JPS643152A - Production of glycol esters - Google Patents
Production of glycol estersInfo
- Publication number
- JPS643152A JPS643152A JP62156496A JP15649687A JPS643152A JP S643152 A JPS643152 A JP S643152A JP 62156496 A JP62156496 A JP 62156496A JP 15649687 A JP15649687 A JP 15649687A JP S643152 A JPS643152 A JP S643152A
- Authority
- JP
- Japan
- Prior art keywords
- carboxylic acid
- aliphatic carboxylic
- catalyst
- component
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
PURPOSE: To obtain the titled compound useful as an intermediate in high efficiency, by reacting a lower aliphatic carboxylic acid with an olefin in the presence of oxygen and a catalyst containing Pd, a metal and halogen component and a nitrogen-containing oxide via several steps.
CONSTITUTION: Glycol esters are produced by reacting a lower aliphatic carboxylic acid an olefin in the presence of O and a catalyst containing a palladium component (e.g., sodium palladium chloride), a metal component of group IA, IB, IIA, IIB, VA, VIIB or VIII of the periodic table, a halogen component (e.g. Cl) and a nitrogen-containing oxide (e.g., nitric acid). The above process includes the following 4 steps. (1) Introduction of hydrogen after the reaction to reduce the Pd catalyst. (2) Filtration of the reduced liquid into reduced palladium and reaction liquid. (3) Distillation of the reaction liquid to separate the lower aliphatic carboxylic acid from the objective compound. (4) Addition of an aliphatic carboxylic acid, the distillation residue of the step 3, a halogen and a nitrate ion source to the reduced Pd of the step 2 and the introduction of the prepared catalyst liquid into the reaction system.
COPYRIGHT: (C)1989,JPO&Japio
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62-156496A JPH013152A (en) | 1987-06-25 | Method for producing glycol esters | |
EP88109713A EP0296503B1 (en) | 1987-06-25 | 1988-06-17 | Process for producing glycol esters |
DE3887779T DE3887779T2 (en) | 1987-06-25 | 1988-06-17 | Process for the preparation of glycol esters. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62-156496A JPH013152A (en) | 1987-06-25 | Method for producing glycol esters |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS643152A true JPS643152A (en) | 1989-01-06 |
JPH013152A JPH013152A (en) | 1989-01-06 |
Family
ID=
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5235145A (en) * | 1992-01-13 | 1993-08-10 | Otis Elevator Company | Elevator with linear motor drive assembly |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5163114A (en) * | 1974-11-27 | 1976-06-01 | Kuraray Co | |
JPS58177936A (en) * | 1982-04-12 | 1983-10-18 | Idemitsu Kosan Co Ltd | Preparation of glycol ester |
JPS61140545A (en) * | 1984-12-12 | 1986-06-27 | Idemitsu Kosan Co Ltd | Production of glycol ester |
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5163114A (en) * | 1974-11-27 | 1976-06-01 | Kuraray Co | |
JPS58177936A (en) * | 1982-04-12 | 1983-10-18 | Idemitsu Kosan Co Ltd | Preparation of glycol ester |
JPS61140545A (en) * | 1984-12-12 | 1986-06-27 | Idemitsu Kosan Co Ltd | Production of glycol ester |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5235145A (en) * | 1992-01-13 | 1993-08-10 | Otis Elevator Company | Elevator with linear motor drive assembly |
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