JPS62201556A - Processed whole egg and production thereof - Google Patents

Processed whole egg and production thereof

Info

Publication number
JPS62201556A
JPS62201556A JP61148155A JP14815586A JPS62201556A JP S62201556 A JPS62201556 A JP S62201556A JP 61148155 A JP61148155 A JP 61148155A JP 14815586 A JP14815586 A JP 14815586A JP S62201556 A JPS62201556 A JP S62201556A
Authority
JP
Japan
Prior art keywords
whole egg
liquid
egg
whole
eggs
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP61148155A
Other languages
Japanese (ja)
Other versions
JPH0586175B2 (en
Inventor
Masayuki Arazoe
新添 正之
Atsushi Sekiyama
関山 厚史
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Asahi Chemical Industry Co Ltd
Original Assignee
Asahi Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Chemical Industry Co Ltd filed Critical Asahi Chemical Industry Co Ltd
Priority to JP61148155A priority Critical patent/JPS62201556A/en
Publication of JPS62201556A publication Critical patent/JPS62201556A/en
Publication of JPH0586175B2 publication Critical patent/JPH0586175B2/ja
Granted legal-status Critical Current

Links

Abstract

PURPOSE:To obtain processed whole egg which has the same function as that of unheated liquid whole egg, improved hygienic shelf stability, partially thermally denatured protein of egg and fixed viscosity, is liquid and shows no gel properties, by sterilizing blended liquid whole egg under heating and homogenizing. CONSTITUTION:Whole egg blended in a liquid state is sterilized under heating (preferably 65-72.5 deg.C for 1-300min) and then homogenized (preferably cutting type homogenizer under reduced pressure or pressure type homogenizer at >=50kg/cm<2>) to give the aimed whole egg wherein protein of the whole egg is partially denatured by heating, the amount of the undenatured part is 50-90wt% based on raw whole egg by salt-soluble protein ratio, having 10-4,000 cp viscosity, uniform liquid and showing no gel properties in a flow curve. The whole egg blended in a liquid state is preferably homogenized and then sterilized under heating.

Description

【発明の詳細な説明】 (産業上の利用分野) 本発明は、未加熱の液全卵と同等の機能を持ち。[Detailed description of the invention] (Industrial application field) The present invention has the same function as an uncooked liquid whole egg.

かつ従来の液全卵よシ衛生的であ夛、保存性のすぐれ几
加工全卵およびその製造法に関するものでおる。
The present invention also relates to a processed whole egg that is more hygienic than conventional liquid whole eggs and has excellent preservability, and a method for producing the same.

(従来の技術) 全卵はサルモネラ、大腸菌等に汚染されやすく。(Conventional technology) Whole eggs are easily contaminated with salmonella, E. coli, etc.

そのためFAO/W)10の勧告基準案では一般生菌数
50,000 / f以下、大腸菌群1072以下。
Therefore, according to the FAO/W) 10 draft recommendation standards, the number of general viable bacteria is 50,000/f or less, and the coliform bacteria is 1072 or less.

サルモネラ園251当り陰性という数値が示されており
、加熱殺菌が必要でおる。高温での高い殺菌レベルの加
熱を行なうと、卵の蛋白質が熱変性。
The salmonella garden showed a negative value of 251, and heat sterilization was required. When heated to high sterilization levels at high temperatures, egg proteins are thermally denatured.

凝固し、凝固能、乳化能、M立能など全卵に必要とされ
る機能を失うと共に、流動性を失うと考えられている。
It is thought that the whole egg coagulates and loses the functions necessary for whole eggs, such as coagulation ability, emulsification ability, and M-ability, as well as fluidity.

そのため、液全卵はサルモネラの殺菌金目的とし次ハス
ツール殺菌と呼ばれる55Cから65Cの温度での10
〜1分間程度の低温短時間殺菌が行なわれている。これ
らの全卵は、殺菌が不充分であり、冷蔵で3〜6日しか
保存できず、さらに。
Therefore, liquid whole eggs are used for Salmonella sterilization purposes and are subjected to sterilization at a temperature of 55C to 65C for 10 days, which is called Hasstool sterilization.
Low-temperature short-time sterilization for about 1 minute is performed. These whole eggs are poorly pasteurized and can only be kept refrigerated for 3-6 days;

製造後1日で上澄、沈澱が生じる。ま九、長期保存のた
めには、冷凍下での保存が必要でおる。現在、液全卵は
一部が冷蔵目配商品として流通しておシ、大部分は冷凍
品として流通している。冷凍品は解凍の平置さが轟然の
ことながらあシ1作業上の大きな問題となっている。ま
友、解凍後、凍結変性を受ける友め1部分的なゲル化、
離水が生じると共に、全卵としての機能が低下するとの
報告もある。この凍結変性を防止するため、糖および塩
の添加が行なわれているが、解凍の平置さの解決にはな
らず、また、高a度のmまtは塩のため、用途を限定し
てしまう弊害を持っている。
A supernatant and a precipitate form within one day after production. For long-term storage, storage under refrigeration is necessary. Currently, some liquid whole eggs are distributed as refrigerated products, and the majority are distributed as frozen products. Frozen products have to be laid flat during thawing, which is a major problem when working with reeds. After thawing, Mayu undergoes freeze denaturation. Partial gelation.
There are also reports that syneresis occurs and the function of whole eggs decreases. In order to prevent this freezing denaturation, sugar and salt are added, but this does not solve the problem of flattening during thawing, and since high aluminium chloride is salt, its uses are limited. It has the disadvantage of causing

一方、加熱殺菌をよシ高温で行ない、殺菌レベルを高め
る方法として、全卵の蛋白変性温度を上昇させること、
あるいは蛋白の熱安定性を高めることを目的に、pHi
!I!整、糖、塩類、金属塩等の添加、全卵の希釈など
が考案されている。これらはいずれも全卵と比較して、
味1色、凝固後の物性の変化が見られると同時に、目的
とする殺菌が前述のパスツール殺菌の温度1時間の範囲
であシ。
On the other hand, as a method to perform heat sterilization at a higher temperature and increase the sterilization level, it is possible to increase the protein denaturation temperature of whole eggs.
Alternatively, pHi
! I! Various methods have been devised, including adding sugar, salts, metal salts, etc., and diluting whole eggs. All of these are compared to whole eggs.
One color in taste and changes in physical properties after solidification were observed, and at the same time, the desired sterilization was carried out within the above-mentioned Pasteur sterilization temperature range of 1 hour.

長期間の保存には、その殺菌レベルでは不適であり、保
存中の液の上澄、沈澱の分離も生じる。
The sterilization level is not suitable for long-term storage, and separation of supernatant and precipitate occurs during storage.

ここで、従来の技術について以下詳述する。Here, the conventional technology will be described in detail below.

パスツール殺菌と呼ばれる低温殺菌については。Regarding pasteurization called Pasteur sterilization.

「卯と科学と技術」(学窓社、 W、J、Stadel
man。
“Rabbits, Science and Technology” (Gakusousha, W, J, Stadel)
man.

0、J、Cotterill @ 、森田重広訳)、「
全卵の科学と利用」(地球社、佐藤泰編〕、「鶏卵の知
識」(食品化学新聞社、今井忠平著)K現在実用されて
いる方法について詳述されているが、それらは蛋白凝固
が生じないことを前提としたサルモネラ殺mを目的とし
7255〜66C(全卵に訃いては58〜66C)の低
温での2〜4分という短時間の殺菌であり、蛋白変性を
前提とし7’166C以上の殺菌あるいは液の安定性に
りいては言及していない。
0, J. Cotterill @, translated by Shigehiro Morita), “
``Science and Utilization of Whole Eggs'' (Chikyu-sha, edited by Yasushi Sato), ``Knowledge of Hen Eggs'' (Food Chemical Newspaper, written by Tadahei Imai) K. Currently used methods are detailed, but these include protein coagulation. It is a short-time sterilization of 2 to 4 minutes at a low temperature of 7255 to 66 C (58 to 66 C for whole eggs) to kill Salmonella on the premise that protein denaturation will not occur. There is no mention of sterilization above 166C or stability of the liquid.

1次、米国1日本等の特許には次のものがある。The following patents are available in the United States, Japan, etc.

卵白および全卵の殺菌法として、米国特許第55619
80 (特公昭46.−56185)には、卵白にアル
カリポリホスフェートとCaまたはZnイオンを添加し
、 51.7〜62.80で30秒から10分間加熱す
る低温殺菌法があシ、特公昭46−341130には、
卵白にアルカリポリホスフェートを0.2〜2%添加し
、さらに、pHを8〜10に調整し、低温殺菌する方法
が記載されている。
U.S. Patent No. 55619 for pasteurizing egg whites and whole eggs
80 (Japanese Patent Publication No. 46.-56185) describes a pasteurization method in which alkaline polyphosphate and Ca or Zn ions are added to egg whites and heated at 51.7 to 62.80 for 30 seconds to 10 minutes. 46-341130 has
A method is described in which 0.2 to 2% of alkaline polyphosphate is added to egg white, the pH is further adjusted to 8 to 10, and the egg white is pasteurized.

特公昭46−34181には、卵白のp Ht−0,5
から1.5単位上昇させ、カタラーゼを不活性化するた
めの低温加熱後、応答量の過酸化物を添加し。
Japanese Patent Publication No. 46-34181 describes the pH of egg white as Ht-0.5.
After heating at a low temperature to inactivate the catalase, a responsive amount of peroxide is added.

再度低温殺1Mをする方法が記載されている。特公昭4
7−255B6には、リン酸、硫酸、炭酸のアルカリ金
属塩の過酸化水素化物の有効量を添加し、低温殺菌を行
なう方法が記載されている。その他特公昭42−221
1111.%開昭50−111256、特開昭58−6
5546.西ドイツ特許1816896.オランダ特許
71791等もあるが、これらの方法は、全て卵の蛋白
質が凝固。
The method of performing low temperature killing at 1M again is described. Tokuko Showa 4
No. 7-255B6 describes a method of pasteurizing by adding an effective amount of hydrogen peroxide of an alkali metal salt of phosphoric acid, sulfuric acid, or carbonic acid. Other special public service 1977-221
1111. % 1986-111256, 1982-6
5546. West German patent 1816896. There is also Dutch patent 71791, but all of these methods coagulate egg proteins.

蛋白変性をすることなくサルモネラの殺菌全行なう九め
のものであり、その一般生菌の殺菌程度は低く、液の分
離もあプ、未凍結状態での長期保存には不適である。ま
;I’ll、pH調整、塩類、金属塩等の添加物が必要
でらシ、味1色、凝固物の物性が変fヒする問題もある
This is the ninth product that completely sterilizes Salmonella without protein denaturation, but its sterilization level against general viable bacteria is low, and liquid separation is also poor, making it unsuitable for long-term storage in an unfrozen state. However, there are also problems such as pH adjustment, the need for additives such as salts and metal salts, a discolored taste, and changes in the physical properties of the coagulated product.

全卵の部分的な蛋白変性により増粘させる特許は、米国
特;FFtiZ2.45B、A49.特開昭57−68
76二7jiめる。これらはケーキ類の膨fヒ性向上を
目的とした本ので、前者は135〜15Ω”F (57
,2〜65.6 iC)で3〜30分間、後者は67〜
75Cで3〜30分間加熱することが記載されている。
The patent for thickening whole eggs through partial protein denaturation is US Patent No. FFtiZ2.45B, A49. Japanese Unexamined Patent Publication 1983-1986
7627jimeru. These books are aimed at improving the swelling properties of cakes, and the former is 135 to 15 Ω"F (57
, 2-65.6 iC) for 3-30 minutes, the latter at 67-65.6 iC)
It is described that heating at 75C for 3 to 30 minutes.

しかし、ホモゲナイズすることについては言及して2ら
ず、前者では殺菌レベルが低く、保存中。
However, there is no mention of homogenization, and the sterilization level in the former is low, so it is being stored.

液の分離が発生する。また、後者は、液卵が著しく増粘
し、ゲル状物となるという問題がある。
Liquid separation occurs. In addition, the latter has the problem that the liquid egg significantly thickens and becomes a gel-like substance.

卵白および全卵の加熱殺菌温度を従来のパスツール殺菌
よシ^温で行なう方法では、特公昭5761589、特
公昭43−1690.特公昭59−530’111%公
昭60−9746%開昭49−50565がある。
In the method of heat sterilization of egg whites and whole eggs at a temperature lower than that of conventional Pasteur sterilization, Japanese Patent Publication No. 5761589, Japanese Patent Publication No. 43-1690. There is a special public service of 111%, 1985-530', 111%, 9746% of 1986-9746, and 50565 of 1977.

特公昭57.−61389は、リン酸ナトリウム塩と有
機酸塩を添加し加熱する方法であり、卵白は65Cまで
、全卵は75Cまで加熱殺菌でき。
Tokuko Showa 57. -61389 is a method in which sodium phosphate and organic acid salts are added and heated, and egg whites can be heat sterilized up to 65C and whole eggs can be sterilized up to 75C.

加熱殺菌時間は温度により任意に設定できると記載され
ている。この方法においては、リン酸塩。
It is stated that the heat sterilization time can be set arbitrarily depending on the temperature. In this method, phosphate.

有機酸塩が0.5〜5チと高濃度であり、製品の色。The color of the product is due to the high concentration of organic acid salts at 0.5-5%.

i 味が大きく変質する問題を生じる。ま友、保存中の
液分離を生じる。、ま九、この方法における加熱温度1
時間Vi卵白お上び全卵が変性凝固しない範囲と規定し
てお5.66C以上では加熱時間が大巾に制約される。
i This causes the problem of significant change in taste. However, liquid separation occurs during storage. , Maku, Heating temperature 1 in this method
Time Vi is defined as the range in which egg whites and whole eggs do not undergo denaturation and coagulation, and heating time is severely restricted above 5.66C.

特公昭45−B69Dは、含抛卵蛋白質溶液の製造方法
についてのものであり、糖とクエン酸ソーダを鶏卵液に
加え、80〜?DCで1〜2時間加熱する方法で、全卵
の蛋白は全て変性した溶液についてのものである。
Japanese Patent Publication No. 45-B69D is about a method for producing an egg-containing protein solution, in which sugar and sodium citrate are added to a chicken egg solution. By heating with DC for 1 to 2 hours, all the whole egg proteins are in a denatured solution.

特公昭59−53011は、滅菌液卵の大造方法につい
てのものであり、全卵を水による希釈とpH調整するこ
とにより、115C1秒間以上の殺菌を行なう方法であ
るが、全卵が1.5倍以上の水で希釈される几め、li
l固能を利用する全卵の用途には全く不向きでアリ、単
なる栄養補強的添加物あるいは卵飲料等の用途に限定さ
れる。
Japanese Patent Publication No. 59-53011 is about a large production method for sterilized liquid eggs, in which whole eggs are diluted with water and pH adjusted to sterilize them for more than 115C for 1 second. Diluted with more than twice as much water, li
It is completely unsuitable for uses of whole eggs that utilize solidity, and is limited to uses such as simple nutritional additives or egg drinks.

特公昭60−974は、1a 〜50%g度に希釈した
卵白を加熱変性させ、それを均質化処理し。
Japanese Patent Publication No. 60-974 heats and denatures egg white diluted to 1a to 50% g and then homogenizes it.

次いでプロテアーゼ処理を行なう飲料原料としての完全
に熱変性した卵白液についてのものであり。
Next, it concerns completely heat-denatured egg white liquid as a beverage raw material that is subjected to protease treatment.

生卵とは全く異なるものである。It is completely different from raw eggs.

特開昭49−50565は、加熱無菌卵黄の製造に関す
るものであり、純粋m楯を47.5〜52.5係添加後
、減圧下で70〜74Cで20〜50分間加熱殺菌する
方法でおるが、高a度の糖の添加により、その用途が限
定される問題点を持つ。ま友、全卵については何ら言及
していな一0全卵をホモゲナイズする方法に関する特許
は。
JP-A No. 49-50565 relates to the production of heat-sterilized egg yolk, which involves adding 47.5 to 52.5 parts of pure M-shield, followed by heat sterilization at 70 to 74 C for 20 to 50 minutes under reduced pressure. However, the addition of high ag sugars has the problem of limiting its uses. Friend, there is no mention of whole eggs in this patent regarding a method for homogenizing whole eggs.

米国特許第2956240.同第5095487がある
U.S. Patent No. 2956240. There is the same number 5095487.

前者は冷凍全卵の改良全目的とし、蛋白凝固することの
ない1ao  F(4oC’)で数分という低温殺菌後
、1000psi以上の圧力でホモゲナイズすることが
記載されているが、殺菌レベルを上げた蛋白変性、凝固
を生じる温度以上のものKついては言及していない。こ
こで行なうホモグナイイ紳 み7df d=+ /7”
lの9社塾点め入tめの暇のである。
The former is intended for the purpose of improving frozen whole eggs, and is described as pasteurizing for several minutes at 1ao F (4oC'), which does not cause protein coagulation, and then homogenizing at a pressure of 1000 psi or more. There is no mention of temperatures higher than those that cause protein denaturation and coagulation. The homogeneous gentlemanly conduct here 7df d=+ /7”
It's my 9th day of free time.

後者は凝固のないサルモネラフリーのホモゲナイズ卵夷
品についての本ので4fi、65.5〜76.7Cの殺
菌を行なうことが記載されているが、熱凝固しないよう
、全卵に油脂、乳固形分を添加し。
The latter is a book about salmonella-free homogenized egg products that do not coagulate, and it states that they should be sterilized at 4fi, 65.5-76.7C. Add.

自然卵の固形物量、水分量Kv4整し次、いわゆる希釈
全卵についてのものであり、液全卵の機能。
This is about the so-called diluted whole egg after adjusting the solid content and water content Kv4 of natural eggs, and the function of liquid whole egg.

味、物性上問題を有している。It has problems with taste and physical properties.

(発明が解決しようとする問題点) 以上のように、未加熱の全卵と同等の凝固能。(Problem to be solved by the invention) As mentioned above, the coagulation ability is equivalent to that of uncooked whole eggs.

乳化能、泡立能を保有し、かつ衛生的であり、保存中の
分離を生じない未凍結の保存性の高い液全卵は、未だ開
発されておらず、その開発が望まれている。
An unfrozen, highly shelf-stable liquid whole egg that has emulsifying ability and foaming ability, is hygienic, and does not separate during storage has not yet been developed, and its development is desired.

(問題点を解決するための手段) 本発明は、未凍結の冷蔵温度で長期間、衛生的。(Means for solving problems) The present invention is hygienic for long periods of time at unfrozen, refrigerated temperatures.

安定に保存できる。生全卵と同等の機能を有する加工全
卵の提供を目的に鋭意検討を重ねた結果。
Can be stored stably. The result of extensive research aimed at providing processed whole eggs that have the same functionality as raw whole eggs.

液状全卵を65〜72,5 Cの温度で1〜300分間
の任意の時間加熱殺菌を行なつ友後、加熱により生じる
ゲルを機械的にホモゲナイズを行なうか。
After heat sterilizing liquid whole eggs at a temperature of 65 to 72.5 C for an arbitrary period of time of 1 to 300 minutes, the gel produced by heating is mechanically homogenized.

あるいは液状全卵全泡立ちを起こさないようにホモゲナ
イズ後、65〜72,5 Cの温度で1〜300分間の
任意の加熱殺菌を行なうことにより、蛋白を10〜50
%変性させ、生全卵の凝固能、乳化能、泡立能とほぼ同
等の機能を保有し、生全卵より極めて衛生的かつ保存性
の高い、安定な10〜4o o o cpの粘度の液状
の加工全卵を得る本発明に到達した。
Alternatively, after homogenization to avoid foaming of liquid whole eggs, optional heat sterilization at a temperature of 65 to 72.5 C for 1 to 300 minutes can reduce the protein content by 10 to 50%.
% denatured, has functions almost equivalent to the coagulating ability, emulsifying ability, and foaming ability of raw whole eggs. The present invention for obtaining liquid processed whole eggs has been achieved.

以下1本発明の詳細な説明する。The present invention will be explained in detail below.

本発明においては、原料として生全卵液を用いる。生全
卵液とは、!Q)卵のaを割った後の生全卵を混合、濾
過して、卵殻の破片、カラザ等を除去し比ものを言う。
In the present invention, raw whole egg fluid is used as a raw material. What is raw whole egg liquid? Q) Mix and filter raw whole eggs after cracking the eggs to remove eggshell fragments, chalaza, etc.

殺菌前の衛生状態が殺菌後の衛生状態に大きく影響する
ため、望ましくは卵殻洗浄をよく行ない1割卵、混合、
濾過を衛生的に行なう万がよい。
The sanitary conditions before sterilization greatly affect the sanitary conditions after sterilization, so it is preferable to thoroughly wash the eggshells, crack eggs, mix eggs, etc.
It is best to perform filtration hygienically.

この生全卵液t−65C以上72.5 C以下に昇温し
、1〜300分間の任意の時間保持殺菌した後。
After raising the temperature of this raw whole egg liquid to t-65C or higher and 72.5C or lower, and holding and sterilizing it for an arbitrary period of time from 1 to 300 minutes.

ホモゲナイズを行なう。あるいは生全卵液をホモゲナイ
ズした後、65C以上72.5C以下に昇温し、1〜3
00分間の任意の時間保持殺菌する。
Perform homogenization. Alternatively, after homogenizing raw whole egg liquid, raise the temperature to 65C or higher and 72.5C or lower for 1 to 3 hours.
Sterilize by holding for an arbitrary time of 00 minutes.

殺菌温度は、よシ高い殺菌レベルを得る九めに69〜7
2.5 Cが望ましいが、72.5Cを超えないよう調
整が必要でおる。殺菌時間は加熱前の暇数にもよるが1
通常、69〜70C30分間の加熱で殺菌前の一般生菌
数の1710’〜1 / 10’のレベルまで殺菌され
る。ま九、最も低下しやすい泡立性の機能を保持する友
め、69〜71.5 Cで90分間以下が望ましい。加
熱の方法は、@度コントロールが行なえる攪拌機付タン
クもしくはプレート式熱交換機を使用すればよい。この
時。
The sterilization temperature is 69-7 to obtain a higher sterilization level.
2.5C is desirable, but adjustments must be made so that it does not exceed 72.5C. The sterilization time depends on the number of breaks before heating, but 1
Usually, by heating at 69 to 70C for 30 minutes, bacteria are sterilized to a level of 1710' to 1/10' of the general viable count before sterilization. Ninth, it is preferable to maintain the foaming function, which is most likely to deteriorate, at 69 to 71.5 C for 90 minutes or less. As for the heating method, a tank with a stirrer or a plate heat exchanger that can control temperature may be used. At this time.

液温か72.5 Gを超えないよう調整する。ま几。Adjust so that the liquid temperature does not exceed 72.5G. Well done.

加熱中の水分量が変化しないように水分調整することが
望ましい。
It is desirable to adjust the moisture content so that the amount of moisture during heating does not change.

品温か650未満では、サルモネラは光分殺菌されるが
、一般生菌を殺菌する温度としては不充分であり、かつ
蛋白変性量が少なく、卵液の保存中の安定性も不充分で
あり、生全種同様に分mを生ずる。また、72.SC以
上では全卵の蛋白変性が急激に進行するtめ、全卵の凝
固能、乳化能。
If the product temperature is less than 650, Salmonella will be sterilized by light, but the temperature is insufficient to sterilize general viable bacteria, the amount of protein denaturation is small, and the stability of egg fluid during storage is insufficient. Like all fresh species, it produces minutes. Also, 72. Above SC, the protein denaturation of whole eggs rapidly progresses, and the coagulation and emulsifying ability of whole eggs.

泡立能といった機能が大巾に低下する。Functions such as foaming ability are greatly reduced.

ホモゲナイズは、殺菌全卵液Kfi動性を与え。Homogenization gives sterile whole egg fluid Kfi kinetics.

使用簡便性を得る定め、および液の安定性を得る次めに
行なう、ホモゲナイズは、ホモゲナ、イズくよる泡立を
防止する几め、減圧下でs o o o rpms分間
以上程度のカッティング式ホモゲナイザーあるいは50
′kg/c!It以上の圧力式ホモゲナイザーで行なう
のが望ましい。
To obtain ease of use and to obtain stability of the liquid, homogenization is carried out using a cutting type homogenizer under reduced pressure for at least 1 minute at s o o o rpms, with a method to prevent foaming. Or 50
'kg/c! It is preferable to use a pressure homogenizer with a pressure of It or higher.

加熱前にホモゲナイズを行なう場合は、ホモゲナイズ後
の生全卵液の粘度が10 cp以下で曳糸性がなくなる
程度まで行なう、このホモゲナイズによプ、65〜72
.5C,1〜300分の蛋白変性をおこす加熱を行なっ
ても1分散した状態で蛋白変性し、ゲル化を生ぜず液状
である。ホモゲナイズを行なわない生全卵液は、60C
以上の温度で10分間以上の加熱疋よりゲル化を始め、
流動性を失なう。
When homogenizing is carried out before heating, the homogenization should be carried out until the viscosity of the raw whole egg fluid after homogenization is 10 cp or less and the stringiness is lost.65-72
.. Even when heated to cause protein denaturation at 5C for 1 to 300 minutes, the protein denatures in a dispersed state and remains liquid without gelation. Raw whole egg liquid without homogenization is 60C.
Gelation begins by heating at the above temperature for 10 minutes or more,
Lose liquidity.

加熱後にホモゲナイズを行なう場合は、加熱により蛋白
変性して生じ次グルを、ホモゲナイズにより破壊分散し
、均質な流動性を持つ九卵液とする。
When homogenizing is performed after heating, the protein is denatured by heating and the resulting glue is broken down and dispersed by homogenization to form a homogeneous fluid.

加熱・ホモゲナイズ処理した全卵は、蛋白か−、簡便性
している几め生全卵よシ粘度が増加するが。
Whole eggs that have been heated and homogenized have an increased viscosity due to their protein content, compared to the simpler raw whole eggs.

そのため、かえって保存中に分離のない安定な全卵が得
られる。生全卵をホモゲナイズした未加熱のものは、保
存中に液の分離を生じる。
Therefore, stable whole eggs that do not separate during storage can be obtained. Unheated, homogenized raw whole eggs cause liquid separation during storage.

加熱・ホモゲナイズ処理により1分離のない均質な加工
全卵が得られるが、望ましくは、加熱殺菌後の操作(ホ
モケナイズ、冷却、充填、包装)を無菌的に行なうとよ
い。加熱後にホモゲナイズ管行なう方法において、加熱
後の操作を無菌的に行なえない時は、ホモゲナイズ処理
後、充填、包装してから65’C以上72,5 C以下
のImfで任意の時間、殺菌を行なえばよい。
Homogeneous processed whole eggs without any separation can be obtained by heating and homogenizing, but it is preferable to perform the operations after heat sterilization (homogenizing, cooling, filling, packaging) aseptically. In the method of performing homogenization in a tube after heating, if the operation after heating cannot be performed aseptically, sterilization can be performed at an IMF of 65'C or more and 72.5C or less for an arbitrary period of time after homogenization, filling, and packaging. Bye.

加熱による卵液の蛋白変性量については、0.5M食塩
溶液可溶蛋白量の変fヒから算出すると、生全卵の蛋白
質の10〜50%が熱変性しておシ。
Regarding the amount of protein denaturation in egg fluid due to heating, it is calculated from the change in the amount of soluble protein in 0.5M saline solution, and 10 to 50% of the protein in raw whole eggs is denatured by heat.

90〜50饅が未変性である。塩可溶性蛋白量の測定は
、卵液を0.3M食塩溶液で希釈溶解後、遠心分離し、
その上澄の蛋白4度をフェノール試薬法で測定した。こ
の卵液の粘度は、BL型回転粘度計(東京計器1ft)
で測定しt結果、測定温度25C9回転数S Orpm
でto〜4000cpでめった。まt、流動曲線(HA
AKElli粘度計:測定温度25C)測定の結果よ)
、ホモゲナイズによりゲル性が消失することが示される
。卵液の蛋白変性は、示差走査熱量計による分析からも
、蛋白変性の吸熱ピーク中の78’C以下のピークが減
少るるいは一部が消失することKよシ示される。
90-50 buns are unaltered. To measure the amount of salt-soluble protein, the egg fluid was diluted and dissolved in 0.3M salt solution, and then centrifuged.
The protein level of the supernatant was measured by the phenol reagent method. The viscosity of this egg liquid was measured using a BL type rotational viscometer (Tokyo Keiki 1ft).
Measured at t result, measurement temperature 25C9 rotation speed S Orpm
I got it at ~4000cp. The flow curve (HA
AKElli viscometer: Measurement temperature 25C) Measurement results)
, it is shown that the gel properties disappear upon homogenization. Analysis of protein denaturation in egg fluid using a differential scanning calorimeter also shows that the endothermic peak of protein denaturation at 78'C or lower decreases or partially disappears.

第1図に加熱時間に伴う蛋白未変性率の変化、に2図に
蛋白変性率と粘度の関係、第3図KDS・C(示差走差
熱量計)の蛋白変性吸熱ピーク、第4図に流動曲線を示
す。
Figure 1 shows the change in protein nondenaturation rate with heating time, Figure 2 shows the relationship between protein denaturation rate and viscosity, Figure 3 shows the protein denaturation endothermic peak of KDS-C (differential scanning calorimeter), and Figure 4 shows the relationship between protein denaturation rate and viscosity. Shows the flow curve.

なお、に1図の加熱時間に伴う蛋白未変性率の変化にお
いて、加熱は5oHc予備加熱後、各々の温度のWat
er Bath中で、フィルムに充填シールした卵液を
加熱した。加熱時間はWater Ba1h投入後の時
間でおる。第3図のDSCの蛋白変性吸熱ピークにおい
て、(4)は生全卵、(B)はパスツール殺菌全卵(6
0C,4分)、(0は70C,30分殺菌したホモゲナ
イズ全卵、@は70C,90分殺菌し几ホモゲナイズ全
卵、(匂は75C,30分殺菌したホモゲナイズ全卵、
 (F′)は100 C’ e15分加熱し几全卵を示
す。第4図の流動曲線において、1は生全卵液〔サンプ
ル(イ)〕、2はホモゲナイズ全卵液〔サンプルに):
]、s、s’は69C加熱全卵液〔サンプル(ロ)〕、
4はホモゲナイズ後。
In addition, in the change in protein undenatured rate with heating time shown in Figure 1, heating was performed at various temperatures after preheating at 5oHc.
The egg wash filled and sealed into a film was heated in an er Bath. The heating time is the time after Water Ba1h is added. In the DSC protein denaturation endothermic peak in Figure 3, (4) is a raw whole egg, (B) is a Pasteur pasteurized whole egg (6
0C, 4 minutes), (0 is homogenized whole egg sterilized at 70C for 30 minutes, @ is homogenized whole egg sterilized at 70C for 90 minutes, (odor is 75C, homogenized whole egg sterilized for 30 minutes,
(F') indicates a whole egg heated at 100 C'e for 15 minutes. In the flow curves in Figure 4, 1 is raw whole egg fluid [sample (A)], 2 is homogenized whole egg fluid [sample]:
], s, s' are whole egg liquid heated at 69C [sample (b)],
4 is after homogenization.

69C加熱全卵液〔サンプル(ホ)〕、5は69C加熱
液、ホモゲナイズ全卵液〔サンプルe→〕を示し。
69C heated whole egg liquid [sample (e)], 5 shows 69C heated liquid, homogenized whole egg liquid [sample e→].

測定はHAAKE社粘度計で、3′以外はNV型ロータ
ー、3′はMVDIN型ロータ型金−ター 111定温
度25C1回輯数変化率128rpm / IMLで行
った。
The measurement was carried out using a HAAKE viscometer using an NV type rotor for all parts other than 3', and an MVDIN type rotor for 3' at a constant temperature of 25C and a rate of change of one cycle of 128 rpm/IML.

(発明の効果) 以上の操作により得られる加工全卵は、生全卵とほぼ同
等の凝固能、乳化能、泡立能を保有し。
(Effects of the Invention) The processed whole eggs obtained by the above operations have coagulation ability, emulsification ability, and foaming ability almost equivalent to raw whole eggs.

かつ衛生的で1L保存中に分離、f質することなく長期
保存が可能である。
It is also hygienic and can be stored for a long time without separating or deteriorating during 1L storage.

また1本発明は、全卵を主原料とし、谷痕調味香辛料、
出し汁、牛乳類、油脂類などのいずれかを添加混合した
液状のオムレッミックス、プリンミックス、茶碗蒸し、
卵豆腐などの全卵加工食品に一応用できるものである。
In addition, 1 the present invention uses whole eggs as the main raw material, and has a seasoning spice,
Liquid omelet mixes, pudding mixes, chawanmushi, which are made by adding and mixing dashi stock, milk, oils, etc.
This can be applied to whole egg processed foods such as egg tofu.

さらに、蛋白変性温度を上昇させる物質を添加すること
により、塩加溶性蛋白量比による蛋白変性量を10〜5
0%とする@度まで上げることも可能でめる。
Furthermore, by adding a substance that increases the protein denaturation temperature, the amount of protein denaturation based on the salt-soluble protein amount ratio can be reduced by 10 to 5.
It is also possible to increase it to 0%.

(実施例) 実施例および試験例により、さらに詳細に説明する。(Example) This will be explained in more detail with reference to Examples and Test Examples.

実施例1 殻付鶏卵を洗浄割卵し、ノ・ンドミキサー(ナショナル
MK 1005 )で機械的にミキシング後。
Example 1 Chicken eggs with shells were washed and cracked, and then mechanically mixed using a mixer (National MK 1005).

20メツシユのステンレス裏編で卵殻片、カラザ’t濾
過除云し、生全卵液5に9作成した。これをナイロン・
ポリプロピレンラミネートフィルム袋(150+uX1
130u)中に100tずつ分割シールした。袋に詰め
九生全卵液’1i55C温水中で10分間予備加熱後、
70〜71.5Cil!(コントロールし交電水中に入
れ、全卵液@が6SCに達した後、30分間加熱し開封
し、真空ホモゲナイザ−(特殊機fヒエ業Type M
 )で真空度700 winHの減圧下で Ioooo
 rpm 10分間ホモゲナイズし。
The eggshell pieces were filtered and removed using a stainless steel backing of 20 meshes, and raw whole egg liquids were prepared by 5 to 9 times. This is nylon
Polypropylene laminate film bag (150+uX1
100t each was sealed in 130u). After preheating the whole egg solution in a bag for 10 minutes in 55C warm water,
70~71.5Cil! (Put in controlled energized water, and after the whole egg solution reaches 6SC, heat it for 30 minutes, open the package, and use a vacuum homogenizer (special equipment type M).
) under reduced pressure of vacuum degree 700 winH Ioooo
Homogenize for 10 minutes at rpm.

再びナイロン・ポリプロピレン袋(150miXt8o
mm)[100tずつ分割シールした。これf:69〜
70C!/cコントロールし交電水中で30分間加熱殺
菌を行ないただちKR,水で冷却した。
Again nylon/polypropylene bag (150miXt8o
mm) [100t each was divided and sealed. This f:69~
70C! /c control, heat sterilization was carried out in energized water for 30 minutes, and immediately cooled with KR and water.

実施例2 生全卵液tokgを作成し次。これを実施例1と同様に
、70〜71.50に調整し几温水を循環させたジャケ
ットと、内部攪拌羽根を備え友密閉型殺菌タンク(ステ
ンレス製満水30t)内に入れ。
Example 2 Tokg of raw whole egg liquid was prepared. As in Example 1, this was adjusted to a temperature of 70 to 71.50 and placed in a sealed sterilization tank (made of stainless steel, full of 30 tons of water) equipped with a jacket in which warm water was circulated and an internal stirring blade.

攪拌混合しながら加熱殺菌を行なつt、殺菌時間は全卵
液温が65Cに達してから45分間であつ次。この時、
全卵の最高@度は70CT:あった。
Heat sterilization was performed while stirring and mixing, and the sterilization time was 45 minutes after the temperature of the whole egg mixture reached 65C. At this time,
The highest degree of all eggs was 70 CT.

殺菌後、タンク底部から蒸気滅菌済みのサニタリーポン
プ付貯槽(ステンレス製満水50t)に無菌的に移し、
さらに、蒸気滅菌した圧力式ホモゲナイザー(マントン
ゴーりン15 M−8TAfi)で吐出圧200kp/
cmで均質化した後、無菌的に蒸気殺菌済みのサニタリ
ーポンプ付貯W1(ジャケット、攪拌機付ステンレス製
満水50t)K入れ。
After sterilization, aseptically transfer from the bottom of the tank to a steam-sterilized storage tank with a sanitary pump (50 tons of stainless steel water).
Furthermore, a steam sterilized pressure homogenizer (Manton Gorin 15 M-8TAfi) was used at a discharge pressure of 200 kp/
After homogenizing with cm, put in storage W1 (50 tons of stainless steel water with jacket and stirrer) with sanitary pump that has been aseptically steam sterilized.

10Cまで冷却し、無菌的に500dサンプルビン(5
00tRt容滅菌済みガラスビン)に充填した。
Cool to 10C and aseptically place in a 500d sample bottle (5
00tRt capacity sterilized glass bottle).

実施例3 実施例1と同様に生全卵液10ゆを作成した。Example 3 In the same manner as in Example 1, 10 servings of raw whole egg liquid were prepared.

これを、70〜71,5CVc調整し′fi−温水を循
壊さぜ几ジャケットと内部攪拌羽根を備え比密閉屋殺函
タンク(ステンレス製満水30t)内圧入れ、攪拌混合
しながら加熱殺菌を行なつ友。殺菌時間は全卵液温が6
9CVc達してから20分間であつ次。この時、全卵液
の最高温度は7G、5Cであつ友。殺菌後、夕/り低部
から全卵液を取シ出し。
This was adjusted to 70 to 71.5 CVc, and heated to sterilize it by circulating hot water and pressurizing it into a sealed tank (stainless steel, 30 tons full of water) equipped with a jacket and an internal stirring blade. friend. The sterilization time is when the temperature of the whole egg liquid is 6.
20 minutes after reaching 9CVc. At this time, the maximum temperature of the whole egg liquid is 7G, which is 5C. After sterilization, remove the whole egg liquid from the bottom of the tank.

真空ホモゲナイザー(特殊機化工業農Type −M 
)で真空度701]llmHgの減圧下で、  10.
00Orpm10分間ホモゲナイズし、ナイロン、ポリ
プロピレンラミネート袋(500m1X 250mm 
) K800Vずつ分割シールした。これを68〜70
Cにコントロールし′fi−温水中で、30分間加加熱
段を行ない、ただちに流水で冷却した。
Vacuum homogenizer (Special Mechanized Industrial Agriculture Type-M
) under reduced pressure of vacuum degree 701] 11 mHg, 10.
Homogenize for 10 minutes at 00 rpm and place in a nylon/polypropylene laminate bag (500 m x 250 mm).
) K800V was divided and sealed. This is 68-70
A heating stage was carried out for 30 minutes in 'fi-warm water controlled at 100°C, and immediately cooled with running water.

実施例4 生全卵fQi 5 kgを作成した。これを実施例1と
同様に、圧力式ホモゲナイザー(マントンゴーリン15
M−8TAfi) で吐出圧200 kg/calT:
均質化しt後、ナイロン・ポリプロピレンラミネート袋
(t30mg+x180msnK100fずつ分割シー
ルした。これ全69〜70cにコントロールし次温水中
で、3G分間(66O以上になっ几後)加熱段−を行な
い、fcだちに流水で冷却し比。
Example 4 5 kg of raw whole eggs fQi were prepared. This was carried out using a pressure homogenizer (Manton-Gorlin 15) in the same manner as in Example 1.
M-8TAfi) with a discharge pressure of 200 kg/calT:
After homogenization, the bag was divided and sealed into nylon/polypropylene laminate bags (30mg x 180msnK100f).The total temperature was controlled to 69-70C, and then a heating stage was performed for 3G in warm water (after the temperature reached 66O or higher), and the bag was immediately placed in fc. Cool with running water and mix.

実施例5 生全卵液10kgを作成した。これを実施例1と同様に
、カッティング式真空ホモゲナイザ−(特殊機化工業製
’fype −M )で真空度650 +uHg (D
減圧下で5002ずつ、  10000 rpm 10
分間のホモゲナイズを行なつ几。このホモゲナイズ全卵
液を、70〜71,50に調整し7t@水を循環さぜ友
ジャケットと内部攪拌羽根を備え′fI−密閉屋殺菌タ
ンク(ステンレス製満水30t)内に入れ、攪拌混合し
ながら加熱段#iを行なつ友。殺菌時間は全卵液温が6
6Cに違してから30分間であつ几。
Example 5 10 kg of raw whole egg liquid was prepared. As in Example 1, the vacuum degree was 650 + uHg (D
5002 each under reduced pressure, 10000 rpm 10
Homogenize for minutes. This homogenized whole egg liquid was adjusted to 70 to 71,50, and placed in a sealed sterilization tank (made of stainless steel, 30 tons full of water) equipped with a circulation jacket and an internal stirring blade with 7 tons of water, and stirred and mixed. A friend who performs heating stage #i while doing so. The sterilization time is when the temperature of the whole egg liquid is 6.
It was hot in 30 minutes after changing to 6C.

この時、全卵の最高温度は70.5 Gでbつ次。At this time, the highest temperature of all eggs was 70.5 G, which was second to highest.

殺菌後、タンク底部から蒸気殺菌済みのサニタリーポン
プ付貯槽(ジャケット、攪拌機付ステンレス製満水50
t)Ic入れ、10Cまで冷却し。
After sterilization, a steam sterilized sanitary pump equipped storage tank (stainless steel with jacket and agitator) is filled with water from the bottom of the tank.
t) Add Ic and cool to 10C.

無菌的に500−サンプルとン(s o oy容[1済
みガラスとン)に充填した。
Filled aseptically into a 500-sample bottle.

実施例1〜5の蛋白変性量および粘度は1表1のと1?
夛でめった。
The protein denaturation amount and viscosity of Examples 1 to 5 are as shown in Table 1 and 1?
I was disappointed with the number.

表 1  実施例1〜5の蛋白未変性量と粘度0.3M
食食塩浴溶液可溶性蛋白量測定(サンプ# 2,5 f
 f Oj M NaC6溶液に希釈溶解し1tとし、
15000rpm+60mの遠心後、上液をサンプルと
し、フェノール試薬法(LOWryらの方法)で測定し
た。蛋白率は生全卵2.5f/1tを100とし、生全
卵濃度を01で変化さぜ几検量線よシ求め之、、) また、実施例1.4で得たサンプルめ殺菌程度。
Table 1 Undenatured protein amount and viscosity 0.3M of Examples 1 to 5
Measurement of soluble protein in saline bath solution (samp #2, 5 f
f diluted and dissolved in Oj M NaC6 solution to make 1 t,
After centrifugation at 15,000 rpm + 60 m, the supernatant was used as a sample and measured by the phenol reagent method (method of LOWry et al.). The protein rate was determined using a calibration curve, with raw whole egg 2.5f/1t as 100 and the raw whole egg concentration changed at 01. Also, since the sample was obtained in Example 1.4, it was sterilized.

保存性1機能性、安定性、用途についての比較試験結果
を以下詳述する。
Comparative test results regarding storage stability 1 functionality, stability, and usage are detailed below.

比較試験例1  保存性試験 実施例1と同様に割卵、混合、濾過し九生全卵液を10
01ずつ袋に分割シールし、生全卵液サンプルとした。
Comparative Test Example 1 In the same manner as in Preservation Test Example 1, eggs were broken, mixed, and filtered, and 100% of nine-year-old whole egg liquid was prepared.
Each sample was divided and sealed into bags to obtain raw whole egg fluid samples.

ま友、生全卵液を実施例4の方法でホモゲナイズした未
加熱全卵液をサンプル(a) トした。サンプル(a)
に腐敗全卵g1係を混合したものをサンプル[有])と
し、サンプル(b)’t 実施例40方法で加熱殺菌し
たものをサンプル(C)、サンプルΦ)を60010分
間温水殺菌したものをサンプル(d)とした。実施例1
.4および生全卵、サンプル(a)。
Sample (a) of unheated whole egg liquid obtained by homogenizing raw whole egg liquid using the method of Example 4 was prepared. Sample (a)
Sample (b)'t was prepared by mixing rotten whole egg g1 with rotten whole egg g1. This was designated as sample (d). Example 1
.. 4 and raw whole eggs, sample (a).

(b)、 (C)、 (d)を10Cで保存し、一般生
函数と液性を比較評価し0表2の結果のとおシ1本発明
品は保存性にすぐれてbた。
(b), (C), and (d) were stored at 10C, and the general raw functions and liquid properties were comparatively evaluated. According to the results shown in Table 2, the products of the present invention had excellent storage stability.

表 2 保存性試験   ケ/1 (生全卵、サンプルa、b、dは1日後から沈澱が確認
された。) 比較試験例2  機能および安定性評価比較試験例1の
生全卵液、サンプル(a)、 (d)と実施例1.4の
加工全卵について、M置部、乳化能。
Table 2 Preservation test K/1 (Precipitation was confirmed in raw whole eggs, samples a, b, and d after 1 day.) Comparative test example 2 Function and stability evaluation Raw whole egg liquid and samples of comparative test example 1 (a), (d) and the processed whole eggs of Example 1.4, M position and emulsifying ability.

泡立能、安定性について比較した。A comparison was made regarding foaming ability and stability.

凝固能は、サンプル40 ft−50−ビーカーに入れ
、庫内温度aOCで蒸し、できた凝固物の硬さをレオメ
ータ−(サン科学R−UDJ −DM )で測定した。
The coagulation ability was determined by placing the sample in a 40 ft-50 beaker, steaming it at an internal temperature of aOC, and measuring the hardness of the coagulated product using a rheometer (Sun Scientific R-UDJ-DM).

乳化能は、す/プル5ftIC水47,5 f 、サラ
ダ油47.5 fを加えホモゲナイズ(日本精機2A−
t4000 rpm)L7を後、100mシリンダーに
入れ、16時間後の下層部に分離し几水層部の量を測定
し次。
Emulsifying ability is determined by homogenizing by adding 5 ft of water, 47.5 ft of IC water, and 47.5 ft of salad oil (Nippon Seiki 2A-
After t4000 rpm) L7 was placed in a 100m cylinder, separated into the lower layer after 16 hours, and the amount of the diluted water layer was measured.

泡立能は、サンプル60ノを160φ關ノホールに入れ
、ハンドミキサー(ナショナルMK100!でホイツピ
ングし、泡立の高さを御j足した。
To determine the foaming ability, 60 samples were placed in a 160φ hole and whipped with a hand mixer (National MK100!) to adjust the foaming height.

安定性は、サンプルIQfk試験管に入れ。For stability, put the sample into an IQfk test tube.

500 (l rpmで遠心(佐久間製作所、冷却式高
速遠心分離機50− B −5*ローター9B−3)を
行ない、沈澱、液の分離を観察し之。
Centrifugation was performed at 500 l rpm (Sakuma Seisakusho, refrigerated high-speed centrifuge 50-B-5*rotor 9B-3), and precipitation and liquid separation were observed.

凝固能、乳化能、泡立能1女定性の結果を表3゜4 、
5 、6に示す。
Table 3.4 shows the results of coagulation ability, emulsifying ability, and foaming ability.
Shown in 5 and 6.

表3 凝固能 表4  乳化能 表5 泡立能 表6 安定性 本発明品は、液の安定性および衛生的K特にすぐれてお
シ、また。卵の機能面からも何ら焔色なかつ友。
Table 3 Coagulation ability Table 4 Emulsifying ability Table 5 Foaming ability Table 6 Stability The product of the present invention has particularly excellent liquid stability and hygiene. Eggs are a perfect friend from a functional standpoint.

比較試験例5 卯加工原料としての評価 実施例1.4の加工全卵と割卵前の新鮮卵を使用して、
オムレッ、薄焼き卵、茶碗蒸し、カスタードプリン、ス
ポンジケーキを作成し、官能評価および調理性評価を行
なつ之。それぞれ卵料理の配合を表7に示す。表8に示
すように1本発明品は9wk卵よシ調理時間が大巾に短
縮され、使いやすく簡夏であった。ま友、ブレーンオム
レッ、カスタードプリン、茶碗蒸しでは1本発明品が硬
くなる傾向にあシ、加熱時間が短縮できる。官能的には
、同一加熱時間では本発明品の方が前述のように硬くな
る傾向にあるが1時間を短縮することにより、はぼ同一
の食感が得られる。スポンジケーキでは1本発明品の方
がキメが細かく食感がよく、ナイフでのカット面がしつ
かシしていた。加熱時間の短い薄焼き卵は1時間を調整
できないため、若干硬めの食感であったが、調理の失敗
は全くなく、g理性が著しく向上した。
Comparative Test Example 5 Evaluation of Rabbit as a Raw Material for Processing Using the processed whole eggs and unbroken fresh eggs of Example 1.4,
We made omelets, lightly fried eggs, steamed egg custard, custard pudding, and sponge cake, and conducted sensory evaluations and cookability evaluations. Table 7 shows the formulation of each egg dish. As shown in Table 8, the product of the present invention greatly shortened the cooking time for 9wk egg and was easy to use and easy to use. For rice cakes, brain omelets, custard pudding, and chawan mushi, the products of the present invention tend to be hard, so the heating time can be shortened. Sensory-wise, the product of the present invention tends to be harder as described above if the heating time is the same, but by shortening the heating time by one hour, almost the same texture can be obtained. Regarding the sponge cake, the inventive product had a finer texture and a better texture, and the cut surface with a knife was firm. Thinly baked eggs with a short heating time could not be adjusted for 1 hour, so the texture was a little hard, but there were no cooking failures and the gability was significantly improved.

表 7  卵加工品原料配合 比較試験例4  流動曲線の比較 実施例1と同様に生全卵液〔サンプル(イ)〕を作成し
、これをナイロン・ポリプロピレンラミネート袋(13
0闘×180冨1)中に200vずつ分割シールシ友。
Table 7 Comparative test example 4 of blending raw materials for processed egg products Comparison of flow curves Raw whole egg liquid [sample (a)] was prepared in the same manner as in Example 1, and this was placed in a nylon polypropylene laminate bag (13
0 battle x 180 1) Seal shield friend divided into 200v each.

68.5〜69.5C7l’l:コントロールした温水
中に入れ、全卵液温が65Cに違した後。
68.5-69.5C7l'l: After placing in controlled warm water to bring the temperature of the whole egg mixture to 65C.

25分間加熱し几〔サンプル(ロ)〕。これ’t7tだ
ちに流水で冷却した後、開封し、真空ホモゲナイザ−(
特殊機化工業Type −M )で真空度650mmH
gの減圧下で、10000 rpm5分間ホモゲナイズ
し。
Heat for 25 minutes [Sample (B)]. Immediately cool it under running water, open it, and use a vacuum homogenizer (
Tokushu Kika Kogyo Type-M) vacuum degree 650mmH
Homogenize at 10,000 rpm for 5 minutes under reduced pressure of 10,000 g.

ざらに圧力式ホモゲナイザー(マントンゴーリフ15M
−8TA型)で吐出圧40qkg/cr/lで均質化し
、サンプルeうを作成した。ま九、サンプル(イ)ヲ圧
力式ホモゲナイザ−(マントンゴーリン15M−8TA
型)で吐出圧400Icg/c+y!で均質化した生全
卵液〔サンプルに)〕を、ナイロン・ポリプロピレンラ
ミネート袋(tsom履×180關)中に200fずつ
分割シールし、68.5〜69.5 ’Cにコントロー
ルした温水中に入れ、全卵液温が65C[達した後、2
5分間加熱した。これをただちに流水で冷却し、サンプ
ル(ホ)を作成した。
Rough pressure homogenizer (Manton Gaurif 15M
-8TA type) at a discharge pressure of 40 qkg/cr/l to prepare sample e. 9. Sample (a) Pressure homogenizer (Manton Gorlin 15M-8TA
) with a discharge pressure of 400Icg/c+y! The homogenized raw whole egg liquid (sample) was sealed in nylon/polypropylene laminate bags (Tsom shoes x 180 mm) in 200 f portions, and placed in warm water controlled at 68.5 to 69.5'C. After the temperature of the whole egg mixture reaches 65C [2
Heated for 5 minutes. This was immediately cooled under running water to prepare a sample (e).

サンプル0)、(ロ)、(ハ)、に)、(ホ)の流動曲
線ハ第4図のとシシで1本発明品は、加熱したにもかか
わらず低粘度で、かつゲル性を示さない均質な液状の加
工全卵であった。
The flow curves of samples 0), (b), (c), ni), and (e) are shown in Fig. 4.1 The product of the present invention has a low viscosity and shows gel properties despite being heated. There was no homogeneous liquid processed whole egg.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は加熱時間に伴う蛋白未変性率の変化を示すグラ
フ、第2図は蛋白変性本と粘度の関係を示すグラフ、第
3図は卵のDSCパターンを示すグラフ、第4図は流動
曲線を示すグラフである。 第1図 力D 熱 @  k’)   (min)第2図 蛋白変性率(×) 温度(°C) 勇lη応力(Pa)
Figure 1 is a graph showing the change in protein undenatured rate with heating time, Figure 2 is a graph showing the relationship between protein denaturation and viscosity, Figure 3 is a graph showing the DSC pattern of eggs, and Figure 4 is a graph showing the flow rate. It is a graph showing a curve. Figure 1 Force D Heat @k') (min) Figure 2 Protein denaturation rate (x) Temperature (°C) Stress (Pa)

Claims (7)

【特許請求の範囲】[Claims] (1)全卵の蛋白質の一部が加熱により変性しており、
その未変性部分が塩可溶性蛋白量比で生全卵の50〜9
0%、粘度が10〜4000cpの均質な液状であり、
かつ流動曲線においてゲル性を示さないことを特徴とす
る加工全卵。
(1) Some of the proteins in whole eggs are denatured by heating.
The undenatured part has a salt-soluble protein content ratio of 50 to 9 compared to raw whole eggs.
0%, a homogeneous liquid with a viscosity of 10 to 4000 cp,
A processed whole egg characterized by not exhibiting gel properties in its flow curve.
(2)全卵の蛋白質の一部が加熱により変性しており、
その未変性部分が塩可溶性蛋白量比で生全卵の50〜9
0%、粘度が10〜4000cpの範囲内の均質な液状
であり、かつ流動曲線においてゲル性を示さない加工全
卵を製造するに当り、液状に混合した全卵を加熱殺菌し
た後、ホモゲナイズすることを特徴とする加工全卵の製
造法。
(2) Some of the proteins in whole eggs are denatured by heating.
The undenatured part has a salt-soluble protein content ratio of 50 to 9 compared to raw whole eggs.
0%, a homogeneous liquid with a viscosity in the range of 10 to 4000 cp, and a processed whole egg that does not show gelatinity in the flow curve, the whole egg mixed into a liquid is heat sterilized and then homogenized. A method for producing processed whole eggs characterized by:
(3)ホモゲナイズを減圧下でのカッティング式ホモゲ
ナイザーあるいは50kg/cm^3以上の圧力式ホモ
ゲナイザーで行なう特許請求の範囲第2項記載の加工全
卵の製造法。
(3) The method for producing processed whole eggs according to claim 2, wherein the homogenization is carried out using a cutting type homogenizer under reduced pressure or a pressure type homogenizer at 50 kg/cm^3 or more.
(4)加熱殺菌温度が65〜72.5℃であり、加熱殺
菌時間が1〜300分間の範囲である特許請求の範囲第
2項または第3項記載の加工全卵の製造法。
(4) The method for producing processed whole eggs according to claim 2 or 3, wherein the heat sterilization temperature is 65 to 72.5°C and the heat sterilization time is in the range of 1 to 300 minutes.
(5)全卵の蛋白質の一部が加熱により変性しており、
その未変性部分が塩可溶性蛋白量比で生全卵の50〜9
0%、粘度が10〜4000cpの範囲内の均質な液状
であり、かつ流動曲線においてゲル性を示さない加工全
卵を製造するに当り、液状に混合した生卵をホモゲナイ
ズした後、加熱殺菌することを特徴とする加工全卵の製
造法。
(5) Some of the proteins in whole eggs are denatured by heating.
The undenatured part has a salt-soluble protein ratio of 50 to 9 compared to raw whole eggs.
0%, a homogeneous liquid with a viscosity in the range of 10 to 4000 cp, and in producing processed whole eggs that do not show gel properties in the flow curve, the raw eggs mixed into a liquid are homogenized and then heat sterilized. A method for producing processed whole eggs characterized by:
(6)ホモゲナイズを減圧下でのカッティング式ホモゲ
ナイザーあるいは50kg/cm^3以上の圧力式ホモ
ゲナイザーで行なう特許請求の範囲第5項記載の加工全
卵の製造法。
(6) The method for producing processed whole eggs according to claim 5, wherein the homogenization is carried out using a cutting type homogenizer under reduced pressure or a pressure type homogenizer at 50 kg/cm^3 or more.
(7)加熱殺菌温度が65〜72.5℃であり、加熱殺
菌時間が1〜300分間の範囲である特許請求の範囲第
5項または第6項記載の加工全卵の製造法。
(7) The method for producing processed whole eggs according to claim 5 or 6, wherein the heat sterilization temperature is 65 to 72.5°C and the heat sterilization time is in the range of 1 to 300 minutes.
JP61148155A 1985-11-21 1986-06-26 Processed whole egg and production thereof Granted JPS62201556A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP61148155A JPS62201556A (en) 1985-11-21 1986-06-26 Processed whole egg and production thereof

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP25972985 1985-11-21
JP60-259729 1985-11-21
JP60-261540 1985-11-22
JP26154085 1985-11-22
JP61148155A JPS62201556A (en) 1985-11-21 1986-06-26 Processed whole egg and production thereof

Publications (2)

Publication Number Publication Date
JPS62201556A true JPS62201556A (en) 1987-09-05
JPH0586175B2 JPH0586175B2 (en) 1993-12-10

Family

ID=27319504

Family Applications (1)

Application Number Title Priority Date Filing Date
JP61148155A Granted JPS62201556A (en) 1985-11-21 1986-06-26 Processed whole egg and production thereof

Country Status (1)

Country Link
JP (1) JPS62201556A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63164866A (en) * 1986-12-27 1988-07-08 Q P Corp Production of process whole egg
JP2007222099A (en) * 2006-02-24 2007-09-06 Ise Delica Kk Method for producing pasteurized liquid whole egg, and food using liquid whole egg food
JP2008054610A (en) * 2006-09-01 2008-03-13 Q P Corp Processed liquid albumen
JP2012125230A (en) * 2011-03-14 2012-07-05 Sanshu Shokuhin Kk Method of manufacturing sterilized liquid egg
JP2015023827A (en) * 2013-07-26 2015-02-05 キユーピー株式会社 Method for preventing the turbidity of egg soup, sterilization working liquid whole egg for egg soup, egg soup using the sterilization working liquid whole egg, and method for producing the egg soup

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3093487A (en) * 1961-02-27 1963-06-11 Jones Eynon Egg products and processes for preparing same
US3113872A (en) * 1960-01-26 1963-12-10 Prep Foods Inc Method of treating shelled eggs
JPS576872A (en) * 1980-06-13 1982-01-13 Minolta Camera Co Ltd Toner replenishing device

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3113872A (en) * 1960-01-26 1963-12-10 Prep Foods Inc Method of treating shelled eggs
US3093487A (en) * 1961-02-27 1963-06-11 Jones Eynon Egg products and processes for preparing same
JPS576872A (en) * 1980-06-13 1982-01-13 Minolta Camera Co Ltd Toner replenishing device

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63164866A (en) * 1986-12-27 1988-07-08 Q P Corp Production of process whole egg
JP2007222099A (en) * 2006-02-24 2007-09-06 Ise Delica Kk Method for producing pasteurized liquid whole egg, and food using liquid whole egg food
JP4630834B2 (en) * 2006-02-24 2011-02-09 イセデリカ株式会社 Sterilization liquid whole egg manufacturing method and liquid whole egg food
JP2008054610A (en) * 2006-09-01 2008-03-13 Q P Corp Processed liquid albumen
JP4671934B2 (en) * 2006-09-01 2011-04-20 キユーピー株式会社 Food using meringue made of processed egg white
JP2012125230A (en) * 2011-03-14 2012-07-05 Sanshu Shokuhin Kk Method of manufacturing sterilized liquid egg
JP2015023827A (en) * 2013-07-26 2015-02-05 キユーピー株式会社 Method for preventing the turbidity of egg soup, sterilization working liquid whole egg for egg soup, egg soup using the sterilization working liquid whole egg, and method for producing the egg soup

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