KR100457710B1 - liquor wine brewage method by means of acanthopanax - Google Patents

liquor wine brewage method by means of acanthopanax Download PDF

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KR100457710B1
KR100457710B1 KR10-2001-0051639A KR20010051639A KR100457710B1 KR 100457710 B1 KR100457710 B1 KR 100457710B1 KR 20010051639 A KR20010051639 A KR 20010051639A KR 100457710 B1 KR100457710 B1 KR 100457710B1
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alcohol
leaching
liqueur
liquor
sugar
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KR20020024775A (en
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이주희
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주식회사 자생당
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/05Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides
    • C12G3/055Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides extracted from plants
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/06Precipitation by physical means, e.g. by irradiation, vibrations
    • C12H1/063Separation by filtration
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/22Ageing or ripening by storing, e.g. lagering of beer

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  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
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  • Wood Science & Technology (AREA)
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  • Food Science & Technology (AREA)
  • Toxicology (AREA)
  • Botany (AREA)
  • Nutrition Science (AREA)
  • Alcoholic Beverages (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

본 발명은 리큐르 기존 제조방법에서 획기적인 품질 개선으로 명실공이 세계화된 술을 만들기 위하여 오가피를 주로 하는 한약재를 당류와 구연산을 혼합한 수용액으로 미리 침출하여 상법에 따라 주정 및 정제수로 혼합 여과 숙성하는 리큐르의 제조방법이다.The present invention is a liqueur of liqueurs by leaching the medicinal medicinal herbs mainly made of agap to an aqueous solution mixed with sugar and citric acid in order to make the world-class liquor in the liqueur conventional manufacturing process by the filtration of alcohol and purified water according to the conventional method It is a manufacturing method.

Description

오가피를주재로한리큐르주제조방법{liquor wine brewage method by means of acanthopanax}Liquor wine brewage method by means of acanthopanax}

리큐르주 제조에서 오가피를 주로 하는 한약재의 침출시 고농도 알콜40%이상으로 침출하는 것이 보통이나, 불필요한 물질이 녹고 알콜에 녹지 않는 물질도 있어,향취가 달라지거나 부족한 편이라 생각되어 진다.In the liquor production, the leaching of the herbal medicine mainly used in the liqueur, it is common to leach more than 40% of high-alcohol alcohol, but there are also substances that do not dissolve unnecessary substances and do not dissolve in alcohol, it is thought that the flavor is different or insufficient.

본 발명자는 상기 문제점들을 해결하여 오가피를 주재로하는 한약재의 향미가 풍부하고, 잡미나 이취가 없으며 신선하고 부드러운 맛의 리큐르주의 제조방법을 제공하려는 것이다.The present inventors have solved the above problems to provide a method of producing a liqueur wine of rich flavor, herbal and odor free, fresh and soft taste mainly oogapi.

도1은 본 발명의 제조 공정도로서, 상세하게는 오가피를 주재로하는 한약재를 미리 당류와 구연산수에 침출하여, 주정과 정제수를 혼합,여과 숙성하는 리큐르주를 제조하는 공정도면이다.1 is a manufacturing process diagram of the present invention, in detail, a process drawing for preparing a liqueur liquor which leaches saccharides and citric acid, predominantly medicinal herbs, mainly mixed with ogapi, and mixes and filters alcohol and purified water.

본 발명은 한약재를 당류와 구연산 수용액으로 침출하여 만드는 리큐르주의 제조에서 포도당, 설탕, 등의 당류 50∼55%,구연산 2∼3%의 혼합수용액 1600㎖에 오가피 120g,모과 20g,당귀 15g, 사인 15g, 구기자, 소회향, 산사자, 하수오, 복분자, 오미자 각 2g 합계 182g을 혼합, 20∼30일간 10∼30℃에서 침출하여 리큐르 원료로 사용한다.The present invention in the preparation of liqueur wine prepared by leaching herbal medicines with an aqueous solution of saccharides and citric acid, in a mixed solution of 50-55% of sugars, such as glucose and sugar, and 2-3% of citric acid, 120 g of Ogapi, 20 g of Chinese quince, 15 g of Angelica, sine 182g of 15g, wolfberry, small fennel, mountain lion, sewage, bokbunja, and Schisandra chinensis 2g each are mixed and leached at 10-30 ° C for 20-30 days to be used as a liqueur raw material.

한약재의 종류 상태에 따라 다소간의 차이는 있으나 오가피를 주로 할 경우 pH는 2.0 내외였으며, 당류를 증가할 경우 점도가 높아 침출이 용이치 않았으며, 줄일 경우 야생효모가 증식하므로 50∼55% 내외가 적당하였다.Although there are some differences depending on the type of herbal medicine, the pH of the agar is mainly around 2.0, and it is not easy to leach because the viscosity of the sugar is increased. It was suitable.

리큐르주의 제조시 알콜 40%이상에 침출하여 사용하는 경우보다, 향취가 강하며 맛이 부드러운 장점이 있다.In the production of liqueur wine, the odor is stronger than when used by leaching in more than 40% alcohol, there is an advantage that the taste is soft.

이것은 높은 농도의 알콜에 불필요한 성분이 녹아 당에 일어나는 현상및 당액에 녹는 성분의 차이에서 일어나는 현상으로 보아진다.This is considered to be caused by the dissolution of unnecessary components in high concentration alcohol and the difference between the components dissolved in sugar solution.

알콜을 사용하지 않는 한약재 침출은 오염이 가장 큰 문제이므로, 당류 55%만으로 침출하였을 경우 세균은 번식하지 않았지만 내당성 야생효모류는 죽지 않고 10일정도 지나면 조금씩 활성을 보이는 현상을 나타내므로 당과 함께 구연산을 첨가하여 pH를 떨어뜨리므로 오염문제를 해결하였다.Since the leaching of herbal medicine without alcohol is the biggest problem, when leaching with only 55% of saccharides, bacteria did not breed, but the sugar-resistant wild yeast did not die and showed little activity after 10 days. The addition of the pH lowered the problem of contamination.

아래의 표1은 침출용액과 한약재의 구성을 적었으며 일부 거친 한약재는 분쇄하여 사용하였다.Table 1 below shows the composition of the leaching solution and herbal medicines, and some of the rough herbal medicines were used by grinding.

한약재 침출내용Chinese herbal medicine leaching content 용재timber 한약재Herbal Medicine 포도당glucose 1,100㎖1,100 ml 오가피Ogapi 120g120 g 구연산Citric acid 32g32 g 모 과Quince 20g20 g 수돗물tap water 1000㎖1000 ml 당 귀Party ear 15g15 g 사 인sign 15g15 g 구기자Wolfberry 2g2 g 소회향Small fennel 2g2 g 산사자Mountain lion 2g2 g 하수오Shouao 2g2 g 복분자Bokbunja 2g2 g 오미자Schisandra 2g2 g 합 계Sum 약 1,600㎖1,600 ml 합 계Sum 182g182 g

※ 정제 포도당 사용※ use of purified glucose

※ 침출 중 pH 2.0※ pH 2.0 during leaching

표2는 당류만으로 침출시 약재추출은 양호하나 야생효모는 대부분이 죽지않고 활성을 나타내었으며, 구연산 1% 농도에서는 외관상 오염은 없었으나 20일 후의 맥아배지에 도말하여 야생효모의 활성여부를 검사한 결과 극히 소수나마 존재하며 구연산 2% 첨가시는 추출과 오염에 문제가 없었다.Table 2 shows that the medicinal extracts were good when leached only with sugars, but most of the wild yeasts showed activity without dying, and at 1% concentration of citric acid, there was no visible contamination, but they were smeared on malt medium after 20 days and tested for wild yeast activity. As a result, only a few were present and there was no problem in extraction and contamination when 2% citric acid was added.

침출중의 현미경 및 향취변화Microscope and Odor Changes During Leaching 침출일내용물Leaching Date Contents 3일3 days 6일6 days 9일9th 12일12 days 15일15th 18일18 days 21일21st 향취Aroma 활성검사Activity test 설탕 55%pH 4.5Sugar 55% pH 4.5 -- ++ ++++ ++++++ CO2발생CO 2 generation CO2발생CO 2 generation CO2발생CO 2 generation 발효취 및산막효모취Fermented Odor and Acid Yeast Odor 대부분 활성Mostly active 설탕 55%구연산 1%pH 2.0내외Sugar 55% citric acid 1% pH 2.0 -- -- -- -- -- -- -- 오가피향 양호Good smell of organ 소수활성Hydrophobic activity 설탕 55%구연산 2%pH 1.8내외Sugar 55% Citric acid 2% pH 1.8 -- -- -- -- -- -- -- 오가피향 양호Good smell of organ 활성 없음No activity 주정 40%40% spirit -- -- -- -- -- -- -- 오가피향 보통Ogapi flavor 활성 없음No activity

또한 일반적으로 한약재추출주는 2∼3개월 침출하여야만 약재성분 및 향취가 충분히 추출되어 약효를 발휘하는 것으로 알려져 왔다. (참조. 병을 치료하는 민간약술.권혁세지음)In addition, herbal extracts have been known to exert medicinal medicinal properties and sufficient medicinal ingredients extracted only 2-3 months leaching. (See folk medicine to cure illness.

그러나 본 실험에서는 20∼30일 추출후 알콜에 2∼3개월 침출한 것보다 한약재 향이 강하고 육안으로 보아 진한 침출 효과를 보였다.In this experiment, however, herbal extracts were stronger than those extracted in alcohol for 2 to 3 months after extraction for 20 to 30 days and showed a strong leaching effect with the naked eye.

[리큐르주 제조]통상적으로 한약재 포함 리큐루주 제조는 효과적인 추출과 변질을 우려하여 95% 주정을 정제수로 알콜분 30∼40%로 희석한액에 한약제를 혼합하여 통상 실온에서 2∼3개월 침출하여 여과 정제 숙성한후 포장전에 다시 음용에 적당한 알콜분으로 정제수로 희석 필요하면 조미하여 포장출고 한다.Liqueurous liquor preparations usually contain medicinal herbs for effective extraction and deterioration.They are mixed with a dilution of 95% alcohol with 30 to 40% alcohol content in purified water. After filtration and filtering, dilute with purified water with alcohol suitable for drinking and repacking before seasoning.

비 교 예 : 별도로 주정을 정제수로 알콜분 40%로 희석한 액 100㎖에 표1과 같은 비율의 한약재 182g를 10∼30℃ 약 1개월 침출하여, 여과 정제한 액을 주정과 정제수를 첨가하여 알콜분 25%, 2,000㎖로 20배되게 희석하여 리큐르주를 만들어 맛을 비교하였다.Comparative Example: Separately, 182 g of the herbal medicine in the ratio shown in Table 1 was leached at 10 to 30 ° C. for about 1 month in 100 ml of alcohol diluted with 40% alcohol content in purified water. The liquor was made by diluting 20 times with 25% of alcohol content and 2,000 ml to make a taste.

실 시 예 1 : 본 발명에 따른 표1의 20일 침출 여액 100㎖에 주정과 정제수를 첨가하여 알콜 20%, 2000㎖로 20배 희석하여 여과 정제하여 맛을 비교하였다.Example 1: Taste and purified water were diluted 20 times with 20% alcohol and 2000ml by adding alcohol and purified water to 100ml of the 20-day leaching filtrate of Table 1 according to the present invention.

실 시 예 2 : 실시예1과 동일하게 표1의 20일 침출여액 100㎖에 주정과 정제수를 첨가하여 알콜분 25%, 2000㎖로 20배 희석하여 여과 정제하여 리큐르주를 만들었다.Example 2 As in Example 1, ethanol and purified water were added to 100 ml of the 20-day leaching filtrate in Table 1, and diluted 20 times with 25% alcohol and 2000 ml to form a liqueur liquor.

표3에서 보는 바와 같이 당류와 산에 침출한 리큐르가 별도 감미 산미 첨가없이도 향이 강하고 맛이 부드러우며 좋았으나,비교예의 리크류주는 별도 산미 감미를 첨가해야 하며, 오가피를 포함한 향취가 실시예보다 못하다.As shown in Table 3, the liqueur leached into sugars and acids was strong in flavor, smooth and good without adding sweetness and acidity, but the liqueurs of the comparative example had to add a separate acidic sweetness, and the odor including the ogapi was worse than the example. .

내용Contents 주정도Around 당도Sugar content 산도Acidity pHpH 맛향Taste 산미Acidity 감미Sweetness 비교예Comparative example 25%25% 0.3%0.3% 0.3%0.3% 5.45.4 향미 보통Flavor normal 없음none 없음none 실시예1Example 1 20%20% 2.4%2.4% 1.5%1.5% 4.04.0 향미 강Flavor river 적당moderation 적당moderation 실시예2Example 2 25%25% 2.4%2.4% 1.5%1.5% 4.24.2 향미 강Flavor river 적당moderation 적당moderation

본 발명의 방법에 의해 제조된 리큐르주는 자극취가 줄어들고 오가피를 중심으로 한 독특한 향취가 강하면서도 순하고 부드러운 술을 제조하므로 동양의 특성을 잘 살려 세계화 할수 있는 가능성과 오가피를 위시한 한약재 소비로 인한 농민소득증대에 기여하는 효과가 있을 것으로 생각되는 유용한 발명인 것이다.Liqueurs produced by the method of the present invention reduces the irritation odor and produces a strong, mild and soft liquor centered around the agapi, thus increasing the farmer's income due to the possibility of globalizing by utilizing the oriental characteristics and the consumption of herbal medicines including the agapi. It is a useful invention that is thought to have an effect that contributes to.

Claims (1)

오가피를 주재하는 한약재를 포도당,설탕 등의 당류 50∼55%, 구연산 2∼3% 의 수용액에 혼합 20∼30일간 침출한 여액을 원액으로 주정과 정제수를 혼합해 20∼25%의 알콜분의 리큐르주를 제조함을 특징으로 하는 오가피를 주재로한리큐르주 제조방법.The herbal medicine which presides over the ogapi is mixed with 50-55% of sugars, such as glucose and sugar, and 2-3% of citric acid, and the filtrate is leached for 20-30 days. Liqueur liquor manufacturing method mainly based on organza characterized by manufacturing liqueur liquor.
KR10-2001-0051639A 2001-08-27 2001-08-27 liquor wine brewage method by means of acanthopanax KR100457710B1 (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR910007606A (en) * 1989-10-17 1991-05-30 게르하트 레벨 디에터 마이어 호프 Valve for discharging molten metal from metallurgy vessel
KR940000618A (en) * 1992-06-22 1994-01-03 박홍기 Spinnerets for manufacturing cross-section fibers
KR20010096226A (en) * 2000-04-18 2001-11-07 신연주 A method of producing green tea using green branch, green leaves and umes, and a green tea produced by this method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR910007606A (en) * 1989-10-17 1991-05-30 게르하트 레벨 디에터 마이어 호프 Valve for discharging molten metal from metallurgy vessel
KR940000618A (en) * 1992-06-22 1994-01-03 박홍기 Spinnerets for manufacturing cross-section fibers
KR20010096226A (en) * 2000-04-18 2001-11-07 신연주 A method of producing green tea using green branch, green leaves and umes, and a green tea produced by this method

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