JPWO2018012477A1 - Micro-foamed beverage and method for producing the same - Google Patents

Micro-foamed beverage and method for producing the same Download PDF

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JPWO2018012477A1
JPWO2018012477A1 JP2018527605A JP2018527605A JPWO2018012477A1 JP WO2018012477 A1 JPWO2018012477 A1 JP WO2018012477A1 JP 2018527605 A JP2018527605 A JP 2018527605A JP 2018527605 A JP2018527605 A JP 2018527605A JP WO2018012477 A1 JPWO2018012477 A1 JP WO2018012477A1
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beverage
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specific gravity
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JP6744407B2 (en
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研一朗 山本
研一朗 山本
祐子 四元
祐子 四元
貴史 塩野
貴史 塩野
智弘 豊澤
智弘 豊澤
宏 寺田
宏 寺田
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Kirin Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation

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Abstract

本発明は、これまで実現されたことがない「泡融け感」が付与された新規な微細泡飲料の提供をその目的とする。本発明によれば、ゾル比重が0.85以下であり、かつ、分離速度が0.7mm/秒以下である、微細泡飲料(ここで、「ゾル比重」は一定容量の非微細泡飲料の質量に対する一定容量の微細泡飲料の質量の比率をいい、「分離速度」は微細泡飲料を評価用容器に注いだときの、容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離(mm)から容器満注時の容器底から微細な泡の最も低い位置までの垂直距離(mm)を引いた値を100秒で除した値をいう)が提供される。飲料は好ましくは清涼飲料である。  An object of the present invention is to provide a novel micro-foamed beverage having a "feeling of melting" which has never been realized. According to the present invention, a microfoam beverage having a sol specific gravity of 0.85 or less and a separation speed of 0.7 mm / sec or less (herein, “sol specific gravity” is a non-microfoam beverage of a fixed volume The ratio of the mass of a fixed volume micro bubble beverage to the mass, "separation speed" is the most of fine bubbles from the bottom of the container 100 seconds after the full filling of the container when the micro foam beverage is poured into the evaluation container The vertical distance (mm) to the lower position minus the vertical distance (mm) from the bottom of the container to the lowest position of the fine foam when the container is full is the value divided by 100 seconds) . The beverage is preferably a soft drink.

Description

関連出願の参照Reference to related applications

本願は、先行する日本国出願である特願2016−137250(出願日:2016年7月12日)の優先権の利益を享受するものであり、その開示内容全体は引用することにより本明細書の一部とされる。   This application claims the benefit of the priority of prior Japanese Patent Application No. 2016-137250 (filing date: July 12, 2016), the entire disclosure of which is incorporated herein by reference. Be part of

本発明は新規な微細泡飲料およびその製造方法に関する。   The present invention relates to a novel microfoam beverage and a method for producing the same.

清涼飲料やアルコール飲料においては、飲用者が泡の感触を楽しむことができるものが市場において好まれている。代表的なものとしては炭酸飲料が挙げられ、これらは飲用時に二酸化炭素の気泡に伴う刺激的な感触を楽しむことができる。   Among soft drinks and alcoholic beverages, those that allow a drinker to enjoy the feel of foam are preferred in the market. Representative ones are carbonated beverages, which can enjoy the irritating feel associated with the bubbles of carbon dioxide when drinking.

一方で、各種の起泡剤の添加や、窒素ガスと飲料液の混合により滑らかな感触の起泡の飲料を提供することが試みられている。このような飲料はいずれも液面上に形成された泡(フォーム)の大きさを細かくすることによってより滑らかな泡の飲料を提供しようとしている(特許文献1)。しかし、液面のみならず飲料全体が微細な泡を含む溶液から構成された飲料はこれまで知られていなかった。   On the other hand, attempts have been made to provide a smooth-feeling foamy beverage by the addition of various foaming agents and the mixing of nitrogen gas and a beverage liquid. Such beverages are all trying to provide a smoother foam beverage by reducing the size of foam formed on the liquid surface (Patent Document 1). However, a beverage composed of a solution containing not only the liquid level but also the whole beverage containing fine foam has hitherto been unknown.

特開2016−59372号公報JP, 2016-59372, A

本発明者らは今般、飲料における泡の感触は、液面に形成された泡のみならず、液中に形成された気泡も重要な役割を果たしていることを新たに見出した。すなわち、飲料全体が微細な泡で構成されるように混合処理して得られた飲料が、従来の飲料では実現されたことがない「泡融け感」を有することを見出し、本発明を完成させた。   The inventors of the present invention have now newly found that not only the foam formed on the liquid surface but also the foam formed in the liquid play an important role in the feeling of foam in the beverage. That is, it is found that the beverage obtained by mixing processing so that the whole beverage is composed of fine bubbles has a "foaming feeling" which has not been realized in the conventional beverage, and the present invention is completed. The

すなわち、本発明はこれまで実現されたことがない「泡融け感」が付与された新規な微細泡飲料とその製造方法を提供することを目的とする。   That is, an object of the present invention is to provide a novel micro-foamed beverage to which a "foam melt feeling" has been imparted which has never been realized, and a method for producing the same.

本発明によれば以下の発明が提供される。
[1]ゾル比重が0.85以下であり、かつ、分離速度が0.7mm/秒以下である、微細泡飲料(ここで、「ゾル比重」は一定容量の非微細泡飲料の質量に対する一定容量の微細泡飲料の質量の比率をいい、「分離速度」は微細泡飲料を評価用容器に注いだときの、容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離(mm)から容器満注時の容器底から微細な泡の最も低い位置までの垂直距離(mm)を引いた値を100秒(s)で除した値をいう)。
[2]液粘度が2.5mPa・s以下である、上記[1]に記載の微細泡飲料。
[3]飲料が清涼飲料である、上記[1]または[2]に記載の微細泡飲料。
[4]飲料液を3000〜50000rpm、1秒〜60分の条件で混合する工程を含んでなる、微細泡飲料の製造方法。
[5]製造された飲料のゾル比重(ここで、ゾル比重は上記[1]で定義された内容と同義である)が0.85以下である、上記[4]に記載の製造方法。
[6]製造された飲料の分離速度(ここで、分離速度は上記[1]で定義された内容と同義である)が0.7mm/秒以下である、上記[4]または[5]に記載の製造方法。
[7]製造された飲料の液粘度が2.5mPa・s以下である、上記[4]〜[6]のいずれかに記載の製造方法。
[8]窒素を含有する気体の存在下で混合を行う、上記[4]〜[7]のいずれかに記載の製造方法。
[9]飲料が清涼飲料である、上記[4]〜[8]のいずれかに記載の製造方法。
[10]上記[4]〜[9]のいずれかに記載の製造方法により製造された、微細泡飲料。
According to the present invention, the following inventions are provided.
[1] A microfoam beverage having a sol specific gravity of 0.85 or less and a separation speed of 0.7 mm / sec or less (here, “sol specific gravity” is constant with respect to the mass of a fixed volume of non-microfoam beverage The ratio of the mass of microfoamed beverage in the volume, "separation speed" is the lowest position of the microfoam from the bottom of the container to the lowest position 100 seconds after the full filling of the container when the microfoamed beverage is poured into the evaluation container The value obtained by subtracting the vertical distance (mm) from the bottom of the container to the lowest position of the fine bubbles when the container is full is divided by 100 seconds (s)).
[2] The microfoam beverage according to the above [1], which has a liquid viscosity of 2.5 mPa · s or less.
[3] The micro-foamed beverage according to the above [1] or [2], wherein the beverage is a soft drink.
[4] A method for producing a microfoam beverage, comprising the steps of mixing the beverage under conditions of 3000 to 50000 rpm for 1 second to 60 minutes.
[5] The method according to the above [4], wherein the sol specific gravity of the manufactured beverage (herein, the sol specific gravity is the same as the content defined in the above [1]) is 0.85 or less.
[6] In the above [4] or [5], the separation speed of the manufactured beverage (here, the separation speed is the same as the contents defined in the above [1]) is 0.7 mm / sec or less Manufacturing method described.
[7] The method according to any one of the above [4] to [6], wherein the liquid viscosity of the manufactured beverage is 2.5 mPa · s or less.
[8] The production method according to any one of the above [4] to [7], wherein the mixing is performed in the presence of a nitrogen-containing gas.
[9] The method according to any one of the above [4] to [8], wherein the beverage is a soft drink.
[10] A microfoam beverage manufactured by the method according to any one of the above [4] to [9].

本発明の微細泡飲料は飲料全体が微細な泡を含む溶液で構成され、飲用者はこれまで経験したことがない「泡融け感」を楽しむことができる。すなわち、本発明は従来にはない飲用感を有する飲料を提供するものであり、消費者の新たな嗜好やニーズに応えることができる点で有利である。   The micro-foamed beverage of the present invention is composed of a solution in which the whole beverage contains fine foams, and the drinker can enjoy the "feeling of melting" which has never been experienced. That is, the present invention is to provide a drink having an unprecedented feeling of drinking, and is advantageous in that it can meet new tastes and needs of consumers.

図1Aは混合処理前のコーヒー飲料を容器に満注した写真である。FIG. 1A is a photograph in which a coffee beverage before mixing processing is filled in a container. 図1Bは気体との混合処理後のコーヒー飲料を容器に満注した後、容器満注時から数秒後の試験区1の飲料の写真である。FIG. 1B is a photograph of the beverage in Test Zone 1 several seconds after the full filling of the container after fully filling the container with the coffee beverage after mixing treatment with gas. 図1Cは気体との混合処理後のコーヒー飲料を容器に満注した後、容器満注時から100秒経過後の試験区1の飲料の写真である。FIG. 1C is a photograph of the beverage in Test Zone 1 after 100 seconds have elapsed since the container was fully filled after the coffee beverage after mixing processing with gas was fully filled in the container.

発明の具体的説明Detailed Description of the Invention

本発明の微細泡飲料は、飲料中に微細な泡が形成されてなる飲料である。飲料中に微細な泡が形成されることにより、後述するような「泡融け感」が飲料に付与されることから、本発明の飲料は所定量の気泡を含むことを特徴とし、飲料中の気泡量は脱泡処理に付されて微細な泡が消失した脱泡処理後の微細泡飲料(非微細泡飲料)に対する本発明の飲料の比重(ゾル比重)により特定することができる。   The microfoam beverage of the present invention is a beverage in which fine foam is formed in the beverage. The formation of fine bubbles in the beverage imparts to the beverage a "feeling of melting" as described later, so that the beverage of the present invention is characterized by containing a predetermined amount of air bubbles, The amount of bubbles can be specified by the specific gravity (sol specific gravity) of the beverage of the present invention with respect to the defoamed fine-bubble beverage (non-fine-foamed beverage) subjected to defoaming treatment and the fine bubbles disappeared.

本発明において「ゾル比重」とは、一定容量の非微細泡飲料の質量(g)に対する一定容量の微細泡飲料の質量(g)の比率をいう。ゾル比重は同一体積で比較した場合にどの程度気泡を含む飲料であるかを示す指標ということができ、ゾル比重が小さい微細泡飲料はより多量の気泡を含む飲料ということができる。本発明の微細泡飲料のゾル比重は0.85以下とすることができ、好ましくは0.80以下、より好ましくは0.40〜0.80、さらに好ましくは0.50〜0.80である。   In the present invention, “sol specific gravity” refers to the ratio of the mass (g) of a fixed volume of microfoamed beverage to the mass (g) of a fixed volume of non-microfoamed beverage. The sol specific gravity can be said to be an index indicating how much the beverage contains bubbles when compared in the same volume, and the microfoam beverage having a low sol specific gravity can be said to be a beverage containing a larger amount of bubbles. The sol specific gravity of the microfoam beverage of the present invention can be 0.85 or less, preferably 0.80 or less, more preferably 0.40 to 0.80, still more preferably 0.50 to 0.80. .

本発明の微細泡飲料においてゾル比重を算出する場合には、まず、微細泡飲料の製造完了後、直ちに一定容量当たりの質量を測定し、次いで、微細泡飲料を適切な方法で脱泡処理に付し、脱泡後の飲料(非微細泡飲料)の一定容量当たりの質量を測定し、これらの測定値に基づいてゾル比重を算出することができる。脱泡処理は、例えば減圧脱泡や遠心エバポレーター、真空撹拌脱泡装置などを使用することができる。   In the case of calculating the sol specific gravity in the microfoam beverage of the present invention, first, after the completion of the production of the microfoam beverage, the mass per fixed volume is measured, and then the microfoam beverage is defoamed by an appropriate method. It is possible to measure the mass per fixed volume of the defoamed beverage (non-microfoam beverage) and calculate the sol specific gravity based on these measured values. For the degassing treatment, for example, a vacuum degassing, a centrifugal evaporator, a vacuum stirring degassing apparatus or the like can be used.

本発明の微細泡飲料は、飲料中に微細な泡を形成させることにより飲料中に気体を含有する飲料である。微細な泡を構成する気体としては窒素を含有する気体(例えば、空気)および窒素ガスが挙げられ、好ましくは窒素を含有する気体であり、より好ましくは空気である。   The microfoam beverage of the present invention is a beverage containing gas in the beverage by forming fine bubbles in the beverage. Gases that constitute fine bubbles include nitrogen-containing gases (for example, air) and nitrogen gas, preferably nitrogen-containing gases, and more preferably air.

本発明の微細泡飲料は、製造直後は飲料のほぼ全体が微細な泡から構成されているが、時間が経過するにつれ、微細な泡から構成される部分と微細な泡を含まない部分の二つの部分に徐々に分離する。このため本発明の飲料は微細な泡から構成される部分が微細な泡を含まない部分に分離する速度(分離速度)により特定することができる。   The micro-foamed beverage of the present invention is almost entirely composed of fine foam immediately after production, but as time passes, it is divided into two parts, one composed of fine foam and the other without fine foam. Gradually separate into two parts. For this reason, the beverage of the present invention can be identified by the speed (separation speed) at which the portion composed of fine foams is separated into the fine foam-free portion.

本発明において「分離速度」(mm/秒)とは本発明の微細泡飲料を評価用容器に注いだときの、容器満注時から100秒後の容器底から微細泡の最も低い位置までの垂直距離(mm)から容器満注時の容器底から微細な泡の最も低い位置までの垂直距離を引いた値を100秒(s)で除した値をいう。分離速度を測定する際には本発明の微細泡飲料を製造完了後、直ちに空の評価用容器に注いで、容器が満量になった時点と容器満注から100秒後の微細泡の最低位置を容器底から計測する。容器に既に飲料が存在する場合には、該飲料を除いてから計測を行うことはいうまでもないが、仮に該飲料が存在したまま計測を行う場合には、該飲料の液面から微細泡の最も低い位置までの距離を計測する。また、製造完了時にすべての原料飲料液が微細な泡に変化せず、該飲料液が残存していることがあり、該飲料液が評価用容器に注がれることがあるが、このような場合には製造完了時に残存している原料飲料液のうち評価容器に注がれた飲料液の体積分を垂直距離から差し引くことで、分離速度をより正確に算出することができる。   In the present invention, “separation speed” (mm / sec) means the distance from the bottom of the container to the lowest position of the micro bubbles 100 seconds after the full filling of the container when the microfoam beverage of the present invention is poured into the evaluation container. The value obtained by subtracting the vertical distance from the bottom of the container from the bottom of the container to the lowest position of the fine bubbles when the container is full is divided by 100 seconds (s). When measuring the separation speed, the microfoam beverage of the present invention is poured into an empty evaluation container immediately after the production is completed, and the minimum amount of microfoam after 100 seconds from when the container is fully filled when the container is full Measure the position from the bottom of the container. It goes without saying that if a beverage already exists in the container, the measurement is carried out after removing the beverage, but if the measurement is carried out with the beverage still present, micro bubbles from the liquid surface of the beverage Measure the distance to the lowest position of In addition, when the production is completed, all the raw beverage liquids do not change into fine foams, and the beverage liquid may remain, and the beverage liquid may be poured into the evaluation container. In this case, the separation speed can be calculated more accurately by subtracting the volume of the beverage liquid poured into the evaluation container among the raw beverage liquids remaining at the completion of production from the vertical distance.

分離速度の測定に使用する評価用容器は、容器の材質や口径による測定値のぶれを防ぐため、分離速度評価用ガラス(容量300mL、φ52mm、高さ140mm)を使用する。上記の分離速度評価用ガラス以外の容器を使用して分離速度を測定した場合には、得られた分離速度を該容器の口径と高さに基づいて分離速度評価用ガラスでの測定値に換算することができる。分離速度を測定する場合にはまた、容器内で最も低い位置に存在する微細泡の位置を正確に測定するため、色評価用蛍光ランプなどの照明装置を使用することが好ましい。分離速度は一定時間内にどの程度の速さで微細泡飲料から微細泡を含まない飲料液に変化するかを示す指標ということができ、分離速度が小さい飲料は微細泡飲料の状態をより長く維持できる飲料ということができる。本発明の微細泡飲料の分離速度は0.7mm/秒以下とすることができ、好ましくは0.68mm/秒以下、より好ましくは0.6mm/秒以下である。また、本発明の微細泡飲料の分離速度は0.05mm/秒以上とすることができ、好ましくは0.1mm/秒以上である。本発明の微細泡飲料の分離速度は、0.05〜0.7mm/秒とすることができ、好ましくは0.1〜0.6mm/秒である。   The evaluation container used to measure the separation speed uses glass for evaluation of the separation speed (volume 300 mL, φ 52 mm, height 140 mm) in order to prevent blurring of measured values due to the material and diameter of the container. When the separation speed is measured using a container other than the above-mentioned separation speed evaluation glass, the obtained separation speed is converted into a measurement value with the separation speed evaluation glass based on the diameter and height of the container. can do. In the case of measuring the separation speed, it is preferable to use a lighting device such as a color evaluation fluorescent lamp in order to accurately measure the position of the micro bubbles present at the lowest position in the container. The separation speed can be considered as an index indicating how quickly the microfoamed beverage changes to the microfoam-free beverage liquid within a certain time, and the beverage with a small separation speed has a longer state of microfoamed beverage It can be called a drink that can be maintained. The separation speed of the microfoam beverage of the present invention can be 0.7 mm / sec or less, preferably 0.68 mm / sec or less, more preferably 0.6 mm / sec or less. Moreover, the separation speed of the microfoam beverage of the present invention can be 0.05 mm / sec or more, preferably 0.1 mm / sec or more. The separation speed of the microfoam beverage of the present invention can be 0.05 to 0.7 mm / sec, preferably 0.1 to 0.6 mm / sec.

本発明の微細泡飲料は、微細泡飲料を評価用容器に注いだときの、容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離を90mm以下とすることができ、好ましくは70mm、より好ましくは50mmとすることができる。   The microfoam beverage of the present invention has a vertical distance of 90 mm or less from the bottom of the container to the lowest position of the microbubble 100 seconds after the full filling of the container when the microfoam beverage is poured into the evaluation container And preferably 70 mm, more preferably 50 mm.

本発明の微細泡飲料は、市販の炭酸飲料などと比較すると微細な泡が消失しにくい飲料ということができる。飲料中に消泡効果を有する成分が含まれていると、微細な泡が消失する速度が速くなることから、本発明の微細泡飲料は消泡成分の含有量が0.01%以下、好ましくは0.001%以下の飲料とすることができ、より好ましくは消泡成分を実質的に含まない飲料である。ここで、消泡成分としては、乳化剤、シリコーン系消泡剤、液状油が挙げられる。   The micro-foamed beverage of the present invention can be said to be a beverage in which fine bubbles are less likely to disappear as compared with commercially available carbonated beverages and the like. If the beverage has a component having an antifoaming effect, the rate of disappearance of the fine foam is increased, so the content of the antifoaming component of the microfoam beverage of the present invention is preferably 0.01% or less, Is a beverage that can be 0.001% or less, and more preferably, substantially free of the antifoam component. Here, as a defoaming component, an emulsifier, a silicone type antifoamer, and a liquid oil are mentioned.

本発明の微細泡飲料において分離速度を算出する場合には、微細泡飲料を製造後、直ちに透明または半透明の容器に注ぎ、製造完了時から100秒後の容器底から微細な泡の最も低い位置までの距離を目視で測定し、その距離(mm)を100秒で割ることにより分離速度を算出することができる。   In the case of calculating the separation speed in the microfoam beverage of the present invention, the microfoam beverage is immediately poured into a transparent or translucent container after production, and the lowest of the microfoam from the bottom of the container 100 seconds after the completion of production The separation velocity can be calculated by visually measuring the distance to the position and dividing the distance (mm) by 100 seconds.

本発明の微細泡飲料はまた、液粘度により特定することができる。本発明の微細泡飲料において液粘度を算出する場合には、微細泡飲料を適切な方法で脱泡処理に付し、脱泡後の飲料(非微細泡飲料)について液粘度を測定することができる。脱泡処理は、例えば減圧脱泡や遠心エバポレーター、真空撹拌脱泡装置などを使用することができる。液粘度は例えば落球式粘度測定法により測定することができ、落球式マイクロ粘度計(アントンパール社製)などの市販の測定機器を用いて測定をすることができる。本発明の微細泡飲料の液粘度は2.5mPa・s以下とすることができ、好ましくは2.2mPa・s以下、より好ましくは0.7〜2.2mPa・sである。   The microfoam beverage of the present invention can also be identified by liquid viscosity. In the case of calculating the liquid viscosity in the microfoam beverage of the present invention, the microfoam beverage may be subjected to a defoaming treatment by an appropriate method, and the liquid viscosity may be measured for the defoamed beverage (non-microfoam beverage) it can. For the degassing treatment, for example, a vacuum degassing, a centrifugal evaporator, a vacuum stirring degassing apparatus or the like can be used. The liquid viscosity can be measured by, for example, a falling ball viscosity measurement method, and can be measured using a commercially available measuring device such as a falling ball micro viscometer (manufactured by Anton Paar Co., Ltd.). The liquid viscosity of the microfoam beverage of the present invention can be 2.5 mPa · s or less, preferably 2.2 mPa · s or less, and more preferably 0.7 to 2.2 mPa · s.

本発明の微細泡飲料は上記のように2.5mPa・s以下の液粘度をとることができるが、市販のスムージー飲料などと比較すると粘度が十分低い飲料ということができる。本発明の微細泡飲料はまた、流動性を十分に持ち、飲用に適した液性を有する。   The micro-foamed beverage of the present invention can have a liquid viscosity of 2.5 mPa · s or less as described above, but it can be said that the beverage has a sufficiently low viscosity as compared with commercially available smoothie beverages and the like. The micro-foamed beverage of the present invention is also sufficiently fluid and has liquid properties suitable for drinking.

本発明の微細泡飲料のベースとなる飲料液は微細な泡を形成させることができる限り、特に限定されるものではなく、清涼飲料、アルコール飲料、果汁飲料、乳飲料、野菜汁飲料などが挙げられる。清涼飲料としては、コーヒー飲料、緑茶飲料、紅茶飲料、酸性飲料、炭酸飲料、乳清飲料などが挙げられ、好ましくは、ビールテイスト飲料を除くものである。アルコール飲料は好ましくは、麦汁を含有するビールテイスト飲料を除くものである。   The beverage used as the base of the micro-foamed beverage of the present invention is not particularly limited as long as it can form fine foams, and includes soft drinks, alcoholic drinks, fruit juice drinks, milk drinks, vegetable juice drinks, etc. Be As a soft drink, a coffee drink, a green tea drink, a black tea drink, an acidic drink, a carbonated drink, a whey drink etc. are mentioned, Preferably, a beer taste drink is remove | excluded. The alcoholic beverage is preferably a beer-taste beverage containing wort.

本発明の微細泡飲料は従来の飲料では実現されたことがない「泡融け感」を有する。すなわち、本発明の飲料を摂取した場合には以下の3つの飲用感が得られる。
(A)口腔内に十分な気泡が含有された飲料を含むことで、さらさらとした溶液が気泡を含んで軽くエアリーな食感が得られる。含んだ気泡は弾性がなく柔らかい。
(B)口腔内に含んだ気泡は、飲用中に発泡し弾けることなく口腔内で静かに消失し、溶液としての流動性を十分に感じることができる
(C)嚥下後に口腔内での後残りがなく、優しく、刺激が少ないためごくごくと飲用できる。
The microfoam beverage of the present invention has a "feeling of melting out" which has not been realized in conventional beverages. That is, when the beverage of the present invention is ingested, the following three feeling of drinking can be obtained.
(A) By containing the beverage in which sufficient air bubbles are contained in the oral cavity, the free flowing solution contains air bubbles so that a light and airy texture can be obtained. The contained air bubbles are not elastic and soft.
(B) The bubbles contained in the oral cavity foam and disappear gently while drinking, and can be gently dissipated in the oral cavity, and the fluidity as a solution can be sufficiently felt. (C) The remaining residue in the oral cavity after swallowing Because there is no, it is gentle, and it can be consumed extremely because of its low irritation.

本発明の微細泡飲料はまた、時間が経過するとともに微細な泡を含む飲料液と微細な泡が消失した飲料液とに徐々に分離するという特徴を有する(図1Bおよび図1C参照)。本発明の微細泡飲料は、飲料全体が微細な泡を含む溶液で構成された飲料のみならず、時間経過により微細な泡を含む飲料液と微細な泡が消失した飲料液とを含む飲料も包含するものとする。   The micro-foamed beverage of the present invention is also characterized in that it gradually separates into a beverage containing fine foam and a beverage from which fine foam has disappeared over time (see FIGS. 1B and 1C). The micro-foamed beverage according to the present invention is not only a beverage composed of a solution containing fine foams as a whole, but also a beverage containing a beverage containing fine foams and a beverage from which the fine foams have disappeared over time It shall be included.

本発明の微細泡飲料の製造方法は、原料となる飲料液に微細泡を形成させることができれば特に限定されないが、例えば、気体と飲料液とを混合することにより製造することができる。すなわち、飲料液を準備し、容器中で3000〜50000rpm、1秒〜60分の条件で混合し、飲料液中に微細泡を形成させて気体を飲料液中に取り込ませることで本発明の微細泡飲料を製造することができる。気体としては、窒素を含有する気体(例えば、空気)および窒素ガスが挙げられ、好ましくは窒素を含有する気体であり、より好ましくは空気である。   Although the manufacturing method of the micro-foamed drink of this invention will not be specifically limited if a micro-bubble can be formed in the drink liquid used as a raw material, For example, it can manufacture by mixing a gas and a drink liquid. That is, the beverage liquid is prepared, mixed in a container under conditions of 3000 to 50000 rpm and 1 second to 60 minutes, and fine bubbles are formed in the beverage liquid to incorporate gas into the beverage liquid. A foamy beverage can be produced. The gas includes a nitrogen-containing gas (eg, air) and a nitrogen gas, preferably a nitrogen-containing gas, more preferably air.

飲料液の混合は容器中で行うことができる。微細泡を構成する気体が空気である場合、容器中で飲料液を混合することにより本発明の微細泡飲料を製造することができる。容器中で上記の混合強度および混合時間で飲料液を混合する場合には、攪拌機や混合容器、気液混合機を用いて混合を行うことができる。具体的には、攪拌機としてはジューサーミキサー、ミキサー、フードプロセッサー、ブレンダ―、高速分散機を用いることができ、混合容器としてはシェーカー、気体混合用加圧容器を用いることができ、気液混合機としてはスプレーガン、二流体ノズル、エアーストーンを用いることができる。   The mixing of the beverage liquid can be carried out in a container. When the gas constituting the fine foam is air, the fine foam beverage of the present invention can be produced by mixing the beverage liquid in a container. When the beverage liquid is mixed in the container with the above mixing strength and mixing time, mixing can be performed using a stirrer, a mixing container, or a gas-liquid mixer. Specifically, as a stirrer, a juicer mixer, a mixer, a food processor, a blender, a high-speed disperser can be used, and as a mixing container, a shaker, a pressure container for gas mixing can be used, and a gas-liquid mixer As a spray gun, a two fluid nozzle, an air stone can be used.

製造された微細泡飲料はグラスやコップなどの容器に注がれ、飲用者に提供することができる。本発明の微細泡飲料は時間が経過すると、微細な泡から構成される部分と微細な泡を含まない部分に分離することから、上記(A)、(B)および(C)の作用効果をよりよく発揮させるために、製造完了後、直ちに容器に注ぎ、飲用者に提供することが望ましい。ここで、本発明の微細泡飲料を気体と飲料液とを混合することにより製造する場合は、原料飲料液の全量について混合が完了したことをもって製造完了とみなすことができる。   The micro-foamed beverage produced can be poured into a container such as a glass or a cup and provided to a drinker. Since the micro-foamed beverage of the present invention separates into a portion composed of fine bubbles and a portion free of fine bubbles over time, the effects of the above (A), (B) and (C) It is desirable to pour it into a container immediately after the completion of manufacture and provide it to the drinker for better performance. Here, when manufacturing the micro-foamed beverage of the present invention by mixing a gas and a beverage liquid, the completion of the mixing for the whole amount of the raw beverage liquid can be regarded as the production completion.

本発明の微細泡飲料は、製造完了時にすべての原料飲料液が微細な泡に変化せず、原料飲料液が残存していることがあるが、このような飲料も上記(A)、(B)および(C)の作用効果を発揮する限り本発明の微細泡飲料に包含される。   In the micro-foamed beverage of the present invention, all the raw beverage liquids do not change to fine foams when the production is completed, and the raw beverage liquids may remain, but such beverages also have the above-mentioned (A) and (B) And (C) is included in the microfoam beverage of the present invention as long as it exerts the effects.

以下の例に基づいて本発明をより具体的に説明するが、本発明はこれらの例に限定されるものではない。   The present invention will be more specifically described based on the following examples, but the present invention is not limited to these examples.

例1:微細泡飲料の製造および各種物性値の分析(1)
(1)飲料の調製
コーヒー飲料をベースとする微細泡飲料を調製した。具体的には、コーヒー豆(キリマンジャロ)をコーヒーミルで中挽きに粉砕し、ペーパーフィルターに粉砕したコーヒー豆100gを入れ、95℃の熱水で抽出した。ろ液1000gを採取したところで抽出を止め、1000gのコーヒー抽出液を得た。得られたコーヒー抽出液を20℃まで冷却して、該抽出液のpHが6.5になるように調製しながら炭酸水素ナトリウムを加え、イオン交換水を用いて全量を2000gとした(コーヒー調合液)。コーヒー調合液を90℃に加温し、飲料用スチール缶に190gを充填後、121℃、5分間でレトルト殺菌処理してブラックコーヒー飲料ベース(以下、「コーヒー飲料ベース1」ということがある)を調製した。
Example 1: Production of microfoam beverage and analysis of various physical property values (1)
(1) Preparation of Beverage A coffee beverage-based microfoam beverage was prepared. Specifically, coffee beans (Kilimanjaro) were ground to a ground in a coffee mill, and 100 g of ground coffee beans were put in a paper filter and extracted with hot water at 95 ° C. Extraction was stopped when 1000 g of filtrate was collected, and 1000 g of coffee extract was obtained. The obtained coffee extract was cooled to 20 ° C., sodium bicarbonate was added while adjusting the pH of the extract to be 6.5, and the total amount was adjusted to 2000 g using ion exchanged water (coffee preparation liquid). The coffee preparation is warmed to 90 ° C, and after filling 190g in a steel can for beverage, it is retort sterilized at 121 ° C for 5 minutes and black coffee beverage base (hereinafter sometimes referred to as "coffee beverage base 1") Was prepared.

上記のようにして調製したコーヒー飲料ベース1をあらかじめ液温が5℃になるように準備した。内径110mm、高さ130mmの円柱状のステンレス容器にコーヒー飲料ベース330gを入れ、液温が5℃〜10℃を保つよう保冷した。ハンディーフードプロセッサー(バーミックスM300、エスゲー社)にアタッチメント(ウイスク、エスゲー社)を装着し、アタッチメント先端をステンレス容器底部につけて「低速」で30秒間混合処理してコールドタイプの微細泡飲料(試験区1)を調製した。製造完了時にコーヒー飲料液のすべてが微細な泡が形成された飲料に変化していることを目視で確認した。   The coffee beverage base 1 prepared as described above was prepared in advance to have a liquid temperature of 5 ° C. In a cylindrical stainless steel container having an inner diameter of 110 mm and a height of 130 mm, 330 g of the coffee beverage base was placed and cooled so that the liquid temperature was maintained at 5 ° C to 10 ° C. Attach an attachment (Wish, Esge) to a handy food processor (Burmix M300, Esge), attach the tip of the attachment to the bottom of the stainless steel container, and mix for 30 seconds at "low speed" 1) was prepared. It was visually confirmed that all of the coffee beverage was converted to a fine foam-formed beverage when the production was completed.

次に、コーヒー飲料ベース1をあらかじめ液温が70℃になるように準備した。内径110mm、高さ130mmの円柱状のステンレス容器にコーヒー飲料ベース330gを入れ、液温が65℃〜70℃を保つよう保温した。ハンディーフードプロセッサー(バーミックスM300、エスゲー社)にアタッチメント(ウイスク、エスゲー社)を装着し、アタッチメント先端をステンレス容器底部につけて「高速」で30秒間混合処理してホットタイプの微細泡飲料(試験区2)を調製した。製造完了時にコーヒー飲料液のすべてが微細な泡が形成された飲料に変化していることを目視で確認した。   Next, the coffee beverage base 1 was prepared in advance to have a liquid temperature of 70.degree. In a cylindrical stainless steel container having an inner diameter of 110 mm and a height of 130 mm, 330 g of the coffee beverage base was placed and kept warm so that the liquid temperature was maintained at 65 ° C to 70 ° C. Attach an attachment (Wish, Esge) to a handy food processor (Burmix M300, Esge), attach the tip of the attachment to the bottom of the stainless steel container, and mix for 30 seconds at “high speed” 2) was prepared. It was visually confirmed that all of the coffee beverage was converted to a fine foam-formed beverage when the production was completed.

また、比較対照品として市販のビール飲料(ギネス、キリンビール社)(試験区3)、スムージー飲料(黒ゴマ豆乳バナナスムージー、ユニマットリケン社)(試験区4)、コーラ飲料(メッツコーラ、キリンビバレッジ社)(試験区5)、コーヒー飲料(振って泡立つプレミアム、ダイドードリンコ社)(試験区6)を準備した。   In addition, commercially available beer drinks (Guinness, Kirin Brewery Co., Ltd.) (test area 3), smoothie drinks (black sesame soybean milk banana smoothie, Unimat Riken Co., Ltd.) (test area 4), cola drinks (Mezcola, Kirin Beverage) as comparative products. Co., Ltd. (test area 5), coffee beverage (stirring foamy premium, Daido Drinko) (test area 6) was prepared.

(2)飲料の分析
各試験区の飲料は以下の手順でゾル比重、分離速度、液粘度を測定した。
(2) Analysis of Beverage The beverage of each test area was measured for sol specific gravity, separation speed and liquid viscosity according to the following procedure.

ア ゾル比重
微細泡飲料を製造完了後、直ちにプラスチック製カップ(容量150mL、旭化成社製、プロマックスEI−150D)に満量となるまで注ぎ、満注容量の質量を測定した。次に、微細泡飲料を遠心エバポレーター(Genevac社製)を用いて脱泡処理に付し、脱泡後の飲料(非微細泡飲料)の満注容量の質量を微細泡飲料と同様に測定した。
Azole specific gravity Immediately after completion of the production of the micro-foamed beverage, it was poured into a plastic cup (volume 150 mL, Promax EI-150D, manufactured by Asahi Kasei Co., Ltd.) until full, and the mass of the fully-filled volume was measured. Next, the fine foam beverage was subjected to defoaming treatment using a centrifugal evaporator (manufactured by Genevac), and the mass of the full capacity of the defoamed beverage (non-fine foam beverage) was measured in the same manner as the fine foam beverage .

ゾル比重は下記数式(I)に基づいて算出した。

Figure 2018012477
The sol specific gravity was calculated based on the following formula (I).
Figure 2018012477

イ 分離速度
微細泡飲料を製造完了後、直ちに分離速度評価用ガラス(容量300mL、φ52mm、高さ140mm)に満量となるまで注ぎ、容器満注時と容器満注時から100秒後に容器内で最も低い位置に存在する微細泡の位置を、底部からの距離(mm)として測定した。微細泡の有無は、色評価用蛍光ランプを用いて2000±500luxとなる環境下に分離速度評価用ガラスを設置し、目視によって判定した。容器満注時から数秒後の試験区1の飲料と容器満注時から100秒経過後の試験区1の飲料はそれぞれ図1Bおよび図1Cに示される通りである。なお、試験区1および2の飲料は、容器満注時に飲料ベースのすべてが微細な泡が形成された飲料となっていることを目視で確認した(下記数式(II)においてY=0(mm))。
B. Separating speed Immediately after the production of the microfoam beverage is completed, pour into a glass for evaluating the separating speed (volume 300 mL, φ 52 mm, height 140 mm) until it is full, and 100 seconds after full filling and 100 seconds after full filling of the container The position of the microbubbles present at the lowest position of was measured as the distance from the bottom (mm). The presence or absence of the fine bubbles was determined by visually setting the separation speed evaluation glass under an environment of 2000 ± 500 lux using a color evaluation fluorescent lamp. The beverage in the test area 1 several seconds after the full filling of the container and the beverage in the test area 1 100 seconds after the full filling of the container are as shown in FIGS. 1B and 1C, respectively. In addition, it was visually confirmed that the beverages in the test areas 1 and 2 were beverages in which all of the beverage base formed fine bubbles when the container was fully filled (Y = 0 (mm in the following formula (II)) )).

分離速度は下記数式(II)に基づいて算出した。

Figure 2018012477
X=容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離(mm)
Y=容器満注時の容器底から微細な泡の最も低い位置までの垂直距離(mm)The separation speed was calculated based on the following formula (II).
Figure 2018012477
X = Vertical distance (mm) from the bottom of the container to the lowest position of fine bubbles 100 seconds after the container is filled
Y = vertical distance (mm) from the bottom of the container to the lowest position of fine bubbles when the container is full

ウ 液粘度
微細泡飲料は遠心エバポレーター(Genevac社製)を用いて脱泡処理に供し、脱泡後の溶液について液粘度を測定した。液粘度の測定は落球式マイクロ粘度計(アントンパール社製)により実施した。測定時の溶液温度は20℃とし、対象の液粘度に応じてキャピラリーおよびボールを、該粘度計指定の方法に従って選択して測定を行った。
C. Liquid Viscosity The microfoamed beverage was subjected to defoaming treatment using a centrifugal evaporator (manufactured by Genevac), and the liquid viscosity of the defoamed solution was measured. The liquid viscosity was measured with a falling ball micro viscometer (manufactured by Anton Paar). The solution temperature at the time of measurement was 20 ° C., and the capillary and the ball were selected and measured according to the method specified by the viscometer according to the liquid viscosity of the object.

(3)官能評価
各試験区の飲料は、さらに官能評価に供した。官能評価は訓練されたパネリスト6名により実施した。具体的には、各試験区の飲料について、以下の4項目を評価し、最も得票数が多かった評価点を採用した。ただし、得票数が同数の場合は、より低い評価点を採用した。
(3) Sensory evaluation The drink of each test area was further subjected to sensory evaluation. Sensory evaluation was performed by six trained panelists. Specifically, the following four items were evaluated about the drink of each test area, and the evaluation score with the largest number of votes was adopted. However, in the case of the same number of votes, lower score was adopted.

(a)飲用直後
A:口腔内に含んだ溶液がさらさらとして、気泡を含んで軽くエアリーな食感が得られ、且つ、含んだ気泡は弾性がなく柔らかい。
B:口腔内に含んだ溶液が気泡を含んで少しエアリーな食感が得られ、且つ、含んだ気泡が柔らかい。
C:口腔内に含んだ溶液が気泡を含んでいることは感じられるが、エアリーではない。
D:口腔内に含んだ溶液に気泡を感じられない。
(A) Immediately after drinking A: A solution contained in the oral cavity is free flowing, and a light and airy texture is obtained containing bubbles, and the contained bubbles are not elastic and soft.
B: The solution contained in the oral cavity contains bubbles to give a slightly airy texture, and the bubbles contained are soft.
C: It is felt that the solution contained in the oral cavity contains bubbles, but it is not airy.
D: Air bubbles can not be felt in the solution contained in the oral cavity.

(b)飲用中
A:口腔内に含んだ気泡が弾けることなく静かに、次々に消失し、溶液としての流動性が十分に感じられる。
B:口腔内に含んだ気泡の一部が弾けることなく消失し、溶液としての流動性が感じられる。
C:口腔内に含んだ気泡が少し消失した感覚があるものの、溶液としての流動性が得られにくい。
D:口腔内に含んだ気泡がとどまり続け、嚥下に少し抵抗感がある。
(B) During drinking A: The bubbles contained in the oral cavity are gently dissipated one after another without popping, and the fluidity as a solution is sufficiently felt.
B: Some of the bubbles contained in the oral cavity disappear without popping, and the fluidity as a solution is felt.
C: Although there is a feeling that bubbles contained in the oral cavity have disappeared a little, it is difficult to obtain fluidity as a solution.
D: Bubbles contained in the oral cavity continue to stay, and there is a slight resistance to swallowing.

(c)嚥下後
A:口腔内での後残りがなく、キレがとても良く感じられる。
B:口腔内での後残りが少なく、キレが良く感じられる。
C:嚥下後も口腔内に少し溶液が感じられ、キレが悪い。
D:嚥下後も口腔内に残液感がある。
(C) After swallowing A: There is no after residue in the oral cavity, and it feels very well.
B: There is little after-residue in the oral cavity, and you can feel good feeling.
C: A little solution is felt in the oral cavity even after swallowing, and the feeling is poor.
D: There is a residual liquid feeling in the mouth even after swallowing.

(d)総合評価
A:飲料全体における「泡融け感」を十分に感じる。
B:飲料全体における「泡融け感」を感じる。
C:飲料全体における「泡融け感」があまり感じられない。
D:飲料全体における「泡融け感」が感じられない。
(D) Overall evaluation A: Feel fully the "feeling of foam" in the whole beverage.
B: I feel a "feeling of melting" in the whole beverage.
C: The "feeling of foam" in the whole beverage is not felt so much.
D: "Feeling of foam" in the whole beverage is not felt.

(4)結果
各試験区の飲料の液粘度、ゾル比重、分離速度、官能評価結果は表1に示される通りであった。

Figure 2018012477
(4) Results The liquid viscosity, sol specific gravity, separation speed and sensory evaluation results of the beverages in each test area were as shown in Table 1.
Figure 2018012477

表1の結果から、ゾル比重、分離速度および液粘度が特定の範囲に含まれる微細泡飲料が官能評価項目(a)、(b)、(c)および(d)において望ましい評価結果を示し、これまでにない泡融け感を有する飲料であることが判明した。一方で、ゾル比重が大きい試験区3においては嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。液粘度が大きい試験区4においては、気泡を含んだエアリーで柔らかい食感が得られたものの、口腔内でも気泡が十分に保持され、消失感や流動性が感じられなかった。また、嚥下後ももったりとした飲料液が口腔内に残存する感覚があり、泡融け感は有していなかった。分離速度が大きい試験区5においては嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。ゾル比重、分離速度および液粘度のすべてが大きい試験区6においては、気泡によるエアリーな食感や口腔内での消失感が得られず、嚥下後ももったりとした飲料液が口腔内に残存し、泡融け感は有していなかった。   From the results in Table 1, it is shown that micro-foamed beverages having a sol specific gravity, separation speed and liquid viscosity in specific ranges show desirable evaluation results in sensory evaluation items (a), (b), (c) and (d), It turned out that it is a drink which has an unprecedented feeling of melting. On the other hand, in the test area 3 where the sol specific gravity is large, although the fineness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and no feeling of melting was found. In the test section 4 where the liquid viscosity was large, airy and soft texture was obtained including air bubbles, but the air bubbles were sufficiently retained even in the oral cavity, and a feeling of disappearance or fluidity was not felt. In addition, there was a feeling that the beverage liquid, which was dull after swallowing, remained in the oral cavity, and did not have a feeling of foamy melting. In the test area 5 where the separation speed was large, although the fineness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and the foam did not have a melting feeling. In the test section 6 where all of the sol specific gravity, the separation speed and the liquid viscosity are large, airy texture due to air bubbles and disappearance feeling in the oral cavity can not be obtained, and the beverage liquid which remains after swallowing remains in the oral cavity And had no feeling of melting.

例2:微細泡飲料の製造および各種物性値の分析(2)
表2に従って試験用飲料ベースを調製し、該飲料ベースと気体との混合処理を行い、微細泡飲料(試験区7〜19)を調製した。製造完了時に試験用飲料ベースのすべてが微細な泡が形成された飲料に変化していることを目視で確認した。
Example 2: Production of microfoam beverage and analysis of various physical property values (2)
A test beverage base was prepared according to Table 2, mixed with the beverage base and a gas, and a microfoam beverage (test areas 7 to 19) was prepared. It was visually confirmed that at the completion of production all of the test beverage bases had been converted to a fine foam-formed beverage.

Figure 2018012477
Figure 2018012477

各試験区の飲料について、例1(2)および(3)に記載された手順に従ってゾル比重、分離速度、液粘度を測定するとともに、官能評価を行った。なお、分離速度の測定にあたっては、容器満注時に試験用飲料ベースのすべてが微細な泡が形成された飲料となっていることを目視で確認した(前記数式(II)においてY=0(mm))。   About the drink of each test area, while measuring sol specific gravity, the isolation | separation speed, and liquid viscosity according to the procedure described in Example 1 (2) and (3), sensory evaluation was performed. In the measurement of the separation speed, it was visually confirmed that all of the test beverage base was a beverage in which fine bubbles were formed when the container was fully filled (Y = 0 (mm in the above formula (II)) )).

各試験区の飲料の液粘度、ゾル比重、分離速度、官能評価結果は表3に示される通りであった。

Figure 2018012477
The liquid viscosity, sol specific gravity, separation rate and sensory evaluation results of the beverages in each test area were as shown in Table 3.
Figure 2018012477

表3の結果から、飲料のゾル比重を0.85以下となるように調整し、かつ、分離速度を0.7mm/秒以下となるように調整し、かつ、液粘度を2.5mPa・s以下となるように調整することにより、官能評価項目(a)、(b)、(c)および(d)において好ましい結果を有する微細泡飲料が得られることが明らかとなった。   From the results in Table 3, the sol specific gravity of the beverage is adjusted to 0.85 or less, and the separation speed is adjusted to 0.7 mm / sec or less, and the liquid viscosity is 2.5 mPa · s. It became clear that the fine foam beverage which has a preferable result in sensory evaluation item (a), (b), (c) and (d) is obtained by adjusting so that it may become the following.

試験区7、8、14、19においては、分離速度および液粘度が同程度であり、かつ、ゾル比重が異なる飲料が調製され、試験区7、8は十分な泡融け感を有していた。一方で、試験区19では嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。   In the test areas 7, 8, 14 and 19, beverages having the same separation speed and liquid viscosity and different sol specific gravity were prepared, and the test areas 7 and 8 had a sufficient feeling of foam melting. . On the other hand, in the test section 19, although the fineness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and no feeling of melting was felt.

試験区8、9、10、11、12、14、15においては、ゾル比重および液粘度が同程度であり、かつ、分離速度が異なる飲料が調製され、試験区8、9、10、11は十分な泡融け感を有していた。一方で試験区12、15では嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感が不足していると感じられ、口腔内での気泡の消失感も感じられず、泡融け感は有していなかった。   In the test areas 8, 9, 10, 11, 12, 14, 15, beverages having the same sol specific gravity and liquid viscosity and different separation speeds are prepared, and the test areas 8, 9, 10, 11 It had a sufficient foamy feeling. On the other hand, in the test sections 12 and 15, although the fineness after swallowing was felt, it was felt that the softness and airy texture due to the inclusion of air bubbles were lacking, and the feeling of air bubbles in the oral cavity was not felt either , I did not have a feeling of melting.

試験区10、16、17、18においては、ゾル比重および分離速度が同程度であり、かつ、液粘度が異なる飲料が調製され、試験区10、16は十分な泡融け感を有していた。一方で、試験区18では気泡を含んだエアリーで柔らかい食感が得られたものの、口腔内でも気泡が保持され、消失感や流動性が感じられなかった。また、嚥下後ももったりとした飲料液が口腔内に残存する感覚があり、泡融け感は有していなかった。   In the test areas 10, 16, 17, and 18, beverages having similar sol specific gravity and separation speed and different liquid viscosity were prepared, and the test areas 10 and 16 had a sufficient foamy feeling. . On the other hand, in the test area 18, airy and soft texture was obtained including air bubbles, but air bubbles were retained even in the oral cavity, and no feeling of disappearance or fluidity was felt. In addition, there was a feeling that the beverage liquid, which was dull after swallowing, remained in the oral cavity, and did not have a feeling of foamy melting.

ゾル比重および分離速度が大きい試験区13においては、嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。   In the test area 13 where the sol specific gravity and the separation speed were large, although the fineness after swallowing was felt, neither softness nor airy texture due to the inclusion of air bubbles was felt, and no feeling of melting of bubbles was observed.

例3:微細泡飲料の製造および各種物性値の分析(3)
表4に従って試験用飲料ベースを調製し、該飲料ベースと気体との混合処理を行い、微細泡飲料(試験区20〜30)を調製した。製造完了時に試験用飲料ベースのすべてが微細な泡が形成された飲料に変化していることを目視で確認した。
Example 3: Production of microfoam beverage and analysis of various physical property values (3)
A test beverage base was prepared according to Table 4, mixed with the beverage base and a gas, and a microfoam beverage (test area 20 to 30) was prepared. It was visually confirmed that at the completion of production all of the test beverage bases had been converted to a fine foam-formed beverage.

Figure 2018012477
Figure 2018012477

各試験区の飲料について、例1(2)および(3)に記載された手順に従ってゾル比重、分離速度、液粘度を測定するとともに、官能評価を行った。なお、分離速度の測定にあたっては、容器満注時に試験用飲料ベースのすべてが微細な泡が形成された飲料となっていることを目視で確認した(前記数式(II)においてY=0(mm))。   About the drink of each test area, while measuring sol specific gravity, the isolation | separation speed, and liquid viscosity according to the procedure described in Example 1 (2) and (3), sensory evaluation was performed. In the measurement of the separation speed, it was visually confirmed that all of the test beverage base was a beverage in which fine bubbles were formed when the container was fully filled (Y = 0 (mm in the above formula (II)) )).

各試験区の飲料の液粘度、ゾル比重、分離速度、官能評価結果は表5に示される通りであった。

Figure 2018012477
The liquid viscosity, sol specific gravity, separation rate and sensory evaluation results of the beverages in each test area are as shown in Table 5.
Figure 2018012477

表5の結果から、飲料のゾル比重を0.85以下となるように調整し、かつ、分離速度を0.7mm/秒以下となるように調整し、かつ、液粘度を2.5mPa・s以下となるように調整することにより、官能評価項目(a)、(b)、(c)および(d)において好ましい結果を有する微細泡飲料が得られることが明らかとなった。   From the results in Table 5, the sol specific gravity of the beverage is adjusted to 0.85 or less, the separation speed is adjusted to 0.7 mm / sec or less, and the liquid viscosity is 2.5 mPa · s. It became clear that the fine foam beverage which has a preferable result in sensory evaluation item (a), (b), (c) and (d) is obtained by adjusting so that it may become the following.

試験区20、25においては、分離速度および液粘度が同程度であり、かつ、ゾル比重が異なる飲料が調製され、試験区25は十分な泡融け感を有していた。一方で、試験区20では嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。   In the test areas 20 and 25, drinks having the same separation speed and liquid viscosity and different sol specific gravity were prepared, and the test area 25 had a sufficient foamy feeling. On the other hand, in the test area 20, although the fineness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and there was no foam melting feeling.

試験区21、23、24においては、ゾル比重および分離速度が同程度であり、
かつ、液粘度が異なる飲料が調製され、試験区23、24は十分な泡融け感を有していた。一方で、試験区21では気泡を含んだエアリーで柔らかい食感が得られたものの、嚥下後ももったりとした飲料液が口腔内に残存する感覚があり、泡融け感は有していなかった。
In the test sections 21, 23, 24, the sol specific gravity and the separation speed are comparable,
And the drink from which liquid viscosity differs was prepared, and the test sections 23 and 24 had sufficient foamy feeling. On the other hand, although the airy and soft texture containing air bubbles was obtained in the test area 21, there was a feeling that the beverage liquid which was dull after swallowing remained in the oral cavity, and it did not have a feeling of foam melting .

Claims (10)

ゾル比重が0.85以下であり、かつ、分離速度が0.7mm/秒以下である、微細泡飲料(ここで、「ゾル比重」は一定容量の非微細泡飲料の質量に対する一定容量の微細泡飲料の質量の比率をいい、「分離速度」は微細泡飲料を評価用容器に注いだときの、容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離(mm)から容器満注時の容器底から微細な泡の最も低い位置までの垂直距離(mm)を引いた値を100秒で除した値をいう)。   A micro-foamed beverage having a sol specific gravity of 0.85 or less and a separation speed of 0.7 mm / sec or less (here, “sol specific gravity” refers to a fixed volume of fines with respect to a fixed volume of non-micro-foamed beverage The ratio of the mass of the bubble beverage is the "separation speed" is the vertical distance from the bottom of the container to the lowest position of fine bubbles 100 seconds after the container is filled when the microfoam beverage is poured into the evaluation container The value obtained by subtracting the vertical distance (mm) from the bottom of the container from the bottom of the container to the lowest position of fine bubbles (mm) from (mm) divided by 100 seconds). 液粘度が2.5mPa・s以下である、請求項1に記載の微細泡飲料。   The micro-foamed beverage according to claim 1, wherein the liquid viscosity is 2.5 mPa · s or less. 飲料が清涼飲料である、請求項1または2に記載の微細泡飲料。   The micro-foamed beverage according to claim 1 or 2, wherein the beverage is a soft drink. 飲料液を3000〜50000rpm、1秒〜60分の条件で混合する工程を含んでなる、微細泡飲料の製造方法。   A method for producing a microfoam beverage, comprising the steps of mixing a beverage liquid under conditions of 3000 to 50000 rpm for 1 second to 60 minutes. 製造された飲料のゾル比重(ここで、ゾル比重は請求項1で定義された内容と同義である)が0.85以下である、請求項4に記載の製造方法。   The method according to claim 4, wherein the sol specific gravity (wherein the sol specific gravity is as defined in claim 1) of the manufactured beverage is 0.85 or less. 製造された飲料の分離速度(ここで、分離速度は請求項1で定義された内容と同義である)が0.7mm/秒以下である、請求項4または5に記載の製造方法。   The method according to claim 4 or 5, wherein the separation speed of the manufactured beverage (wherein the separation speed is the same as the contents defined in claim 1) is 0.7 mm / sec or less. 製造された飲料の液粘度が2.5mPa・s以下である、請求項4〜6のいずれか一項に記載の製造方法。   The manufacturing method as described in any one of Claims 4-6 whose liquid viscosity of the manufactured drink is 2.5 mPa * s or less. 窒素を含有する気体の存在下で混合を行う、請求項4〜7のいずれか一項に記載の製造方法。   The method according to any one of claims 4 to 7, wherein the mixing is performed in the presence of a nitrogen-containing gas. 飲料が清涼飲料である、請求項4〜8のいずれか一項に記載の製造方法。   The method according to any one of claims 4 to 8, wherein the beverage is a soft drink. 請求項4〜9のいずれか一項に記載の製造方法により製造された、微細泡飲料。   The microfoam drink manufactured by the manufacturing method as described in any one of Claims 4-9.
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