KR100618461B1 - a manufacturing method for paste - Google Patents

Abstract

The present invention relates to a method for producing a non-toxic doubly paste, and more particularly, by adding mineral powders such as chromite and illite to starch doubly paste, strong adsorption capacity, anion substitution ability, and large amount of anion and far-infrared ray emitting effect of minerals. By non-toxic and long-term distribution does not deteriorate, but to neutralize the toxicity of concrete to create a comfortable living environment.

Features of the present invention described above are the steps of collecting minerals such as illite, chromite; Crushing the collected minerals into coarse particles to remove impurities, and then drying the water into a drying furnace to completely dry the moisture contained in the minerals while applying heat of 500 to 700 ° C .; Pulverizing the dried minerals finely to form a fine powder of mineral powder by sieving each of them with a sieve maintaining a particle size of 200 mesh or more; 88 to 92% by weight of flour, 4 to 6% by weight of potato powder, 2.5 to 3.5% by weight of illite powder, 1.5 to 2.5% by weight of chromite powder, to complete the dosing powder mixture; A kneading step of mixing the powder mixture and water to a volume ratio of 1: 6 and then stir evenly to prevent burning while heating on a low heat; Aging for 20 to 24 hours while cooling the green grass forming a thin dough in a natural state; It is characterized in that it consists of a step of sealing and then packing the aged paper paste to the drum.

Description

Manufacturing method for non-toxic paper grass {a manufacturing method for paste}             

1 is a manufacturing process chart sequentially listing the manufacturing process of the paper according to the invention step by step,

Figure 2 is a schematic device diagram of a paper paste dough apparatus in the present invention,

3 is a gas concentration curve over time.

Explanation of symbols on the main parts of the drawings

10 tank

10a: heater

11: cover

20: reduction motor

21: axis of rotation

22: wing

30: reduction motor

31: transfer screw

32: outlet

The present invention relates to a method for producing a non-toxic drawing paper, and more particularly, by adding mineral powders such as chromite and illite to starch drawing paper, strong adsorption power, anion substitution ability and a large amount of anions. The present invention relates to a non-toxic and long-term distribution due to the effect of far-infrared radiation, such that it does not deteriorate and neutralizes the toxicity of concrete to create a pleasant living environment.

In general, when painting wallpaper or floorboard, chemical adhesives or starch paper pastes mixed with industrial bonds are mainly used. Among them, chemical adhesives are most commonly used as paper pastes because of the strong adhesive strength and rapid curing. do.

However, the papering paste made of chemical adhesives not only adversely affects the human body due to the toxicity of the industrial bonds while having a strong irritant odor, but also takes a long time to neutralize the toxicity generated in the adhesive even after the papering. In the end, the living environment could not be maintained comfortably.

In addition, the starch dopant is starch powder is kneaded with water to maintain a gel (gel) state and contains a considerable amount of water, so when the starch paste is circulated for a long period of time, easily rotted lungs are generated.

Therefore, in order to prevent the end of decay and to prevent mold, after the completion of the dopant paste, industrial preservatives are mixed with strong preservatives in order to prevent the occurrence of mold and the like. I couldn't keep it safe.

In some cases, in order to minimize the use of preservatives, the paper is distributed in powder form and mixed with water in the field, but at this time, the starch powder is melted in water to have adhesion. Since a large amount of chemical dispersants and adhesives were used, the toxicity caused by the dispersants and adhesives adversely affected the residents, and the indoor environment could not be maintained comfortably.

Particularly, cement, which is the main raw material of concrete building, is composed of strong alkali and emits toxic substances for a long time. Since these toxic substances have worsened residents' health, there is an urgent need for proposals to neutralize the toxicity of concrete. Applicants have proposed a papering pool that contains minerals that can neutralize the toxicity of concrete to the papering pool.

The present invention has been made in view of the above problems, and its object is to add mineral powders such as chromite and illite to starch dopant, which has strong adsorption capacity, anion substitution ability, and a large amount of anion and far infrared emission effects. It is to provide a method for producing a non-toxic paper pool that can create a comfortable living environment by neutralizing the toxicity of concrete, even if it is non-toxic and long-term distribution.

A feature of the present invention for achieving the above object is a mineral powder, such as illite, chlorite, and the like of fine powder filtered through a sieve maintaining a particle size of 200 mesh or more, flour, potato flour and water. In the method of manufacturing a paper pool to prepare a paper pool by mixing the steps, collecting minerals such as illite, chlorite; Crushing the collected minerals into coarse particles to remove impurities, and then drying the water into a drying furnace to completely dry the moisture contained in the minerals while applying heat of 500 to 700 ° C .; 88 to 92% by weight of flour, 4 to 6% by weight of potato powder, 2.5 to 3.5% by weight of illite powder, 1.5 to 2.5% by weight of chlorite powder to complete the dosing powder mixture ; A kneading step of mixing the powder mixture and water to a volume ratio of 1: 6 and then stir evenly to prevent burning while heating on a low heat; Aging for 20 to 24 hours while cooling in a natural state the gel paste forming a thin dough; It can be achieved by the method of producing a non-toxic dopant, characterized in that the step of injecting the aged dopant to the drum and then sealed and packaged.

Hereinafter, described in detail by the manufacturing process of Figure 1 attached to a preferred embodiment for achieving the above object as follows.

Example

Minerals such as illite and chlorite, which exist as natural minerals in nature, were collected.

Subsequently, the collected minerals are respectively put into a crusher and broken into particles having a size of about 35 mm or less, the particles are sorted to remove impurities, and the minerals are put into a drying furnace, followed by heat of 500 to 700 ° C. After drying, the water contained in the mineral was completely dried.

In this step, the crushed mineral particles are selected, washed with water, and then naturally dried to further remove fine foreign matter remaining on the surface of the minerals.

The drying furnace is composed of a drying furnace in the form of a thermal kiln, and may be dried by adding minerals, but by adding minerals to a conveyor moving through the kiln and moving it for about 10 to 20 minutes, and drying by applying heat of about 600 ° C. or more. This mass production is possible because it is preferable.

Of course, in some cases, it is possible to inject minerals into a rotary furnace that is mounted to be inclined and heated so as to dry them in the present invention, it is not limited to the drying method of the minerals in the present invention.

Subsequently, the dried minerals were put in a grinder and finely ground, and then filtered through a sieve having a particle size of 200 mesh and stored in different containers.

The grinder used a conventional grinder in which the cutters are rotated facing each other and grind by grinding by milling when the grinding particles become smaller in stages.

Subsequently, 1.8Kg of flour, 100g of potato flour, 60g of illite powder, 60g of chlorite powder, and 40g of chlorite powder were added to the stirrer, and mixed evenly to complete 2Kg of a dosing powder mixture.

In some cases, corn flour may be used without using flour in the above mixtures.

The stirrer allowed the mixture to be stirred evenly using a conventional stirrer in which stirring blades mounted inside the tank were slowly rotated by the power of a motor.

Subsequently, the powder mixture and water were mixed to have a volume ratio of 1: 6, and then injected into a tank and stirred evenly for about 30 minutes so as not to burn while being heated on a low heat. A gel paste forming a thin dough was completed.

Heating and stirring of the dough may be carried out in various ways, but here, as shown in FIG. 2, a heat of about 300 ° C. is applied to the heater 10a mounted below the tank 10 to heat the tank 10. It is transmitted to the inside, while rotating the reduction motor 20 mounted on the lid 11 while heating the mixture of the powder mixture and water introduced into the tank 10 for stirring blades 22 mounted on the lower portion of the rotary shaft 21 While the dough is slowly rotated and stirred for about 30 minutes while stirring to prevent burning, when the kneading of the paper paste is completed, the speed reduction motor 30 mounted at the bottom of the tank 10 is operated to rotate the transfer screw 31 to discharge the outlet ( 32) An automated device was used to store the paper in the container when it was dropped.

Subsequently, the dough was aged for about 24 hours while cooling in a natural state, and then the aged dopant was injected into a drum to seal the stopper. Thus, the preparation of the packaged non-toxic dopant was completed.

Test Example 1 Measurement of Deodorizing Effect

The deodorizing effect was measured by requesting the drawing paste completed by the manufacturing process of the present invention to the Korea Far Infrared Ray Application Evaluation Institute, and the test method was performed by injecting 500 ppm of ammonia gas into the container containing the sample and the container without the sample to improve the deodorization rate. Test KFIA-FI-1004 test standard was used.

As a result, as shown in the deodorization rate (%) test results of Table 1 and the gas concentration curve according to the time elapse of FIG. 3, the gas concentration was measured every 30 minutes using a gas detector tube. After 90 minutes, the deodorization rate was 90%, the deodorization rate was 93% at 60 minutes, the deodorization rate was 95% at 90 minutes, and the deodorization rate was 96% at 120 minutes. Most of the adsorption and removal was very high deodorization efficiency.

In addition, the deodorization rate (%) was not changed in the container into which the sample was not injected, except for the amount of ammonia gas that naturally disappears as the sample was collected by the gas detector tube.

Test Items Elapsed time (minutes) Blank concentration (ppm) Sample concentration (ppm) Deodorization rate (%)   Deodorization test Early 500 500 - 30 490 50 90 60 480 35 93 90 460 25 95 120 450 20 96

(Note) Blank: Measured without sample. End.

1) Test Method: KFIA-FI-1004

2) Sample: Dougul 30g

3) Test gas name: Ammonia

4) Gas concentration measurement: gas detector

Experimental Example  2: anion Of emission  Measurement test

The dopant pool completed by the manufacturing process of the present invention was commissioned by Korea Far Infrared Application Evaluation Institute, and the anion emission amount was measured under the conditions of room temperature 27 ℃, humidity 49%, and anion number 108 / cc in the air. KFIA-FI-1042 test standard was used to measure and express the number of ions per unit volume.

The results showed that the anion number was 186 / cc as shown in the results of Table 2, releasing anions twice as close as the anion number 108 / cc in the atmosphere.

                            Item Sample Name  Anion (ION / cc)    Grass  186

1) Test Method: KFIA-FI-1042

2) Sample: 30g of grass paste

Experimental Example  3: Measurement test of far infrared radiation energy

The far-infrared radiant energy was measured under the conditions of room temperature 37 ℃ by the DOUBLE pull completed by the manufacturing process of the present invention at room temperature of 37 ° C. The result is far infrared emissivity (5 ~ 20). Μm) was 90.2%, and the radiation energy (W / m ² · µm, 37 ° C) was 3.48 × 10 ² , indicating that the far-infrared emissivity was high and the amount of radiation energy was large.

 Emissivity (5-20㎛)  Radiation energy (W / m2 · ㎛, 37 ℃)  0.902 3.48 × 10 ²

Remarks) This test was conducted under the condition of 37 ℃ according to the request of the client, and it is the result of comparing the black body using the ET-IR Spectrometer.

Test Example 4 Measurement of Sterilization Effect

The antimicrobial effect was measured by requesting the DOUBLE POOL completed by the manufacturing process of the present invention to the Korea Far Infrared R & D Institute, and the test method was added with E. coli cultured in the container for 18 hours and the DOUBLE POOL sample prepared according to the present invention. In another container, only the E. coli was added, and after 24 hours, the number of bacteria in the control sample and the test sample was compared, and the reduction rate of E. coli was measured.

In addition, the reduction rate of Pseudomonas aeruginosa cultured for 18 hours by the method described above was measured together.

As a result of the bacterium reduction rate (%) test results of Table 4, the bacterium concentration was measured after 24 hours, and the bacterium reduction rate was 95.8% in the E. coli culture vessel into which the sample was added. In the container, the bacteriostatic rate was 94.1%, indicating that the sterilization and antimicrobial efficiency of Daffodil was very high.

 Test Items  Sample classification  Initial concentration  Concentration after 24 hours  Bacteriostatic reduction rate (%)   Antibacterial test by E. coli  Blank 3.2 × 10 ⁵ 9.2 × 10 ⁵  -  Grass 3.9 × 10 ⁴  95.8   Antibacterial test by Pseudomonas aeruginosa  Blank 3.9 × 10 ⁶ 9.7 × 10 ⁶  -  Grass 5.7 × 10 ⁶  94.1

(Note) 1) Blank: Measured without sample.

     2) The number of bacteria on the medium is calculated by multiplying the dilution factor.

1) Test Method: KFIA-FI-1003

2) Use strain: Escherichia coli Escherichia coil ATCC 25922

Pseudomonas aeruginosa ATCC 15442

When the paper is finished with the above-mentioned manufacturing process, it is made of natural minerals such as chromite and illite, which emits negative ions and far infrared rays in the natural state, and non-toxic natural substances such as wheat flour and potato flour, which are harmful to the human body. Since organic and inorganic chemicals are not included at all, there are advantages such as keeping residents' health safe and keeping the indoor environment pleasant.

Further, the particulate material while removing corrupt material by the adsorption effect by adsorption to drop the clay minerals with a strong anion, causing the oxidation reaction by the substituted ability hydroxyl (OH ^-) of the mineral, because that could strongly reduce the ions bombard pool Even if it is stored for a long time, it prevents decay and deterioration, so it is possible to smoothly distribute gels in gel state, and it is possible to increase the adhesive strength of the entire papers by the strong viscosity of potato powder contained in the papers. Due to the sterilization and antimicrobial effect of minerals, it is possible to effectively prevent the disintegration such as mold generation or corrosion by moisture even after the completion of the papering.

In addition, after the completion of the dosing, not only can it absorb and neutralize the toxicity of cement by the adsorption effect of particulate matter contained in the dosing pool, but also it can adsorb and remove the irritating odor emitted from the cement, making the indoor environment comfortable. It is possible to keep the health of the residents to keep safe and to solve the sick house syndrome, which is now emerging as a social problem.

In addition, chromite, one of important materials included in the manufacturing process of the present invention, is known to radiate negative ions in a natural state as well as to radiate rotating electromagnetic waves (π-RAY) as published in recent academic fields. Rotating electromagnetic wave (π-RAY) was found to be able to absorb and neutralize the toxicity of cement, and to remove the irritating odor.

On the other hand, the properties of the minerals used in the manufacturing method of the present invention are as follows.

Chlorite is a mineral belonging to monoclinic system. It is called chlorite and its main component is hydrous silicate (Mg, Fe, Al) ₁₂ (Si) of aluminum, iron and magnesium. , Al) ₈ O ₂₀ (OH) ₁₆ .

The chlorite is widely found in various types of sedimentary rocks, low-temperature metamorphic rocks, and igneous rocks deteriorated by hot water. Mainly ions, hornblende, fluorite, etc. By irradiating electromagnetic waves (π-RAY) to adsorb particulate matter or to separate particulate matter of different sizes, it is possible to remove the irritating odor by neutralizing by adsorbing toxic.

Illite is a fine mica mineral belonging to a monoclinic system whose chemical composition is (K, H ₃ O) Al ₂ (Si, Al) ₄ O ₁₀ (H ₂ O , OH) ₂ , which is produced in sedimentary rocks of heterogeneous or tuff-rich structures rich in aluminum, and is produced as altered minerals of hydrothermal deposits. It has the function of neutralizing and deodorizing effect of toxic emission.

Although the preferred embodiments of the present invention have been illustrated and described above, the present invention is not limited to the above-described embodiments, and the present invention is not limited to the above-described embodiments without departing from the spirit of the present invention as claimed in the claims. Various modifications can be made by those skilled in the art, and such modifications are intended to fall within the scope of the appended claims.

Douple grass, which has been completed through the manufacturing process as described above, is made of natural minerals that emit negative ions and far infrared rays in a natural state such as chromite and illite, and nontoxic natural substances such as wheat flour and potato flour. Because it does not contain any inorganic chemicals, it can protect residents' health safely and keep the living environment pleasant and at the same time, by adsorbing and removing the decayed substances due to the adsorption effect of fine particles of minerals, hydroxyl group (OH ^-), causing an oxidation reaction by a strong anion substituted ability because that the ions can be strongly reduced, even if long storage period, the bombard full decay and deterioration is prevented gel (gel) state bombard full distribution is smoothly made of Not only can the strong amount of potato powder Viscosity has the advantage of increasing the adhesive strength of the entire paper pool.

In addition, in the case of adhering the packaging box with the paper paste prepared according to the present invention, it is possible to neutralize by adsorbing the toxicity of the pesticide remaining in the agricultural and marine products contained in the box due to the adsorption effect of the fine particles of minerals, and in particular, it is emitted from the marine products. It is possible to prevent the occurrence of unnecessary odors when transporting boxes by absorbing and removing irritating odors, and to maintain high freshness by preventing decay even if the agricultural products are stored for a long time by strong anion substitution ability of clay minerals. Since it can be actively used as an adhesive of a box for packaging various organisms such as aquatic products, livestock products, and forest products, the paper according to the present invention can be used more variously.

Claims (2)

In the method of manufacturing a grass paste by mixing mineral powder, such as illite, chlorite, etc., of fine powder filtered through a sieve maintaining a particle size of 200 mesh or more, flour, potato powder, and water In Extracting minerals such as illite and chlorite; Crushing the collected minerals into coarse particles to remove impurities, and then drying the water into a drying furnace to completely dry the moisture contained in the minerals while applying heat of 500 to 700 ° C .; 88 to 92% by weight of flour, 4 to 6% by weight of potato powder, 2.5 to 3.5% by weight of illite powder, 1.5 to 2.5% by weight of chlorite powder to complete the dosing powder mixture ; A kneading step of mixing the powder mixture and water to a volume ratio of 1: 6 and then stir evenly to prevent burning while heating on a low heat; Aging for 20 to 24 hours while cooling in a natural state the gel paste forming a thin dough; Method of producing a non-toxic dopant, characterized in that the step of sealing the packaging after injecting the aged dopant to the drum. The method of claim 1, wherein corn flour is used in place of the flour used in the manufacturing step.

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