JPS62287038A - Co-ni-sn metal-base diamond sintered compact - Google Patents
Co-ni-sn metal-base diamond sintered compactInfo
- Publication number
- JPS62287038A JPS62287038A JP12919686A JP12919686A JPS62287038A JP S62287038 A JPS62287038 A JP S62287038A JP 12919686 A JP12919686 A JP 12919686A JP 12919686 A JP12919686 A JP 12919686A JP S62287038 A JPS62287038 A JP S62287038A
- Authority
- JP
- Japan
- Prior art keywords
- powder
- diamond
- sintered body
- diamond sintered
- metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000010432 diamond Substances 0.000 title claims abstract description 25
- 229910003460 diamond Inorganic materials 0.000 title claims abstract description 24
- 239000000843 powder Substances 0.000 claims abstract description 14
- 239000000919 ceramic Substances 0.000 claims abstract description 11
- 239000002184 metal Substances 0.000 claims description 11
- 229910052751 metal Inorganic materials 0.000 claims description 11
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 5
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 4
- 230000001747 exhibiting effect Effects 0.000 claims description 4
- 239000011159 matrix material Substances 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 229910020676 Co—N Inorganic materials 0.000 claims 1
- 238000005245 sintering Methods 0.000 abstract description 5
- 239000000203 mixture Substances 0.000 abstract description 4
- 229910052759 nickel Inorganic materials 0.000 abstract description 4
- 229910018100 Ni-Sn Inorganic materials 0.000 abstract 1
- 229910018532 Ni—Sn Inorganic materials 0.000 abstract 1
- 229910017052 cobalt Inorganic materials 0.000 description 3
- 239000010941 cobalt Substances 0.000 description 3
- 229910020630 Co Ni Inorganic materials 0.000 description 2
- 229910052581 Si3N4 Inorganic materials 0.000 description 2
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 2
- 229910010271 silicon carbide Inorganic materials 0.000 description 2
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 description 2
- 229910002440 Co–Ni Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- -1 natural Chemical compound 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
Abstract
Description
【発明の詳細な説明】
３、発明の詳細な説明
〔産業上の利用分野〕
この発明は、窒化珪素、炭化珪素、酸化アルミニウノ、
等のファインセラミックスのＭ 密Ｊｉｆｆ 前用に使
用されろ＝７バル）・−・二−ツ）１ル一錫系金属基グ
イヤモンド焼結体に関するものである。[Detailed Description of the Invention] 3. Detailed Description of the Invention [Field of Industrial Application] This invention provides silicon nitride, silicon carbide, aluminum oxide,
This invention relates to a sintered body of a tin-based metal, which is used for fine ceramics such as 7 bars), 2, and 2).
従来、ニツケノＬ、−錫系並びに銅−錫系金属基クィヤ
モ、ド焼結体が＝１フィンセラミックスの精密研削に広
く１吏用されてきたが、研削性か劣り研削に当たって、
被研削材にチッピングを生しさせる等の支障を来してい
た。Conventionally, Nitsukeno L, tin-based and copper-tin based metal-based sintered bodies have been widely used for precision grinding of =1 fin ceramics, but they have poor grindability and are difficult to grind.
This has caused problems such as chipping of the material to be ground.
それ故、優れた研削性を示すダイヤモンド焼結体が要望
されていた。Therefore, there has been a demand for a diamond sintered body that exhibits excellent grindability.
本発明は、前述の従来のニラ）１ルー錫系並びに銅−錫
系金属基グイ−１” ’（ニー ニー１〜焼結体の欠点
を解決したファインセラミックスの精密研削用のＣｏ−
Ｎ ｉ −−Ｓ ｎ系金属基ダイヤモ、ド焼結体を提供
することを目的とする。The present invention is a Co-based metal base for precision grinding of fine ceramics that solves the drawbacks of the conventional sintered bodies.
An object of the present invention is to provide a N i --S n metal-based diamond and a de-sintered body.
本発明は、窒化珪素、炭化珪素、酸化アルミニウム等の
ファインセラミックスのｉｆ Ｉ 研ＭＩＪ ニ使用さ
れるダイヤモンド焼結体において、平均粒径１〜１０μ
Ｉｌ＋以下のコバノＬ１〜粉、ニッケル粉、及び１０〜
１００μｍの錫粉に３０〜３００μ町のダイヤモンド粉
末を１０重量％以上乃至３０重量％未満保持混入焼結さ
れているものから成り、該ダイヤモンド粉末が５〜３０
重量％のニッケルおよび錫、残部コバルトから成る不均
一組織を呈する母相によって保持されていることを特徴
とするＣｏ Ｎｉ−８ｎ系金属基ダイヤモンド焼結体
であり、
更に前記焼結体において、該不均一組織を呈する母相に
対し、粒度１〜２０μｍのＡ Ｉ２Ｏ３，Ｔ ｉＣ。The present invention provides a diamond sintered body for use in fine ceramics such as silicon nitride, silicon carbide, and aluminum oxide, with an average grain size of 1 to 10μ.
Kobano L1~ powder below Il+, nickel powder, and 10~
It consists of 100 μm tin powder mixed with diamond powder of 30 to 300 μm and held at 10% by weight or more to less than 30% by weight and sintered.
A CoNi-8n based metal-based diamond sintered body characterized by being held by a parent phase exhibiting a heterogeneous structure consisting of nickel and tin in the weight% and the balance cobalt; A I2O3, TiC with a particle size of 1 to 20 μm for a matrix exhibiting a heterogeneous structure.
ＷＣから選ばれた一種又は二種以上のセラミックス粉末
を５〜２０重量％添加混入するＣｏ Ｎｉ Ｓｎ系
金属基ダイヤモンド焼結体である。This is a Co Ni Sn based metal-based diamond sintered body containing 5 to 20% by weight of one or more types of ceramic powder selected from WC.
本発明のファインセラミックスの精密研削に使用される
Ｃｏ−Ｎｉ Ｓｎ系金属基ダイヤモンド焼結体は、金
属間化合物形成元素としてのＳｎが５〜３０重量％残部
Ｃｏの７トリソクスからなるため、ダイヤモンドの保持
力が良く、更に７）・リソクスには適度の耐摩耗性と脆
性が付加されること（こＪ、り研削性を向上させる、。The Co-Ni Sn-based metal-based diamond sintered body used for precision grinding of fine ceramics of the present invention consists of 7 trisoxes containing 5 to 30% by weight of Sn as an intermetallic compound-forming element and the balance being Co. It has good holding power, and 7) Risox has appropriate wear resistance and brittleness (this improves grindability).
又必要に応じて、母材にＡ Ｉ ２ｏ、、、 Ｔ’ ｉ
Ｃ。Also, if necessary, add A I 2o,..., T' i to the base material.
C.
ＷＣ等のセラミックス粉末を５〜２０重景％足形混入さ
せることによって、脆性が賦与され、ダイヤモンドの保
持力が優れる。By incorporating ceramic powder such as WC in an amount of 5 to 20%, brittleness is imparted and diamond retention is excellent.
本発明のＣｏ−・Ｎ ｉ−３ｎ基金属基ダイヤモンド焼
結体は、コバルト、ニジナル及び錫粉にダイヤモンド粉
末を添加混合し、６５０〜８５０℃にて、焼結し、得ら
れるものであるが、焼結温度は８５０℃以下であるのて
、ダイヤモンドの黒船化の心配は無い。The Co-・Ni-3n-based metal-based diamond sintered body of the present invention is obtained by adding and mixing diamond powder to cobalt, natural, and tin powder, and sintering the mixture at 650 to 850°C. Since the sintering temperature is 850° C. or lower, there is no need to worry about black diamond formation.
更に、本発明の焼結体は焼結後ホソ）・ガＬスによって
作製しても普通焼結体同様の効果を奏するものである。Furthermore, even if the sintered body of the present invention is made of gas after sintering, it exhibits the same effects as a normal sintered body.
本発明の焼結体は、け材が適当に軟質且つ脆性に富むた
め一７グイシセラぐツクスの精密研削に使用した場合、
優れた研削性を示すものであろう次に本発明の実施例に
ついて述−・、る、。Since the sintered body of the present invention is suitably soft and brittle, when used for precision grinding of 17-gushicera
Next, examples of the present invention will be described which will show excellent grindability.
原料粉末として用いる粒子径１〜１０μｍのコバルト、
ニッケル粉、１０〜１００μｍの錫粉及び３０〜３００
μｍのダイヤモンド粉末を次の第１表に示す配合に従っ
て混合し、非酸化性雰囲気中で６５０〜８５０℃の温度
で３０〜１２０分間焼結し、焼結体を得た。Cobalt with a particle size of 1 to 10 μm used as raw material powder,
Nickel powder, 10-100μm tin powder and 30-300μm
Diamond powder of .mu.m was mixed according to the formulation shown in Table 1 below and sintered at a temperature of 650 to 850.degree. C. for 30 to 120 minutes in a non-oxidizing atmosphere to obtain a sintered body.
更に前記焼結後、これをホットブし・スによって作製し
ても本発明の焼結体同様なものが得られるものである。Further, even if the sintered body is produced by hot-brushing after the sintering, a sintered body similar to the sintered body of the present invention can be obtained.
第１表 原料配合（重量％）
以上の結果、得らオ］たダイヤモンド焼結体を用いて、
従来品（銅−錫系金属基ダイヤモンド焼結体Ｎ０９）と
切断試験の比較を実施したところ、第２表に示す如く、
研削比において約２．５〜３．５倍の成績を示し、本発
明のダイヤモンド焼結体が擾れていることは明らかであ
る。Table 1 Raw material composition (wt%) Using the diamond sintered body obtained as a result of the above,
When comparing the cutting test with the conventional product (copper-tin based metal-based diamond sintered body N09), as shown in Table 2,
It is clear that the diamond sintered body of the present invention has a grinding ratio of about 2.5 to 3.5 times.
又、前記母相にＡ１２０３１ｏ重量％を添加配合したも
のは、Ｎｏ、 ９の従来品に比へて約２倍のυ［前止を
示した。In addition, the product in which A12031o was added in an amount of % by weight to the matrix showed about twice the υ[pre-stop] compared to the conventional product No. 9.
第２表 研削試験成績
デツピング無し二〇
チッピノゲ有り： ×
〔発明の効果〕
本光明のＧ ｏ −Ｎ ｉ−３ｎ系金属基グイヤモノＦ
焼結体によれば、ファイノセラミックス等の精密研削に
用いた場合、浸れた研削性を示すばかりてなく他の月利
の研削（こ当たっても同様な成績を奏し、甚だ有用なも
のである。Table 2 Grinding test results: No tapping, 20 chips, no grinding:
According to the sintered body, when used for precision grinding of phynoceramics, etc., it not only shows excellent grinding properties, but also produces similar results even when used for other types of grinding, making it extremely useful. be.
Claims (2)
イヤモンド焼結体において、平均粒径１〜１０μｍのコ
バルト粉、ニッケル粉、及び１０〜１００μｍ錫粉に３
０〜３００μｍのダイヤモンド粉末を１０重量％以上乃
至３０重量％未満保持混入焼結されているものから成り
、該焼結体はダイヤモンド粉末が５〜３０重量％のニッ
ケル及び錫、残部コバルトから成る不均一組織を呈する
母相によって保持されていることを特徴とするＣｏ−Ｎ
ｉ−Ｓｎ系金属基ダイヤモンド焼結体。(1) In diamond sintered bodies used for precision grinding of fine ceramics, cobalt powder, nickel powder with an average particle size of 1 to 10 μm, and tin powder of 10 to 100 μm are mixed with 3
The sintered body contains diamond powder of 0 to 300 μm in an amount of 10% to less than 30% by weight and is sintered therein. Co-N characterized by being held by a matrix exhibiting a uniform structure
i-Sn metal-based diamond sintered body.
０μｍのＡｌ＿２Ｏ＿３、ＴｉＣ、ＷＣ等のセラミック
スから選ばれた一種又は二種以上のセラミックス粉末を
５〜２０重量％添加混入させたことを特徴とする特許請
求の範囲第１項記載のＣｏ−Ｎｉ−Ｓｎ系金属基ダイヤ
モンド焼結体。(2) For the matrix exhibiting the above-mentioned heterogeneous structure, the particle size is 1 to 2.
Co-Ni- according to claim 1, characterized in that 5 to 20% by weight of one or more ceramic powders selected from ceramics such as Al_2O_3, TiC, and WC with a diameter of 0 μm are mixed. Sn-based metal-based diamond sintered body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12919686A JPS62287038A (en) | 1986-06-05 | 1986-06-05 | Co-ni-sn metal-base diamond sintered compact |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12919686A JPS62287038A (en) | 1986-06-05 | 1986-06-05 | Co-ni-sn metal-base diamond sintered compact |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS62287038A true JPS62287038A (en) | 1987-12-12 |
Family
ID=15003516
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP12919686A Pending JPS62287038A (en) | 1986-06-05 | 1986-06-05 | Co-ni-sn metal-base diamond sintered compact |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62287038A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2676673A1 (en) * | 1991-05-23 | 1992-11-27 | Eurotungstene Poudres | Use of cobalt powders with nonagglomerated spherical particles for the preparation of carbides cemented with a cobalt binder |
| US5441693A (en) * | 1991-04-10 | 1995-08-15 | Sandvik Ab | Method of making cemented carbide articles and the resulting articles |
-
1986
- 1986-06-05 JP JP12919686A patent/JPS62287038A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5441693A (en) * | 1991-04-10 | 1995-08-15 | Sandvik Ab | Method of making cemented carbide articles and the resulting articles |
| US5619000A (en) * | 1991-04-10 | 1997-04-08 | Sandvik Ab | Method of making cemented carbide articles and the resulting articles |
| FR2676673A1 (en) * | 1991-05-23 | 1992-11-27 | Eurotungstene Poudres | Use of cobalt powders with nonagglomerated spherical particles for the preparation of carbides cemented with a cobalt binder |
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