JPS63176324A - Production of preform for optical fiber - Google Patents
Production of preform for optical fiberInfo
- Publication number
- JPS63176324A JPS63176324A JP553487A JP553487A JPS63176324A JP S63176324 A JPS63176324 A JP S63176324A JP 553487 A JP553487 A JP 553487A JP 553487 A JP553487 A JP 553487A JP S63176324 A JPS63176324 A JP S63176324A
- Authority
- JP
- Japan
- Prior art keywords
- optical fiber
- eccentricity
- base material
- core
- center
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000013307 optical fiber Substances 0.000 title claims abstract description 39
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 claims abstract description 31
- 238000012545 processing Methods 0.000 claims abstract description 27
- 239000000463 material Substances 0.000 claims description 46
- 238000005253 cladding Methods 0.000 claims description 18
- 238000012937 correction Methods 0.000 claims description 15
- 239000011521 glass Substances 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 6
- 230000002093 peripheral effect Effects 0.000 claims 1
- 238000005259 measurement Methods 0.000 abstract description 3
- 238000010586 diagram Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 4
- 230000006866 deterioration Effects 0.000 description 3
- 238000003754 machining Methods 0.000 description 3
- 239000012808 vapor phase Substances 0.000 description 3
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/01205—Manufacture of preforms for drawing fibres or filaments starting from tubes, rods, fibres or filaments
- C03B37/01225—Means for changing or stabilising the shape, e.g. diameter, of tubes or rods in general, e.g. collapsing
- C03B37/01228—Removal of preform material
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacture, Treatment Of Glass Fibers (AREA)
Abstract
Description
【発明の詳細な説明】
〔産業上の利用分野〕
本発明はコアおよびクラッドからなる光フアイバ用母材
の製造方法に関し、と(にクラッド中心に対するコア中
心の偏心量の少ない光フアイバ用母材の製造方法に関す
るものである。[Detailed Description of the Invention] [Industrial Application Field] The present invention relates to a method for manufacturing an optical fiber preform consisting of a core and a cladding, and (in particular, an optical fiber preform having a small eccentricity of the core center with respect to the cladding center. The present invention relates to a manufacturing method.
従来、光フアイバ用母材の製造方法としては、たとえば
VAD法(Vapor Phase Axial De
position:気相軸付法) 、MCVD法(Mo
dified ChemicalVapor Phas
e Deposition :肉付化学気相堆積法)、
OVD法(0utside Vapor Phas
e 0xidationDeposition :外
付気相酸化法)などが行われているが、これらいずれの
製造方法においても、クラッド中心に対するコア中心の
偏心が発生する可能性は避けられず、−aにこの偏心を
少くするため、上記の各種それぞれの光フアイバ用母材
の製造方法における製造工程において、コアの偏心発生
要因を可能な限り抑制する方法がとられている。しかし
、コアの偏心の少ない母材を製造することは極めて困難
で、母材としての不良品の発生を完全になくすことは不
可能であった。また不良品とまではならなくとも、コア
の偏心量の大きいものについては、母材を線引きし、フ
ァイバ化した際、接続損失が増加する、あるいは接続が
非常に難しくなることから、母材の段階で選別を行って
いる。Conventionally, methods for manufacturing optical fiber base materials include, for example, the VAD method (Vapor Phase Axial De
position: vapor phase axis method), MCVD method (Mo
dified Chemical Vapor Phas
eDeposition: fleshed chemical vapor deposition method),
OVD method
e OxidationDeposition: External vapor phase oxidation method), but in any of these manufacturing methods, the possibility of eccentricity of the core center with respect to the cladding center is unavoidable, and it is necessary to reduce this eccentricity in -a. Therefore, in the manufacturing process of each of the above-mentioned methods for manufacturing optical fiber preforms, methods are taken to suppress the causes of core eccentricity as much as possible. However, it is extremely difficult to manufacture a base material with a minimal eccentricity of the core, and it has been impossible to completely eliminate the occurrence of defective products as a base material. In addition, even if it is not a defective product, if the core has a large eccentricity, the splice loss will increase or the splice will be extremely difficult when the base material is drawn and made into a fiber. Selection is done in stages.
従来の光フアイバ用母材の製造方法では、製造した母材
の段階で、折角母材化したにもかかわらず、コアの偏心
が発生した場合、この偏心を修正する技術がないため、
母材を選別するはかなく、母材から光ファイバへの歩留
りが悪くなるという問題がある。In conventional manufacturing methods for optical fiber base materials, if core eccentricity occurs at the stage of manufacturing the base material, even though it has been made into a base material, there is no technology to correct this eccentricity.
There is a problem that the selection of the base material is ephemeral and the yield from the base material to the optical fiber is poor.
本発明は従来の問題点を解決し、母材化後のコアの偏心
修正を目的として、これにより光フアイバ製造の生産性
向上を可能とするもので、コアおよびクラッドからなる
光フアイバ用のガラス母材の製造方法において、クラッ
ドの中心に対するコアの中心の偏心を測定し、ガラス母
材のクラッド部分に、測定したコアの偏心量の修正加工
を施すことを特徴とし、とくにコアの偏心量の修正加工
は、クラッド外周部を火炎加熱し、ガラス蒸発させるこ
とにより行うことを特徴としている。The present invention solves the conventional problems and aims to correct the eccentricity of the core after it is made into a base material, thereby making it possible to improve the productivity of optical fiber manufacturing. The method for manufacturing the base material is characterized in that the eccentricity of the center of the core with respect to the center of the cladding is measured, and the cladding part of the glass base material is subjected to a correction process for the measured eccentricity of the core. The modification process is characterized in that it is performed by flame heating the outer periphery of the clad to evaporate the glass.
本発明は、光フアイバ用母材の製造において、透明ガラ
ス母材化した段階以降にコアのクラッド中心に対する偏
心を測定し、偏心の大きいものについては、偏心を減少
するよう透明ガラス母材に物理的な修正を加え、たとえ
ば火災を用いてクラッド外周部のff−7スを蒸発させ
ることにより透明ガラス母材の構造を変化させ、これに
よりコアの偏心の少ない光フアイバ用母材を製造するこ
とができ、製造歩留りの向上、光ファイバの製造価格の
低減を可能とし、経済的効果が顕著となる。以下図面に
もとづき実施例について説明する。In the production of optical fiber base materials, the present invention measures the eccentricity of the core with respect to the center of the cladding after the stage of producing a transparent glass base material, and if the eccentricity is large, it is physically applied to the transparent glass base material to reduce the eccentricity. The structure of the transparent glass base material is changed by modifying the structure of the transparent glass base material by, for example, evaporating the FF-7 gas on the outer periphery of the clad using fire, thereby producing a base material for optical fiber with less eccentricity of the core. This makes it possible to improve the manufacturing yield and reduce the manufacturing cost of optical fibers, resulting in significant economic effects. Examples will be described below based on the drawings.
第1図は本発明の光フアイバ用母材の製造方法の実施例
の要部概要を説明する図である。10は光フアイバ用母
材、11はコア、12はクラッド、13はクラッド中心
、14はクラッド中心13とコア11の中心のずれを修
正する加工の一例として、火炎を用いて光フアイバ用母
材10のクラッド12の部分のガラスを蒸発させ、修正
加工を行う加工用バーナである。FIG. 1 is a diagram illustrating an outline of the main parts of an embodiment of the method for manufacturing an optical fiber base material of the present invention. 10 is a base material for an optical fiber, 11 is a core, 12 is a cladding, 13 is a cladding center, and 14 is a base material for an optical fiber using a flame, as an example of processing for correcting the misalignment between the cladding center 13 and the center of the core 11. This is a processing burner that evaporates the glass in the cladding 12 of No. 10 and performs correction processing.
本実施例のコア偏心の修正加工として、火炎によるクラ
ッド部の構造変化を例示したが、この他に機械的にクラ
ッド部のガラスを研削する修正加工、あるいは化学反応
を利用したクラッド、部のガラスエツチングによる修正
加工も本発明の態様に含まれる。しかし、前者の機械加
工の場合には、クラッド部の研削面の強度劣化や残留ひ
ずみによる割れなどの問題が生ずる恐れがあり、また後
者の薬品などを用いたエツチングによる化学反応を用い
た修正加工の場合は、研削量、研削方向の制御性に制限
があり、微細加工が難かしいという問nがある。これに
対し本実施例の火炎を用いる修正加工は、機械的強度劣
化の恐れがなく、また火炎を絞るとか、加熱時間、加熱
量を変えるなどの方法により、微細加工が容易に可能な
ことから、本発明のコア偏心修正加工としては好ましい
態様である。As an example of the core eccentricity correction process in this example, structural change of the cladding part due to flame is shown as an example, but other methods include mechanically grinding the glass in the cladding area, or using chemical reactions to change the structure of the cladding part. Correction processing by etching is also included in the aspect of the present invention. However, in the case of the former type of machining, there is a risk of problems such as deterioration of the strength of the ground surface of the cladding and cracking due to residual strain, and in the case of the latter type of machining, there is a risk of problems such as cracking due to the deterioration of the strength of the ground surface of the cladding. In this case, the controllability of the amount of grinding and the direction of grinding is limited, and microfabrication is difficult. On the other hand, the modification process using flame in this example has no fear of mechanical strength deterioration, and microfabrication is easily possible by narrowing the flame or changing the heating time and amount. This is a preferred embodiment of the core eccentricity correction process of the present invention.
なお、本発明におけるコア中心とクラッド中心とのずれ
量の指標としての偏心率εは次式で定義されるものであ
る。Incidentally, the eccentricity ε as an index of the amount of deviation between the core center and the clad center in the present invention is defined by the following equation.
δ
ここでδはコア中心とクラッド中心のずれ量、Dはクラ
ッド直径を示す。δ Here, δ represents the amount of deviation between the core center and the cladding center, and D represents the cladding diameter.
次に本発明により製造した光フアイバ用母材の具体例に
ついて述べる。Next, a specific example of the optical fiber base material manufactured according to the present invention will be described.
具体例1:
直径25mmφの光フアイバ用母材について、あらかし
めコアの偏心を測定し、コア中心の、外径中心、すなわ
ちクラッド中心からのずれ量およびずれの方向を記録し
た。この測定・記録結果をもとに、コアの偏心を減少さ
せる方向に、酸水素火炎を用いて修正加工を行った。加
工用バーナは同心円状の二重管を用い、この二重管構造
の加工用バーナを5本、被加工体である光フアイバ用母
材を中心とする同一円周上の位置に配置した。第2図は
本具体例の加工用バーナの配置概要である。Specific Example 1: For an optical fiber base material having a diameter of 25 mmφ, the eccentricity of the swaged core was measured, and the amount and direction of deviation of the center of the core from the center of the outer diameter, that is, the center of the cladding, were recorded. Based on the results of this measurement and recording, correction processing was performed using an oxyhydrogen flame in the direction of reducing the eccentricity of the core. The processing burners used were concentric double pipes, and five processing burners having the double pipe structure were arranged at positions on the same circumference around the optical fiber base material as the workpiece. FIG. 2 shows an outline of the arrangement of processing burners in this specific example.
20は光フアイバ用母材の被加工体、21は加工用バー
ナを示す。第3図は、加工用バーナによる加熱時間と光
フアイバ用母材のクラッド部の加工量の関係を示す図で
ある。Reference numeral 20 indicates a workpiece of an optical fiber base material, and 21 indicates a processing burner. FIG. 3 is a diagram showing the relationship between the heating time by the processing burner and the processing amount of the cladding portion of the optical fiber base material.
本具体例における光フアイバ用母材は、GeO□−3i
n、ガラスコア、Sin、ガラスクラッドからなるもの
を使用し、加工用バーナ1本当り水素毎分20リツトル
、酸素毎分6リツトル流した。The optical fiber base material in this specific example is GeO□-3i
20 liters of hydrogen per minute and 6 liters of oxygen per minute were flowed per processing burner.
光フアイバ用母材の被加工体に対し、加工用バーナを毎
分50mmの速度で、被加工体の長手方向に移動させな
がら片側のみ加熱したところ、被加工体の光フアイバ用
母材の直径が約280μm減少した。この修正加工を施
すことにより、本具体例の光フアイバ用母材のコアの偏
心率は2.0%であつたものが、偏心修正加工後の偏心
率は0.9%に修正された。When heating only one side of the workpiece, which is the base material for optical fiber, while moving the processing burner in the longitudinal direction of the workpiece at a speed of 50 mm per minute, the diameter of the base material for optical fiber of the workpiece was decreased by about 280 μm. By performing this correction process, the eccentricity of the core of the optical fiber base material of this specific example was 2.0%, but the eccentricity after the eccentricity correction process was corrected to 0.9%.
具体例2:
直径60mmφの具体例1と同じ材質および構造の光フ
アイバ用母材に対して、具体例1と同様の偏心修正加工
を施した。ただし、光フアイバ用母材に対する加工用バ
ーナの移動速度は毎分30mmとした。この偏心修正加
工を施すことにより、偏心修正加工前に比べ光フアイバ
用母材の外径は0゜5mmN少し、偏心率は2.0%で
あったものが、偏心修正加工後の偏心率−1,2%に修
正された。Concrete Example 2: An eccentricity correction process similar to that of Concrete Example 1 was performed on an optical fiber base material having a diameter of 60 mm and having the same material and structure as Concrete Example 1. However, the moving speed of the processing burner with respect to the optical fiber base material was 30 mm per minute. By applying this eccentricity correction process, the outer diameter of the optical fiber base material was slightly smaller by 0°5 mmN and the eccentricity was 2.0% compared to before the eccentricity correction process, but after the eccentricity correction process, the eccentricity was - It was revised to 1.2%.
なお以上の具体例においては、加工用の火炎として酸水
素火炎を用いたが、これに限定するものではなく、メタ
ン、プロパンなどのガスを用いてもよく、また加工用バ
ーナの数は、必要な加工量に対し適宜選定することによ
り同等の効果が得られる。In the above specific example, an oxyhydrogen flame was used as the flame for processing, but the flame is not limited to this, and gases such as methane and propane may also be used, and the number of burners for processing may vary depending on the number of burners required. The same effect can be obtained by appropriately selecting the amount of processing.
以上述べたように、本発明は光フアイバ用母材の製造工
程において、光フアイバ用母材の段階でクラッド中心に
対するコア中心の偏心を測定し、測定の結果得られたコ
ア偏心量を減少するよう光フアイバ用母材のクラッド部
に偏心修正加工を行うことにより、コア偏心の少ない光
フアイバ用母材を製造することができ、光フアイバ用母
材の製造歩留りの向上、光ファイバの製造価格の低減が
可能となり、その効果顕著である。As described above, the present invention measures the eccentricity of the core center with respect to the cladding center at the optical fiber base material stage in the manufacturing process of the optical fiber base material, and reduces the core eccentricity obtained as a result of the measurement. By performing eccentricity correction processing on the cladding part of the optical fiber base material, it is possible to manufacture an optical fiber base material with less core eccentricity, improving the manufacturing yield of the optical fiber base material and reducing the manufacturing price of the optical fiber. The effect is remarkable.
第1図は本発明の光フアイバ用母材の製造方法の概要を
説明する図、第2図は本発明による加工用バーナの配置
例の概要図、第3図は加工用バーナによる被加工体の加
熱温度と加工量との関係を示す図である。
10・・・光フアイバ用母材、11・・・コア、12・
・・クラッド、13・・・クラッド中心、14・・・加
工用バーナ、20・・・被加工体、21・・・加工用バ
ーナ
本発明の尤ファイバ用母材製造方法概要説明図第 1
図
2″1.力[用ハ゛−す
本発明による加工用バーナの配置例M図第2図
力ロ然時間と加工量の関係を示す図
第3図FIG. 1 is a diagram illustrating an overview of the method for manufacturing an optical fiber base material according to the present invention, FIG. 2 is a schematic diagram of an example of the arrangement of processing burners according to the present invention, and FIG. 3 is a diagram showing a workpiece to be processed by the processing burner. FIG. 3 is a diagram showing the relationship between heating temperature and processing amount. 10... Base material for optical fiber, 11... Core, 12...
...Clad, 13...Clad center, 14... Burner for processing, 20... Workpiece, 21... Burner for processing Outline explanatory diagram of the method for manufacturing a base material for fiber of the present invention No. 1
Fig. 2 1. Example of arrangement of machining burners according to the present invention using force Fig. 2 Fig. 3 showing the relationship between force time and processing amount
Claims (2)
ス母材の製造方法において、 前記クラツドの中心に対する前記コアの中心の偏心を測
定し、 前記ガラス母材のクラツドの部分に、前記測定した偏心
量修正加工を施す工程を含んでなることを特徴とする光
フアイバ用母材の製造方法。(1) In a method for manufacturing a glass base material for an optical fiber consisting of a core and a cladding, the eccentricity of the center of the core with respect to the center of the cladding is measured, and the measured eccentricity is applied to the cladding portion of the glass base material. A method for producing a base material for an optical fiber, the method comprising the step of performing correction processing.
炎加熱し、ガラス蒸発させることにより行うことを特徴
とする特許請求の範囲第1項記載の光フアイバ用母材の
製造方法。(2) The method for manufacturing an optical fiber base material according to claim 1, wherein the eccentricity correction process is performed by flame heating the outer peripheral portion of the clad to evaporate the glass.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP553487A JPH0672022B2 (en) | 1987-01-13 | 1987-01-13 | Method for manufacturing base material for optical fiber |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP553487A JPH0672022B2 (en) | 1987-01-13 | 1987-01-13 | Method for manufacturing base material for optical fiber |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS63176324A true JPS63176324A (en) | 1988-07-20 |
JPH0672022B2 JPH0672022B2 (en) | 1994-09-14 |
Family
ID=11613853
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP553487A Expired - Lifetime JPH0672022B2 (en) | 1987-01-13 | 1987-01-13 | Method for manufacturing base material for optical fiber |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH0672022B2 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0878449A1 (en) * | 1997-05-13 | 1998-11-18 | Shin-Etsu Chemical Company, Ltd. | Method for making a preform for optical fibers by drawing a sintered preform boule |
EP0976689A1 (en) * | 1998-07-29 | 2000-02-02 | Shin-Etsu Chemical Co., Ltd. | Process of producing a preform for an optical fibre and product produced by the process |
-
1987
- 1987-01-13 JP JP553487A patent/JPH0672022B2/en not_active Expired - Lifetime
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0878449A1 (en) * | 1997-05-13 | 1998-11-18 | Shin-Etsu Chemical Company, Ltd. | Method for making a preform for optical fibers by drawing a sintered preform boule |
US6131414A (en) * | 1997-05-13 | 2000-10-17 | Shin-Etsu Chemical Co., Ltd. | Method for making a preform for optical fibers by drawing a mother ingot |
EP0976689A1 (en) * | 1998-07-29 | 2000-02-02 | Shin-Etsu Chemical Co., Ltd. | Process of producing a preform for an optical fibre and product produced by the process |
Also Published As
Publication number | Publication date |
---|---|
JPH0672022B2 (en) | 1994-09-14 |
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