and pectinase can be used. These enzymes may be non-thermostable or thermostable enzymes.

米は糊化する工程と糖化処理する工程をそれぞれ単独、同時平行して行ってもよい。酵素添加量は糖化液全容量に対して、0.0005〜5.0%w/vで、好ましくは0.00.1〜2.0%w/vである。米麹使用量は米麹用の米及び掛け原料用の米の重量に対する米麹用の米の重量の比率が0〜100%の範囲で設定できる。   For rice, the step of gelatinization and the step of saccharification treatment may be carried out independently or simultaneously in parallel. The amount of enzyme added is 0.0005 to 5.0% w / v, preferably 0.00.1 to 2.0% w / v, based on the total volume of the saccharified solution. The amount of rice bran used can be set such that the ratio of the weight of rice for rice bran to the weight of rice for rice bran and rice for hanging raw material is in the range of 0 to 100%.

米麹を用いる糖化処理の場合は5〜50%、好ましくは10〜30%である。固液比は糖化液全体の重量に対しての使用米重量が2〜70%、好ましくは5〜60%である。温度条件と処理時間は米は糊化する工程及び/又は米を糖化する工程の最適温度と処理時間を適宜設定すればよく、例えば米は、糊化する工程は50〜120℃、好ましくは60〜100℃で、処理時間は5分〜24時間、好ましくは10分〜10時間、さらに好ましくは、作業の操作上から1〜7時間である。米を糖化する工程は30〜120℃、好ましくは35〜100℃で、処理時間は5分〜100時間、好ましくは1時間〜96時間である。米糖化液は米糖化物及び/又は固液分離した液部分を用いる。   In the case of saccharification treatment using rice bran, it is 5 to 50%, preferably 10 to 30%. The solid-liquid ratio is such that the weight of rice used relative to the total weight of the saccharified solution is 2 to 70%, preferably 5 to 60%. What is necessary is just to set suitably the optimal temperature and the processing time of the process which gelatinizes a rice, and / or the process of saccharifying rice, and the temperature conditions and processing time, for example, the process of gelatinizing 50-120 degreeC, Preferably 60 is preferable. At -100 ° C, the treatment time is 5 minutes to 24 hours, preferably 10 minutes to 10 hours, and more preferably 1 to 7 hours from the viewpoint of operation. The step of saccharifying rice is 30 to 120 ° C, preferably 35 to 100 ° C, and the treatment time is 5 minutes to 100 hours, preferably 1 hour to 96 hours. As the rice saccharified solution, a saccharified rice product and / or a solid-liquid separated liquid part is used.

抽出方法は特に限定はないが、ハマナスのアルコール及び米糖化液に対する比率は、重量比で5〜60%、好ましくは10〜50%である。さらに抽出操作上からは15〜45%である。ハマナスの成分、例えば香味成分が引き立ち、米糖化液の成分とのバランスと調熟により、濃醇でハマナスの香味が生かされたハマナスの熟成感の両方を兼ね備えた特性を満足するには、漬け込み温度として、例えば、漬け込みによる抽出では0〜60℃、好適には40〜50℃、さらには最適で42〜48℃であり、抽出時間は1〜15日、好ましくは2〜10日であり、ハマナスを抽出後取り出して抽出液を上記抽出温度の範囲で熟成させてもよい。   Although there is no particular limitation on the extraction method, the ratio of Hermanus to alcohol and rice saccharified solution is 5 to 60% by weight, preferably 10 to 50%. Furthermore, it is 15 to 45% in terms of extraction operation. In order to satisfy the characteristics of both the ripening of Hermanus, which is rich in herbs, the flavor of Hermanus is enhanced by balance and ripening with the ingredients of Hermanus, for example, flavor components, and rice saccharified liquid. The temperature is, for example, 0 to 60 ° C., preferably 40 to 50 ° C., more preferably 42 to 48 ° C. in extraction by soaking, and the extraction time is 1 to 15 days, preferably 2 to 10 days. Hermanus may be extracted after extraction and the extract may be aged within the above extraction temperature range.

この時、酵素、例えば滓成分の除去のためペクチナーゼ及び香り成分増強のためエステラーゼ等を作用させてもよい。生ハマナスを用いる場合、2回以上の浸漬法を用いてもよい。すなわち、ハマナスをアルコール及び米糖化液存在下で漬け込み抽出、固液分離後、残ったハマナスはアルコール及び米糖化液へ再度漬け込み再抽出する。この操作を繰り返して1〜5回、香味の上からは1〜3回繰り返す。それぞれ目的にかなう酒質の抽出液が得られるが、品質の安定化を求めるには、再抽出液をブレンドして調合することができる。これによって、ハマナスの果肉部分の抽出成分を主体とし、かつ種子成分の香味の抽出が軽減され、穏和で上品なハマナス成分含有が得られる。   At this time, an enzyme, for example, a pectinase for removing the wrinkle component and an esterase for enhancing the scent component may be allowed to act. When using raw chanus, two or more dipping methods may be used. In other words, after extraction and solid-liquid separation in the presence of alcohol and rice saccharified solution, the remaining genus is again immersed in alcohol and rice saccharified solution and re-extracted. This operation is repeated 1 to 5 times, and 1 to 3 times from the top of the flavor. Extracts of liquor quality can be obtained for each purpose, but re-extracted liquids can be blended and formulated in order to seek stabilization of quality. As a result, extraction of the flavor component of the seed component is reduced, and a mild and elegant herb component is obtained.

生ハマナスの持つ酵素類や添加酵素は、抽出時のアルコール及び米糖化液存在下でハマナス及びアルコールや米糖化液に作用し、例えばペクチナーゼ等によりペクチン及び低分化ペクチンを生成し、またエステラーゼはハマナスにより生成された成分とアルコールが反応してエステル類を生成し、香気成分を生成する。またハマナスに含まれる酸化酵素はアルコールによる反応阻害を受けて抑制される。すなわち、本発明によりハマナスをアルコール及び米糖化液存在下でハマナスが含有する酵素及び/又は添加酵素により処理することを特徴とするハマナス成分含有酒が提供される。   Enzymes and additive enzymes possessed by raw genus act on genus and alcohol and rice saccharified solution in the presence of alcohol and rice saccharified solution at the time of extraction, for example, produce pectin and poorly differentiated pectin by pectinase, etc. The component produced by the above and the alcohol react to produce an ester and produce an aroma component. Moreover, the oxidase contained in Hermanus is inhibited by reaction inhibition by alcohol. That is, according to the present invention, there is provided a liquor-containing liquor characterized by treating hermanus with an enzyme and / or an additional enzyme contained in hermanus in the presence of alcohol and a rice saccharified solution.

本発明において、生ハマナスが含有する酵素としては、アルコール及び米糖化液存在下の浸漬で作用するハマナス及び米糖化液に由来する酵素であれば特に限定はないが、例えばアミラーゼ、プロテアーゼ、カルボキシペプチダーゼ、セルラーゼ、ヘミセルラーゼ、リパーゼ、エステラーゼ、及びペクチナーゼからなる群より選ばれた少なくとも一つ以上の酵素が例示される。   In the present invention, the enzyme contained in the raw genus is not particularly limited as long as it is an enzyme derived from the genus Hermanus and rice saccharified solution acting in the presence of alcohol and rice saccharified solution. For example, amylase, protease, carboxypeptidase And at least one enzyme selected from the group consisting of cellulase, hemicellulase, lipase, esterase, and pectinase.

また、添加酵素としては、香味成分を生成および、高分子成分を低分子化する酵素であれば特に限定はなく、動植物及び微生物の起源を問わず、例えば、アミラーゼ、イソメラーゼ、トランスグルコシダーゼ、プロテアーゼ、カルボキシペプチダーゼ、セルラーゼ、ヘミセルラーゼ、リパーゼ、エステラーゼ、及びペクチナーゼからなる群より選ばれた少なくとも一つ以上の酵素を用いることができる。   In addition, the additive enzyme is not particularly limited as long as it is an enzyme that generates a flavor component and lowers the molecular component, and regardless of the origin of animals, plants, and microorganisms, for example, amylase, isomerase, transglucosidase, protease, At least one enzyme selected from the group consisting of carboxypeptidase, cellulase, hemicellulase, lipase, esterase, and pectinase can be used.

添加酵素の添加量としては、特に限定はないが、例えば添加量は抽出時の全容量に対して0.0005〜5.0%w/vであり、0.001〜2.0%w/vである。
またハマナスが合有する酵素及び/又は添加酵素の反応時間としては、特に限定はないが、反応時間としては、例えば、漬け込みによる抽出では0〜60℃、好適には40〜50℃、さらには最適で42〜48℃であり、抽出時間は1〜15日、好ましくは2〜10日であり、ハマナスを抽出後取り出して抽出液を上記抽出温度の範囲で熟成させてもよい。
The addition amount of the added enzyme is not particularly limited. For example, the addition amount is 0.0005 to 5.0% w / v with respect to the total volume during extraction, and 0.001 to 2.0% w / v. v.
In addition, the reaction time of the enzyme and / or the added enzyme that is included in Hermanus is not particularly limited, but the reaction time is, for example, 0 to 60 ° C., preferably 40 to 50 ° C., more preferably optimal for extraction by soaking. The extraction time may be 1 to 15 days, preferably 2 to 10 days, and the extract may be aged in the range of the above extraction temperature by taking out the hermanus after extraction.

またここで使用するハマナスとしては生ハマナスでも加工ハマナスである加工品でもよい。生ハマナスに比べて含水量の少ない加工ハマナスを用いる場合、ハマナス成分が濃厚になるとこれらの酵素による反応量も多くなり、ハマナスの熟成感を生かし、更に濃醇感が強調された、濃厚なハマナス成分含有酒が得られる。   Further, as the Hermanus used here, it may be a raw Hermanus or a processed product that is a processed Hermanus. When using processed Hermanus, which has a lower water content than raw Hermanus, the amount of the reaction caused by these enzymes increases when the Hermanus component is concentrated, making use of the ripening feeling of Hermanus, and the rich Hermanus that emphasizes the feeling of darkness. An ingredient-containing liquor is obtained.

本発明において、ハマナス成分含有酒は濃縮することができる。濃縮方法は特に限定はないが、例えば、凍結濃縮や減圧濃縮が挙げられる。また、ハマナス抽出液へさらにハマナスを入れ、抽出・調熟を繰り返してもよい。抽出・濃縮された液中のアルコール濃度は防腐や品質保持の面から18.0〜45.0%v/vがよく、得られた抽出・濃縮されたハマナス成分含有酒は、そのまま飲用に利用できるが、リキュールとしてカクテルや低アルコール飲料等に混合して利用できる。   In the present invention, the liquor-containing liquor can be concentrated. The concentration method is not particularly limited, and examples thereof include freeze concentration and vacuum concentration. Further, it is also possible to repeat the extraction and ripening by adding the genus to the genus extract. The alcohol concentration in the extracted and concentrated liquid is preferably 18.0 to 45.0% v / v from the standpoint of preserving and maintaining the quality, and the extracted and concentrated liquor containing the humanus component is used for drinking as it is. Yes, it can be used as a liqueur mixed with cocktails or low alcohol beverages.

以下、実施例を示すことにより本発明をより具体的に示す。なお、本発明はもとよりこれらの実施例に限定されるものではない。   Hereinafter, the present invention will be described more specifically by showing examples. The present invention is not limited to these examples.

米粉末(3000g)、井水(3000g)及び市販のアミラーゼ(1.6g)及びプロテアーゼ(1.6g)を混合し、50〜60℃で5時間、液化・糖化した。その後100℃まで昇温し、20分保った。その後、55℃まで品温を降下させ、米麹(900g)を添加して3日間糖化した。得られた糖化物(6900g)を試験室の圧搾機で固液分離をし、搾汁(6400ml、7550g)を得た。搾汁はエキス分76.7%w/v、全糖68%w/v、フォルモール態窒素171mgN%w/vであった。これを米糖化液とした。これにフォルモール態窒素の影響を検討するため、全糖68%w/vとなるよう水分30%の分解度が85%になるよう調製した含窒素成分を含まない精製水飴、アミノ酸液及び蒸留水でフォルモール態窒素濃度が(1)15、(2)35、(3)69、(4)100、(5)171、(6)200、(7)300、(8)400、(9)500(何れもmg%w/v)になるよう調製したモデル米糖化液をそれぞれ、640ml調製した。それぞれのフォルモール態窒素濃度に調製したモデル米糖化液(640ml)に本格米焼酎アルコール40%v/v(405ml)及びハマナス果実383gを混合し、45℃で4日間抽出、調塾し、その後井水(334ml)添加して、濾紙濾過してハマナス含有酒を得て官能評価を行った。   Rice powder (3000 g), well water (3000 g), and commercially available amylase (1.6 g) and protease (1.6 g) were mixed and liquefied and saccharified for 5 hours at 50-60 ° C. Thereafter, the temperature was raised to 100 ° C. and kept for 20 minutes. Thereafter, the product temperature was lowered to 55 ° C., and rice bran (900 g) was added for saccharification for 3 days. The obtained saccharified product (6900 g) was subjected to solid-liquid separation using a laboratory press to obtain juice (6400 ml, 7550 g). The juice contained 76.7% w / v extract, 68% w / v total sugar, and 171 mg N% w / v formol nitrogen. This was used as a rice saccharified solution. In order to investigate the effect of formol-type nitrogen on this, purified syrup, amino acid solution and distillation not containing nitrogen-containing components prepared so that the decomposition degree of water 30% is 85% so that the total sugar is 68% w / v The formol-type nitrogen concentration in water is (1) 15, (2) 35, (3) 69, (4) 100, (5) 171, (6) 200, (7) 300, (8) 400, (9 ) Each model rice saccharified solution prepared to 500 (mg% w / v) was prepared. Authentic rice shochu alcohol 40% v / v (405 ml) and 383 grams of hamanas fruit are mixed with model rice saccharified solution (640 ml) adjusted to each formol nitrogen concentration, extracted at 45 ° C for 4 days, and then prepared. Well water (334 ml) was added, and filter paper filtration was performed to obtain a liquor-containing liquor, and sensory evaluation was performed.

得られた実験区(1)〜(9)の一般分析値と官能評価(パネルメンバー5名、5段階評価で5が最良、1が最悪として評価)として合計点を得た。以下の表1はこの結果を示す。   The total points were obtained as general analysis values and sensory evaluations of the obtained experimental sections (1) to (9) (5 panel members, 5 being the best, 5 being the best, and 1 being the worst). Table 1 below shows the results.

Figure 2006129821
Figure 2006129821

表1よりエキス分に対するフォルモール態窒素の比率と官能評価の結果、実験区(2)〜(8)までは香り、味及び総合で20点以上が得られられ、ハマナスの香味が引き立ち熟成感と濃醇感があり、口当たりがよいという感想であった。実験区(1)は濃醇感に乏しく味のバランスが崩れていた。実験区(9)は濃醇感が強く味バランス的にもやや劣る傾向にあった。
従って、エキス分に対するフォルモール態窒素の比率は0.4〜5.0が好ましい。
As a result of sensory evaluation, the ratio of formol-type nitrogen to the extract content from Table 1, more than 20 points were obtained in the experimental sections (2) to (8), and the fragrance of Hermanus stands out and matured. There was a feeling of dark blue and the impression that it was palatable. The experimental plot (1) had a poor dark blue feel and the balance of taste was lost. The experimental group (9) had a strong dark blue sensation and a slightly poor taste balance.
Therefore, the ratio of formol nitrogen to the extract is preferably 0.4 to 5.0.

実施例1と同様にして米糖化液を調製した。本格米焼酎アルコール40%v/vと、最終の添加井水の量を調節して、量を調製して2種類のハマナス成分含有酒を調製した。試作(1)はアルコール18.0%v/v、エキス分25.0%w/v、ブドウ糖18.0%w/v、フォルモール態窒素50.4mg%w/v、pH4.4、エキス分(%w/v)に対するフォルモール態窒素(mg%w/v)の比率2.02である。
試作(2)はアルコール7.0%v/v、エキス分9.0%w/v、ブドウ糖5.0%w/v、フォルモール態窒素20.4mg%w/v、pH3.7、エキス分(%w/v)に対するフォルモール態窒素(mgN%w/v)の比率2.27である。これらを調合して種々成分のハマナス成分含有酒を調製し、容量で試作(1)が100%単独、試作(1)が75%と試作(2)が25%の混合、試作(1)が50%と試作(2)が50%の混合、試作(1)が25%と試作(2)が75%の混合の区分をそれぞれ分析し、官能評価を実施例1と同様にして行った。その結果を表2に示す。
A rice saccharified solution was prepared in the same manner as in Example 1. Authentic rice shochu alcohol 40% v / v and the amount of final added well water were adjusted to prepare the amount of two kinds of hamanas component-containing sake. Prototype (1): alcohol 18.0% v / v, extract 25.0% w / v, glucose 18.0% w / v, formol nitrogen 50.4 mg% w / v, pH 4.4, extract The ratio of formol nitrogen (mg% w / v) to minutes (% w / v) is 2.02.
Prototype (2): alcohol 7.0% v / v, extract 9.0% w / v, glucose 5.0% w / v, formol nitrogen 20.4 mg% w / v, pH 3.7, extract The ratio of formol nitrogen (mgN% w / v) to minutes (% w / v) is 2.27. These are prepared to prepare various kinds of liquor-containing liquor, and by volume, the prototype (1) is 100% alone, the prototype (1) is 75%, the prototype (2) is 25%, and the prototype (1) is 50% and 50% of the prototype (2) were mixed, and 25% of the prototype (1) and 75% of the prototype (2) were analyzed, and sensory evaluation was performed in the same manner as in Example 1. The results are shown in Table 2.

Figure 2006129821
Figure 2006129821

表2より、総合で20点以上を示した範囲は試作(1)の100%〜試作(2)の100%であり、ハマナスの香味が引き立ち熟成感と濃醇感があり、口当たりがよいという感想であった。従って、アルコール7.0〜18.0%v/v、エキス分9.0〜25%w/v、フォルモール態窒素20〜50mg%w/v、が目的とする酒質を得る成分範囲であり、更に細かくは、アルコール7.0〜18.0%v/v、エキス分9.0〜25%w/v、ブドウ糖5.0〜18.0w/v、フォルモール態窒素20〜50mg%w/v、pH3.6〜4.4が糖質成分の特定と濃度並びに酸度すなわちpH規定した酒質の成分範囲となる。   From Table 2, the total range of 20 points or more is 100% of the trial production (1) to 100% of the trial production (2), and the flavor of Hermanus is accentuated with a sense of maturity and darkness, and is palatable. It was an impression. Therefore, alcohol 7.0-18.0% v / v, extract 9.0-25% w / v, formol nitrogen 20-50mg% w / v in the component range to obtain the desired liquor quality Yes, more specifically, alcohol 7.0-18.0% v / v, extract 9.0-25% w / v, glucose 5.0-18.0 w / v, formol nitrogen 20-50 mg% w / v, pH 3.6 to 4.4 is the component range of the liquor that specifies the concentration and the acidity, that is, the pH, of the sugar component.

実施例1の製造と同様の配合とフローでハマナス成分含有酒を調製する工程で、一方はペクチナーゼを抽出液中に液汁重量当たり0.01%添加して抽出した。対照は無添加で行った。得られた抽出液を濾紙濾過した濾過液をそれぞれ分析及び官能評価をした。一般的な分析値は同様であったが、肉眼による官能評価では外観で、ペクチナーゼ処理した抽出液の照り、つやが対照に比べて優れており、食感では舌触りが良好との評価であった。   In the process of preparing the liquor containing the humanus component with the same composition and flow as in the production of Example 1, 0.01% of pectinase was added to the extract and extracted. The control was performed without addition. The filtrate obtained by filtering the obtained extract with filter paper was analyzed and sensory evaluated. General analysis values were the same, but the sensory evaluation by the naked eye was the appearance, the shine and gloss of the pectinase-treated extract was superior to the control, and the texture was evaluated to be good to the touch .

以上詳述したように、本発明で提供されるハマナス成分及び米糖化液成分を含有するハマナス成分含有酒はアルコール及び米糖化液存在下で、ハマナスが含有する酵素及び/又は添加酵素により処理したハマナス成分を含有することを特徴とするハマナス成分含有酒であり、抽出されたハマナスの香味がアルコールと米糖化液の成分とで調熟し、ハマナスの香味を引き立たせた熟成感と濃醇感があり、口当たりのよい酒質のハマナス成分含有酒となる。また、本発明において、工場生産に適した製造法も提供することができる。   As described above in detail, the hermanus component-containing liquor containing the hermanus component and the rice saccharified solution component provided in the present invention was treated with the enzyme and / or additive enzyme contained in the hermanus in the presence of alcohol and rice saccharified solution. It is a liquor containing a hermanus component, characterized by containing a hermanus component, and the flavor of the extracted hermanus is ripened with the components of alcohol and rice saccharified liquid, and the aging and darkness that enhances the flavor of hermanus Yes, it is a liquor-containing liquor-containing liquor-containing Hamanasu component. In the present invention, a manufacturing method suitable for factory production can also be provided.

本発明は、ハマナス本来の香味成分を豊富に含有し、熟成感と口当たりのよい濃醇な新規な酒質の嗜好性の高い飲用物として利用できるのは当然であるが、ハマナスの薬効等が確認できれば医薬品或いは医薬部外品として、医薬品産業による製品の生産販売の可能性も十分あるものである。   Naturally, the present invention contains abundant flavor components of Hermanus, and it can be used as a highly drinkable drink with a rich and fresh taste that is rich in taste and mouthfeel. If it can be confirmed, there is a possibility of production and sales of the product by the pharmaceutical industry as a medicine or quasi-drug.

Claims (5)

抽出処理したハマナス成分及び米糖化液成分を含有することを特徴とするハマナス成分含有酒。 A hermanus component-containing liquor comprising an extracted hermanus component and a rice saccharified solution component. アルコール 7.0〜18.0%v/v、エキス分 9.0〜25%w/v、フォルモール態窒素 20〜50mg%w/v、エキス分(%w/v)に対するフォルモール態窒素 mg%(w/v)の比率 0.8〜5.0であることを特徴とする請求項1記載のハマナス成分含有酒。 Alcohol 7.0 to 18.0% v / v, extract 9.0 to 25% w / v, formol nitrogen 20 to 50 mg% w / v, formol nitrogen to extract (% w / v) The ratio of mg% (w / v) is 0.8 to 5.0, and the liquor component-containing liquor according to claim 1. ハマナスをアルコール及び米糖化液存在下でハマナスが含有する窒素及び/又は添加酵素により処理したハマナス成分を含有することを特徴とする請求項1又は2記載のハマナス成分含有酒。 3. A hermanus component-containing liquor according to claim 1 or 2, characterized by containing a hermanus component obtained by treating hermanus with nitrogen and / or an additional enzyme contained in hermanus in the presence of alcohol and rice saccharified solution. 抽出されたハマナスの香味がアルコールと米糖液の成分とで調熟し、ハマナスの香味を引き立たせた熟成感と濃醇感の請求項1乃至3の何れかに記載のハマナス成分含有酒。 4. The hermanus component-containing liquor according to any one of claims 1 to 3, wherein the extracted flavor of Hermanus is ripened with alcohol and a component of rice sugar solution, and has a ripening and dark blue feel that enhances the flavor of Hermanus. ハマナスをアルコール及び米糖化液存在下で40〜50℃でハマナスが含有する酵素及び/又は添加酵素により処理する工程を含有することを特徴とするハマナス成分含有酒の製造方法。 A method for producing a liquor containing a humanus component, comprising a step of treating hermanus with an enzyme and / or an additional enzyme contained in the red pepper at 40 to 50 ° C. in the presence of alcohol and a rice saccharified solution.
JP2004324764A 2004-11-09 2004-11-09 Rice wine containing rosa rugosa component and method for producing the same Pending JP2006129821A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007167030A (en) * 2005-12-26 2007-07-05 Hinomaru Jozo Kk Method for producing fruit liqueur
CN103497869A (en) * 2013-10-18 2014-01-08 重庆市万州区食品工业研究所 Red-heart kiwi fruit wine and preparation method thereof
CN103497865A (en) * 2013-09-30 2014-01-08 宾婧羽 Rosa laevigata wine brewing method
CN104830588A (en) * 2015-06-03 2015-08-12 劲牌有限公司 Red wine with anti-oxidation, bowel relaxing and immunity enhancing functions and method for making red wine
CN104830617A (en) * 2015-05-13 2015-08-12 杨子明 Method for producing watermelon red wine
JP2018082643A (en) * 2016-11-22 2018-05-31 群栄化学工業株式会社 Alcoholic beverage
CN112877161A (en) * 2021-03-02 2021-06-01 广西横县创志酒业有限公司 Method for producing jasmine flower wine by compounding glutinous rice yellow wine and distilled liquor

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007167030A (en) * 2005-12-26 2007-07-05 Hinomaru Jozo Kk Method for producing fruit liqueur
CN103497865A (en) * 2013-09-30 2014-01-08 宾婧羽 Rosa laevigata wine brewing method
CN103497869A (en) * 2013-10-18 2014-01-08 重庆市万州区食品工业研究所 Red-heart kiwi fruit wine and preparation method thereof
CN104830617A (en) * 2015-05-13 2015-08-12 杨子明 Method for producing watermelon red wine
CN104830588A (en) * 2015-06-03 2015-08-12 劲牌有限公司 Red wine with anti-oxidation, bowel relaxing and immunity enhancing functions and method for making red wine
JP2018082643A (en) * 2016-11-22 2018-05-31 群栄化学工業株式会社 Alcoholic beverage
CN112877161A (en) * 2021-03-02 2021-06-01 广西横县创志酒业有限公司 Method for producing jasmine flower wine by compounding glutinous rice yellow wine and distilled liquor

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