KR100383077B1 - Process for preparation germanium water concentration powder and the apparatus - Google Patents
Process for preparation germanium water concentration powder and the apparatus Download PDFInfo
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- KR100383077B1 KR100383077B1 KR10-2000-0044940A KR20000044940A KR100383077B1 KR 100383077 B1 KR100383077 B1 KR 100383077B1 KR 20000044940 A KR20000044940 A KR 20000044940A KR 100383077 B1 KR100383077 B1 KR 100383077B1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
- B01D1/24—Evaporating by bringing a thin layer of the liquid into contact with a heated surface to obtain dry solids
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
- B01D1/221—Composite plate evaporators
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G17/00—Compounds of germanium
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Abstract
본 발명은 게르마늄수 농축분말 제조방법 및 그 장치에 관한 것으로서, 게르마늄수(水)를 증류시켜 분말상태의 게르마늄으로 농축하는 방법 및 그 장치를 얻기 위한 것인 바,The present invention relates to a method for producing germanium water concentrate powder and apparatus therefor, and to obtain a method and apparatus for distilling germanium water and concentrating it into powdered germanium.
증발기에 게르마늄수를 공급하고 동시에 측면에서 팬을 이용하여 통풍건조시키고 사각상자 밑으로 빠진 게르마늄수는 다시 증발기에 공급하여 초기 게르마늄수의 1/4 수준으로 증류를 반복한 후 얻어진 게르마늄 증류액을 원심분리하여 중금속을 분리, 제거한 다음 저온 건조대에 넣고 저어주면서 건조시키므로서,Germanium water is supplied to the evaporator, and at the same time, it is ventilated and dried by using a fan on the side, and germanium water dropped under the box is fed back to the evaporator, and the distillation of the germanium distillate obtained after distillation is repeated to 1/4 level of the initial germanium water. By separating and removing heavy metals, and then put them in a low temperature drying rack and stir to dry
게르마늄을 함유하고 있는 수(水)를 증류하여 농축하여 게르마늄분말을 얻을 수 있는 효과가 있으며, 또한 저온에서 빠르게 대량 생산할 수 있어 제조단가가 저렴한 뛰어난 효과가 있다.It is effective to obtain germanium powder by distilling and concentrating germanium-containing water, and also to produce a large amount at a low temperature quickly, so that the manufacturing cost is excellent.
Description
본 발명은 게르마늄수 농축분말 제조방법 및 그 장치에 관한 것이다. 더욱 상세하게는, 본 발명은 게르마늄수(水)를 증류시켜 분말상태의 게르마늄으로 농축하는 방법 및 그 장치에 관한 것이다.The present invention relates to a method for producing germanium water concentrate powder and apparatus thereof. More specifically, the present invention relates to a method and apparatus for distilling germanium water to concentrate it in powdered germanium.
종래에 많은 사람들이 게르마늄수가 인체의 건강증진에 효과가 있음을 확인하고 이를 손발온욕기, 좌욕기, 사우나기 등에 적용하여 널리 사용하여왔다.In the past, many people have confirmed that germanium water is effective in improving the health of the human body, and has been widely used by applying it to the hands, feet, baths, saunas, and the like.
그러나, 게르마늄수에는 게르마늄 외에 철, 알루미늄, 납, 아연 등과 같은 인체에 유해한 중금속이 다량 함유되어 있어 식용 음료수로 복용이 불가능할 뿐만 아니라 신체에 적용하는 것도 꺼려왔었다.However, since germanium water contains a large amount of heavy metals harmful to the human body, such as iron, aluminum, lead, and zinc, in addition to germanium, it is not only possible to take it as an edible drink but also has been reluctant to apply it to the body.
본 발명자는 상기와 같은 점에 착안하여, 강원도 정선군 소재 함백산에서 채취한 게르마늄수를 높은 온도 가열증류가 아닌 방법으로 증류하여 농축시킨 후 원심분리하여 게르마늄수에 포함된 중금속 및 이 물질의 농도를 줄이도록 한 게르마늄 분말을 단시간에 다량 제조함으로써 본 발명을 완성하였다.In view of the above, the present inventors distilled and concentrated the germanium water collected from Hambaeksan, Jeongseon-gun, Gangwon-do in a manner other than high temperature heating distillation, and centrifuged to reduce the concentration of heavy metals and foreign substances contained in the germanium water. The present invention was completed by preparing a large amount of germanium powder in a short time.
따라서, 본 발명의 목적은 게르마늄을 함유하고 있는 수(水)를 증류하여 농축함으로서 게르마늄 분말을 단시간에 다량 제조하는 방법을 제공함에 있다.Accordingly, an object of the present invention is to provide a method for producing a large amount of germanium powder in a short time by distilling and concentrating water containing germanium.
본 발명의 다른 목적은 게르마늄 수 농축분말을 대량생산할 수 있어 제조단가가 저렴하고 제조시간을 단축한 분말제조장치를 제공하는 데 그 목적이 있다.Another object of the present invention is to provide a powder manufacturing apparatus which can mass-produce germanium water-enriched powder, which is low in manufacturing cost and shortened in production time.
본 발명의 상기 목적은 관통구가 형성된 사각상자와 증류모가 차례로형성된 증류기에 높은 온도로 가열하지 않은 게르마늄수 또는 저온으로 가열한 게르마늄수를 통과시키면서 통풍건조시켜 증류하고 증류되지 않고 남은 게르마늄수는 다시 상기 과정을 반복하여 얻은 게르마늄 증류액을 원심분리하여 침전물과 게르마늄수에 포함된 중금속 및 이 물질의 농도를 줄여 저온에서 서서히 건조시켜 분말 상태의 게르마늄을 제조함으로써 달성하였다.The object of the present invention is to pass through the germanium water not heated to a high temperature or the germanium water heated to a low temperature through a rectangular box in which a through-hole is formed and a distillation cap is formed in turn through the air-dried distillation and the germanium water remaining without distillation again The germanium distillate obtained by repeating the above process was centrifuged to reduce the concentration of the heavy metal and the substance contained in the precipitate and the germanium water, and was slowly dried at low temperature to produce a powdered germanium.
이하, 본 발명의 구성을 설명한다.Hereinafter, the configuration of the present invention will be described.
도 1은 본 발명의 바람직한 실시예의 게르마늄수 농축분말 제조방법에 의한 장치를 도시한 사용 상태도,1 is a state diagram showing the use of the apparatus according to the germanium water concentrate powder production method of a preferred embodiment of the present invention,
도 2는 본 발명의 게르마늄수 농축분말 제조장치의 받이부와 양증류모판부를 도시한 사시도,Figure 2 is a perspective view showing the receiving portion and the positive distillation bed portion of the germanium water concentrate powder production apparatus of the present invention,
도 3은 본 발명의 게르마늄수 농축분말 제조장치의 탱크부를 도시한 상태도이다.Figure 3 is a state diagram showing the tank portion of the germanium water concentrated powder production apparatus of the present invention.
* 도면의 주요부분에 대한 부호의 설명** Explanation of symbols for the main parts of the drawings *
10 : 구멍 20 : 받이판10: hole 20: receiving plate
30 : 긴 증류모 40 : 짧은 증류모30: long distilled hair 40: short distilled hair
50 : 양증류모판부 60 : 송풍팬50: positive distillation bed 60: blowing fan
100 : 칸막이 120 : 수분증발부100: partition 120: water vaporization
130 : 원심분리부 170 : 건조수단부130: centrifuge 170: drying means
180 : 분쇄부180: crushing unit
본 발명은 직경 2 ∼ 3mm의 미세한 구멍이 15 ∼ 20cm 간격으로 형성된 사각상자를 층층이 6 ∼ 10층 정도 쌓고 사각상자의 층과 층사이에 증류모를 형성한 본 발명 증발기에 가열하지 않은 게르마늄수를 공급하고 동시에 상하에서 팬을 이용하여 통풍건조시키고 받이부 밑으로 빠진 게르마늄수는 다시 증발기에 공급하여 초기 게르마늄수의 1/4 수준으로 증류를 반복한 후 얻어진 게르마늄 증류액을 원심분리하여 무게에 따라 게르마늄수에 포함된 중금속 및 이 물질의 농도를 줄인 게르마늄 증류액을 다시 수분증발부에 공급하여 수분을 증발시키고 다시 저온 건조대에 넣고 저어주면서 건조시켜 덩어리지지 않는 본 발명 게르마늄수 농축분말을 제조하는 공정; 상기와 동일한 방법으로 실시하되 가열하여 35 ∼ 45℃ 수온을 나타내는 게르마늄수를 증발기에 공급하여 본 발명 게르마늄수 농축분말을 제조하는 공정; 상기와 동일한 방법으로 실시하되 가열하여 75 ∼ 85℃ 수온을 나타내는 게르마늄수를 증발기에 공급하여 본 발명 게르마늄수 농축분말을 제조하는 공정으로 구성된다.The present invention supplies germanium water that is not heated to the present evaporator, in which a rectangular box formed with fine pores having a diameter of 2-3 mm at intervals of 15 to 20 cm is stacked about 6 to 10 layers, and distilled hair is formed between the rectangular box layers and layers. At the same time, ventilate dry using a fan at the top and bottom, and the germanium water dropped under the receiving part is fed back to the evaporator, and the distillation is repeated to 1/4 level of the initial germanium water, and the germanium distillate obtained is centrifuged to separate germanium according to the weight. Preparing a germanium water concentrated powder of the present invention that is not lumped by supplying germanium distillate having reduced concentration of the heavy metal and the substance contained in the water to the water evaporation unit and evaporating the water and then putting it in a low temperature drying stand and stirring; Performing the same method as described above, but supplying germanium water having a water temperature of 35 to 45 ° C. to an evaporator to produce the germanium water concentrated powder of the present invention; It is carried out in the same manner as above but heated to supply a germanium water having a water temperature of 75 ~ 85 ℃ evaporator is composed of a process for producing a germanium water concentrated powder of the present invention.
이하, 본 발명의 구체적인 방법을 도면과 실시예를 들어 상세히 설명하고자 하지만 본 발명의 권리범위는 이들 실시예에 만 한정되는 것은 아니다.Hereinafter, the specific method of the present invention will be described in detail with reference to the accompanying drawings and examples, but the scope of the present invention is not limited to these embodiments.
도 1은 본 발명의 바람직한 실시예의 게르마늄수 농축분말 제조방법에 의한 장치를 도시한 사용 상태도이고, 도 2는 본 발명의 게르마늄수 농축분말 제조장치의 받이부와 양증류모판부를 도시한 사시도이고, 도 3은 본 발명의 게르마늄수 농축분말 제조장치의 탱크부를 도시한 상태도이다.1 is a state diagram showing the apparatus according to the germanium water concentrate powder manufacturing method of the preferred embodiment of the present invention, Figure 2 is a perspective view showing the receiving portion and the positive distillation bed portion of the germanium water concentrate powder manufacturing apparatus of the present invention, Figure 3 is a state diagram showing the tank portion of the germanium water concentrated powder production apparatus of the present invention.
먼저, 본 발명의 바람직한 실시예의 게르마늄수 농축분말 제조방법에 대하여 설명한다.First, a method for producing germanium water concentrated powder of a preferred embodiment of the present invention will be described.
실시예 1: 가열하지 않은 게르마늄수를 이용한 본 발명 게르마늄수 농축분말 제조Example 1 Preparation of Germanium Water Concentrate Powder of the Invention Using Unheated Germanium Water
본 실시예에서 사용한 게르마늄수는 강원도 정선군 소재 함백산에서 채취한 것으로 가열처리하지 않은 자연상태의 것이다. 게르마늄수 18L을 본 발명 증발기에 공급하여 증발기 아래로 게르마늄수가 4.5L 용출될 때까지 증류를 반복하였다. 이때, 건조는 증발기 상하로 팬을 이용하여 통풍건조시켰다. 증류되어 나온 게르마늄 증류액을 원심분리기에 옮겨 원심분리함으로서 분자량이 무거운 납, 아연과 같은 중금속과 그 밖의 불순물을 줄인 후 이를 건조대에 옮겨 저어주면서 건조시켰다. 건조시에는 게르마늄이 건조판에 눌어붙거나 덩어리지지 않도록 계속적으로 저어주어야 하며 온도는 70℃가 넘지 않도록 하였다. 건조된 게르마늄은 고운 분말로 파쇄하여 제품화하였으며 최종 게르마늄 분말은 20g이였다.The germanium water used in this example is taken from Hambaeksan, Jeongseon-gun, Gangwon-do, and is in a natural state without heat treatment. Distillation was repeated until 18 L of germanium water was fed to the present invention evaporator and 4.5 L of germanium water eluted under the evaporator. At this time, the drying was ventilated dry using a fan up and down the evaporator. The distilled germanium distillate was transferred to a centrifuge to reduce the heavy metals such as lead and zinc, and other impurities, which were then dried on a drying rack. At the time of drying, the germanium must be continuously stirred to prevent it from sticking or agglomerating on the drying plate and the temperature should not exceed 70 ° C. The dried germanium was crushed into fine powder and commercialized, and the final germanium powder was 20 g.
실시예 2: 저온 가열한 게르마늄수를 이용한 본 발명 게르마늄수 농축분말 제조Example 2 Preparation of Germanium Water Concentrate Powder of the Present Invention Using Germanium Water Heated at Low Temperature
상기 실시예 1과 동일한 방법으로 게르마늄수 농축분말을 제조하되, 사용한 게르마늄수 18L을 가열탱크에서 35 ∼ 45 ℃로 저온 가열한 후 본 발명 증발기에 적용하여 최종 게르마늄 분말 22g를 수득하였다.The germanium water concentrate powder was prepared in the same manner as in Example 1, but 18 g of the used germanium water was heated at 35 to 45 ° C. at a low temperature in a heating tank and then applied to the evaporator of the present invention to obtain 22 g of the final germanium powder.
실시예 3: 고온 가열한 게르마늄수를 이용한 본 발명 게르마늄수 농축분말 제조Example 3 Preparation of Germanium Water Concentrate Powder of the Present Invention Using Germanium Water Heated at High Temperature
상기 실시예 1과 동일한 방법으로 게르마늄수 농축분말을 제조하되, 사용한 게르마늄수 18L을 가열탱크에서 70℃로 저온 가열한 후 본 발명 증발기에 적용하여 최종 게르마늄 분말 23g를 수득하였다.The germanium water concentrate powder was prepared in the same manner as in Example 1, but 18 g of the used germanium water was heated at 70 ° C. at a low temperature in a heating tank, and then applied to the evaporator of the present invention to obtain 23 g of the final germanium powder.
상기 실시예 1, 2, 3에서 게르마늄수의 온도와 건조시 온도는 게르마늄 분말이 건강증진 효과를 나타내는데 중요한 역할을 하는 것으로 게르마늄 온도는 10 ∼ 90℃ 정도면 어느 것이나 사용가능하나 바람직하게는 30 ∼ 40℃이며 건조시 온도는 40 ∼ 50℃의 저온도 무방하나 온도가 낮으면 시간이 장기간 소요되고 80 ∼ 90 ℃ 의 고온에서는 단시간에 건조되나 게르마늄의 건강증진 효과가 감소되므로 65 ∼ 75℃의 온도가 바람직하다.In Examples 1, 2, and 3, the temperature of the germanium water and the drying temperature play an important role in showing the health promotion effect of the germanium powder, and the germanium temperature may be any of 10 to 90 ° C., but preferably 30 to 30 ° C. The temperature is 40 ℃ and the temperature of drying is 40 ~ 50 ℃, but if the temperature is low, it takes a long time. If the temperature is 80 ~ 90 ℃, it is dried for a short time, but the health promotion effect of germanium is reduced, so it is 65 ~ 75 ℃. Is preferred.
이하, 본 발명 게르마늄 농축을 위한 증발 장치를 도면에 의거하여 상세히 설명하고자 한다.Hereinafter, the present invention will be described in detail with reference to the evaporation apparatus for germanium concentration.
먼저, 도 1 내지 도 3에 도시한 본 발명의 게르마늄수 농축분말 제조방법에 의한 장치는 양증류모판부(50)와 다공이 형성된 받이판을 다단으로 적층하여 그 상부에 게르마늄수를 떨어뜨려 강제송풍에 의해 수분을 증발하는 수분증발부(120)와, 일정양의 수분이 증발된 게르마늄수에 포함된 중금속 및 이 물질의 농도를 줄이도록 원심분리부(130)와, 수분을 완전히 제거하는 건조수단부(170)와, 건조된 게르마늄을 분쇄하여 분말화시키는 분쇄부(180)를 포함하여 구성된다.First, the apparatus according to the germanium water concentrate powder manufacturing method of the present invention shown in Figs. 1 to 3 by laminating the positive distillation bed portion 50 and the receiving plate formed with pores in multiple stages by dropping the germanium water on the top Water evaporation unit 120 to evaporate moisture by blowing, centrifuge 130 to reduce the concentration of heavy metals and foreign substances contained in the germanium water evaporated a certain amount of water, and dry to completely remove the moisture And a means unit 170 and a pulverizing unit 180 for pulverizing and drying the dried germanium.
다음, 상기 수분증발부(120)는 다공(10)이 형성된 게르마늄수 받이판(20)과, 상부는 긴 증류모(30)와 하부는 짧은 증류모(40)를 삽입하여 게르마늄수가 건풍에 의해 건조가 되도록 형성한 양증류모판부(50)를 받이판의 상단에 올려놓은 구조를 1세트로 하여 다단으로 적층되도록 구성하고, 상기의 양증류모판(50)에 건풍이 공급되도록 다수개의 송풍팬(60,60-1)으로 구성하고, 상기 다단의 적층된 받이판(20)을 거처 하단의 탱크부(70)로 이동된 게르마늄수를 상부 받이판으로 공급하도록 펌프(80)와 파이프(90)로 구성된다. 또한 탱크내에는 다단의 칸막이(100)가 형성되어 상부 받이판으로 공급하는 물이 가열되도록 끝단에 배출 파이프를 장착하였고, 그 하단에는 일정한 온도로 가열하도록 가열부(110)가 구성된다.Next, the water vaporization unit 120 is a germanium water receiving plate 20 formed with a porous 10, the upper part of the long distilled hair 30 and the lower part of the short distilled hair 40 by inserting the germanium water by dry wind A multi-stage blower fan 50 is formed so as to be stacked in a multi-stage structure by placing the positive distillation bed plate 50 formed on the upper end of the receiving plate as a set, and a plurality of blower fans are supplied to the positive distillation bed plate 50 above. (80, 60-1), the pump 80 and the pipe 90 to supply the germanium water moved to the tank portion 70 at the bottom through the stacked support plate 20 of the multi-stage to the upper support plate. It is composed of In addition, a multi-stage partition 100 is formed in the tank, and a discharge pipe is mounted at the end to heat the water supplied to the upper support plate, and a heating unit 110 is configured at the lower end thereof to heat at a constant temperature.
상기 원심분리부(130)는 수분증발부(120)에서 일정량의 수분을 증발한 게르마늄수에 포함된 중금속 및 이 물질의 농도를 줄이도록 장착한다. 상기 원심분리기는 회전력을 이용한 기계류를 사용한다.The centrifuge 130 is mounted to reduce the concentration of heavy metals and foreign matter contained in the germanium water evaporated a certain amount of water in the water evaporation unit 120. The centrifuge uses machinery using rotational force.
상기 원심분리부(130)에서 다시 수분증발부(120)로 게르마늄수를 펌프(80-1)로 공급하여 제 2차 수분을 증발하도록 구성한다.The centrifugal separator 130 is configured to supply germanium water to the water evaporation unit 120 to the pump 80-1 to evaporate the second moisture.
한편, 상기 건조수단부(170)는 수분증발부에서 게르마늄수를 완전 건조하기 위해 이송하도록 장착된 펌프(80-2)와 가열부(140)와, 상기 가열부에 의해 게르마늄수가 응고방지 및 건조가 되도록 가로대(150)와 상기 가로대가 왕복운동하도록 장착된 엑츄레이터(160)로 구성되어 엑츄레이터(160)가 왕복운동을 함으로써 수분을 증발시키고 응고되지 않도록 장착하였다.On the other hand, the drying means unit 170 is the pump 80-2 and the heating unit 140, which is mounted to transfer to completely dry the germanium water in the water evaporation unit, and the germanium water by the heating unit to prevent the solidification and drying It consists of a crossbar 150 and the actuator 160 is mounted so that the crossbar reciprocates so that the actuator 160 reciprocates and mounted to prevent water from evaporating and solidifying.
상기 건조수단부(170)에서 건조된 게르마늄 덩어리를 분쇄하여 분말화 시키는 분쇄부(180)를 장착하여 분쇄하여 게르마늄 분말을 얻도록 하였다.The drying means unit 170 was equipped with a pulverization unit 180 for pulverizing and drying the germanium lumps to be pulverized to obtain germanium powder.
예컨대, 본 발명은 상술한 실시예에 한정되지 아니하며, 특허청구범위에서 청구한 본 발명의 요지를 벗어남이 없이 본 발명이 속하는 기술분야에 통상의 지식을 가진 자라면 다양한 변형 실시가 가능한 것임은 물론이고, 그와 같은 변경은 본 발명의 청구범위내에 있게 된다.For example, the present invention is not limited to the above-described embodiment, and various modifications can be made by those skilled in the art without departing from the gist of the present invention as claimed in the claims. Such changes are intended to be within the scope of the present invention.
이상, 상기 실시예를 통하여 설명한 바와 같이, 본 발명은 게르마늄을 함유하고 있는 수(水)를 증류하여 농축하여 게르마늄분말을 얻을 수 있는 효과가 있으며, 또한 저온에서 빠르게 대량 생산할 수 있어 제조단가가 저렴한 뛰어난 효과가 있으므로 게르마늄 분말 제조산업상 매우 유용한 발명인 것이다.As described above, the present invention has the effect of distilling and concentrating germanium-containing water to obtain germanium powder, and also can produce large quantities quickly at low temperature, and thus, the manufacturing cost is low. Since it is an excellent effect, it is a very useful invention in the germanium powder manufacturing industry.
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| KR20030069000A (en) * | 2002-02-19 | 2003-08-25 | 김고정 | Method and device for extracting germanium from mineral water |
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| KR100522783B1 (en) * | 2001-05-14 | 2005-10-19 | 백한기 | A method and apparatus for sintering germanium |
| CN108686394A (en) * | 2018-08-21 | 2018-10-23 | 河南卓立膜材料股份有限公司 | Waste ink processing apparatus |
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|---|---|---|---|---|
| JPS4634601Y1 (en) * | 1968-12-13 | 1971-11-30 | ||
| JPS6336828A (en) * | 1986-07-30 | 1988-02-17 | Showa Denko Kk | Production of dried particulate material and vacuum freeze dryer |
| JPH035265A (en) * | 1989-05-17 | 1991-01-11 | General Motors Corp <Gm> | Antilock brake system |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPS4634601Y1 (en) * | 1968-12-13 | 1971-11-30 | ||
| JPS6336828A (en) * | 1986-07-30 | 1988-02-17 | Showa Denko Kk | Production of dried particulate material and vacuum freeze dryer |
| JPH035265A (en) * | 1989-05-17 | 1991-01-11 | General Motors Corp <Gm> | Antilock brake system |
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| KR20030069000A (en) * | 2002-02-19 | 2003-08-25 | 김고정 | Method and device for extracting germanium from mineral water |
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