KR100285929B1 - Method for producing aromatic adhesive - Google Patents

Method for producing aromatic adhesive Download PDF

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Publication number
KR100285929B1
KR100285929B1 KR1019970042046A KR19970042046A KR100285929B1 KR 100285929 B1 KR100285929 B1 KR 100285929B1 KR 1019970042046 A KR1019970042046 A KR 1019970042046A KR 19970042046 A KR19970042046 A KR 19970042046A KR 100285929 B1 KR100285929 B1 KR 100285929B1
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KR
South Korea
Prior art keywords
water
adhesive
solution
soluble
fragrance
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KR1019970042046A
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Korean (ko)
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KR19990018811A (en
Inventor
임세호
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임세호
주식회사세원화학
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Priority to KR1019970042046A priority Critical patent/KR100285929B1/en
Publication of KR19990018811A publication Critical patent/KR19990018811A/en
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Publication of KR100285929B1 publication Critical patent/KR100285929B1/en

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

PURPOSE: Provided is a method for producing aromatic adhesive, which exudes an aroma for a long time when is applied to object, and which can be used as adhesives for numerous stationery and impart a pleasant feeling to the user. CONSTITUTION: The method comprises the steps of (i) adding about 7-10 g of emulsifier and 400 g of water to 100 g of aromatics to obtain mixture; (ii) stirring the mixture in a speed of 5000 rpm at 50-60deg.C for 30 minutes to form a milkwhite solution; (iii) adding an alcohol to the milkwhite solution in amount corresponding to a half of that of the aromatics and stirring the solution at room temperature; (iv) mixing the solution with 17 g of water to obtain an aqueous solution, one hour after stirring; (v) mixing the aqueous solution with water soluble adhesive in the ratio of 1:1 or 1:10 at room temperature.

Description

향수 접착제 제조법Perfume glue recipe

본 발명은 수용성 향수 접착제 제조 방법에 관한 것이다. 물체에 향기를 내게할 때 향료단체(香料單體)로 쓰이는 것이 아니라 이들을 조합한 것을 쓰게 되는데 모든 공업용 향료는 거의 오일(OIL)로 되어 있어서 물성면에서 수용성 접착제와 조합되지 아니하므로 수용성 접착제에 향기를 내기가 어려웠고 간혹 앨범 등에 향기를 내게 하기 위하여 향료가 묻은 거즈를 앨범 표지 이면에 대고 셀로판지를 덮어 씌웠거나 분말 또는 방향제가 도포된 물체를 장식구에 넣어서 향기를 발산케한것 등도 있으나 이 경우에는 방향제에 혼가된 알코올 성분에 의하여 향기가 빨리 발산되어 그 효과를 발휘못할 뿐만 아니라 모양새도 좋지 못하였다.The present invention relates to a method for producing a water-soluble perfume adhesive. When fragrance is given to objects, it is not used as a fragrance group, but a combination of them. All industrial fragrances are almost oils and are not combined with water-soluble adhesives in terms of physical properties. In some cases, the gauze with fragrance was put on the back of the album cover to cover the album cover, or the powder or fragrance-coated object was put on the ornament to give off the fragrance. The fragrance quickly dissipated by the alcohol component mixed with the fragrance, not only exerting the effect but also the appearance was not good.

본 발명은 이와 같은 문제점을 해소하기 위하여 유용성 방향제를 유화제와 알코올로 처리하여 수용성으로 변환시킨 것을 수용성 접착제와 한데 섞어서 조합하여 조성한 것으로 이하 본 발명을 상세하게 설명하면 다음과 같다.In order to solve such a problem, the present invention is described in detail by mixing the oil-soluble fragrance with water-soluble adhesive and converting the oil-soluble fragrance into water-soluble adhesive.

방향제 100g(비중기준g/단위)에 유화제 약 7-10g와 물(H2O) 400g을 주가하여 50-60℃에서 r.p.m. 5000이상의 고속 회전으로 약 30분간 교반하여 유백색의 용액을 얻은 다음 이 유백색 용액에 알코올을 방향제의 약 1/2(50g) 정도 투입하여 교반하고 1-2시간 경과후에 물(H2O)17g과 혼합하여 수용성으로 변환시킨 것을 수용성 접착제와 상온에서 1:1 또는 1:10비율로 섞어서 조합하여 조성된 향수 접착제 제조법이다.Add about 7-10g of emulsifier and 400g of water (H 2 O) to 100g (specific gravity g / unit) of fragrance, and stir for about 30 minutes at a high speed rotation of rpm 5000 at 50-60 ℃ to obtain milky white solution. About 1/2 (50 g) of alcohol was added to the solution and stirred. After 1-2 hours, the mixture was mixed with 17 g of water (H 2 O) and converted to water-soluble 1: 1 or 1: at room temperature. It is a fragrance adhesive preparation formulated by mixing at a ratio of 10.

본 발명의 작용 효과를 설명하면 다음과 같다.The operational effects of the present invention are described as follows.

모든 공업용 향료는 거의 오일로 되어 있기 때문에 물성상 수용성 접착제와 조합이 이루어지지 아니하므로 수용성으로 변화시켜야 하는데 이때 계면활성제 등 유화제를 투여하므로서 서로 혼합되지 아니하는 2종의 액체 즉 유용성의 방향제와 수용성의 접착제가 안정된 에멀전으로 변환되고 독성이 없는 알코올을 투여하므로서 에멀전의 수용성을 돕는 작용을 한다.Since all industrial fragrances are almost oils, they cannot be combined with water-soluble adhesives in their physical properties, so they must be changed to water-soluble. At this time, two types of liquids that are not mixed with each other by administering emulsifiers such as surfactants, that is, oil-soluble fragrances and water-soluble The adhesive converts into a stable emulsion and acts to help the emulsion's solubility by administering nontoxic alcohol.

이와 같은 유용성 방향제를 수용성으로 변화된 것을 통상적인 앨범용 대지 코팅용 접착제, PVAC접착제(초산비닐수지), EVA접착제(에틸렌, 초산비닐공중합체), 아크릴수지계접착제, 에폭시수지계접착제, 천연고무 라텍스, 합성고무 라텍스 등에 혼합하여 사용하면 된다.Such oil-soluble fragrances were converted into water-soluble adhesives for general album coating, PVAC adhesive (vinyl acetate resin), EVA adhesive (ethylene, vinyl acetate copolymer), acrylic resin adhesive, epoxy resin adhesive, natural rubber latex, synthetic It is good to mix and use rubber latex.

[실시예]EXAMPLE

제1공정 : 방향제 100 g(비중기준 g/단위)에 분자량 약 10 ㏖ 정도의 계면활성제(noigen) 약 7-10%와 물(H2O) 400g을 주가하여 50-60℃에서 5000의 r.p.m. 으로 약 30분간 교반하여 유백색 용액을 얻는다.The first step: 100 g of fragrance (specific gravity g / unit), added about 7-10% of a surfactant (noigen) and 400 g of water (H 2 O) with a molecular weight of about 10 mol and 5000 rpm at 50-60 ° C. Stir for about 30 minutes to obtain a milky white solution.

제2공정 : 제1공정에서 얻어진 유백색 용액에 알코올 약 1/2 (50g) 투입하여 상온에서 교반한 다음 1시간 경과후에 물 17g 을 주가하여 혼합하여 수용성으로 변환시킨다.Second step: About 1/2 (50 g) of alcohol is added to the milky white solution obtained in the first step, stirred at room temperature, and after 1 hour, 17 g of water is added and mixed to convert into water-soluble.

제3공정 : 제2공정에서 얻어진 수용성 방향제를 수용성 접착제와 상온에서 1:1 또는 1:10으로 섞어서 조합하여 향수 접착제를 조성한다.Third step: The water-soluble fragrance obtained in the second step is mixed with a water-soluble adhesive at room temperature 1: 1 or 1:10 to form a perfume adhesive.

이상과 같이 본 발명은 앨범용 접착제, 문방구용 접착제, 스캇치 테이프용 접착제, 파스용 접착제, 스티카용 접착제, 천연고무 라텍스 접착제 및 합성고무 라텍스 접착제 등에 사용하므로서 사용자에게 신선한 쾌감을 주고 방향을 즐길 수 있는 매우 유용한 것이다.As described above, the present invention can be used to provide a fresh feeling to the user by using an adhesive for an album, an adhesive for stationery, an adhesive for a tape tape, an adhesive for a paste, an adhesive for a stick, a natural rubber latex adhesive and a synthetic rubber latex adhesive. That would be very useful.

Claims (1)

방향제 100g(비중기준 g/단위)에 유화제 약 7-10g와 물(H2O) 400g을 주가하여 50-60℃에서 고속 r.p.m. 5000이상으로 약 30분 교반하여 얻어진 유백색 용액에 알코올을 방향제의 1/2(50g) 정도 투입하여 상온에서 교반하고 약 1시간 경과후에 물 17g을 혼합하여 수용성으로 변환시킨 것을 수용성 접착제와 상온에서 1:1 또는 1:10으로 섞어서 조합하여 조성함을 특징으로 하는 향수 접착제 제조법.Alcohol was added to the milky white solution obtained by adding about 7-10 g of emulsifier and 400 g of water (H 2 O) to 100 g (specific gravity g / unit) of fragrance and stirring it at a high speed rpm 5000 or more at 50-60 ° C. for about 30 minutes. / 2 (50g) was added at about room temperature, stirred at about 1 hour after mixing 17g of water to convert to water-soluble perfume and a composition comprising a mixture of water-soluble adhesives and 1: 1 or 1:10 at room temperature Adhesive recipe.
KR1019970042046A 1997-08-28 1997-08-28 Method for producing aromatic adhesive KR100285929B1 (en)

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KR1019970042046A KR100285929B1 (en) 1997-08-28 1997-08-28 Method for producing aromatic adhesive

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KR100285929B1 true KR100285929B1 (en) 2001-04-16

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20020032446A (en) * 2002-01-23 2002-05-03 김도연 Paste having a color and a perfume and method of the same

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100405336B1 (en) * 2001-07-26 2003-11-12 손경옥 Adhesive of transfered perform and Manufacturing method

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR900016411A (en) * 1989-04-25 1990-11-13 백재덕 Method for producing gel type gelatin adhesive and composition thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR900016411A (en) * 1989-04-25 1990-11-13 백재덕 Method for producing gel type gelatin adhesive and composition thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20020032446A (en) * 2002-01-23 2002-05-03 김도연 Paste having a color and a perfume and method of the same

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