KR100720812B1 - A composite of bio-inorganic coating material with antibiosis and anti-mold and deodorization property as a cement product's surface finishing material - Google Patents
A composite of bio-inorganic coating material with antibiosis and anti-mold and deodorization property as a cement product's surface finishing material Download PDFInfo
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Abstract
본 발명은 탈취 기능과 항균, 항곰팡이 특성이 우수한 대나무 추출액에 윤활성 세라믹 재료와 흡착 기능에 의한 악취 제거용 세라믹 광물 등으로 구성된 액상형 바이오 무기질 코팅재 조성물에 관한 것으로The present invention relates to a liquid bio-inorganic coating composition composed of a lubricating ceramic material and a ceramic mineral for removing odor by adsorption function in a bamboo extract having excellent deodorizing function and antibacterial and antifungal properties.
본 발명에 의한 코팅재는 대나무 추출액을 사용하여 곰팡이 서식 및 곰팡이 발생을 억제하고, 이미 발생한 곰팡이 등의 세균을 소독하는 항균기능을 부여하고, 바름재 구성재료 중의 유기물에서 발생하는 인체에 유해한 성분을 분해함으로서 최적의 청정 환경을 위한 식물성 추출물을 이용한 시멘트 제품의 표면 마감용 바이오 무기질 코팅재에 관한 것이다.The coating material according to the present invention uses a bamboo extract to inhibit mold incubation and mold development, impart antimicrobial function to disinfect bacteria such as mold, and decompose harmful components to human body generated from organic matter in the material of the coating material. The present invention relates to a bio-inorganic coating material for surface finishing of cement products using vegetable extracts for an optimal clean environment.
대나무 추출액, 항균, 항곰팡이, 탈취, 세라믹, Bamboo extract, antibacterial, antifungal, deodorant, ceramic,
Description
본 발명은 건축물에 사용되는 여러 가지 시멘트계 재료의 표면 마감용 바이오 무기질 코팅재에 관한 것이다. 보다 상세하게는 시멘트 패널, 시멘트 보드, 석고보드, 콘크리트 벽 등에 사용하기 위한 건축물의 표면 마감용 코팅제로서 종래에 사용되고 있는 마감용 코팅제의 단점인 마감용 재료에 함유되어 있는 유기물에 의한 악취 발생을 방지하고, 각종 건축자재에 함유되어 있는 유해물질을 분해 및 흡착 탈취하고, 항균 기능이 있는 건축물 내벽 또는 시멘트 제품의 표면 마감용 바이오 무기질 코팅재의 제조방법에 관한 것이다.The present invention relates to a bioinorganic coating material for surface finishing of various cement-based materials used in buildings. More specifically, it prevents odors caused by organic substances contained in finishing materials, which are disadvantages of conventional finishing coatings as a surface finishing coating for buildings for use in cement panels, cement boards, gypsum boards, and concrete walls. The present invention relates to a method for producing a bio-inorganic coating material for surface finishing of building interior walls or cement products having an antibacterial function, by decomposing and adsorption and deodorizing harmful substances contained in various building materials.
현재 일반주택이나 공동주택 등 건축물에서는 다양한 형태의 시멘트 제품이 사용되고 있다. 시멘트 제품의 종류로는 석고보드, 시멘트 보드, 경량시멘트 패널, 등이 가장 많이 사용되고 있다. 이들 제품은 그 형태로서 표면의 마감이 끝나는 것이 아니고 다시 제품의 표면 위에 벽지를 바르거나 페인트, 또는 페인트와 유사한 형태의 표면 마감재를 사용한다. 이러한 표면 마감재를 사용할 경우 건축물의 내,외부의 온도차에 의한 결로 현상으로 인하여 곰팡이 등이 발생하여 심각한 환경 문제를 야기 시키고 있다. 또한 페인트 또는 페인트와 유사한 마감용 코팅제의 경우 사용되는 원료에 휘발성 유기 화합물이 다량 함유되어 있어 코팅 작업 시 작업자에게 심각한 위해를 가하고 있다. 또한 이들 함유된 유기 화합물은 작업이 완료된 후에도 쉽게 분해되지 않아 인체에 심각한 피해를 기도 한다.Currently, various types of cement products are used in buildings such as general houses and apartment houses. As a kind of cement products, gypsum board, cement board, lightweight cement panel, etc. are most used. These products do not finish the surface in their form, but again use wallpaper, paint, or paint-like surface finish on the product's surface. In the case of using such surface finishing material, mold occurs due to condensation caused by temperature difference between inside and outside of the building, causing serious environmental problems. In addition, paints or paint-like finishing coatings contain a large amount of volatile organic compounds in the raw materials used, which poses a serious hazard to workers during coating operations. In addition, these organic compounds are not easily decomposed even after the work is completed, causing serious damage to the human body.
최근 이를 방지하기 위하여 여러 가지 세라믹재료를 활용하는 방안이 검토되고 있으며, 일부 검증되지 않은 재료도 사용되고 있는 실정이다.Recently, to prevent this, various ways of utilizing ceramic materials have been examined, and some unproven materials are also used.
곰팡이 및 세균은 적당한 온도와 습기, 그리고 옷감이나, 벽지, 도료, 등에서의 영양분 공급, PH 4.5에서 6.5 정도의 약산성 환경에서 잘 서식한다. 이러한 특징때문에 온도 습도를 조절할 수 있는 재료를 사용하거나 오존 등의 재료를 사용하기도 한다.Fungi and bacteria live well at moderate temperatures and humidity, as well as in nutrient supply from cloth, wallpaper, paints, etc., and in mildly acidic environments ranging from pH 4.5 to 6.5. Because of this feature, it is possible to use materials that can control temperature and humidity, or to use materials such as ozone.
이러한 재료들은 가격이 고가이며, 그 충분한 기능을 만족하기 위해서는 상당한 량의 재료를 사용해야 함은 물론 부착성능 및 벽체에의 흡수성능 등을 만조하기 위해서는 또 다른 유기 접착제를 사용해야 하는 부담이 있다. 유기 접착제를 사용함으로서 오히려 악취 발생을 유발하는 효과가 발생하기도 한다.These materials are expensive and there is a burden of using a large amount of materials to satisfy their sufficient functions, as well as the use of another organic adhesive to control the adhesion and absorption to the wall. Rather, the use of organic adhesives may have the effect of causing odors.
이러한 종래 기술의 문제점의 해결방안으로 대한민국 공개특허공보 특 2003- 0032633호에는 원적외선 방사기능, 항균성 및 탈취기능 등 특수기능을 갖는 견운모 분말 및 황토를 주성분으로 하고 여기에 팽창성 시멘트, 석회, 마이크로실리카, 변성아크릴수지, 고화제 및 경화제를 첨가한 수경화성 바름재 조성물에 관한 기술이 개시되어 있다. 그러나, 이때 구성되는 견운모 및 황토의 량이 전체의 45 내지 65 wt%로서 재료 자체의 경화특성이 부족하여 CSA 시멘트나 석회만으로는 부착성능을 만족할 수 없으며, 더구나 부착성능을 위하여 변성 아크릴 모노머 등 유기화합물을 사용하고 있는데, 이를 사용함으로 오히려 유기물에 의한 탈취효과가 저감될 수 있는 문제점이 있다.In order to solve the problems of the prior art, Korean Patent Laid-Open Publication No. 2003-0032633 has mainly composed of mica powder and loess having special functions such as far-infrared radiation function, antibacterial and deodorizing function, and include expandable cement, lime, micro silica, Disclosed is a technique related to a curable coating material composition containing a modified acrylic resin, a hardening agent, and a curing agent. However, the amount of biotite and loess constituted at 45 to 65 wt% of the whole is insufficient of the curing property of the material itself, and thus, CSA cement or lime alone cannot satisfy the adhesion performance. Furthermore, organic compounds such as modified acrylic monomers may be used for adhesion performance. Although it is used, there is a problem that by using this rather deodorizing effect by the organic matter can be reduced.
본 발명자는 이와 같은 문제점을 개선하기 위해 연구를 계속한 결과, 은행나무에서 추출한 은행나무 추출액이 항균, 항 곰팡이 재료로서 우수한 기능을 발휘하는 것을 확인하였으며, 이를 이용한 바이오 바름재를 한국특허 10-0519844로 출원하여 등록된 바 있다. 그러나 은행나무 추출액은 항균, 항곰팡이 성능만 우수한 재료이다. 이에 본 발명인은 다른 식물성 추출액에 대하여 연구를 거듭한 결과 대나무 추출액의 경우 추출액이 항균, 항곰팡이 성능은 물론 약산성으로서 악취성 화합물과 반응하여 고착염을 형성함으로서 탈취기능을 발휘함을 확인하고 본 발명을 완성하게 되었다.As a result of continuing research to improve such a problem, the inventors have confirmed that the ginkgo biloba extract extracted from ginkgo biloba has an excellent function as an antibacterial and antifungal material. Has been filed and registered. However, ginkgo biloba extract is an excellent material for antibacterial and antifungal performance only. Accordingly, the inventors have conducted research on other vegetable extracts, and in the case of bamboo extracts, the extracts exhibited antibacterial and antifungal performance as well as weakly acidic odors and reacted with the malodorous compound to form a fixed salt, thereby demonstrating the deodorizing function. To complete.
대나무 추출액은 이미 그 탈취효과가 검증되어 축사 등의 냄새 제거용으로 활용되고 있으나, 본 발명에서와 같이 세라믹 원료와 혼합 사용되어 그 탈취효과를 극대화하는 시도는 아직까지는 발표된바 없다.Bamboo extract is already used to remove the odor of the barn and the like has been verified the deodorizing effect, but has been unpublished attempts to maximize the deodorizing effect by mixing with a ceramic raw material as in the present invention.
이러한 대나무 추출액을 기본 구성 재료로 하여 강한 흡착용 재료인 규조토를 코팅제 내부의 유기화합물의 냄새를 흡착시키는 재료로 선정하고 일정량의 석회계 광물과 혼합하여 액체상태의 항균 항 곰팡이, 탈취 성능이 우수한 표면 마무리용 바이오 무기질 코팅재에 대한 본 발명을 완성하게 되었다.With the bamboo extract as a basic material, diatomaceous earth, a strong adsorption material, is selected as a material to adsorb the odor of organic compounds inside the coating material, and mixed with a certain amount of lime-based minerals to provide excellent antibacterial and deodorizing properties in liquid form. The present invention has been completed for a bio-inorganic coating material for finishing.
본 발명은 다양한 시멘트 제품 및 콘크리트 벽체의 바탕 면에 대한 얇은 마무리용 코팅제로서 수경성 바름재로서 요구되는 일반적인 물성을 구비하면서 항균, 항 곰팡이, 탈취 기능이 우수한 액상 표면 마무리용 바이오 코팅재 조성물을 제공함에 목적이 있으며 구체적으로는 항균, 항곰팡이, 탈취 성능이 우수한 대나무 추출액을 주성분으로 하고, 탄산칼슘과 돌로마이트를 주원료로 사용함으로서 우수한 항균성, 탈취기능이 부여되는 표면 마무리용 바이오 코팅재 조성물을 제공함에 있다.An object of the present invention is to provide a bio-coating material composition for liquid surface finishing having excellent antibacterial, anti-fungal, deodorizing function while having the general physical properties required as a hydraulic coating material as a thin finish coating agent for the surface of various cement products and concrete walls. In particular, the antimicrobial, anti-mildew, deodorizing performance of the bamboo extract with excellent performance as a main ingredient, by using calcium carbonate and dolomite as the main ingredient to provide a bio-coating material composition for the surface finish that is given excellent antimicrobial, deodorizing function.
본 발명에 따른 코팅재는 대나무 추출액에 의해 항균, 항곰팡이, 탈취 성능이 우수하고, 시멘트계 제품 또는 콘크리트 구체의 바탕 면에의 부착성능의 강화 및 작업성을 확보하기 위하여 시멘트계 재료와 유사한 특성을 갖는 탄산칼슘과 돌로마이트를 사용하며, 작업성을 고려하여 액상형으로 제조되며, 유기 접착제로서 친환경성인 폴리비닐 알콜과 식물성 셀루로오스계의 증점제, 부착용 수지로서 휘발성 유기화합물이 함유되지 않아 친환경성 수지로 사용되는 부틸 아크릴레이트/스티렌 공중합물을 혼합 사용하는 것으로서 부착성능이 우수하고 바이오 기능이 뛰어난 코팅재로 사용될 수 있다. 또한 규불화염은 물 중에서 해리되어 불소 이온을 방출하는 바 이 불소 이온에 의해 항균, 항곰팡이 성능이 더욱 크게 발현된다.The coating material according to the present invention has excellent antibacterial, anti-fungal, deodorizing performance by bamboo extract, and carbonic acid having properties similar to those of cement-based materials in order to secure workability and reinforcement of adhesion to the base surface of cement-based products or concrete spheres. Calcium and dolomite are used and manufactured in liquid form considering workability. It is an eco-friendly resin that does not contain volatile organic compounds as an organic adhesive, eco-friendly polyvinyl alcohol, vegetable cellulose thickener, and adhesion resin. By using a mixture of butyl acrylate / styrene copolymer, it can be used as a coating material having excellent adhesion performance and excellent bio function. In addition, siliceous salts dissociate in water to release fluorine ions, and thus the antibacterial and antifungal performances are more greatly expressed by the fluorine ion.
본 발명은 탄산칼슘 10 내지 20 wt%, 돌로마이트 15 내지 40 wt%, 규조토 3 내지 10 wt%, 셀루로오스 염과 폴리비닐 알코올이 3-5:5-8의 비율로 혼합된 접착용 재료가 0.2 내지 0.5 wt%, 부틸 아크릴레이트/스티렌 공중합물 10 내지 20 wt%, 대나무 추출액 20 내지 40 wt%, 규불화염 0.5 내지 3 wt%, 그리고 통상의 소포제 및 분산제 가 전체 재료를 100으로 하였을 경우 이에 대해 2 wt% 이내로 첨가되어 구성되는 것으로 한다.In the present invention, the adhesive material in which calcium carbonate 10 to 20 wt%, dolomite 15 to 40 wt%, diatomaceous earth 3 to 10 wt%, cellulose salt and polyvinyl alcohol are mixed in a ratio of 3-5: 5-8. 0.2 to 0.5 wt%, 10 to 20 wt% of butyl acrylate / styrene copolymer, 20 to 40 wt% of bamboo extract, 0.5 to 3 wt% of silicides, and common antifoaming and dispersing agents if the total material is 100 It is supposed to be added within 2 wt%.
상기 탄산칼슘는 350번 체 통과량 85% 이상의 재료로서 CaO 함량 48 wt% 이상의 순도를 갖는 것으로 하며, 돌로마이트 역시 350번 체 통과량 85% 이상의 재료로 한다. 또한 규조토 역시 350번체 통과량 100%로 하며 실리카 함량 기준으로 85% 이상의 재료를 사용하는 것으로 한다. 셀루로오스염은 메틸 셀루로오스 및 에틸 셀루로오스로 이루어지는 군에서 선택되는 한가지 이상일 수 있다.The calcium carbonate has a purity of CaO content of 48 wt% or more as the material having a sieving amount of 85% or more, and the dolomite is also made of a material having a sieving amount of 85% or more of the 350 body. In addition, diatomaceous earth is also 100% passing through 350, and the silica content based on 85% or more materials are to be used. The cellulose salt may be at least one selected from the group consisting of methyl cellulose and ethyl cellulose.
이하 본 발명을 하기 실시예에 의하여 더욱 상세하게 설명하고자 한다. 단, 하기 실시예는 본 발명을 예시하기 위한 것일 뿐, 본 발명의 범위가 이들만으로 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to the following examples. However, the following examples are only for illustrating the present invention, and the scope of the present invention is not limited thereto.
실시예Example
제조예Production Example
350번체 통과율 85% 이상이고 CaO 순도 48wt% 이상인 탄산칼슘 135 kg과, 셀루로오스 염과 폴리비닐 알코올이 4:6의 비율로 혼합된 조성물 4 kg, 규조토 60 kg, 돌로마이트 347 kg, 규불화 마그네슘 10 kg, 부틸 아크릴레이트/스티렌 공중합물 168 kg, 대나무 추출액 268 kg, 멜라민계 분산제 4 kg, 실리콘계 소포제 4 kg을 혼합하여 약 30분간 분당 600 회전 이상으로 혼합하여 바이오 코팅재를 제조하였다.135 kg of calcium carbonate with a pass rate of 350% or more and a CaO purity of 48 wt% or more, 4 kg of a composition containing a cellulose salt and polyvinyl alcohol in a ratio of 4: 6, 60 kg of diatomaceous earth, 347 kg of dolomite, and magnesium silicate A biocoating material was prepared by mixing 10 kg, 168 kg of butyl acrylate / styrene copolymer, 268 kg of bamboo extract, 4 kg of melamine-based dispersant, and 4 kg of silicone-based antifoaming agent at about 600 revolutions per minute for about 30 minutes.
시험예 1: 바이오 코팅 물성시험 결과Test Example 1: Bio-Coating Property Test Results
제조예에서 제조된 코팅재의 물성 시험을 하였다.The physical property test of the coating material manufactured in the preparation example was carried out.
시료의 항균시험결과를 표1에 나타내었으며, 본 측정방법은 한국건자재시험연구원의 시험규정인 KICM-FIR-1003에 의해 실험하였으며, 사용 균주는 Escherichia coli ATCC 25922와 Pseudomonas aeruginosa ATCC 15442 이었다.The antimicrobial test results of the samples are shown in Table 1, and the measurement method was tested by KICM-FIR-1003, a test standard of Korea Institute of Construction Materials, and the strains used were Escherichia coli ATCC 25922 and Pseudomonas aeruginosa ATCC 15442.
표.2에는 탈취기능 시험을 한 결과를 나타내었으며, 시험방법은 KICM-FIR-1004에 의해 시험하였다. 대상 가스는 암모니아 가스로 하였으며, 측정은 가스 검지관에 의해 측정하였다.Table 2 shows the results of the deodorant function test, and the test method was tested by KICM-FIR-1004. The object gas was made into ammonia gas, and the measurement was measured by the gas detector tube.
표 1. 항균 시험 결과Table 1. Antimicrobial Test Results
표 3. 탈취 시험 결과Table 3. Deodorization Test Results
이상의 결과로 보아 본 발명의 코팅재는 항균 및 탈취 기능이 매우 우수함을 확인할 수 있었다.As a result, the coating material of the present invention was confirmed that the antibacterial and deodorizing function is very excellent.
본 발명에 따른 바이오 무기질 코팅재는 일반적인 표면 미장용 바름재와는 달리 항균, 탈취 등의 바이오 기능을 갖춘 코팅재로서, 일반 주택 또는 공동주택에 사용되는 시멘트계 재료인 시멘트 보드, 석고 보드, 콘크리트 표면 등의 표면 코팅용 재료로서 곰팡이 등 균의 서식을 방지하는 항균, 탈취 또는 악취 제거 등의 용도를 위한 청정 생활환경용 재료로 사용될 수 있다.Bio-inorganic coating material according to the present invention is a coating material having a bio-function such as antibacterial, deodorant, unlike a general surface plastering coating material, such as cement board, gypsum board, concrete surface, etc. As a surface coating material, it can be used as a material for a clean living environment for the use of antibacterial, deodorant or odor removal to prevent the growth of bacteria such as mold.
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KR20030032186A (en) * | 2001-10-16 | 2003-04-26 | 황영희 | Composition for screening underground water-vein wave and method for preparing the same, and waterproof screener of water-vein wave |
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KR20010001186A (en) * | 1999-06-02 | 2001-01-05 | 손연호 | Fireproofing and sound-absorbing composition |
KR20030032186A (en) * | 2001-10-16 | 2003-04-26 | 황영희 | Composition for screening underground water-vein wave and method for preparing the same, and waterproof screener of water-vein wave |
KR20030086199A (en) * | 2002-05-03 | 2003-11-07 | 삼손퍼라이트 주식회사 | Covering composite for fire resistance and sound absorption |
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