KR100372526B1 - Method for simultaneous analysis of multiple elements of hair sample by inductively coupled plasma mass spectrometry(icp-ms) - Google Patents

Method for simultaneous analysis of multiple elements of hair sample by inductively coupled plasma mass spectrometry(icp-ms) Download PDF

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Publication number
KR100372526B1
KR100372526B1 KR1020020056212A KR20020056212A KR100372526B1 KR 100372526 B1 KR100372526 B1 KR 100372526B1 KR 1020020056212 A KR1020020056212 A KR 1020020056212A KR 20020056212 A KR20020056212 A KR 20020056212A KR 100372526 B1 KR100372526 B1 KR 100372526B1
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South Korea
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intensity
mass
sample
hair sample
multiple elements
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KR1020020056212A
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Korean (ko)
Inventor
Myoung Jin Cha
Jun Mo Kang
Sung Hyun Kim
Joung Hae Lee
Chang Joon Park
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Sung Hyun Kim
Medinex
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Priority to KR1020020056212A priority Critical patent/KR100372526B1/en
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Publication of KR100372526B1 publication Critical patent/KR100372526B1/en

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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/34—Purifying; Cleaning
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/38—Diluting, dispersing or mixing samples
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/48—Biological material, e.g. blood, urine; Haemocytometers
    • G01N33/483—Physical analysis of biological material
    • G01N33/4833—Physical analysis of biological material of solid biological material, e.g. tissue samples, cell cultures

Abstract

PURPOSE: A method for simultaneous analysis of multiple elements of hair sample by inductively coupled plasma mass spectrometry is provided to precisely analyze the nutrition elements of ppm level and heavy metal elements of low ppb level simultaneously. CONSTITUTION: A method for simultaneous analysis of multiple elements of hair sample by inductively coupled plasma mass spectrometry includes the steps of washing a hair sample with surfactant, deionized water, and acetone, preparing a sample solution by radiating microwave to a nitric acid diluted solution receiving the washed hair sample, grouping the sample solution per detecting element by diluting the sample solution into two groups of 200-300times and 2000-30000times, and simultaneously analyzing the multiple elements contained in the hair sample by carrying out the ICP-MS for the diluted sample solutions and correcting the result values by the formulas. Wherein Inet represents the intensity of mass number 75 from which ArCl molecular ion interface is removed, Im represents the intensity of mass number 75 in which the influence of interface is included before the correction, Im represents the intensity of mass number 51, Im represents the intensity of mass number 77, Im represents the intensity of mass number 82, and a is mass discrimination per unit mass of a used mass analyzer.
KR1020020056212A 2002-09-16 2002-09-16 Method for simultaneous analysis of multiple elements of hair sample by inductively coupled plasma mass spectrometry(icp-ms) KR100372526B1 (en)

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KR1020020056212A KR100372526B1 (en) 2002-09-16 2002-09-16 Method for simultaneous analysis of multiple elements of hair sample by inductively coupled plasma mass spectrometry(icp-ms)

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Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101107052B1 (en) 2009-10-29 2012-01-25 한국지질자원연구원 Method for Analysis of Lithium Isotope
EP2518474A1 (en) 2011-04-27 2012-10-31 Well Dynamics Applications S.r.l. WDA Method for the determination of analytes in the hair
CN103940786A (en) * 2014-04-18 2014-07-23 中盐金坛盐化有限责任公司 Mineral nutrition block sample pretreatment method based on inductively coupled plasma (ICP) analysis
KR20160052185A (en) * 2014-11-04 2016-05-12 (주)아모레퍼시픽 Quantitative analytic method for lead or arsenic
KR20160052188A (en) * 2014-11-04 2016-05-12 (주)아모레퍼시픽 Quantitative analytic method for antimon or cadmium
KR20160052186A (en) * 2014-11-04 2016-05-12 (주)아모레퍼시픽 Quantitative analytic method for antimon or cadmium
KR20160052187A (en) * 2014-11-04 2016-05-12 (주)아모레퍼시픽 Quantitative analytic method for lead or arsenic
RU2589960C1 (en) * 2015-04-29 2016-07-10 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Казанский (Приволжский) федеральный университет" (ФГАОУВПО КФУ) Method for laser atomic emission spectral analysis of hair
KR101746397B1 (en) * 2017-02-20 2017-06-13 대한민국 Method for monitoring of metabolic disease or stress, and monitoring device using the same
EP3517934A1 (en) 2018-01-24 2019-07-31 I Love My Body Research S.r.l. Method for the determination of analytes in the hair
CN112946103A (en) * 2021-01-27 2021-06-11 山东英盛生物技术有限公司 Pretreatment method and detection method for detecting content of 21 elements in hair
KR20210078881A (en) 2019-12-19 2021-06-29 중앙대학교 산학협력단 Multi-elemental analysis of urine by inductively coupled plasma/mass spectrometry
KR20210078882A (en) 2019-12-19 2021-06-29 중앙대학교 산학협력단 Multi-elemental analysis of blood by inductively coupled plasma/mass spectrometry
KR102339658B1 (en) 2021-03-25 2021-12-14 주식회사 피피엠아이 A method for analysis of heavymetal and nutritional minerals in hair

Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101107052B1 (en) 2009-10-29 2012-01-25 한국지질자원연구원 Method for Analysis of Lithium Isotope
EP2518474A1 (en) 2011-04-27 2012-10-31 Well Dynamics Applications S.r.l. WDA Method for the determination of analytes in the hair
CN103940786A (en) * 2014-04-18 2014-07-23 中盐金坛盐化有限责任公司 Mineral nutrition block sample pretreatment method based on inductively coupled plasma (ICP) analysis
KR102152639B1 (en) 2014-11-04 2020-09-08 (주)아모레퍼시픽 Quantitative analytic method for lead or arsenic
KR102152652B1 (en) 2014-11-04 2020-09-08 (주)아모레퍼시픽 Quantitative analytic method for lead or arsenic
KR20160052186A (en) * 2014-11-04 2016-05-12 (주)아모레퍼시픽 Quantitative analytic method for antimon or cadmium
KR20160052187A (en) * 2014-11-04 2016-05-12 (주)아모레퍼시픽 Quantitative analytic method for lead or arsenic
KR20160052188A (en) * 2014-11-04 2016-05-12 (주)아모레퍼시픽 Quantitative analytic method for antimon or cadmium
KR102152654B1 (en) 2014-11-04 2020-09-09 (주)아모레퍼시픽 Quantitative analytic method for antimon or cadmium
KR102152646B1 (en) 2014-11-04 2020-09-09 (주)아모레퍼시픽 Quantitative analytic method for antimon or cadmium
KR20160052185A (en) * 2014-11-04 2016-05-12 (주)아모레퍼시픽 Quantitative analytic method for lead or arsenic
RU2589960C1 (en) * 2015-04-29 2016-07-10 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Казанский (Приволжский) федеральный университет" (ФГАОУВПО КФУ) Method for laser atomic emission spectral analysis of hair
KR101746397B1 (en) * 2017-02-20 2017-06-13 대한민국 Method for monitoring of metabolic disease or stress, and monitoring device using the same
WO2019145402A1 (en) 2018-01-24 2019-08-01 I Love My Body Research S.r.l. Method for the determination of analytes in the hair
EP3517934A1 (en) 2018-01-24 2019-07-31 I Love My Body Research S.r.l. Method for the determination of analytes in the hair
KR20210078881A (en) 2019-12-19 2021-06-29 중앙대학교 산학협력단 Multi-elemental analysis of urine by inductively coupled plasma/mass spectrometry
KR20210078882A (en) 2019-12-19 2021-06-29 중앙대학교 산학협력단 Multi-elemental analysis of blood by inductively coupled plasma/mass spectrometry
CN112946103A (en) * 2021-01-27 2021-06-11 山东英盛生物技术有限公司 Pretreatment method and detection method for detecting content of 21 elements in hair
KR102339658B1 (en) 2021-03-25 2021-12-14 주식회사 피피엠아이 A method for analysis of heavymetal and nutritional minerals in hair

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