KR100321821B1 - Method of producing pine salt solution - Google Patents

Abstract

In preparing a pine salt solution, a method of preparing a pine salt solution in which a pine salt is obtained by dissolving the salt in water without emulsifying a mixture of salt and rosin and heat-adsorbing the salt, and preparing the pine salt solution in an aqueous solution. The manufacturing method of is disclosed. According to the present invention, the pulverized rosin is added to a salt water at room temperature with a predetermined surfactant and then emulsified to have a particle diameter of 3,000 Pa or less using ultrasonic waves to form a pine salt solution. By spray drying the thus prepared pine salt solution, fine powdery pine salt can be obtained, and pine salt ointment can be prepared by mixing petroleum jelly with petroleum jelly. In addition, the pine salt solution may be prepared by mixing stone powder, magnesium carbonate, sodium fluoride, sodium bicarbonate, glycerol, and sodium lauryl sulfate in the pine salt solution. Pine salt solution according to the present invention can be applied in various ways depending on the application method, it is effective to heal wounds or pain in the oral cavity, the pine salt can be used for the treatment of skin wounds, athlete's foot and eczema.

Description

Method for preparing pine salt solution and method for preparing pine salt, pine salt ointment and pine salt toothpaste using pine salt solution {Method of producing pine salt solution}

The present invention relates to the preparation of a pine salt solution, and more particularly, to a pine salt solution in an aqueous state by emulsifying the rosin while dissolving salt in water without using a conventional pine salt processing method obtained by heating and adsorbing a mixture of salt and rosin. The present invention relates to a method for preparing a pine salt solution and a pine salt ointment and pine salt toothpaste using the pine salt solution.

According to the conventional herbal medicine Dongbobogam or herbal herb, rosin and salt are known to have various pharmacological effects on the human body. Therefore, in recent years, great attention has been paid to the synergistic effect of pine salt mixed with these two substances. The pharmacological action of pine salt is to increase the concentration of salt in aqueous solution as the salt in pine salt is dissolved in water, thereby stimulating human tissue by osmotic pressure to activate it. In addition, the same effect has a disinfecting effect on the bacteria in the wound tissue, it is believed that the pharmacological action of rosin has a great effect on the regeneration and pain of the wound tissue.

Generally, polar substances such as salts are soluble in polar solvents such as water, and large molecular weight and nonpolar substances such as rosin are insoluble in polar solvent water. Therefore, pine salt was obtained by heating a mixture of salt and rosin during processing, and it is known that the additives such as alum were mixed together to increase the effect of pharmacological action.

By the way, pine salt has been used in a mixed heated powder state, because the rosin is adsorbed on the surface of the salt particles, it is difficult to dissolve the salt and direct action with the wound area, it was difficult to dissolve in water, it was inconvenient to use. In addition, although the powder state, but the rosin is adsorbed on the particles of the salt, the size of the particles are large, so the use of the good feeling and the foreign matter giving a sense of foreign matter was limited in use despite the pharmacological effect.

In particular, pine salt is known to be effective in toothache or stomatitis in the oral cavity, but the amount of rosin attached or adsorbed on the salt is not constant for each salt particle. It could have been an unpleasant feeling.

The present invention has been made to solve the above-mentioned conventional problems, and a first object of the present invention is to dissolve salt in water without using the conventional pine salt processing method obtained by heating and adsorbing a mixture of salt and rosin. It is to provide a processing method of the pine salt solution to emulsify the rosin while obtaining a pine salt solution in an aqueous solution.

A second object of the present invention is to provide a method for producing pine salt using a pine salt solution obtained in an aqueous solution state by emulsifying rosin while dissolving salt in water.

It is a third object of the present invention to provide a method for producing a pine salt ointment using a pine salt solution obtained in an aqueous solution state by emulsifying rosin while dissolving salt in water.

It is a fourth object of the present invention to provide a method for producing a pine salt toothpaste using a pine salt solution obtained in an aqueous solution state by emulsifying rosin while dissolving salt in water.

In order to achieve the first object as described above, the present invention,

The method of producing a pine salt solution, characterized in that the pulverized rosin in a salt water at room temperature with a predetermined surfactant and then emulsified by spraying using a nozzle or emulsified to have a particle diameter of less than 3,000 kPa using ultrasonic waves. to provide.

The surfactant consists of sorbitan trioleate.

In addition, in order to achieve the second object as described above, the present invention,

The pulverized rosin is added to sorbitan trioleate in salt water at room temperature, and then emulsified to have a particle diameter of 3,000 kPa or less using ultrasonic waves to make a pine salt solution, and the pine salt solution is spray dried to prepare a fine powder. It provides a method for producing a pine salt characterized by the above-mentioned.

In addition, in order to achieve the third object as described above, the present invention,

The pulverized rosin is added with sorbitan trioleate to room temperature in brine and emulsified to have a particle diameter of 3,000 Å or less using ultrasonic waves to make a pine salt solution, and the pine salt solution is spray-dried to obtain a pine salt and then Provided is a method for preparing a pine salt ointment, which is prepared by mixing with petroleum jelly or glycerol.

In addition, in order to achieve the fourth object as described above, the present invention,

The pulverized rosin is added to a salt water at room temperature with a predetermined surfactant and emulsified to have a particle diameter of 3,000 kPa or less using ultrasonic waves to form a pine salt solution. Glycerol, Sodium Lauryl Sulfate (Sodium Lauryl Sulfate) by providing a method for producing a toothpaste toothpaste characterized in that it is prepared in the form of dough.

When making the dough, it is also possible to further mix Spearmint Oil (Spearmint Oil) as a fragrance in the pine salt solution.

As mentioned above, according to the present invention, in obtaining a pine salt solution, a pine salt solution is obtained in an aqueous state by emulsifying the rosin while dissolving the salt in water without heat-adsorbing a mixture of salt and rosin, thereby obtaining the pine salt solution. Using to prepare pine salt, pine salt ointment and pine salt toothpaste.

Hereinafter, a method of preparing a pine salt solution and a pine salt ointment and pine salt toothpaste using the pine salt solution according to the present invention will be described in detail.

Preparation of pine salt solution

In general, the solubility of salt is around 40, but slightly different depending on the temperature, and is an ionic substance that is well dissolved in water to form a homogeneous solution in an aqueous state. Rosin, on the other hand, is difficult to dissolve in water and, although partially soluble, is only a very small amount.

Therefore, in order to obtain rosin in a state of being mixed with water, when the rosin particles are very finely emulsified in water, a rosin solution in a relatively uniform state can be obtained. At this time, the particle of the rosin should be maintained at a diameter of less than 3,000 kPa can be emulsified for a long time. At this time, when the surfactant is mixed, the emulsified state can be maintained semi-permanently.

In order to emulsify rosin, there is a method using a blade while spraying rosin from a small hole (nozzle) in water, and there is a method of emulsifying in water by crushing particles using ultrasonic waves. When emulsifying rosin by using a nozzle, the nozzle must be managed so that the nozzle is not blocked by rosin, and it is effective to raise the water temperature.

In addition, it is possible to maximize the emulsification by using a surfactant so that the emulsified rosin particles are not separated from the water. At this time, the surfactant to be used may be different depending on the purpose of the pine salt solution. That is, the concentration of salt can be adjusted from 0 to 35%, the concentration of rosin can be controlled from 0 to 20%, although somewhat different depending on the concentration and type of surfactant used.

Preparation of pine salt and pine salt ointment

The pine salt solution emulsified in the above method can be applied in various ways depending on the application method. In particular, pine salt is effective in healing wound tissues and pain in the oral cavity, and vitiligo is effective in treating stomatitis, so it can be used by dissolving alum in the aforementioned pine salt solution.

When the pine salt solution is spray-dried or centrifugal rotary spray-drying to powderize, very fine powder-like pine salt particles can be obtained.

The resulting pine salt is mixed with a substance that can be applied directly to the skin, such as petroleum jelly or glycerol, to obtain a pine salt ointment that can be used to treat wounds, athlete's foot, eczema and the like.

Preparation of Pine Salt Toothpaste

The salt solution can be used as a mouthwash as the solution itself, and toothpaste can be prepared using the salt solution. In general, there are various kinds of toothpaste that can be purchased on the market and can be roughly classified into dough-type toothpaste and cream-type toothpaste and tooth powder. The above-mentioned pine salt solution can be used for toothpaste of dough type or cream of toothpaste, and powdered pine salt obtained by spray drying can be mixed with tooth powder.

Regardless of the type of toothpaste, toothpaste is basically a tooth-grinding agent and a dispersant is added so that these abrasives can spread evenly to the tooth during grinding, and neutralize it when acid is generated due to food or glucose decay between the teeth. Neutralizing agents and fragrances are used. To make the dough according to the shape of the toothpaste, the dough material is added and both the dough and creamy toothpaste are mixed with water to make it easy to use. At this time, the water used can be utilized as a salt solution.

DETAILED DESCRIPTION The toothpaste in the form of dough will be described in detail.

As materials used to remove and polish tartar, stone powder and soda bicarbonate and aluminum oxide (alumina) or silica zirconium silicate or alumino silicate soda added with soda bicarbonate are used. At this time, the size of the abrasive used is approximately 10μ or less and specific gravity is 1.3 or less.

Many different kinds of substances are used to neutralize the acid that forms with the decay of food or glucose in the teeth, usually consisting of fluorine compounds. Sodium fluoride is widely used as a commonly used material. Recently, titania (Titanium Dioxide), which has a great polishing effect, is sometimes used.

Glycerol, sorbitol, polyethylene glycol, mannitol, etc., are kneaded with water to form the dough. There are many other dough forming materials. In addition, there are a number of anionic surfactants, and high fatty acid sulfonated salts are used, and a substance obtained by polymerizing sorbitan monostearate with ethylene oxide as a nonionic surfactant is used. Cationic surfactants and fragrances (such as spearmint oil) are used. In order to knead these substances, a small amount of water is added, and the toothpaste that can treat pain and wounds in the oral cavity can be obtained by using the pineal salt solution obtained in the present invention as water to be used.

<Example>

Preparation of pine salt solution, pine salt and pine salt ointment

30 g of salt, 10 g of crushed rosin (100 mesh), and 2 g of sorbitan trioleate are added to water having a water temperature of 30 ° C. or lower, and emulsified for 10 minutes using an ultrasonic wave of 29,000 Hz. The emulsified solution is milky and tastes salty and bitter. The resulting solution can be used as a mouthwash and can reduce the amount of rosin to reduce the bitter taste.

The solution made here is a pine salt solution, and when it is spray-dried, pine salt in the form of fine powder can be obtained.

Thus obtained pine salt can be dissolved in a small amount of water and applied to the wound or athlete's foot, it can also be used in combination with petrolatum or glycerol.

Preparation of Toothpaste

30 g of pine salt solution prepared as mentioned above, 100 to 150 g of stone powder, 0.1 to 0.5 g of magnesium carbonate, 0.01 to 0.03 g of sodium fluoride, 5 to 20 g of sodium bicarbonate, 10 to 30 g of glycerol, sodium lauryl sulfate 0.3 Dough is prepared by mixing ˜0.7 g and 0.3-2 g of spearmint oil. At this time, the degree of dough can be adjusted by adding or subtracting the salt solution. Spearmint oil used as fragrance may not be used, in which case the rosin scent is dark.

As mentioned above, according to the present invention, in obtaining a pine salt solution, a pine salt solution is obtained in an aqueous state by emulsifying the rosin while dissolving the salt in water without heat-adsorbing a mixture of salt and rosin, thereby obtaining the pine salt solution. Using to prepare pine salt, pine salt ointment and pine salt toothpaste.

The pine salt solution prepared according to the present invention may be variously applied depending on the utilization method. For example, it is effective to heal wounds and pains in the oral cavity, and the pineal salt obtained by drying the pineal salt solution may be used for skin wounds or athlete's foot, and may be applied to the preparation of toothpaste.

Although described above with reference to a preferred embodiment of the present invention, those skilled in the art will be variously modified and changed within the scope of the invention without departing from the spirit and scope of the invention described in the claims below. I can understand that you can.

Claims (8)

The pulverized rosin is prepared in a salt water at room temperature with a predetermined surfactant and then emulsified to have a particle diameter of 3,000 kPa or less using ultrasonic waves. The method of claim 1, wherein the surfactant is made of sorbitan trioleate. A method for producing a pine salt solution, characterized in that the pulverized rosin is added to a salt water at room temperature with a predetermined surfactant and then emulsified to have a particle diameter of 3,000 kPa or less while spraying using a nozzle. The method of claim 3, wherein the surfactant is sorbitan trioleate (Sorbitan Trioleate). The pulverized rosin is added to a salt water at room temperature with a predetermined surfactant and emulsified to have a particle diameter of 3,000 Å or less using ultrasonic waves to make a pine salt solution, and the pine salt solution is spray dried to prepare a fine powder. Method for producing pine salt. The pulverized rosin is added to a salt water at room temperature with a predetermined surfactant and emulsified to have a particle diameter of 3,000 kΩ or less using ultrasonic waves to form a pine salt solution, and the pine salt solution is spray-dried to obtain a pine salt. Or a method for producing a pine salt ointment, characterized in that the mixture is prepared with glycerol. The pulverized rosin is added to a salt water at room temperature with a predetermined surfactant and emulsified to have a particle diameter of 3,000 kPa or less using ultrasonic waves to form a pine salt solution. Glycerol, Sodium Lauryl Sulfate (Sodium Lauryl Sulfate) A method for producing a toothpaste, characterized in that in the form of dough by mixing. 8. The method of claim 7, wherein when the dough is prepared, spearmint oil is additionally mixed with the pine salt solution as a fragrance.