KR100695198B1 - The product composition of a FIRFar Infrared Ray energy emitting permanent wave lotion that contains both of reducing and oxidising agents - Google Patents
The product composition of a FIRFar Infrared Ray energy emitting permanent wave lotion that contains both of reducing and oxidising agents Download PDFInfo
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- KR100695198B1 KR100695198B1 KR1020050013928A KR20050013928A KR100695198B1 KR 100695198 B1 KR100695198 B1 KR 100695198B1 KR 1020050013928 A KR1020050013928 A KR 1020050013928A KR 20050013928 A KR20050013928 A KR 20050013928A KR 100695198 B1 KR100695198 B1 KR 100695198B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/447—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof containing sulfur
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/04—Preparations for permanent waving or straightening the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
본발명은 원적외선을 방사하는 일욕식 퍼어머넨트액 제조 조성물에 관한 것으로 2단게로 구분되어 진다.The present invention relates to a one-bath permanent liquid manufacturing composition that emits far infrared rays and is divided into two stages.
1단계 : 증류수에 수산화 나트륨을 용해시키고 토르마린 분말을 가하여 강알카리로 한후 염화제2철을 가하여 반응시키고 염산으로 PH7로 중화후 정치후 상등액을 분리하여 증류기에 증류를 하므로서 원적외선이 방출되는 증류수 제조 단계.Step 1: Dissolve sodium hydroxide in distilled water, add tourmaline powder to make strong alkali, react with ferric chloride, neutralize with hydrochloric acid to PH7, and then settle and separate the supernatant and distill the distilled water. .
2단계 : 티오그리콜산암모늄 1내지 7중량％, 에틸렌디아민4초산2나트륨 0.01내지 2중량％, 모노에탄올아민 0.01내지 2중량％, 암모니아수(28％) 0.1내지 4중량％, 로단암모늄 1내지 7중량％, 포리에틸렌그리콜-400 2내지 10중량％, 탄산나트륨 0.1내지 1중량％, 에틸알콜 0.5내지 3중량％, 수산화나트륨 0.1내지 1중량％, 아미노산 0.5내지 3중량％, 소디움 보레이트 0.01내지 0.1중량％, 잔량은 원적외선이 방사되는 증류수를 가하여 100％로 하여 제조되는 단계를 포함한다.Step 2: 1 to 7% by weight of ammonium thioglycolate, 0.01 to 2% by weight of sodium ethylenediamine tetraacetate, 0.01 to 2% by weight of monoethanolamine, 0.1 to 4% by weight of ammonia water (28%), 1 to 1% rhodanammonium 7% by weight, polyethylene glycol-400 2 to 10% by weight, sodium carbonate 0.1 to 1% by weight, ethyl alcohol 0.5 to 3% by weight, sodium hydroxide 0.1 to 1% by weight, amino acid 0.5 to 3% by weight, sodium borate 0.01 to 0.1 weight%, remainder includes the step manufactured by adding distilled water by which far-infrared radiation is made to 100%.
Description
퍼어머넨트액은 미용원에서 필요한 퍼어머액으로서 제1액과 제2액으로 구성되어 있다. 제1액은 환원제이고 제2액은 산화제로 구성되어있는 것이다. 제1액과 제2액을 혼합하면 환원과 산화가 동시에 반응이 일어나기 때문에 일욕식 퍼어머액이 출원하지 못한 이유였다.Permanent liquid is a permanent liquid required by a beauty salon, and consists of a 1st liquid and a 2nd liquid. The first liquid is a reducing agent and the second liquid is composed of an oxidizing agent. Mixing the first liquid and the second liquid caused the reaction to occur simultaneously with reduction and oxidation, which was the reason why the single bath permanent fluid was not filed.
즉 일반적으로 제1액은 주로 티오그리코릭산염과 액의 보호제로 구성된 환원제 이며 제2액은 주로 보롬산나트륨 또는 칼륨으로 구성된 것이다. 이러한 2종의 퍼어머액을 사용시 많은 문제점이 있는것이다.That is, generally, the first liquid is a reducing agent mainly composed of thiogricoric acid salt and a protective agent of the liquid, and the second liquid is mainly composed of sodium borate or potassium. There are many problems when using these two types of permanent fluid.
1) 강한 알카리성액인 환원제, 강한 산화제 사용으로 적정량을 초과사용시 모발의 거칠어짐, 또는 피부에 묻을시 피부의 손상이 있을수있으며1) The use of strong alkaline reducing agent or strong oxidizing agent may cause roughness of the hair when used in excess of the proper amount, or damage to the skin when applied to the skin.
2) 미용사의 1액처리후 다시 2액처리로서 1욕식처리때보다 2번 반복 작업을 하므로서 불편함은 물론 시간이 배로 소요되는 단점이 있는 것이다. 근래에 와서는 1욕식 퍼어머넨트액이 출현하였다. 그러나 펌제성분이 너무 약하여 퍼어머넨트를 한후 3회세발을 하면 거의 펴지는 형편 으로 동양인의 모발에는 맞지 않음을 알수가 있다. 그증거로서 아직도 퍼어먼넨트 시장은 98%가 이욕식 퍼엄제를 선호하고 있는 형편이다.2) After the hairdresser's one-liquid treatment, two-liquid treatment is repeated twice more than the one-bath treatment, which is disadvantageous and time consuming. In recent years, a one bath Permanent liquid has appeared. However, the permants are so weak that after three permenents, three haircuts are almost flattened, which is not suitable for Asian hair. As a proof, the Permanent market is still 98% favoring a bathing suit.
3) 기존 2욕식에서 제1제인 환원제 사용으로 -S=S- --→ -SH기로 되면 측쇄가 유리하여 모발은 연약해지고 늘이면 끊어지기 쉽다.3) When using -S = S--→ -SH as the first reducing agent in the existing two baths, the side chain is advantageous, and the hair becomes soft and easily breaks when stretched.
올바르게 사용하여도 -S=S- 기의 20-30% 유리되는 것으로 추측된다.Even when used correctly, it is estimated that 20-30% of the -S = S- group is liberated.
제1액제를 적용하고 15분, 20분 후 제2액제를 적용하는데 그경과를 숙련도에 의할뿐인 것이다. 또한 제2액제(산화제)를 적용하여 100％ -S=S-기로 환원시켰는지를 알수가 없고 다만 경험에 의존할 수밖에 없는 것이다. 그리고 로드에 감으면 일부에는 반드시 -SH기가 잔유하는 것이다. 이 때문에 모발은 자연상태보다 연약하게 되어 기술적으로 조금만 실수를 하여도 절모(切毛)하게 되며 모발관리 유지에 큰 문제점등이 있는것이다.15 minutes and 20 minutes after the first solution is applied, the second solution is applied only by skill. In addition, it is not known whether the second solution (oxidant) has been reduced to 100% -S = S-group, but only depends on experience. And when the load is wound, some of the -SH group will remain. Because of this, the hair becomes softer than the natural state, and even if a little mistake is made, the hair is cut and there is a big problem in maintaining the hair.
종래의 기술에서 문제점 해결에 목적을두고 연구를 거듭하였다.In order to solve the problems in the prior art, the research has been repeated.
1) 제1액제, 제2액제를 작업하므로서 불편함과 시간절약문제1) Discomfort and time saving problem by working with the first liquid and the second liquid
두발은 단백질의 1종으로 케라틴으로 구성되어 있으며 다량의 유황(4-5％)을 함유하고 있다. 이단백질은 고분자물질로 포리펩타이드(polypeptide : -CO·HN-기를 함유한 2개 이상의 아미노산 화합물)로 되 있으며 긴 포리펩타이드 쇄(
이와같은 모발은 장축의 방향으로 병렬한 포리펩타이드체인(polypeptide chain)과 서로 결합하여 모발이 일정한 형태를 이루고 있는 측쇄로 되어있다. 이측쇄에는 여러종으로 구분되어 지나 그중 가장 관계가 깊은 것은 -S=S-결합 즉 디설파이드링케이지(disulfidelinkage)이다.Such hair has a side chain in which the hair forms a certain form by binding to a polypeptide chain parallel to the long axis. There are several species in this side chain, the most important of which is -S = S-bond, or disulfidelinkage.
2욕식 퍼어머넨트 액제에서 제1액제는 거의가 티오글리콜산염으로 환원반응은 다음과 같다.In the two-bath permanent liquid solution, the first liquid agent is almost thioglycolate, and the reduction reaction is as follows.
즉 -S=S-를 환원시켜 그부분에서 측쇄를 분리하는 것이다.That is, -S = S- is reduced to separate the side chain at that portion.
제2액제로는 취소산칼륨 또는 나트륨, 과산화수소 등으로 되어 있으며 산화반응은 다음과 같다.The second liquid agent consists of potassium succinate or sodium, hydrogen peroxide and the like, and the oxidation reaction is as follows.
로서 본래의 -S=S- 형태로 되돌아가게 하는 작용을 한다. 시중에서 판매하는 제2액제를 중화제라고 부르고 있으나 화학반응에서 중화(中和)의 뜻이 아니고 시스틴교를 산화하여 본래의 상태인 즉-S=S-로 되돌아 가게 한다는 뜻인 것이다.It acts to return to the original -S = S- form. Commercially sold second liquids are called neutralizers, but they are not meant to be neutralized in chemical reactions, but they are meant to oxidize cystine bridges back to their original state, namely -S = S-.
프랑스 과학잡지 (chemical and physical behavior of human hair, c.r. robbins. page 56, 1982년 fragrance)에서 KSCN, NaSCN 적용으로 일욕식에 관한 지식을 얻을수가 있었다. 티오그라이세롤, 칼륨티오시안네이드, 또는 나트륨티오시안네이드를 사용 액제를 제조 시험을 하였다. 그러나 너무약하여 요구되는 퍼어머가 되지 않았다. 이물질로 제품을 만들어 12개월간 시험을 하였다. 8개월째 시험에서 약제효과가 급격이 떨어짐을 알수가 있었다. 티오그라이세롤 대신 암모니움티오그 리콜레이트 와 암모니움 로단을 사용하였을 때 15개월 후에도 성분의 변화가 거의가 없었다. 이것은 환원제인 암모니움그리콜레이드와 암모니움로단에서 동일한 NH₄ - 기로 인하여 펌제의 안정성을 알수가 있었다. 암모니움티오그리콜레이드의 환원반응후에 산화반응이 즉시에 일어남을 알수가 있었다.In the French scientific journal (chemical and physical behavior of human hair, c.r. robbins. Page 56, 1982 fragrance), the application of KSCN and NaSCN provided knowledge about sunbathing. Thioglycerol, potassium thiocyanide, or sodium thiocyanide were used for the preparation of the test solution. But it was too weak to be a required permanent. The product was made of foreign material and tested for 12 months. At eight months, the drug effect dropped sharply. When ammonium thioglycolate and ammonium rodan were used instead of thioglycerol, there was little change in the composition even after 15 months. It was found that the stability of the pump was due to the same NH ₄-groups in the ammonium glycolide and the ammonium rodan. It was found that the oxidation reaction occurred immediately after the reduction reaction of ammonium thioglycolide.
환원반응 
산화반응 
2) 절모(切毛)와 모발의 거칠어짐을 방지키 위하여 아미노산을 첨가시켰다.2) Amino acid was added to prevent roughness of hair and hair.
두발은 단백질로 구성되어 있으며 고분자물질로서 폴리펩타이드 (polypeptide : -CO·HN-를 함유한 2개이상의 아미노산 화합물)를 구성하고 있는 아미노산을 일욕식에 포함시키므로서 절모, 거칠어짐을 방지할수 있음을 알수가 있었다. 아미노산으로서The hair is composed of protein, and it is known that it can prevent hair loss and roughness by including amino acids constituting the polypeptide (polypeptide: two or more amino acid compounds containing -CO · HN-) as a polymer in one bath. There was. As an amino acid
(1) L-글루탐산나트륨( Monosodium L-Glutamate)(1) Sodium L-Glutamate (Monosodium L-Glutamate)
(2) 5'-리보뉴클레오티드나트륨(Sodium 5'-Ribonucleotite)(2) Sodium 5'-Ribonucleotite
(3) L-아스파라긴산 나트륨(Monosodium L-aspartate)(3) Sodium L-aspartate
사용함으로서 매우 만족한 퍼어머넨트 작업을 할수있었다.By using it, I was able to do very satisfactory furmanent work.
3) 모발의 안전성을 기여키 위하여 증류수 대신 원적외선이 방사하는 증류수를 사용하였다.3) In order to contribute to the safety of hair, distilled water radiated by far infrared rays was used instead of distilled water.
토르마린 광석 분말을 알카리 용액에 강알카리로 처리하여 염화제 2철로 반응 시킨후 염산으로 중화시키고 상등액을 증류하여 생산된 증류수에서 원적외선 에너지가 350㎛ 이상 나오는 증류수를 사용하여 모발보호에 최선을 다하였다. 또한 약제를 바르고 로드로 말아서 걸고 전열기를 사용치 않고 몸에서 나오는 37.5℃와 일욕식퍼어머넨트 용액에서 나오는 원적외선에 의한 2내지 3℃를 (합계39.5-40.5℃)이용하여 전열기를 사용치 않아도 목적을 달성할수 있도록 하였다.The tourmaline ore powder was treated with strong alkali in alkaline solution, reacted with ferric chloride, neutralized with hydrochloric acid, and the supernatant was distilled from distilled water. It is also possible to apply the agent without rolling heater by using 37.5 ℃ from the body and 2 ~ 3 ℃ by far infrared rays from the one-bath permanent solution (total 39.5-40.5 ℃) without applying heater. To achieve that.
이렇게하여 제조된 일욕식 퍼어머넨트액을 원적외선 측정을 한결과 150㎛ 이상의 원적외선 에너지를 방출하였다.Far-infrared measurement of the one-bath type permenent liquid prepared in this way to emit far infrared energy of 150㎛ or more.
본발명의 퍼어머넨트 용액으로 퍼머를 할시 로드로 머리를 감은후 열을 보존하는 비닐카바나 모자를 쓰고 20-30분후 머리를 감으면 이것으로 퍼어머가 끝나는 것이다. 일욕식 또는 2욕식 퍼어머제 사용후 열을 공급하기위하여 전기열을 내는 캡을 쓸 필요가 없는 것이다. 이욕식, 또는 일욕식에 비하여 시간이 30분 이상절약을 할 수가 있으며 퍼어머를 할 때 미용원에 가는 것이 관례였으나 이제는 집에서도 스스로 퍼어머를 할 수가 있으며 간혹 전열기캡의 오작동으로 화상의 염려가 없는 21세기의 퍼어머넨트액 제품인 것이다.When perming with the Permanent solution of the present invention, the hair is wrapped with a rod and put on a vinyl cabana cap that preserves heat, and after 20-30 minutes, the hair is finished. It is not necessary to use an electric heat cap to supply heat after using a one- or two-bath transformer. It can save more than 30 minutes compared to a bathing or a sunbathing meal, and it was customary to go to a beauty salon when you are a perm, but now you can perm yourself at home, and sometimes there is a risk of burns due to malfunction of the heater cap. Permanent liquid products of the 21st century.
원적외선이 방출하는 퍼어머넨트용액으로 로드로 머리를 감아고정 시킨후 비닐캡이나 모자를 쓸 때 퍼어머액 자체에서 원적외선이 방사되어 우리몸의 온도는 약 37.5℃로서 원적외선 방사온도 33℃가 넘기 때문에 원적외선이 방사되며 방사로 인하여 2내지 3℃의 열이 오르게 되는 것이다. 몸의자체 온도 37.5℃와 원적외선 방사로 인한 온도에 의하여 약 39내지 40.5℃로서 열원의 전열캡을 사용할 필요가 없게 되어 화상등의 염려를 할필요가 없으며 복잡성을 피하며 전체 퍼어머넨트 시간이 30분내지 40분의 시간을 절약할 수 있는 퍼어머넨트액을 발명하게된 것이다.After the hair is fixed with the rod with the permanent permanent solution emitted by the far infrared rays, and the vinyl cap or the cap is worn, the far infrared rays are emitted from the permanent liquid itself, and the temperature of our body is about 37.5 ℃, and the far infrared radiation temperature exceeds 33 ℃. Far infrared rays are radiated and heat is increased by 2 to 3 ℃ due to the radiation. It is about 39 ~ 40.5 ℃ due to the body's own temperature of 37.5 ℃ and the temperature of far-infrared radiation.There is no need to use the heat transfer cap of the heat source. Invented a permanent liquid that can save a time of minutes to 40 minutes.
A 용기에 증류수 1500내지 3000중량부를 취하고 여기에98％ 수산화나트륨 75내지 210중량부를 용해시킨후 토르마린 350메쉬 이상의 분말 75내지 210중량부를 투입 1700rpm 교반기로 30분이상 교반 강알카리로 한다. 여기에 염화제2철 90내지 300중량부를 가하고 교반기로 60분이상 교반한다. 반응액이 청색에서 갈색으로 완전히 변할 때 반응 종말점으로 하고 12시간이상 정치 숙성시킨다. 여기에 염산을 가하여 PH 7로 중화시킨다. 여기에 증류수 1500내지 3000중량부를 가하고 교반후 숙성정치 시킨다. 24시간후 반응물의 상등액과 침전물을 분리시킨다. 맑고 투명한 상등액 2800내지 5600중량부를 증류기에서 증류한다. 증류된 증류액을 원적외선이 방사하는 증류수로 2700내지 5400중량부가 생산된다.Take 1500 to 3000 parts by weight of distilled water in a container A, dissolve 75 to 210 parts by weight of 98% sodium hydroxide therein, and add 75 to 210 parts by weight of tourmaline 350 mesh or more to a strong alkali for 30 minutes with a 1700 rpm stirrer. 90 to 300 parts by weight of ferric chloride is added thereto and stirred for 60 minutes or more with a stirrer. When the reaction solution completely changes from blue to brown, the reaction end point is allowed to stand for at least 12 hours. Hydrochloric acid is added thereto and neutralized with PH 7. 1500 to 3000 parts by weight of distilled water are added thereto, followed by aging and stirring. After 24 hours, the supernatant and the precipitate of the reaction are separated. 2800 to 5600 parts by weight of a clear and transparent supernatant are distilled in a distiller. 2700 to 5400 parts by weight of distilled distilled water is produced by distilled water radiated by far infrared rays.
B용기에 티오그리콜산암모늄 1내지 7중량 ％, 에틸렌디아민4초산 2나트륨 0.01내지 2중량 ％, 모노에탄올아민 0.01내지 2중량 ％, 암모니아수(28%) 0.1내지 4％, 로단암모늄(Ammonium rhodanatum) 1내지 7％, 포리에틸렌그리콜-400 2내지 10％, 탄산나트륨 0.1내지1중량％, 에틸알콜 0.5내지 3중량％,수산화나트륨 0.1내지 1중량％, 아미노산 0.5내지 3중량％, 소디움보레이트 0.01내지 0.1중량％, 잔량은 원적외선이 방사되는 증류수를 가하여 100％로 한다.1 to 7% by weight of ammonium thioglycolate, 0.01 to 2% by weight of sodium ethylenediamine tetraacetate, 0.01 to 2% by weight of monoethanolamine, 0.1 to 4% of aqueous ammonia (28%), rhodanammonium (Ammonium rhodanatum) 1 to 7%, polyethylene glycol-400 2 to 10%, sodium carbonate 0.1 to 1%, ethyl alcohol 0.5 to 3%, sodium hydroxide 0.1 to 1%, amino acid 0.5 to 3%, sodium borate 0.01 To 0.1% by weight, and the remaining amount is 100% by adding distilled water radiated far infrared rays.
이렇게 제조된 퍼어머넨트 용액은 PH 9.5내지 10이된다. 만일 PH가 높으면 구연산으로 조절하여 PH 9.5내지 10으로 맞추면 된다.The permanent solution thus prepared has a pH of 9.5 to 10. If the pH is high, adjust it with citric acid and adjust the pH to 9.5 to 10.
본발명의 퍼어머넨트 용액을 다음과 같이 사용한다. 우선 삼푸로 머리를 감은후 건조시킨후 용액을 도포하면서 로드로 머리를 감은후 비닐카바나 큰 모자를 쓰고 15분 내지 20분 경과후 전열기 캡을 쓸필요가 없이 비닐카바나 큰모자를 제거후 약 5분 내지 10분 방치후 머리를 샴푸로 감으면 되는것이다.The permanent solution of the present invention is used as follows. First, wash your hair with a shampoo and dry it, and then apply a solution, wind your hair with a rod, wear a vinyl cabana or a large cap, and after 15 to 20 minutes, remove the vinyl cabana or a large cap without having to use a heater cap. After leaving it for 10 minutes, you can wash your hair with shampoo.
[실시예 1]Example 1
A용기에 증류수 1,000g을 취하고 여기에 98% 수산화나트륨 50g을 가하여 용해시킨후 토르마린 분말 50g을 가하고 1700rpm 교반기로 30분이상 교반한후 여기에 염화제2철(37보메) 60g을 투입 강알카리로 한다. 청색반응물이 갈색반응물로 완전이 변할 때 반응종말점으로 한다. 12시간이상 정치숙성 시킨후 염산으로 PH 7로 중화시킨후 증류수 1000g을 가하고 30분정도 교반후 정치시킨다. 정치 24시간후 상등액을 분리시키고 맑고 투명한 상등액 1800g을 증류기에서 증류한다.Take 1,000g of distilled water in A container, add 50g of 98% sodium hydroxide to dissolve it, add 50g of tourmaline powder, stir for more than 30 minutes with 1700rpm stirrer, and add 60g of ferric chloride (37bome) to the strong alkali. do. When the blue reactant turns completely into a brown reactant, it is used as the reaction end point. After aging for 12 hours or more, neutralized with hydrochloric acid to PH 7, and 1000 g of distilled water was added thereto, followed by stirring for about 30 minutes. After 24 hours of standing, the supernatant is separated and 1800 g of a clear and transparent supernatant is distilled off in a distiller.
약 1750g 의 증류수가 생산된다. 이 증류액이 원적외선이 방사되는 증류수 인것이다.About 1750 g of distilled water is produced. This distillate is distilled water from which far infrared rays are radiated.
[실시예 2]Example 2
B용기에 원적외선이 방사되는 증류수 76.65중량％를 취하고 여기에 티오그리콜산암모늄 5중량％, 모노에탄올아민 0.9중량％, 암모니아수(28％) 1.5중량％, 로단암모늄 5중량％, 포리에틸렌그리콜-400 8중량％, 탄산나트륨 0.5중량％, 수산화나트륨 0.2％, 에틸알콜 2중량％, L-글루탐산나트륨 1.2중량％, 붕사 0.05중량％를 순서대로 투입 용해하여 제품으로 한다.Take 76.65% by weight of distilled water from which far-infrared rays are radiated to the B container, and 5% by weight of ammonium thioglycolate, 0.9% by weight of monoethanolamine, 1.5% by weight of ammonia water (28%), 5% by weight of rhodanammonium, and polyethylene glycol -400 8% by weight, sodium carbonate 0.5%, sodium hydroxide 0.2%, ethyl alcohol 2% by weight, 1.2% by weight sodium L-glutamate and 0.05% by weight of borax are added and dissolved in that order.
[실시예 3]Example 3
C용기에 원적외선이 방사되는 증류수 73.24중량％를 취하고 여기에 티오그리콜산암모늄 6중량％, 에틸렌디아민4초산2나트륨 0.2중량％, 모노에탄올아민 1.1중량％, 암모니아수(28％) 1.2중량％, 로단암모늄 6중량％, 포리에틸렌그리콜-400 7중량％, 탄산나트륨 0.6중량％, 수산화나트륨 0.6중량％, 에틸알콜 2.5중량％, 5' 리보뉴클레오티드나트륨 1.5중량％, 붕사0.06중량％를 순서대로 투입 용해하여 제품으로 한다.Take 73.24% by weight of distilled water from which far-infrared rays are radiated to the C container, and 6% by weight of ammonium thioglycolate, 0.2% by weight of sodium ethylenediamine tetraacetate, 1.1% by weight of monoethanolamine, 1.2% by weight of ammonia water (28%), 6% by weight of rhodanammonium, 7% by weight of polyethylene glycol-400, 0.6% by weight of sodium carbonate, 0.6% by weight of sodium hydroxide, 2.5% by weight of ethyl alcohol, 1.5% by weight of 5 'ribonucleotide, and 0.06% by weight of borax Dissolve to product.
[시험 1][Exam 1]
원적외선 에너지를 방사하는 일욕식 퍼어머 액으로 인간의 몸의온도 37.5℃에서 150㎛는 2-3℃온도를 상승시키기 때문에 퍼어머 컬링작업 후 전열기캡이 필요없는 것이다.It is a one-bath permanent liquid that emits far infrared energy. The temperature of human body increases the temperature of 37.5 ℃ to 150㎛ by 2-3 ℃, so no heater cap is required after the curling work.
본발명 원적외선을 방사하는 일욕식 퍼어머넨트액은 컬링강도가 우수하며 컬링작업도 1회로 되고 머리를 감은후 잔존 냄새가 없을뿐만 아니라 일반적으로 컬링작업후 전열기캡에서 온도를 약 40℃ 로 유지 컬을 고정시키는 번거러움이 없을 뿐만 아니라 원적외선이 방사하는 일욕식 퍼어머넨트액으로소 우리몸에서 나오는 37.5℃ 온도와 방사 원적외선으로부터 발산하는 2내 3℃의 열을 이용 10내지 20분 비닐카바만 쓰고도 기존의 전열기캡을 쓰는것과 동일 효과가 있으며 혹시나 전열기 오작동, 온도센서의 고장으로 화상의 염려가 없을뿐만 아니라 전열기가 필요없기 때문에 각가정에서도 퍼어머를 할 수 있는 이점이 있는 것이다. 또한 원적외선은 머리피부에 혈액의 순환을 촉진시키며 아미노산의 작용으로 모발이 더욱 윤택해지는 것이다. 모발은 포리펩타이드(-CO·HN-기를 함유한 2개이상의 아미노산 화합물)와의 친화력으로 장기간 퍼어머로 모발의 손상을 막아주는 역할을 하게 되는 것이다. 또한 일욕식(one step)으로 중화제(엄밀이 말하면 산화역활) 처리가 필요없을 뿐만아니라 전열캡으로 온도를 올려 컬의 고정도 필요가 없는 것으로 21세기의 퍼어머넨트 용액이라고 할 수가 있는것이다.The single-bath permenent liquid that emits far-infrared rays of the present invention has excellent curling strength, curling operation once, no residual odor after washing hair, and generally maintains the temperature at about 40 ℃ in the heater cap after curling. It is not a hassle to fix the heat, and it is a single-type permanent liquid radiated by far-infrared rays using only 37.5 ℃ temperature emitted from our body and 2 ~ 3 ℃ heat emitted from radiation far-infrared. It has the same effect as using the existing heater cap, and there is no risk of burns due to the malfunction of the heater or the failure of the temperature sensor. In addition, far infrared rays promote the circulation of blood to the head skin and make the hair more lustrous by the action of amino acids. Hair has affinity with polypeptides (two or more amino acid compounds containing -CO · HN-groups) to prevent hair damage by long term perm. In addition, the one-step (neutral, oxidative role) treatment is not necessary, and the heat cap does not need to fix the curl by raising the temperature.
[표 1] 각제품의 비교표[Table 1] Comparison table of each product
*전문미용사의 관능평가임* Sensory evaluation of professional hairdressers
* 컬의강도우수, 냄새가없다 만점 10점, 나쁘다,냄새가많다 1점* Excellent strength of curl, no smell 10 points, bad, smelly 1 points
머리결의 윤택도 좋다 10, 나쁘다 1점Moisture of hair is good 10, too bad One point
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| KR100984010B1 (en) | 2010-04-07 | 2010-09-30 | 임춘규 | Compound for trichogenousness and preventing the depilation |
| WO2010096598A3 (en) * | 2009-02-19 | 2011-01-20 | Elc Management Llc | Compositions and methods for permanent shaping of hair |
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| KR950005295A (en) * | 1993-08-31 | 1995-03-20 | 강덕주 | Simultaneous perm dye using oxidative hair dye and perm solution and preparation method thereof |
| KR20020035551A (en) * | 2002-04-24 | 2002-05-11 | 남상용 | Head beautiful clinic method based on mineral powder |
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| KR950005295A (en) * | 1993-08-31 | 1995-03-20 | 강덕주 | Simultaneous perm dye using oxidative hair dye and perm solution and preparation method thereof |
| KR20020035551A (en) * | 2002-04-24 | 2002-05-11 | 남상용 | Head beautiful clinic method based on mineral powder |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2010096598A3 (en) * | 2009-02-19 | 2011-01-20 | Elc Management Llc | Compositions and methods for permanent shaping of hair |
| WO2010096605A3 (en) * | 2009-02-19 | 2011-01-27 | Elc Management Llc | Compositions and methods for protecting hair from chemical and thermal damage |
| WO2010096610A3 (en) * | 2009-02-19 | 2011-02-24 | Elc Management Llc | Compositions and methods for increasing tightly bound water in hair |
| AU2010215969B2 (en) * | 2009-02-19 | 2013-04-18 | Elc Management Llc | Compositions and methods for permanent shaping of hair |
| AU2010215976B2 (en) * | 2009-02-19 | 2013-04-18 | Elc Management Llc | Compositions and methods for protecting hair from chemical and thermal damage |
| AU2010215981B2 (en) * | 2009-02-19 | 2013-05-02 | Elc Management Llc | Compositions and methods for increasing tightly bound water in hair |
| KR101372072B1 (en) * | 2009-02-19 | 2014-03-14 | 이엘씨 매니지먼트 엘엘씨 | Compositions and methods for protecting hair from chemical and thermal damage |
| KR100984010B1 (en) | 2010-04-07 | 2010-09-30 | 임춘규 | Compound for trichogenousness and preventing the depilation |
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