JP7005705B2 - Fine foam beverage and its manufacturing method - Google Patents

Fine foam beverage and its manufacturing method Download PDF

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JP7005705B2
JP7005705B2 JP2020128292A JP2020128292A JP7005705B2 JP 7005705 B2 JP7005705 B2 JP 7005705B2 JP 2020128292 A JP2020128292 A JP 2020128292A JP 2020128292 A JP2020128292 A JP 2020128292A JP 7005705 B2 JP7005705 B2 JP 7005705B2
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研一朗 山本
祐子 四元
貴史 塩野
智弘 豊澤
宏 寺田
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Kirin Holdings Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation

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Description

関連出願の参照Reference of related application

本願は、先行する日本国出願である特願2016-137250(出願日:2016年7月12日)の優先権の利益を享受するものであり、その開示内容全体は引用することにより本明細書の一部とされる。 The present application enjoys the benefit of the priority of the preceding Japanese application, Japanese Patent Application No. 2016-137250 (filed on July 12, 2016), the entire disclosure of which is hereby cited by reference. Be part of.

本発明は新規な微細泡飲料およびその製造方法に関する。 The present invention relates to a novel fine foam beverage and a method for producing the same.

清涼飲料やアルコール飲料においては、飲用者が泡の感触を楽しむことができるものが市場において好まれている。代表的なものとしては炭酸飲料が挙げられ、これらは飲用時に二酸化炭素の気泡に伴う刺激的な感触を楽しむことができる。 Among soft drinks and alcoholic beverages, those that allow the drinker to enjoy the feel of foam are preferred in the market. Typical examples are carbonated drinks, which can enjoy the stimulating feel associated with carbon dioxide bubbles when drinking.

一方で、各種の起泡剤の添加や、窒素ガスと飲料液の混合により滑らかな感触の起泡の飲料を提供することが試みられている。このような飲料はいずれも液面上に形成された泡(フォーム)の大きさを細かくすることによってより滑らかな泡の飲料を提供しようとしている(特許文献1)。しかし、液面のみならず飲料全体が微細な泡を含む溶液から構成された飲料はこれまで知られていなかった。 On the other hand, attempts have been made to provide a foaming beverage having a smooth feel by adding various foaming agents and mixing nitrogen gas and a drinking liquid. All of such beverages are intended to provide a beverage with smoother foam by reducing the size of foam formed on the liquid surface (Patent Document 1). However, no beverage has been known so far, in which not only the liquid surface but also the entire beverage is composed of a solution containing fine bubbles.

特開2016-59372号公報Japanese Unexamined Patent Publication No. 2016-59372

本発明者らは今般、飲料における泡の感触は、液面に形成された泡のみならず、液中に形成された気泡も重要な役割を果たしていることを新たに見出した。すなわち、飲料全体が微細な泡で構成されるように混合処理して得られた飲料が、従来の飲料では実現されたことがない「泡融け感」を有することを見出し、本発明を完成させた。 The present inventors have recently found that not only the bubbles formed on the liquid surface but also the bubbles formed in the liquid play an important role in the feel of bubbles in a beverage. That is, they have found that a beverage obtained by mixing treatment so that the entire beverage is composed of fine bubbles has a "foam melting feeling" that has not been realized by conventional beverages, and completed the present invention. rice field.

すなわち、本発明はこれまで実現されたことがない「泡融け感」が付与された新規な微細泡飲料とその製造方法を提供することを目的とする。 That is, an object of the present invention is to provide a novel fine foam beverage and a method for producing the same, which is given a "foam melting feeling" that has never been realized so far.

本発明によれば以下の発明が提供される。
[1]ゾル比重が0.85以下であり、かつ、分離速度が0.7mm/秒以下である、微細泡飲料(ここで、「ゾル比重」は一定容量の非微細泡飲料の質量に対する一定容量の微細泡飲料の質量の比率をいい、「分離速度」は微細泡飲料を評価用容器に注いだときの、容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離(mm)から容器満注時の容器底から微細な泡の最も低い位置までの垂直距離(mm)を引いた値を100秒(s)で除した値をいう)。
[2]液粘度が2.5mPa・s以下である、上記[1]に記載の微細泡飲料。
[3]飲料が清涼飲料である、上記[1]または[2]に記載の微細泡飲料。
[4]飲料液を3000~50000rpm、1秒~60分の条件で混合する工程を含んでなる、微細泡飲料の製造方法。
[5]製造された飲料のゾル比重(ここで、ゾル比重は上記[1]で定義された内容と同義である)が0.85以下である、上記[4]に記載の製造方法。
[6]製造された飲料の分離速度(ここで、分離速度は上記[1]で定義された内容と同義である)が0.7mm/秒以下である、上記[4]または[5]に記載の製造方法。
[7]製造された飲料の液粘度が2.5mPa・s以下である、上記[4]~[6]のいずれかに記載の製造方法。
[8]窒素を含有する気体の存在下で混合を行う、上記[4]~[7]のいずれかに記載の製造方法。
[9]飲料が清涼飲料である、上記[4]~[8]のいずれかに記載の製造方法。
[10]上記[4]~[9]のいずれかに記載の製造方法により製造された、微細泡飲料。
According to the present invention, the following inventions are provided.
[1] A fine foam beverage having a sol specific gravity of 0.85 or less and a separation rate of 0.7 mm / sec or less (here, the "sol specific gravity" is constant with respect to the mass of a constant volume of non-fine foam beverage). The ratio of the mass of the fine foam beverage by volume, and the "separation rate" is from the bottom of the container 100 seconds after the container is fully filled to the lowest position of the fine foam when the fine foam beverage is poured into the evaluation container. The value obtained by subtracting the vertical distance (mm) from the bottom of the container when the container is fully filled to the lowest position of fine bubbles (mm) is divided by 100 seconds (s)).
[2] The fine foam beverage according to the above [1], which has a liquid viscosity of 2.5 mPa · s or less.
[3] The fine foam beverage according to the above [1] or [2], wherein the beverage is a soft drink.
[4] A method for producing a fine foam beverage, which comprises a step of mixing the beverage liquid at 3000 to 50,000 rpm for 1 second to 60 minutes.
[5] The production method according to the above [4], wherein the produced beverage has a sol specific gravity (here, the sol specific density is synonymous with the content defined in the above [1]) of 0.85 or less.
[6] In the above [4] or [5], the separation rate of the produced beverage (where, the separation rate is synonymous with the content defined in the above [1]) is 0.7 mm / sec or less. The manufacturing method described.
[7] The production method according to any one of [4] to [6] above, wherein the produced beverage has a liquid viscosity of 2.5 mPa · s or less.
[8] The production method according to any one of the above [4] to [7], wherein mixing is performed in the presence of a gas containing nitrogen.
[9] The production method according to any one of the above [4] to [8], wherein the beverage is a soft drink.
[10] A fine foam beverage produced by the production method according to any one of the above [4] to [9].

本発明の微細泡飲料は飲料全体が微細な泡を含む溶液で構成され、飲用者はこれまで経験したことがない「泡融け感」を楽しむことができる。すなわち、本発明は従来にはない飲用感を有する飲料を提供するものであり、消費者の新たな嗜好やニーズに応えることができる点で有利である。 In the fine foam beverage of the present invention, the entire beverage is composed of a solution containing fine foam, and the drinker can enjoy a "foam melting feeling" that has never been experienced before. That is, the present invention provides a beverage having a drinking feeling that has never existed in the past, and is advantageous in that it can meet new tastes and needs of consumers.

図1Aは混合処理前のコーヒー飲料を容器に満注した写真である。FIG. 1A is a photograph of a coffee beverage before mixing treatment filled in a container. 図1Bは気体との混合処理後のコーヒー飲料を容器に満注した後、容器満注時から数秒後の試験区1の飲料の写真である。FIG. 1B is a photograph of the beverage in Test Group 1 several seconds after the container is fully filled with the coffee beverage after the mixing treatment with the gas. 図1Cは気体との混合処理後のコーヒー飲料を容器に満注した後、容器満注時から100秒経過後の試験区1の飲料の写真である。FIG. 1C is a photograph of the beverage in Test Group 1 100 seconds after the container is fully filled with the coffee beverage after the mixing treatment with the gas.

発明の具体的説明Specific description of the invention

本発明の微細泡飲料は、飲料中に微細な泡が形成されてなる飲料である。飲料中に微細な泡が形成されることにより、後述するような「泡融け感」が飲料に付与されることから、本発明の飲料は所定量の気泡を含むことを特徴とし、飲料中の気泡量は脱泡処理に付されて微細な泡が消失した脱泡処理後の微細泡飲料(非微細泡飲料)に対する本発明の飲料の比重(ゾル比重)により特定することができる。 The fine foam beverage of the present invention is a beverage in which fine bubbles are formed in the beverage. The formation of fine bubbles in the beverage gives the beverage a “foam melting feeling” as described later. Therefore, the beverage of the present invention is characterized by containing a predetermined amount of bubbles in the beverage. The amount of bubbles can be specified by the specific gravity (sol specific gravity) of the beverage of the present invention with respect to the fine foam beverage (non-fine foam beverage) after the defoaming treatment in which the fine bubbles disappear after the defoaming treatment.

本発明において「ゾル比重」とは、一定容量の非微細泡飲料の質量(g)に対する一定容量の微細泡飲料の質量(g)の比率をいう。ゾル比重は同一体積で比較した場合にどの程度気泡を含む飲料であるかを示す指標ということができ、ゾル比重が小さい微細泡飲料はより多量の気泡を含む飲料ということができる。本発明の微細泡飲料のゾル比重は0.85以下とすることができ、好ましくは0.80以下、より好ましくは0.40~0.80、さらに好ましくは0.50~0.80である。 In the present invention, the "sol specific gravity" refers to the ratio of the mass (g) of a fixed volume fine foam beverage to the mass (g) of a constant volume non-fine foam beverage. The sol specific gravity can be said to be an index showing how much bubbles are contained in the beverage when compared in the same volume, and the fine foam beverage having a small sol specific gravity can be said to be a beverage containing a larger amount of bubbles. The sol specific gravity of the fine foam beverage of the present invention can be 0.85 or less, preferably 0.80 or less, more preferably 0.40 to 0.80, still more preferably 0.50 to 0.80. ..

本発明の微細泡飲料においてゾル比重を算出する場合には、まず、微細泡飲料の製造完了後、直ちに一定容量当たりの質量を測定し、次いで、微細泡飲料を適切な方法で脱泡処理に付し、脱泡後の飲料(非微細泡飲料)の一定容量当たりの質量を測定し、これらの測定値に基づいてゾル比重を算出することができる。脱泡処理は、例えば減圧脱泡や遠心エバポレーター、真空撹拌脱泡装置などを使用することができる。 When calculating the sol specific gravity in the fine foam beverage of the present invention, first, the mass per fixed volume is measured immediately after the production of the fine foam beverage is completed, and then the fine foam beverage is defoamed by an appropriate method. Then, the mass of the defoamed beverage (non-fine foam beverage) per fixed volume can be measured, and the sol specific gravity can be calculated based on these measured values. For the defoaming treatment, for example, vacuum defoaming, a centrifugal evaporator, a vacuum stirring defoaming device, or the like can be used.

本発明の微細泡飲料は、飲料中に微細な泡を形成させることにより飲料中に気体を含有する飲料である。微細な泡を構成する気体としては窒素を含有する気体(例えば、空気)および窒素ガスが挙げられ、好ましくは窒素を含有する気体であり、より好ましくは空気である。 The fine foam beverage of the present invention is a beverage containing gas in the beverage by forming fine bubbles in the beverage. Examples of the gas constituting the fine bubbles include a gas containing nitrogen (for example, air) and a nitrogen gas, preferably a gas containing nitrogen, and more preferably air.

本発明の微細泡飲料は、製造直後は飲料のほぼ全体が微細な泡から構成されているが、時間が経過するにつれ、微細な泡から構成される部分と微細な泡を含まない部分の二つの部分に徐々に分離する。このため本発明の飲料は微細な泡から構成される部分が微細な泡を含まない部分に分離する速度(分離速度)により特定することができる。 In the fine foam beverage of the present invention, almost the entire beverage is composed of fine foam immediately after production, but as time passes, there are two parts, a portion composed of fine foam and a portion not containing fine foam. Gradually separate into two parts. Therefore, the beverage of the present invention can be specified by the rate (separation rate) at which the portion composed of fine bubbles is separated into the portion not containing fine bubbles.

本発明において「分離速度」(mm/秒)とは本発明の微細泡飲料を評価用容器に注いだときの、容器満注時から100秒後の容器底から微細泡の最も低い位置までの垂直距離(mm)から容器満注時の容器底から微細な泡の最も低い位置までの垂直距離を引いた値を100秒(s)で除した値をいう。分離速度を測定する際には本発明の微細泡飲料を製造完了後、直ちに空の評価用容器に注いで、容器が満量になった時点と容器満注から100秒後の微細泡の最低位置を容器底から計測する。容器に既に飲料が存在する場合には、該飲料を除いてから計測を行うことはいうまでもないが、仮に該飲料が存在したまま計測を行う場合には、該飲料の液面から微細泡の最も低い位置までの距離を計測する。また、製造完了時にすべての原料飲料液が微細な泡に変化せず、該飲料液が残存していることがあり、該飲料液が評価用容器に注がれることがあるが、このような場合には製造完了時に残存している原料飲料液のうち評価容器に注がれた飲料液の体積分を垂直距離から差し引くことで、分離速度をより正確に算出することができる。 In the present invention, the "separation rate" (mm / sec) is from the bottom of the container 100 seconds after the container is fully filled to the lowest position of the fine foam when the fine foam beverage of the present invention is poured into the evaluation container. The value obtained by subtracting the vertical distance from the vertical distance (mm) to the lowest position of fine bubbles from the bottom of the container when the container is fully filled, divided by 100 seconds (s). When measuring the separation rate, the fine foam beverage of the present invention is immediately poured into an empty evaluation container after the production is completed, and the minimum amount of fine foam at the time when the container is full and 100 seconds after the container is fully filled. Measure the position from the bottom of the container. It goes without saying that if the beverage is already present in the container, the measurement is performed after removing the beverage, but if the measurement is performed with the beverage present, fine bubbles are formed from the liquid level of the beverage. Measure the distance to the lowest position of. In addition, when the production is completed, all the raw material beverages do not change into fine bubbles, and the beverages may remain, and the beverages may be poured into the evaluation container. In some cases, the separation rate can be calculated more accurately by subtracting the volume of the beverage liquid poured into the evaluation container from the vertical distance among the raw material beverage liquids remaining at the completion of production.

分離速度の測定に使用する評価用容器は、容器の材質や口径による測定値のぶれを防ぐため、分離速度評価用ガラス(容量300mL、φ52mm、高さ140mm)を使用する。上記の分離速度評価用ガラス以外の容器を使用して分離速度を測定した場合には、得られた分離速度を該容器の口径と高さに基づいて分離速度評価用ガラスでの測定値に換算することができる。分離速度を測定する場合にはまた、容器内で最も低い位置に存在する微細泡の位置を正確に測定するため、色評価用蛍光ランプなどの照明装置を使用することが好ましい。分離速度は一定時間内にどの程度の速さで微細泡飲料から微細泡を含まない飲料液に変化するかを示す指標ということができ、分離速度が小さい飲料は微細泡飲料の状態をより長く維持できる飲料ということができる。本発明の微細泡飲料の分離速度は0.7mm/秒以下とすることができ、好ましくは0.68mm/秒以下、より好ましくは0.6mm/秒以下である。また、本発明の微細泡飲料の分離速度は0.05mm/秒以上とすることができ、好ましくは0.1mm/秒以上である。本発明の微細泡飲料の分離速度は、0.05~0.7mm/秒とすることができ、好ましくは0.1~0.6mm/秒である。 For the evaluation container used for measuring the separation speed, glass for evaluation of the separation speed (capacity 300 mL, φ52 mm, height 140 mm) is used in order to prevent the measured value from fluctuating due to the material and diameter of the container. When the separation rate is measured using a container other than the above glass for evaluation of separation rate, the obtained separation rate is converted into the measured value with the glass for evaluation of separation rate based on the diameter and height of the container. can do. When measuring the separation rate, it is also preferable to use a lighting device such as a fluorescent lamp for color evaluation in order to accurately measure the position of the fine bubbles existing at the lowest position in the container. The separation rate can be said to be an index showing how quickly the fine-foamed beverage changes to a beverage solution containing no fine foam within a certain period of time, and a beverage with a low separation rate makes the state of the fine-foamed beverage longer. It can be said to be a sustainable beverage. The separation rate of the fine foam beverage of the present invention can be 0.7 mm / sec or less, preferably 0.68 mm / sec or less, and more preferably 0.6 mm / sec or less. Further, the separation rate of the fine foam beverage of the present invention can be 0.05 mm / sec or more, preferably 0.1 mm / sec or more. The separation rate of the fine foam beverage of the present invention can be 0.05 to 0.7 mm / sec, preferably 0.1 to 0.6 mm / sec.

本発明の微細泡飲料は、微細泡飲料を評価用容器に注いだときの、容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離を90mm以下とすることができ、好ましくは70mm、より好ましくは50mmとすることができる。 In the fine foam beverage of the present invention, when the fine foam beverage is poured into the evaluation container, the vertical distance from the bottom of the container 100 seconds after the container is fully filled to the lowest position of the fine foam is 90 mm or less. It can be preferably 70 mm, more preferably 50 mm.

本発明の微細泡飲料は、市販の炭酸飲料などと比較すると微細な泡が消失しにくい飲料ということができる。飲料中に消泡効果を有する成分が含まれていると、微細な泡が消失する速度が速くなることから、本発明の微細泡飲料は消泡成分の含有量が0.01%以下、好ましくは0.001%以下の飲料とすることができ、より好ましくは消泡成分を実質的に含まない飲料である。ここで、消泡成分としては、乳化剤、シリコーン系消泡剤、液状油が挙げられる。 It can be said that the fine foam beverage of the present invention is a beverage in which fine foam is less likely to disappear as compared with a commercially available carbonated beverage. If the beverage contains a component having a defoaming effect, the rate at which fine bubbles disappear becomes faster. Therefore, the fine foam beverage of the present invention preferably contains a defoaming component of 0.01% or less. Can be a beverage of 0.001% or less, and more preferably a beverage containing substantially no defoaming component. Here, examples of the defoaming component include emulsifiers, silicone-based defoaming agents, and liquid oils.

本発明の微細泡飲料において分離速度を算出する場合には、微細泡飲料を製造後、直ちに透明または半透明の容器に注ぎ、製造完了時から100秒後の容器底から微細な泡の最も低い位置までの距離を目視で測定し、その距離(mm)を100秒で割ることにより分離速度を算出することができる。 When calculating the separation rate in the fine foam beverage of the present invention, the fine foam beverage is immediately poured into a transparent or translucent container, and the lowest fine foam from the bottom of the container 100 seconds after the completion of production. The separation speed can be calculated by visually measuring the distance to the position and dividing the distance (mm) by 100 seconds.

本発明の微細泡飲料はまた、液粘度により特定することができる。本発明の微細泡飲料において液粘度を算出する場合には、微細泡飲料を適切な方法で脱泡処理に付し、脱泡後の飲料(非微細泡飲料)について液粘度を測定することができる。脱泡処理は、例えば減圧脱泡や遠心エバポレーター、真空撹拌脱泡装置などを使用することができる。液粘度は例えば落球式粘度測定法により測定することができ、落球式マイクロ粘度計(アントンパール社製)などの市販の測定機器を用いて測定をすることができる。本発明の微細泡飲料の液粘度は2.5mPa・s以下とすることができ、好ましくは2.2mPa・s以下、より好ましくは0.7~2.2mPa・sである。 The fine foam beverage of the present invention can also be specified by the liquid viscosity. When calculating the liquid viscosity in the fine foam beverage of the present invention, the fine foam beverage may be subjected to a defoaming treatment by an appropriate method, and the liquid viscosity of the defoamed beverage (non-fine foam beverage) may be measured. can. For the defoaming treatment, for example, vacuum defoaming, a centrifugal evaporator, a vacuum stirring defoaming device, or the like can be used. The liquid viscosity can be measured by, for example, a falling ball type viscosity measuring method, and can be measured by using a commercially available measuring device such as a falling ball type micro viscometer (manufactured by Anton Pearl Co., Ltd.). The liquid viscosity of the fine foam beverage of the present invention can be 2.5 mPa · s or less, preferably 2.2 mPa · s or less, and more preferably 0.7 to 2.2 mPa · s.

本発明の微細泡飲料は上記のように2.5mPa・s以下の液粘度をとることができるが、市販のスムージー飲料などと比較すると粘度が十分低い飲料ということができる。本発明の微細泡飲料はまた、流動性を十分に持ち、飲用に適した液性を有する。 As described above, the fine foam beverage of the present invention can have a liquid viscosity of 2.5 mPa · s or less, but it can be said that the beverage has a sufficiently low viscosity as compared with a commercially available smoothie beverage or the like. The fine foam beverage of the present invention also has sufficient fluidity and liquidity suitable for drinking.

本発明の微細泡飲料のベースとなる飲料液は微細な泡を形成させることができる限り、特に限定されるものではなく、清涼飲料、アルコール飲料、果汁飲料、乳飲料、野菜汁飲料などが挙げられる。清涼飲料としては、コーヒー飲料、緑茶飲料、紅茶飲料、酸性飲料、炭酸飲料、乳清飲料などが挙げられ、好ましくは、ビールテイスト飲料を除くものである。アルコール飲料は好ましくは、麦汁を含有するビールテイスト飲料を除くものである。 The beverage liquid which is the base of the fine foam beverage of the present invention is not particularly limited as long as it can form fine foam, and examples thereof include a soft beverage, an alcoholic beverage, a fruit juice beverage, a milk beverage, and a vegetable juice beverage. Be done. Examples of the soft drink include coffee drinks, green tea drinks, black tea drinks, acidic drinks, carbonated drinks, dairy drinks, and the like, preferably excluding beer-taste drinks. Alcoholic beverages are preferably excluding beer-taste beverages containing wort.

本発明の微細泡飲料は従来の飲料では実現されたことがない「泡融け感」を有する。すなわち、本発明の飲料を摂取した場合には以下の3つの飲用感が得られる。
(A)口腔内に十分な気泡が含有された飲料を含むことで、さらさらとした溶液が気泡を含んで軽くエアリーな食感が得られる。含んだ気泡は弾性がなく柔らかい。
(B)口腔内に含んだ気泡は、飲用中に発泡し弾けることなく口腔内で静かに消失し、溶液としての流動性を十分に感じることができる。
(C)嚥下後に口腔内での後残りがなく、優しく、刺激が少ないためごくごくと飲用できる。
The fine foam beverage of the present invention has a "foam melting feeling" that has never been realized in conventional beverages. That is, when the beverage of the present invention is ingested, the following three drinking sensations can be obtained.
(A) By including a beverage containing sufficient air bubbles in the oral cavity, the smooth solution contains air bubbles and a light and airy texture can be obtained. The bubbles contained are not elastic and soft.
(B) The bubbles contained in the oral cavity foam and disappear quietly in the oral cavity without popping during drinking, and the fluidity as a solution can be sufficiently felt.
(C) After swallowing, there is no residue in the oral cavity, it is gentle and there is little irritation, so it can be drunk very much.

本発明の微細泡飲料はまた、時間が経過するとともに微細な泡を含む飲料液と微細な泡が消失した飲料液とに徐々に分離するという特徴を有する(図1Bおよび図1C参照)。本発明の微細泡飲料は、飲料全体が微細な泡を含む溶液で構成された飲料のみならず、時間経過により微細な泡を含む飲料液と微細な泡が消失した飲料液とを含む飲料も包含するものとする。 The fine foam beverage of the present invention is also characterized in that it gradually separates into a beverage liquid containing fine foam and a beverage liquid in which the fine foam disappears over time (see FIGS. 1B and 1C). The fine foam beverage of the present invention includes not only a beverage in which the entire beverage is composed of a solution containing fine foam, but also a beverage containing a beverage liquid containing fine foam and a beverage liquid in which the fine foam disappears over time. It shall be included.

本発明の微細泡飲料の製造方法は、原料となる飲料液に微細泡を形成させることができれば特に限定されないが、例えば、気体と飲料液とを混合することにより製造することができる。すなわち、飲料液を準備し、容器中で3000~50000rpm、1秒~60分の条件で混合し、飲料液中に微細泡を形成させて気体を飲料液中に取り込ませることで本発明の微細泡飲料を製造することができる。気体としては、窒素を含有する気体(例えば、空気)および窒素ガスが挙げられ、好ましくは窒素を含有する気体であり、より好ましくは空気である。 The method for producing a fine foam beverage of the present invention is not particularly limited as long as the beverage liquid as a raw material can form fine foam, but can be produced, for example, by mixing a gas and a beverage liquid. That is, the fineness of the present invention is obtained by preparing a drinking liquid, mixing it in a container at 3000 to 50,000 rpm, 1 second to 60 minutes, forming fine bubbles in the drinking liquid, and incorporating the gas into the drinking liquid. Foam beverages can be produced. Examples of the gas include a nitrogen-containing gas (for example, air) and a nitrogen gas, preferably a nitrogen-containing gas, and more preferably air.

飲料液の混合は容器中で行うことができる。微細泡を構成する気体が空気である場合、容器中で飲料液を混合することにより本発明の微細泡飲料を製造することができる。容器中で上記の混合強度および混合時間で飲料液を混合する場合には、攪拌機や混合容器、気液混合機を用いて混合を行うことができる。具体的には、攪拌機としてはジューサーミキサー、ミキサー、フードプロセッサー、ブレンダ―、高速分散機を用いることができ、混合容器としてはシェーカー、気体混合用加圧容器を用いることができ、気液混合機としてはスプレーガン、二流体ノズル、エアーストーンを用いることができる。 Beverage liquid mixing can be done in a container. When the gas constituting the fine foam is air, the fine foam beverage of the present invention can be produced by mixing the beverage liquid in the container. When the beverage liquid is mixed in the container at the above mixing strength and mixing time, the mixing can be performed using a stirrer, a mixing container, or a gas-liquid mixer. Specifically, a juicer mixer, a mixer, a food processor, a blender, and a high-speed disperser can be used as the stirrer, and a shaker and a pressurized container for gas mixing can be used as the mixing container. As, a spray gun, a two-fluid nozzle, and an air stone can be used.

製造された微細泡飲料はグラスやコップなどの容器に注がれ、飲用者に提供することができる。本発明の微細泡飲料は時間が経過すると、微細な泡から構成される部分と微細な泡を含まない部分に分離することから、上記(A)、(B)および(C)の作用効果をよりよく発揮させるために、製造完了後、直ちに容器に注ぎ、飲用者に提供することが望ましい。ここで、本発明の微細泡飲料を気体と飲料液とを混合することにより製造する場合は、原料飲料液の全量について混合が完了したことをもって製造完了とみなすことができる。 The produced fine foam beverage can be poured into a container such as a glass or a cup and provided to the drinker. Since the fine foam beverage of the present invention separates into a portion composed of fine foam and a portion not containing fine foam over time, the effects of the above (A), (B) and (C) can be obtained. In order to achieve better performance, it is desirable to pour into a container immediately after the production is completed and provide it to the drinker. Here, when the fine foam beverage of the present invention is produced by mixing a gas and a beverage liquid, it can be considered that the production is completed when the mixing is completed for the entire amount of the raw material beverage liquid.

本発明の微細泡飲料は、製造完了時にすべての原料飲料液が微細な泡に変化せず、原料飲料液が残存していることがあるが、このような飲料も上記(A)、(B)および(C)の作用効果を発揮する限り本発明の微細泡飲料に包含される。 In the fine foam beverage of the present invention, all the raw material beverage liquids do not change to fine foams at the completion of production, and the raw material beverage liquid may remain, but such beverages also have the above (A) and (B). ) And (C) are included in the fine foam beverage of the present invention as long as they exhibit the effects.

以下の例に基づいて本発明をより具体的に説明するが、本発明はこれらの例に限定されるものではない。 The present invention will be described in more detail based on the following examples, but the present invention is not limited to these examples.

例1:微細泡飲料の製造および各種物性値の分析(1)
(1)飲料の調製
コーヒー飲料をベースとする微細泡飲料を調製した。具体的には、コーヒー豆(キリマンジャロ)をコーヒーミルで中挽きに粉砕し、ペーパーフィルターに粉砕したコーヒー豆100gを入れ、95℃の熱水で抽出した。ろ液1000gを採取したところで抽出を止め、1000gのコーヒー抽出液を得た。得られたコーヒー抽出液を20℃まで冷却して、該抽出液のpHが6.5になるように調製しながら炭酸水素ナトリウムを加え、イオン交換水を用いて全量を2000gとした(コーヒー調合液)。コーヒー調合液を90℃に加温し、飲料用スチール缶に190gを充填後、121℃、5分間でレトルト殺菌処理してブラックコーヒー飲料ベース(以下、「コーヒー飲料ベース1」ということがある)を調製した。
Example 1: Manufacture of fine foam beverages and analysis of various physical characteristics (1)
(1) Beverage preparation A fine foam beverage based on a coffee beverage was prepared. Specifically, coffee beans (Kirimanjaro) were crushed into medium grinders with a coffee mill, 100 g of the crushed coffee beans were placed in a paper filter, and the coffee beans were extracted with hot water at 95 ° C. Extraction was stopped when 1000 g of the filtrate was collected, and 1000 g of coffee extract was obtained. The obtained coffee extract was cooled to 20 ° C., sodium hydrogen carbonate was added while adjusting the pH of the extract to 6.5, and the total amount was adjusted to 2000 g using ion-exchanged water (coffee preparation). liquid). The coffee preparation is heated to 90 ° C, 190 g is filled in a steel beverage can, and then retort sterilized at 121 ° C for 5 minutes to make a black coffee beverage base (hereinafter, may be referred to as "coffee beverage base 1"). Was prepared.

上記のようにして調製したコーヒー飲料ベース1をあらかじめ液温が5℃になるように準備した。内径110mm、高さ130mmの円柱状のステンレス容器にコーヒー飲料ベース330gを入れ、液温が5℃~10℃を保つよう保冷した。ハンディーフードプロセッサー(バーミックスM300、エスゲー社)にアタッチメント(ウイスク、エスゲー社)を装着し、アタッチメント先端をステンレス容器底部につけて「低速」で30秒間混合処理してコールドタイプの微細泡飲料(試験区1)を調製した。製造完了時にコーヒー飲料液のすべてが微細な泡が形成された飲料に変化していることを目視で確認した。 The coffee beverage base 1 prepared as described above was prepared in advance so that the liquid temperature was 5 ° C. 330 g of coffee beverage base was placed in a cylindrical stainless steel container having an inner diameter of 110 mm and a height of 130 mm, and kept cold so that the liquid temperature was maintained at 5 ° C to 10 ° C. Attach the attachment (Whisk, Esge) to the handy food processor (Barmix M300, Esge), attach the tip of the attachment to the bottom of the stainless steel container, and mix at "low speed" for 30 seconds to make a cold-type fine foam beverage (test plot). 1) was prepared. It was visually confirmed that all of the coffee beverage liquid was changed to a beverage having fine bubbles formed at the completion of production.

次に、コーヒー飲料ベース1をあらかじめ液温が70℃になるように準備した。内径110mm、高さ130mmの円柱状のステンレス容器にコーヒー飲料ベース330gを入れ、液温が65℃~70℃を保つよう保温した。ハンディーフードプロセッサー(バーミックスM300、エスゲー社)にアタッチメント(ウイスク、エスゲー社)を装着し、アタッチメント先端をステンレス容器底部につけて「高速」で30秒間混合処理してホットタイプの微細泡飲料(試験区2)を調製した。製造完了時にコーヒー飲料液のすべてが微細な泡が形成された飲料に変化していることを目視で確認した。 Next, the coffee beverage base 1 was prepared in advance so that the liquid temperature was 70 ° C. 330 g of coffee beverage base was placed in a cylindrical stainless steel container having an inner diameter of 110 mm and a height of 130 mm, and kept warm so that the liquid temperature was maintained at 65 ° C to 70 ° C. Attach the attachment (Whisk, Esge) to the handy food processor (Barmix M300, Esge), attach the tip of the attachment to the bottom of the stainless steel container, and mix at "high speed" for 30 seconds to make a hot-type fine foam beverage (test plot). 2) was prepared. It was visually confirmed that all of the coffee beverage liquid was changed to a beverage having fine bubbles formed at the completion of production.

また、比較対照品として市販のビール飲料(ギネス、キリンビール社)(試験区3)、スムージー飲料(黒ゴマ豆乳バナナスムージー、ユニマットリケン社)(試験区4)、コーラ飲料(メッツコーラ、キリンビバレッジ社)(試験区5)、コーヒー飲料(振って泡立つプレミアム、ダイドードリンコ社)(試験区6)を準備した。 In addition, as comparative products, commercially available beer beverages (Guinness, Kirin Brewery) (Test Zone 3), smoothie beverages (Black Sesame Soymilk Banana Smoothie, Unimat Riken) (Test Zone 4), Coke Beverages (Mets Cola, Kirin Beverage). (Company) (Test Zone 5), Coffee Beverage (Shaking and Foaming Premium, Daido Drinko Co., Ltd.) (Test Zone 6) were prepared.

(2)飲料の分析
各試験区の飲料は以下の手順でゾル比重、分離速度、液粘度を測定した。
(2) Beverage analysis The sol specific gravity, separation rate, and liquid viscosity of the beverages in each test group were measured by the following procedure.

ア ゾル比重
微細泡飲料を製造完了後、直ちにプラスチック製カップ(容量150mL、旭化成社製、プロマックスEI-150D)に満量となるまで注ぎ、満注容量の質量を測定した。次に、微細泡飲料を遠心エバポレーター(Genevac社製)を用いて脱泡処理に付し、脱泡後の飲料(非微細泡飲料)の満注容量の質量を微細泡飲料と同様に測定した。
Immediately after the production of the sol specific gravity fine foam beverage was completed, it was poured into a plastic cup (capacity 150 mL, manufactured by Asahi Kasei Co., Ltd., Promax EI-150D) until it was full, and the mass of the full volume was measured. Next, the fine foam beverage was subjected to defoaming treatment using a centrifugal evaporator (manufactured by Genevac), and the mass of the full filling capacity of the beverage after defoaming (non-fine foam beverage) was measured in the same manner as the fine foam beverage. ..

ゾル比重は下記数式(I)に基づいて算出した。

Figure 0007005705000001
The sol specific gravity was calculated based on the following formula (I).
Figure 0007005705000001

イ 分離速度
微細泡飲料を製造完了後、直ちに分離速度評価用ガラス(容量300mL、φ52mm、高さ140mm)に満量となるまで注ぎ、容器満注時と容器満注時から100秒後に容器内で最も低い位置に存在する微細泡の位置を、底部からの距離(mm)として測定した。微細泡の有無は、色評価用蛍光ランプを用いて2000±500luxとなる環境下に分離速度評価用ガラスを設置し、目視によって判定した。容器満注時から数秒後の試験区1の飲料と容器満注時から100秒経過後の試験区1の飲料はそれぞれ図1Bおよび図1Cに示される通りである。なお、試験区1および2の飲料は、容器満注時に飲料ベースのすべてが微細な泡が形成された飲料となっていることを目視で確認した(下記数式(II)においてY=0(mm))。
B. Separation rate Immediately after the production of the fine foam beverage is completed, pour it into the glass for evaluation of separation rate (capacity 300 mL, φ52 mm, height 140 mm) until it is full, and inside the container when the container is full and 100 seconds after the container is full. The position of the fine bubbles present at the lowest position was measured as the distance (mm) from the bottom. The presence or absence of fine bubbles was visually determined by installing a separation rate evaluation glass in an environment of 2000 ± 500 lux using a fluorescent lamp for color evaluation. The beverages in Test Group 1 several seconds after the container is fully filled and the beverages in Test Group 1 100 seconds after the container is fully filled are as shown in FIGS. 1B and 1C, respectively. It was visually confirmed that all of the beverage bases of the beverages in Test Groups 1 and 2 were beverages in which fine bubbles were formed when the container was fully filled (Y = 0 (mm) in the following formula (II). )).

分離速度は下記数式(II)に基づいて算出した。

Figure 0007005705000002
X=容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離(mm)
Y=容器満注時の容器底から微細な泡の最も低い位置までの垂直距離(mm) The separation rate was calculated based on the following mathematical formula (II).
Figure 0007005705000002
X = Vertical distance (mm) from the bottom of the container 100 seconds after full filling of the container to the lowest position of fine bubbles.
Y = Vertical distance (mm) from the bottom of the container when the container is fully filled to the lowest position of fine bubbles.

ウ 液粘度
微細泡飲料は遠心エバポレーター(Genevac社製)を用いて脱泡処理に供し、脱泡後の溶液について液粘度を測定した。液粘度の測定は落球式マイクロ粘度計(アントンパール社製)により実施した。測定時の溶液温度は20℃とし、対象の液粘度に応じてキャピラリーおよびボールを、該粘度計指定の方法に従って選択して測定を行った。
C. Liquid viscosity The fine foam beverage was subjected to defoaming treatment using a centrifugal evaporator (manufactured by Genevac), and the liquid viscosity of the defoamed solution was measured. The liquid viscosity was measured with a falling ball type micro viscometer (manufactured by Anton Pearl Co., Ltd.). The solution temperature at the time of measurement was 20 ° C., and the capillaries and balls were selected and measured according to the method specified by the viscometer according to the viscosity of the target liquid.

(3)官能評価
各試験区の飲料は、さらに官能評価に供した。官能評価は訓練されたパネリスト6名により実施した。具体的には、各試験区の飲料について、以下の4項目を評価し、最も得票数が多かった評価点を採用した。ただし、得票数が同数の場合は、より低い評価点を採用した。
(3) Sensory evaluation The beverages in each test group were further subjected to sensory evaluation. Sensory evaluation was performed by 6 trained panelists. Specifically, the following four items were evaluated for the beverages in each test group, and the evaluation score with the highest number of votes was adopted. However, if the number of votes obtained was the same, a lower evaluation score was adopted.

(a)飲用直後
A:口腔内に含んだ溶液がさらさらとして、気泡を含んで軽くエアリーな食感が得られ、且つ、含んだ気泡は弾性がなく柔らかい。
B:口腔内に含んだ溶液が気泡を含んで少しエアリーな食感が得られ、且つ、含んだ気泡が柔らかい。
C:口腔内に含んだ溶液が気泡を含んでいることは感じられるが、エアリーではない。
D:口腔内に含んだ溶液に気泡を感じられない。
(A) Immediately after drinking A: The solution contained in the oral cavity is smooth and contains air bubbles to obtain a light and airy texture, and the contained air bubbles are not elastic and soft.
B: The solution contained in the oral cavity contains air bubbles to obtain a slightly airy texture, and the contained air bubbles are soft.
C: It is felt that the solution contained in the oral cavity contains air bubbles, but it is not airy.
D: No air bubbles can be felt in the solution contained in the oral cavity.

(b)飲用中
A:口腔内に含んだ気泡が弾けることなく静かに、次々に消失し、溶液としての流動性が十分に感じられる。
B:口腔内に含んだ気泡の一部が弾けることなく消失し、溶液としての流動性が感じられる。
C:口腔内に含んだ気泡が少し消失した感覚があるものの、溶液としての流動性が得られにくい。
D:口腔内に含んだ気泡がとどまり続け、嚥下に少し抵抗感がある。
(B) During drinking A: Bubbles contained in the oral cavity disappear quietly one after another without popping, and the fluidity as a solution is sufficiently felt.
B: Some of the bubbles contained in the oral cavity disappear without popping, and the fluidity as a solution is felt.
C: Although there is a feeling that the bubbles contained in the oral cavity have disappeared a little, it is difficult to obtain fluidity as a solution.
D: Bubbles contained in the oral cavity continue to stay, and there is a slight resistance to swallowing.

(c)嚥下後
A:口腔内での後残りがなく、キレがとても良く感じられる。
B:口腔内での後残りが少なく、キレが良く感じられる。
C:嚥下後も口腔内に少し溶液が感じられ、キレが悪い。
D:嚥下後も口腔内に残液感がある。
(C) After swallowing A: There is no residue in the oral cavity, and the sharpness is felt very well.
B: There is little residue in the oral cavity, and the sharpness is felt well.
C: Even after swallowing, a little solution is felt in the oral cavity, and the sharpness is poor.
D: There is a feeling of residual liquid in the oral cavity even after swallowing.

(d)総合評価
A:飲料全体における「泡融け感」を十分に感じる。
B:飲料全体における「泡融け感」を感じる。
C:飲料全体における「泡融け感」があまり感じられない。
D:飲料全体における「泡融け感」が感じられない。
(D) Comprehensive evaluation A: The "feeling of melting foam" in the entire beverage is fully felt.
B: Feel the "melting feeling" in the whole beverage.
C: I don't feel much "melting foam" in the whole beverage.
D: No "feeling of melting foam" is felt in the entire beverage.

(4)結果
各試験区の飲料の液粘度、ゾル比重、分離速度、官能評価結果は表1に示される通りであった。

Figure 0007005705000003
(4) Results The liquid viscosity, sol specific gravity, separation rate, and sensory evaluation results of the beverages in each test group were as shown in Table 1.
Figure 0007005705000003

表1の結果から、ゾル比重、分離速度および液粘度が特定の範囲に含まれる微細泡飲料が官能評価項目(a)、(b)、(c)および(d)において望ましい評価結果を示し、これまでにない泡融け感を有する飲料であることが判明した。一方で、ゾル比重が大きい試験区3においては嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。液粘度が大きい試験区4においては、気泡を含んだエアリーで柔らかい食感が得られたものの、口腔内でも気泡が十分に保持され、消失感や流動性が感じられなかった。また、嚥下後ももったりとした飲料液が口腔内に残存する感覚があり、泡融け感は有していなかった。分離速度が大きい試験区5においては嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。ゾル比重、分離速度および液粘度のすべてが大きい試験区6においては、気泡によるエアリーな食感や口腔内での消失感が得られず、嚥下後ももったりとした飲料液が口腔内に残存し、泡融け感は有していなかった。 From the results in Table 1, fine foam beverages containing a specific range of sol specific gravity, separation rate and liquid viscosity showed desirable evaluation results in the functional evaluation items (a), (b), (c) and (d). It turned out to be a beverage with an unprecedented foaming sensation. On the other hand, in the test group 3 having a large sol specific density, although the sharpness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and the foam did not have a melting feeling. In the test group 4 having a large liquid viscosity, an airy and soft texture containing air bubbles was obtained, but the air bubbles were sufficiently retained even in the oral cavity, and no feeling of disappearance or fluidity was felt. In addition, there was a sensation that the fluffy drinking liquid remained in the oral cavity even after swallowing, and there was no feeling of foam melting. In the test group 5 having a high separation rate, although the sharpness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and the foam did not have a melting feeling. In Test Group 6, where the sol specific gravity, separation rate, and liquid viscosity are all large, the airy texture due to air bubbles and the feeling of disappearance in the oral cavity were not obtained, and the beverage liquid that was moist after swallowing remained in the oral cavity. However, it did not have a feeling of melting bubbles.

例2:微細泡飲料の製造および各種物性値の分析(2)
表2に従って試験用飲料ベースを調製し、該飲料ベースと気体との混合処理を行い、微細泡飲料(試験区7~19)を調製した。製造完了時に試験用飲料ベースのすべてが微細な泡が形成された飲料に変化していることを目視で確認した。
Example 2: Manufacture of fine foam beverages and analysis of various physical property values (2)
A test beverage base was prepared according to Table 2, and the beverage base was mixed with a gas to prepare a fine foam beverage (test groups 7 to 19). Upon completion of production, it was visually confirmed that all of the test beverage base was transformed into a beverage with fine bubbles formed.

Figure 0007005705000004
Figure 0007005705000004

各試験区の飲料について、例1(2)および(3)に記載された手順に従ってゾル比重、分離速度、液粘度を測定するとともに、官能評価を行った。なお、分離速度の測定にあたっては、容器満注時に試験用飲料ベースのすべてが微細な泡が形成された飲料となっていることを目視で確認した(前記数式(II)においてY=0(mm))。 For the beverages in each test group, the sol specific gravity, separation rate, and liquid viscosity were measured according to the procedures described in Examples 1 (2) and (3), and sensory evaluation was performed. In measuring the separation rate, it was visually confirmed that all of the test beverage base was a beverage in which fine bubbles were formed when the container was fully filled (Y = 0 (mm in the above formula (II)). )).

各試験区の飲料の液粘度、ゾル比重、分離速度、官能評価結果は表3に示される通りであった。

Figure 0007005705000005
The liquid viscosity, sol specific gravity, separation rate, and sensory evaluation result of the beverage in each test group were as shown in Table 3.
Figure 0007005705000005

表3の結果から、飲料のゾル比重を0.85以下となるように調整し、かつ、分離速度を0.7mm/秒以下となるように調整し、かつ、液粘度を2.5mPa・s以下となるように調整することにより、官能評価項目(a)、(b)、(c)および(d)において好ましい結果を有する微細泡飲料が得られることが明らかとなった。 From the results in Table 3, the sol specific gravity of the beverage was adjusted to 0.85 or less, the separation speed was adjusted to 0.7 mm / sec or less, and the liquid viscosity was 2.5 mPa · s. It was clarified that by adjusting so as to be as follows, a fine foam beverage having favorable results in the functional evaluation items (a), (b), (c) and (d) can be obtained.

試験区7、8、14、19においては、分離速度および液粘度が同程度であり、かつ、ゾル比重が異なる飲料が調製され、試験区7、8は十分な泡融け感を有していた。一方で、試験区19では嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。 In the test groups 7, 8, 14 and 19, beverages having the same separation rate and liquid viscosity and different sol specific densities were prepared, and the test groups 7 and 8 had a sufficient foam melting feeling. .. On the other hand, in the test group 19, although the sharpness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and the foam did not have a melting feeling.

試験区8、9、10、11、12、14、15においては、ゾル比重および液粘度が同程度であり、かつ、分離速度が異なる飲料が調製され、試験区8、9、10、11は十分な泡融け感を有していた。一方で試験区12、15では嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感が不足していると感じられ、口腔内での気泡の消失感も感じられず、泡融け感は有していなかった。 In test groups 8, 9, 10, 11, 12, 14, and 15, beverages having the same sol specific gravity and liquid viscosity but different separation rates were prepared, and test groups 8, 9, 10 and 11 were prepared. It had a sufficient foam melting feeling. On the other hand, in the test groups 12 and 15, although the sharpness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were felt to be insufficient, and the feeling of disappearance of air bubbles in the oral cavity was not felt. , Did not have a feeling of foam melting.

試験区10、16、17、18においては、ゾル比重および分離速度が同程度であり、かつ、液粘度が異なる飲料が調製され、試験区10、16は十分な泡融け感を有していた。一方で、試験区18では気泡を含んだエアリーで柔らかい食感が得られたものの、口腔内でも気泡が保持され、消失感や流動性が感じられなかった。また、嚥下後ももったりとした飲料液が口腔内に残存する感覚があり、泡融け感は有していなかった。 In the test groups 10, 16, 17 and 18, beverages having the same sol specific gravity and separation rate but different liquid viscosities were prepared, and the test groups 10 and 16 had a sufficient foam melting feeling. .. On the other hand, in the test group 18, although an airy texture containing air bubbles was obtained, the air bubbles were retained even in the oral cavity, and no feeling of disappearance or fluidity was felt. In addition, there was a sensation that the fluffy drinking liquid remained in the oral cavity even after swallowing, and there was no feeling of foam melting.

ゾル比重および分離速度が大きい試験区13においては、嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。 In the test group 13 having a large sol specific density and separation speed, although the sharpness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and the foam did not have a melting feeling.

例3:微細泡飲料の製造および各種物性値の分析(3)
表4に従って試験用飲料ベースを調製し、該飲料ベースと気体との混合処理を行い、微細泡飲料(試験区20~30)を調製した。製造完了時に試験用飲料ベースのすべてが微細な泡が形成された飲料に変化していることを目視で確認した。
Example 3: Manufacture of fine foam beverages and analysis of various physical characteristics (3)
A test beverage base was prepared according to Table 4, and the beverage base was mixed with a gas to prepare a fine foam beverage (test group 20 to 30). Upon completion of production, it was visually confirmed that all of the test beverage base was transformed into a beverage with fine bubbles formed.

Figure 0007005705000006
Figure 0007005705000006

各試験区の飲料について、例1(2)および(3)に記載された手順に従ってゾル比重、分離速度、液粘度を測定するとともに、官能評価を行った。なお、分離速度の測定にあたっては、容器満注時に試験用飲料ベースのすべてが微細な泡が形成された飲料となっていることを目視で確認した(前記数式(II)においてY=0(mm))。 For the beverages in each test group, the sol specific gravity, separation rate, and liquid viscosity were measured according to the procedures described in Examples 1 (2) and (3), and sensory evaluation was performed. In measuring the separation rate, it was visually confirmed that all of the test beverage base was a beverage in which fine bubbles were formed when the container was fully filled (Y = 0 (mm in the above formula (II)). )).

各試験区の飲料の液粘度、ゾル比重、分離速度、官能評価結果は表5に示される通りであった。

Figure 0007005705000007
The liquid viscosity, sol specific gravity, separation rate, and sensory evaluation result of the beverage in each test group were as shown in Table 5.
Figure 0007005705000007

表5の結果から、飲料のゾル比重を0.85以下となるように調整し、かつ、分離速度を0.7mm/秒以下となるように調整し、かつ、液粘度を2.5mPa・s以下となるように調整することにより、官能評価項目(a)、(b)、(c)および(d)において好ましい結果を有する微細泡飲料が得られることが明らかとなった。 From the results in Table 5, the sol specific gravity of the beverage was adjusted to 0.85 or less, the separation speed was adjusted to 0.7 mm / sec or less, and the liquid viscosity was 2.5 mPa · s. It was clarified that by adjusting so as to be as follows, a fine foam beverage having favorable results in the functional evaluation items (a), (b), (c) and (d) can be obtained.

試験区20、25においては、分離速度および液粘度が同程度であり、かつ、ゾル比重が異なる飲料が調製され、試験区25は十分な泡融け感を有していた。一方で、試験区20では嚥下後のキレの良さは感じられたものの、気泡含有による柔らかさやエアリーな食感は感じられず、泡融け感は有していなかった。 In the test groups 20 and 25, beverages having the same separation rate and liquid viscosity and different sol specific densities were prepared, and the test group 25 had a sufficient foam melting feeling. On the other hand, in the test group 20, although the sharpness after swallowing was felt, the softness and airy texture due to the inclusion of air bubbles were not felt, and the foam did not have a melting feeling.

試験区21、23、24においては、ゾル比重および分離速度が同程度であり、かつ、液粘度が異なる飲料が調製され、試験区23、24は十分な泡融け感を有していた。一方で、試験区21では気泡を含んだエアリーで柔らかい食感が得られたものの、嚥下後ももったりとした飲料液が口腔内に残存する感覚があり、泡融け感は有していなかった。

In the test groups 21, 23 and 24, beverages having the same sol specific gravity and separation rate but different liquid viscosities were prepared, and the test groups 23 and 24 had a sufficient foam melting feeling. On the other hand, in the test group 21, although an airy and soft texture containing air bubbles was obtained, there was a sensation that a lumpy drinking liquid remained in the oral cavity even after swallowing, and there was no feeling of foam melting. ..

Claims (7)

ゾル比重が0.85以下であり、分離速度が0.7mm/秒以下であり、かつ、液粘度が2.5mPa・s以下である、微細泡飲料(ここで、「ゾル比重」は一定容量の非微細泡飲料の質量に対する一定容量の微細泡飲料の質量の比率をいい、「分離速度」は微細泡飲料を分離速度評価用ガラス(容量300mL、φ52mm、高さ140mm)に注いだときの、容器満注時から100秒後の容器底から微細な泡の最も低い位置までの垂直距離(mm)(垂直距離A)から容器満注時の容器底から微細な泡の最も低い位置までの垂直距離(mm)を引いた値を100秒で除した値をいう)であって、前記垂直距離Aが90mm以下である、微細泡飲料。 Fine foam beverage with a sol specific gravity of 0.85 or less, a separation rate of 0.7 mm / sec or less, and a liquid viscosity of 2.5 mPa · s or less (here, the "sol specific gravity" is a constant volume. The ratio of the mass of a fixed volume of fine foam beverage to the mass of non-fine foam beverage, "separation rate" is when the fine foam beverage is poured into a glass for evaluation of separation rate (capacity 300 mL, φ52 mm, height 140 mm) . From the vertical distance (mm) (vertical distance A) from the bottom of the container to the lowest position of the fine bubbles 100 seconds after the full filling of the container to the lowest position of the fine bubbles from the bottom of the container when the container is full. A fine foam beverage having a vertical distance (mm) divided by 100 seconds) and having a vertical distance A of 90 mm or less. 飲料のほぼ全体が微細な泡から構成される、請求項1に記載の微細泡飲料。 The fine foam beverage according to claim 1, wherein almost the entire beverage is composed of fine foam. 飲料が清涼飲料である、請求項1または2に記載の微細泡飲料。 The fine foam beverage according to claim 1 or 2, wherein the beverage is a soft drink. 飲料液を6000~50000rpm、30秒~60分の条件で混合する工程を含んでなる、微細泡飲料の製造方法であって、製造された飲料のゾル比重が0.85以下であり、分離速度が0.7mm/秒以下であり、かつ、液粘度が2.5mPa・s以下であり(ここで、ゾル比重および分離速度は請求項1で定義された内容と同義である)、かつ、製造された飲料の垂直距離A(ここで、垂直距離Aは請求項1で定義された内容と同義である)が90mm以下である方法。 A method for producing a fine foam beverage, which comprises a step of mixing the beverage liquid at 6000 to 50,000 rpm and 30 seconds to 60 minutes. The produced beverage has a sol specific gravity of 0.85 or less and a separation speed. Is 0.7 mm / sec or less, and the liquid viscosity is 2.5 mPa · s or less (here, the sol specific gravity and the separation rate are synonymous with the contents defined in claim 1), and the product is manufactured. A method in which the vertical distance A (where vertical distance A is synonymous with the content defined in claim 1) of the beverage is 90 mm or less. 窒素を含有する気体の存在下で混合を行う、請求項4に記載の製造方法。 The production method according to claim 4, wherein the mixing is performed in the presence of a gas containing nitrogen. 製造された飲料が、飲料のほぼ全体が微細な泡から構成されるものである、請求項4または5に記載の製造方法。 The production method according to claim 4 or 5, wherein the produced beverage is composed of almost all fine bubbles. 飲料が清涼飲料である、請求項4~6のいずれか一項に記載の製造方法。 The production method according to any one of claims 4 to 6, wherein the beverage is a soft drink.
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