JPS63274444A - 無機肥料のプリル化方法 - Google Patents
無機肥料のプリル化方法Info
- Publication number
- JPS63274444A JPS63274444A JP62104185A JP10418587A JPS63274444A JP S63274444 A JPS63274444 A JP S63274444A JP 62104185 A JP62104185 A JP 62104185A JP 10418587 A JP10418587 A JP 10418587A JP S63274444 A JPS63274444 A JP S63274444A
- Authority
- JP
- Japan
- Prior art keywords
- zone
- air
- crystallization
- crystallization zone
- purification
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003337 fertilizer Substances 0.000 title claims description 73
- 238000002425 crystallisation Methods 0.000 claims description 153
- 230000008025 crystallization Effects 0.000 claims description 153
- 239000002245 particle Substances 0.000 claims description 108
- 239000007788 liquid Substances 0.000 claims description 103
- 238000001816 cooling Methods 0.000 claims description 89
- 238000004140 cleaning Methods 0.000 claims description 87
- 238000000746 purification Methods 0.000 claims description 72
- 238000000034 method Methods 0.000 claims description 71
- 239000000155 melt Substances 0.000 claims description 48
- 238000005406 washing Methods 0.000 claims description 31
- 230000015572 biosynthetic process Effects 0.000 claims description 23
- 238000007670 refining Methods 0.000 claims description 12
- 238000007599 discharging Methods 0.000 claims description 4
- 238000010128 melt processing Methods 0.000 claims 2
- 239000000126 substance Substances 0.000 claims 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 102
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 79
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 72
- 239000004202 carbamide Substances 0.000 description 51
- 235000013877 carbamide Nutrition 0.000 description 51
- 229910021529 ammonia Inorganic materials 0.000 description 36
- 238000007906 compression Methods 0.000 description 33
- 230000006835 compression Effects 0.000 description 33
- 239000000243 solution Substances 0.000 description 31
- 239000000047 product Substances 0.000 description 29
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 23
- 229910017604 nitric acid Inorganic materials 0.000 description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 22
- 238000004519 manufacturing process Methods 0.000 description 15
- 239000007864 aqueous solution Substances 0.000 description 13
- 239000012467 final product Substances 0.000 description 13
- 238000003860 storage Methods 0.000 description 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- 239000000203 mixture Substances 0.000 description 11
- 238000012958 reprocessing Methods 0.000 description 11
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 238000001159 Fisher's combined probability test Methods 0.000 description 5
- 238000011084 recovery Methods 0.000 description 5
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 4
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 4
- 235000011130 ammonium sulphate Nutrition 0.000 description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 description 4
- 239000011707 mineral Substances 0.000 description 4
- 238000004364 calculation method Methods 0.000 description 3
- ODFGMSVMKUBHQN-UHFFFAOYSA-O diazanium;acetate;nitrate Chemical compound [NH4+].[NH4+].CC([O-])=O.[O-][N+]([O-])=O ODFGMSVMKUBHQN-UHFFFAOYSA-O 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- 230000003321 amplification Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 230000003116 impacting effect Effects 0.000 description 2
- 238000003199 nucleic acid amplification method Methods 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004887 air purification Methods 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
- C05C1/02—Granulation; Pelletisation; Stabilisation; Colouring
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
- B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Fertilizers (AREA)
- Glanulating (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19873712494 DE3712494A1 (de) | 1987-04-13 | 1987-04-13 | Verfahren zum granulieren von mineralischen duengemitteln |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS63274444A true JPS63274444A (ja) | 1988-11-11 |
Family
ID=6325531
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP62104185A Pending JPS63274444A (ja) | 1987-04-13 | 1987-04-27 | 無機肥料のプリル化方法 |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JPS63274444A (OSRAM) |
| DE (1) | DE3712494A1 (OSRAM) |
| FR (1) | FR2614218B1 (OSRAM) |
| NL (1) | NL8700921A (OSRAM) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2022554266A (ja) * | 2019-11-04 | 2022-12-28 | ティッセンクルップ インダストリアル ソリューションズ アクツィエンゲゼルシャフト | 尿素造粒物の製造方法及び製造プラント |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1249057B (it) * | 1991-05-22 | 1995-02-11 | Agrimont Spa | Processo per abbattere con un liquido l'ammoniaca contenuta in uno sfiato. |
| US5718733A (en) * | 1994-12-12 | 1998-02-17 | Rohm And Haas Company | Method for accelerating solidification of low melting point products |
| CN111151192A (zh) * | 2020-02-23 | 2020-05-15 | 河南龙昌机械制造有限公司 | 一种有机肥生产线 |
| WO2025073368A1 (de) * | 2023-10-05 | 2025-04-10 | Flechsig Patent Company Llc | Reaktionssystem und verfahren zur durchführung von chemischen reaktionen in flüssiger phase |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1230402B (de) * | 1963-12-13 | 1966-12-15 | Uhde Gmbh Friedrich | Verfahren zur Herstellung von Granulaten aus Schmelzen oder hochkonzentrierten Loesungen |
| SU822871A1 (ru) * | 1976-10-01 | 1981-04-23 | Предприятие П/Я Р-6603 | Установка дл гранулировани МиНЕРАльНыХ удОбРЕНий |
-
1987
- 1987-04-13 DE DE19873712494 patent/DE3712494A1/de active Granted
- 1987-04-16 NL NL8700921A patent/NL8700921A/nl not_active Application Discontinuation
- 1987-04-22 FR FR8705698A patent/FR2614218B1/fr not_active Expired
- 1987-04-27 JP JP62104185A patent/JPS63274444A/ja active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2022554266A (ja) * | 2019-11-04 | 2022-12-28 | ティッセンクルップ インダストリアル ソリューションズ アクツィエンゲゼルシャフト | 尿素造粒物の製造方法及び製造プラント |
Also Published As
| Publication number | Publication date |
|---|---|
| NL8700921A (nl) | 1988-11-16 |
| DE3712494C2 (OSRAM) | 1990-08-23 |
| FR2614218B1 (fr) | 1989-08-04 |
| FR2614218A1 (fr) | 1988-10-28 |
| DE3712494A1 (de) | 1988-11-03 |
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