KR100335572B1 - Method of manufacture sulfo-soap - Google Patents

Abstract

The present invention by dissolving sulfur powder (S) having an insoluble property in water, alcohol, etc. in soap base, the whitening effect obtained from sulfur hot spring containing sulfur components, dandruff removal, housewife eczema removal, wrinkle removal, skin eczema removal, The present invention relates to a method for producing a barb for soap, which can obtain various effects such as improving hair growth.

The manufacturing method of the sulfur soap for the present invention comprises dissolving sulfur powder in a nonionic surfactant in a temperature range of about 180 ° C. to 250 ° C. to prepare a sulfur solution, and then including mixing soap material with the sulfur solution. It is characterized by being.

Therefore, in the present invention, the sulfur soap for manufacturing the soap according to the manufacturing method of the present invention dissolves sulfur powder, so that it can be commercialized as a soap, there is an effect that can obtain a sulfur hot spring effect at home without going to a hot spring.

In addition, the sulfur soap for the manufacture of the soap according to the manufacturing method of the present invention has a fast and penetrating power to the skin, has a strong and reliable performance even at low concentrations, and also has the advantage of uniformly supplying sulfur components to the skin. .

Description

Method for manufacturing soap for sulfur medicine {METHOD OF MANUFACTURE SULFO-SOAP}

The present invention relates to a method for producing a soap, and in particular, by dissolving sulfur powder (S) having an insoluble property in water, alcohol, etc. in a soap base, the whitening action and dandruff that can be obtained in a sulfur hot spring containing sulfur components The present invention relates to a manufacturing method of the soap for the sulfuric agent that can obtain various effects such as removal, housewife eczema removal, wrinkle removal, skin eczema removal, and hair growth improvement.

Human skin is composed of cystine protein when young, but as it ages gradually, aging occurs when the cystine protein is changed to methionine protein.

That is, the skin of the human body is accompanied by abnormal keratin phenomenon as it ages.

Therefore, the majority of people have a desire to keep the aged skin younger and more elastic, and as one of the solutions to solve this need, the effects of the following sulfur on the human body has been known.

In other words, sulfur converts methionine protein into cystine protein to whiten skin that turns aged black skin into young white skin. In addition, it can treat dandruff, acne, wrinkles, housewife eczema, and skin eczema. The fact that it is possible to improve the protein constitution and increase hair growth has been described in several papers and journals {see, Strakosch, EA (Arch, Dermat syph; 48,384, 1934), Menschel, H. (Arch, f, exper. Path). u.Pharmakol; 110,1,1925), Stuttgen, G., H, W.st; Der matologische wochenschrift, B. 133,308 (1956), Allggra, F.u. M. Jori; Dermatologische Wochenschrift, H. 7, Bd. 141 (1960), Karl Bergwein; Das Drogisten-Fachblatt Darmstadt, 32 J., Nr. 6 (1961), 60-Dec-Day 16D 60D-D 2032D, 61-Dec 21D 61D-D302醫藥 部 外 品 販賣 名 `` Crystal sole- プ It was published in the W.S 』.

Therefore, every year many people enjoy hot spring baths in sulfur hot springs mixed with sulfur components in order to obtain various effects.

Sulfur, which has many effects as described above, is very beneficial to the human body, but when it is below the proper content in the human body, oxygen is diffused into the tissues, thereby losing the viability of cells and promoting keratinogenesis. Therefore, the proper amount of sulfur in the human body is essential.

However, such sulfur is soluble in benzene, toluene, carbon disulfide (CS ₂ ), etc., and has a property of being insoluble in water, alcohol, etc., and used in everyday life. There was a problem that is difficult to process.

In order to solve the above problems, it is an object of the present invention to provide a method for producing a sulfur soap for dissolving sulfur and to easily obtain the effect of sulfur by preparing it as a soap. The manufacturing method of the sulfur soap for the invention comprises sulfur powder dissolved in a nonionic surfactant in the temperature range of about 180 ℃ to 250 ℃ to prepare a sulfur solution, and then mixed with the sulfur solution in the sulfur solution. Is characteristic.

The surfactant may be polyoxyethylene oleyl ether, polyoxyethylene fatty alcohol, polyoxyethylene alkyl phenol ether, polyethylene glycol patty acid ether glycol fatty acid ether) or Fatty acid diethanol amide.

Hereinafter, the present invention will be described in detail.

The method for preparing the sulfur soap for the present invention comprises dissolving sulfur powder in a nonionic surfactant in a temperature range of about 180 ° C. to 250 ° C. to prepare a sulfur solution, and then comprising mixing soap material with the sulfur solution. do.

Through the following Examples 1 and 2 to find the effect on the manufacturing process and the skin of the barb for soap of the present invention.

Example 1

The manufacturing process of the medicinal soap is as follows.

First, polyoxyethylene oleyl which is a nonionic surfactant

6 g of sulfur powder is added to 30 g of ether), and the mixture is heated and stirred at a temperature ranging from 180 ° C to 250 ° C. In the present invention, as the nonionic surfactant, polyoxyethylene oleyl ether was used, but in addition, polyoxyethylene fatty acohol ether, polyoxyethylene alkyl phenol ether, polyethylene glycol patty Acid ether (polyoxyethylene glycol fatty acid ether), Fatty acid diethanol amide, etc. are mentioned.

During heating and stirring, sulfur powder is dissolved in polyoxyethylene oleyl ether, which is a nonionic surfactant, to form a primary sulfur solution of 20%.

Subsequently, the 20% primary sulfur solution was dissolved in polyoxyethylene sorbitan monooleate.

(polyoxyethylene sorbitan mono-oleate) 6% secondary sulfur solution is prepared by mixing in about 65-70g, preferably 64g.

Table 1 shows the blending ratio of soap base, glycerin, fragrance, pigment and the like in the secondary sulfur solution.

To the prepared secondary sulfur solution, as shown in Table 1, soap base material, glycerin, fragrances, pigments may be added in an appropriate amount.

TABLE 1

Soapy (less than 15% moisture) 65-70 g Sulfur solution 0.3% to 3% glycerin 0.05g ~ 0.2g Spices 0.2g-1g Pigment Quantity Sum 70g total

Example 2

Hereinafter, in Table 2, by applying the soap test method of KOREAN INDUSTRIAL STANDARD KSM 2701 to the present invention, compared to the case of dissolving sulfur powder in a surfactant and in the case of not in Table 2 below water insoluble Find out about% of ingredients.

<Table 2>

Analysis item Experiment 1 Experiment 2 Experiment 3 Experiment 4 moisture(%) 14.50 14.10 14.00 14.30 Net Soap Powder (%) 95.51 95.61 95.63 95.44 Free alkali (%) 0.051 0.041 0.042 0.051 Water insoluble ingredient (%) 0.312 0.574 0.011 0.012 Sulfur Theoretical Content (%) 0.240 0.480 0.240 0.480

* Experiment 1 contains 0.24% sulfur powder in soap.

* Experiment 2 contains 0.48% sulfur powder in soap base.

* Experiment 3 prepared sulfur solution by dissolving sulfur 6% in surfactant first, and then mixing 4% sulfur solution into soap base.

* Experiment 4 prepared sulfur solution by dissolving sulfur 6% in surfactant first, and then mixing this sulfur solution in soap base.

As can be seen in Table 2, Experiments 1 and 2 are sulfur powder blended into soap base, water insoluble value is too large to be suitable for soap production, while Experiments 3 and 4 were prepared by dissolving sulfur powder in surfactant. The sulfur solution was added to the soap base again in the formulation, and each water insoluble value is extremely low at 0.011% and 0.012%, which is advantageous for soap production.

For reference, the% value of the water insoluble component can be obtained from the following equation.

Water insoluble ingredient (%) = residual amount (g) / sample (g) * 100

When the sulfur soap for the present invention prepared according to the above method is foamed and contacted to the skin,

2R · S · H + S → R · S · S · R + H ₂ S... … (Ⅰ)

(R stands for alkyl group)

When the skin's methionine protein (R · S · H) comes into contact with sulfur (S), it causes a chemical reaction as in (I) above.

That is, methionine protein (R · S · H) is converted into cystine protein (R · S · S · R) to generate hydrogen sulfide (H ₂ S). At this time, the generated hydrogen sulfide (H ₂ S) acts to sterilize the skin, it is excellent for the removal of dandruff, acne, athlete's foot, housewife eczema, skin eczema and the like.

As described above, the sulfur soap for manufacture according to the manufacturing method of the present invention can dissolve sulfur powder to be commercialized as a soap, it is possible to obtain a sulfur hot spring effect at home without going to a hot spring.

In other words, the medicinal soap prepared by the manufacturing method of the present invention reacts with the skin while soap bubbles come into contact with the skin to change the methionine protein of the aged skin into young cystine protein, and also, dandruff, acne, athlete's foot, housewife Eczema, skin eczema and the like to improve the constitution and promote hair growth.

In addition, the sulfur soap for manufacturing the soap according to the manufacturing method of the present invention has the advantage of fast and penetrating power to the skin, has a strong and reliable performance at low concentration, and also can supply the sulfur component to the skin uniformly.

Claims (6)

After dissolving sulfur powder in a nonionic surfactant in the temperature range of about 180 ~ 250 ℃ to prepare a sulfur solution, A method for producing a soap for sulfur, comprising a mixture of soap and sulfur in the sulfur solution. delete The method according to claim 1, The nonionic surfactant may be polyoxyethylene oleyl ether, polyoxyethylene fatty acohol ether, polyoxyethylene alkyl phenol ether, polyethylene glycol patty acid ether. A method for producing a soap for use as a sulfur, characterized in that any one selected from (polyethylene glycol fatty acid ether) or patty acid diethanol amide (Fatty acid diethanol amide). delete The method according to claim 1, Method for producing a soap for the sulfur, characterized in that the addition of glycerin, fragrance, pigments to the mixed solution after mixing the soap base in the sulfur solution. The method according to claim 1, The method of preparing the sulfur solution is carried out in two separate steps. In the production of the sulfur solution, the sulfur powder is melted with the nonionic surfactant of claim 2 to prepare the primary sulfur solution, and then in the production of the sulfur solution. A method for producing a sulfur soap, characterized in that the sulfur powder is melted with a polyoxyethylene sorbital mono-olate as a nonionic surfactant to prepare a secondary sulfur solution.