JPS62132518A - Porous filter having sealed end part - Google Patents

Porous filter having sealed end part

Info

Publication number
JPS62132518A
JPS62132518A JP60270629A JP27062985A JPS62132518A JP S62132518 A JPS62132518 A JP S62132518A JP 60270629 A JP60270629 A JP 60270629A JP 27062985 A JP27062985 A JP 27062985A JP S62132518 A JPS62132518 A JP S62132518A
Authority
JP
Japan
Prior art keywords
porous
base material
porous filter
filter
pore diameter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP60270629A
Other languages
Japanese (ja)
Inventor
Miki Ishikawa
幹 石川
Noboru Takase
高瀬 昇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NGK Insulators Ltd
Original Assignee
NGK Insulators Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NGK Insulators Ltd filed Critical NGK Insulators Ltd
Priority to JP60270629A priority Critical patent/JPS62132518A/en
Publication of JPS62132518A publication Critical patent/JPS62132518A/en
Pending legal-status Critical Current

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  • Filtering Materials (AREA)
  • Filtration Of Liquid (AREA)

Abstract

PURPOSE:To prevent leak from an end part and to increase filter precision by providing a filter layer having pore diameter smaller than a porous cylindrical base material to at least one face of the base material and sealing at least edge face of one end. CONSTITUTION:A porous filter layer 2 which has narrow pore diameter smaller than a porous cylindrical base material 1 and has <=10mum average narrow pore diameter is provided to the inner peripheral surface of the base material 1. Furthermore a porous filter 4 is formed by providing the end part seals 3a, 3b with a sealing material to both end faces. As material of the base material 1, ceramics, sintered metal and resin, etc., are used. As a manufacturing method of the end part seals 3a, 3b, a method such as dipping, spraying and troweling is used and as the sealing material, glaze, alumina series ceramic bond and a suspension of silicone resin and polytetrafluoroethylene are used.

Description

【発明の詳細な説明】 (産業上の利用分野) 本発明はフィルターの°濾過方向断面において細孔径に
差異がある2層以上の多層構造を有する多孔質フィルタ
ーに関するものである。
DETAILED DESCRIPTION OF THE INVENTION (Field of Industrial Application) The present invention relates to a porous filter having a multilayer structure of two or more layers having different pore sizes in a cross section in the filtration direction of the filter.

(従来の技術) 第3図(a) 、 (b)は従来の多孔質フィルターの
一例を示す断面図および底面図である。第3図において
、多孔質からなる円筒状基材11の外周面に基材よりも
細孔径が小なる30〜200μmの厚みの多孔質濾過層
12を設けた多孔質フィルター13を、その両端面にガ
スケット14a、 14bを設けてトップカバー15に
固定されたタイロフトボルト16をナツト17により締
付けることによりチューブプレート18に取付けていた
。上述した構造の多孔質フィルターでは、濾過すべき原
液をフィルター外表面から通してその濾液を内筒を介し
て外部へ取出してした。
(Prior Art) FIGS. 3(a) and 3(b) are a sectional view and a bottom view showing an example of a conventional porous filter. In FIG. 3, a porous filter 13 is provided on the outer circumferential surface of a porous cylindrical base material 11 with a porous filtration layer 12 having a thickness of 30 to 200 μm and having a smaller pore diameter than the base material. Gaskets 14a and 14b are provided at the top cover 15, and tie loft bolts 16 fixed to the top cover 15 are attached to the tube plate 18 by tightening them with nuts 17. In the porous filter having the above-described structure, the stock solution to be filtered is passed through the outer surface of the filter, and the filtrate is taken out to the outside through the inner cylinder.

(発明が解決しようとする問題点) 上述した多層構造の多孔質フィルターにおいては、多孔
質濾過層12の端部をガスケット14a、 14bにて
完全にシールするのは困難であるとともに、多孔質濾過
層12では濾過抵抗が大きいため濾過力を高くする必要
があるが、濾過圧力を高くするとガスケット14a、1
4bによるシールのみでは第4図(a)に示すようにガ
スケット14a、 14bと濾過層12の接続部から原
液がリークしてしまい信頼性に欠ける欠点があった。
(Problems to be Solved by the Invention) In the above-described porous filter having a multilayer structure, it is difficult to completely seal the ends of the porous filtration layer 12 with the gaskets 14a and 14b, and the porous filtration Since the layer 12 has a large filtration resistance, it is necessary to increase the filtration force, but if the filtration pressure is increased, the gaskets 14a and 1
4b alone, the undiluted solution leaks from the connection between the gaskets 14a and 14b and the filtration layer 12, resulting in a lack of reliability, as shown in FIG. 4(a).

また、この多孔質濾過層12は非常に薄く第4図(b)
に示すようにガスケット14a、 14bと濾過層12
の接続部が欠落し濾過層欠落部19が生じ、この濾過層
欠落部19を介して原液がリークしてしまう欠点もあっ
た。
Moreover, this porous filtration layer 12 is very thin as shown in FIG. 4(b).
Gaskets 14a, 14b and filter layer 12 as shown in FIG.
There was also a drawback that the connection part was missing, resulting in a filtration layer missing part 19, and the stock solution leaked through this filtration layer missing part 19.

本発明の目的は上述した不具合を解消して、フィルタ一
端部からの原液のリークのまったくない完全なシール性
を達成でき信頼性の高い多孔質フィルターを提供しよう
とするものである。
An object of the present invention is to eliminate the above-mentioned problems and provide a highly reliable porous filter that can achieve complete sealing without any leakage of stock solution from one end of the filter.

(問題点を解決するための手段) 本発明の端部シールを有する多孔質フィルターは、多孔
質からなる円筒状基材と該基材の内周面または外周面の
少なくとも一面に基材よりも細孔径が小なる多孔質濾過
層を少なくとも一層結合させた構造の多孔質フィルター
において、前記多孔質濾過層の少なくとも一端縁面がシ
ール材でシールされたことを特徴とするものである。
(Means for Solving the Problems) A porous filter having an end seal according to the present invention includes a porous cylindrical base material and at least one of the inner circumferential surface or outer circumferential surface of the base material. A porous filter having a structure in which at least one porous filtration layer with a small pore diameter is bonded together is characterized in that at least one end surface of the porous filtration layer is sealed with a sealing material.

(作 用) 上述した構成において、多孔質濾過層の端面をシール材
により完全にシールしているため、多孔質濾過層の端部
から原液がリークすることはまったくなく信頼性の高い
多孔質フィルターを得ることができる。
(Function) In the above-mentioned configuration, since the end faces of the porous filtration layer are completely sealed with the sealing material, there is no leakage of the stock solution from the ends of the porous filtration layer, resulting in a highly reliable porous filter. can be obtained.

(実施例) 第1図は本発明の多孔質フィルターの一実施例を示す断
面図である。本実施例では、多孔質からなる円筒状基材
1の内周面に基材よりも細孔径が小であり、平均細孔径
が10μm以下の多孔質濾過層2を設け、さらに両端面
にはシール材により端部シール3a、 3bを設けて多
孔質フィルター4を構成している。多孔質からなる円筒
状基材1の材質としては、セラミックス、焼結金属、樹
脂等が使用可能である。上述した濾過層2が円筒状基材
1の内周面に設けられている実施例においては、濾過す
べき原液を多孔質フィルターの内周面から供給して濾液
を外周面から得ている。
(Example) FIG. 1 is a sectional view showing an example of a porous filter of the present invention. In this example, a porous filtration layer 2 having a smaller pore diameter than the base material and an average pore diameter of 10 μm or less is provided on the inner circumferential surface of a porous cylindrical base material 1, and further, on both end faces. A porous filter 4 is constructed by providing end seals 3a and 3b using a sealing material. As the material of the porous cylindrical base material 1, ceramics, sintered metal, resin, etc. can be used. In the embodiment in which the filtration layer 2 described above is provided on the inner peripheral surface of the cylindrical substrate 1, the stock solution to be filtered is supplied from the inner peripheral surface of the porous filter, and the filtrate is obtained from the outer peripheral surface.

端部シール3a、 3bの作製方法としては、ディッピ
ング、スプレー、コテ塗り等の方法により塗布の場合お
よび含浸の場合、さらには端部の形状と同一形状のシー
ル部材を接着して形成する接着の場合が考えられる。塗
布の場合は第2図(a)に端部の拡大断面図を示すよう
に、端部全体および濾過層2表面の端部から3〜5mm
の範囲に上述した方法によりシール材を塗布して端部シ
ール3を構成する。また、含浸の場合は第2図(b)に
端部の拡大断面図を示すように1円筒状基材1および濾
過層2の端部から3〜5mmの深さの部分全体にシール
材を含浸させ端部シール3を構成している。
The end seals 3a and 3b can be produced by coating by dipping, spraying, troweling, etc., by impregnation, or by bonding a sealing member having the same shape as the end. There are possible cases. In the case of coating, as shown in the enlarged cross-sectional view of the end in FIG.
The end seal 3 is constructed by applying a sealing material to the area by the method described above. In addition, in the case of impregnation, the sealing material is applied to the entire cylindrical base material 1 and the filtration layer 2 at a depth of 3 to 5 mm from the end, as shown in FIG. 2(b), which is an enlarged cross-sectional view of the end. The end seal 3 is formed by impregnation.

これら塗布および含浸の場合のシール材の材料としては
、釉薬、アルミナ系セラミックボンド等の無機質材料お
よびシリコン樹脂、テトラフルオロエチレン−パーフル
オロアルキルビニルエーテル重合体、テトラフルオロエ
チレン−へキサフルオロプロピレン共重合体、ポリテト
ラフルオロエチレン等の樹脂を疎水性コロイド状粒子と
したQi液等の有機質材料を好適に使用することができ
る。
In the case of coating and impregnating, the sealing materials include glaze, inorganic materials such as alumina ceramic bond, silicone resin, tetrafluoroethylene-perfluoroalkyl vinyl ether polymer, and tetrafluoroethylene-hexafluoropropylene copolymer. An organic material such as a Qi liquid containing hydrophobic colloidal particles of a resin such as polytetrafluoroethylene or the like can be suitably used.

さらに、接着の場合は第2図(c)に端部の拡大断面図
を示すように、多孔質フィルター4の端部形状と同一形
状、例えば第1図に示す実施例ではドーナツ状の形状に
3〜5mm厚さのシール材5を作製し、そのシール材5
を接着剤6により端部に接着して端部シール3を構成し
ている。−このとき、シール材5としてステンレス、耐
食金属等の金属材料やA l1zoi等の無機質材料さ
らにはシリコンゴム等の有機質材料を好適に使用するこ
とができる。また、接着剤6の材料としてはエポキシ系
、シリコン系等の有機質材料や釉薬、アルミナ系セラミ
ックボン、ド等の無機質材料を好適に使用できる。
Furthermore, in the case of adhesion, as shown in an enlarged cross-sectional view of the end in FIG. A sealing material 5 having a thickness of 3 to 5 mm is produced, and the sealing material 5 is
is adhered to the end portion with an adhesive 6 to form an end seal 3. - At this time, as the sealing material 5, metal materials such as stainless steel and corrosion-resistant metals, inorganic materials such as Al1zoi, and organic materials such as silicone rubber can be suitably used. Further, as the material for the adhesive 6, organic materials such as epoxy-based and silicon-based materials, and inorganic materials such as glaze and alumina-based ceramic bond or bond can be suitably used.

ス新1矩[ 第1図1こ示す構造の多孔質フィルター4において、端
部シール3としてシリコン樹脂を端部に含浸して本発明
の多孔質フィルター4を得た。含浸方法としてはディッ
ピング法を採用し、まず容器に約7mmの深さに所定濃
度のシリコン樹脂を入れフィルター4の端部を容器の底
へ押す要領で20回/分の含浸操作をおこなった。シリ
コン樹脂の濃度および工程を以下の第1表に示す。
In the porous filter 4 having the structure shown in FIG. 1, the end portions were impregnated with silicone resin as the end seals 3 to obtain the porous filter 4 of the present invention. A dipping method was adopted as the impregnation method, and first, silicone resin of a predetermined concentration was placed in a container to a depth of about 7 mm, and the impregnation operation was performed 20 times/minute by pushing the end of the filter 4 toward the bottom of the container. The silicone resin concentration and process are shown in Table 1 below.

第1表 含浸操作終了後のフィルター4を常温で約2時間乾燥し
たところ、端面より3〜5mmの部分全体にシリコン樹
脂を含浸した端部3a、 3bを有するフィルター4を
得ることができた。
When the filter 4 after the impregnation operation in Table 1 was dried at room temperature for about 2 hours, it was possible to obtain a filter 4 having end portions 3a and 3b in which the entire portion 3 to 5 mm from the end surface was impregnated with silicone resin.

上述した多孔質フィルター4に対してその効果を確認す
るため、確認テストとして両端の端部シール3a、 3
bをガスケットによりシールし空気を一定圧力でその内
部に入れた場合の端部からの発泡現象を確認した。また
、比較の対象として端部シール3a、 3bを有さない
従来のフィルターにも同様の試験を行った。結果は、本
発明の多孔質フィルターでは通気圧2 kg/cm”G
にてフィルターの濾過有効部より発泡を確認したが、こ
の際端部からのリークをまったく確認できないと共に通
気圧を5kg/cm2Gまで昇圧しても同様の結果であ
った。これに対し、従来の多孔質フィルターでは通気圧
2kg/cm2cにおいて濾過有効部だけでなく端部か
らも発泡を確認した。
In order to confirm the effect on the porous filter 4 described above, end seals 3a, 3 at both ends were used as a confirmation test.
b. When sealed with a gasket and air was introduced into the inside at a constant pressure, the phenomenon of foaming from the end was confirmed. For comparison, a similar test was also conducted on a conventional filter that did not have the end seals 3a, 3b. The results show that the porous filter of the present invention has a ventilation pressure of 2 kg/cm"G.
Foaming was confirmed from the effective filtration part of the filter, but no leakage from the ends could be confirmed at all, and the same result was obtained even when the ventilation pressure was increased to 5 kg/cm2G. On the other hand, with the conventional porous filter, foaming was confirmed not only from the effective filtration area but also from the ends at a ventilation pressure of 2 kg/cm2c.

人血拠叢 第1図に示す構造の多孔質フィルター4において、端部
シール3a、 3bとして釉薬を塗布して本考案の多孔
質フィルター4を得た。釉薬の塗布方法としては、基材
1を焼成後多孔質濾過層2を形成して乾燥し、端部全体
および濾過層2表面の端部から3〜5mmの範囲に釉薬
を施釉した。その後全体を乾燥して約1500℃で焼成
して端部シール3a。
A porous filter 4 of the present invention was obtained by applying a glaze to the end seals 3a and 3b of the porous filter 4 having the structure shown in FIG. 1. The glaze was applied by firing the base material 1, forming the porous filtration layer 2, drying it, and applying the glaze to the entire end and the surface of the filtration layer 2 within a range of 3 to 5 mm from the end. Thereafter, the whole is dried and fired at about 1500°C to form the end seal 3a.

3bを存する本発明の多孔質フィルター4を得た。Porous filter 4 of the present invention containing 3b was obtained.

上述した方法により作製した多孔質フィルター4に対し
て実施例1と同様の試験を行ったところ、本実施例によ
る多孔質フィルター4も通気圧5kg/cm”Gにおい
て端部からのリークはまったく確認できなかった。
When the same test as in Example 1 was conducted on the porous filter 4 manufactured by the method described above, no leakage from the end portion was confirmed in the porous filter 4 according to this example at a ventilation pressure of 5 kg/cm''G. could not.

夫11鉗よ 第1図に示す構造の多孔質フィルター4において端部フ
ィルターとして端部の形状と同一形状のシール部材を端
部に接着して本発明の多孔質フィルター4を得た。シー
ル材5としては、5 mn+IWのS[IS 304を
端部形状と同一のドーナツ形に作製したものと、98%
A f 203を同じく端部形状と同一のドーナツ形に
作製したものとを使用した。接着剤6としてはエポキシ
系接着剤を使用し、この接着剤6をフィルタ一端部に塗
布した後上述したシール材5を接着させて端部シールを
形成した。なお、接着剤6の厚さは0.2〜1.01が
好ましい。
In the porous filter 4 having the structure shown in FIG. 1, sealing members having the same shape as the end portions were adhered to the end portions of the porous filter 4 having the structure shown in FIG. 1 to obtain the porous filter 4 of the present invention. The sealing material 5 was made of 5 mn+IW S [IS 304 made into the same donut shape as the end shape, and 98%
An A f 203 having the same donut shape as the end shape was used. An epoxy adhesive was used as the adhesive 6, and after applying this adhesive 6 to one end of the filter, the above-mentioned sealing material 5 was adhered to form an end seal. Note that the thickness of the adhesive 6 is preferably 0.2 to 1.01.

接着後24時間常温にて乾燥させ、本発明の多孔質フィ
ルター4を得た。
After adhesion, it was dried at room temperature for 24 hours to obtain a porous filter 4 of the present invention.

上述した方法により作製した多孔質フィルター4に対し
て実施例1と同様の試験を行ったところ、本実施例によ
る多孔質フィルター4も通気圧5kg/cm”Gにおい
て端部からのリークはまったく確認できなかった。
When the same test as in Example 1 was conducted on the porous filter 4 manufactured by the method described above, no leakage from the end portion was confirmed in the porous filter 4 according to this example at a ventilation pressure of 5 kg/cm''G. could not.

(発明の効果) 以上詳細に説明したところから明らかなように、本発明
の端部シールを有する多孔質フィルターにおいては、フ
ィルタ一端部にシール材を設けることにより端部のシー
ル性を完全にできると共に端部からのリークを皆無にで
きるので、濾過精度の向上を計ることができる。また、
フィルターを濾過器へ組込む際に端部の部分的欠落につ
いて許容範囲を考慮可能であると共に、多孔質濾過層の
保護の点からも有効であり、製品の信頼性の向上を計る
ことができる。
(Effects of the Invention) As is clear from the detailed explanation above, in the porous filter having an end seal of the present invention, by providing a sealing material at one end of the filter, the end sealing performance can be completely achieved. At the same time, since leakage from the ends can be completely eliminated, filtration accuracy can be improved. Also,
When assembling the filter into a filter, it is possible to take into account the tolerance for partial loss at the end, and it is also effective in terms of protecting the porous filtration layer, making it possible to improve the reliability of the product.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は本発明の多孔質フィルターの一実施例を示す断
面図、 第2図(a) 、 (b) 、 (c)はそれぞれ本発
明の多孔質フィルターの端部の一実施例を拡大して示す
断面図、 第3図(a) 、 (b)は従来の多孔質フィルターの
一実施例を示す断面図および底面図、 第4図(a) 、 (b)は従来の多孔質フィルターの
欠点を説明するための拡大断面図である。 1・・・円筒基材     2・・・多孔質濾過層3、
3a、 3b・・・端部シール 4・・・多孔質フィルター 5・・・シール材6・・・
接着剤 第3図    第4図 (b>      (b)
Figure 1 is a sectional view showing an embodiment of the porous filter of the present invention, and Figures 2 (a), (b), and (c) are enlarged views of an embodiment of the end portion of the porous filter of the present invention. 3(a) and (b) are sectional views and bottom views showing an example of a conventional porous filter, and FIG. 4(a) and (b) are a conventional porous filter. FIG. 1... Cylindrical base material 2... Porous filtration layer 3,
3a, 3b... End seal 4... Porous filter 5... Seal material 6...
Adhesive Figure 3 Figure 4 (b> (b)

Claims (1)

【特許請求の範囲】 1、多孔質からなる円筒状基材と該基材の内周面または
外周面の少なくとも一面に基材よりも細孔径が小なる多
孔質濾過層を少なくとも一層結合させた構造の多孔質フ
ィルターにおいて、前記多孔質濾過層の少なくとも一端
縁面がシール材でシールされたことを特徴とする端部シ
ール多孔質フィルター。 2、前記多孔質基材と多孔質濾過層がセラミックスから
なる特許請求の範囲第1項記載の端部シールを有する多
孔質フィルター。 3、前記シール材が無機質材料または有機質材料である
特許請求の範囲第1項記載の端部シールを有する多孔質
フィルター。 4、前記シール材として、金属からなる薄板、細孔径が
小なるセラミックスからなる薄板または有機質材料から
なる薄板のうちいずれかの薄板を接着した特許請求の範
囲第1項記載の端部シールを有する多孔質フィルター。
[Claims] 1. A porous cylindrical base material and at least one porous filtration layer having a smaller pore diameter than the base material bonded to at least one of the inner peripheral surface or outer peripheral surface of the base material. 1. An end-sealed porous filter according to the present invention, wherein at least one end surface of the porous filtration layer is sealed with a sealing material. 2. A porous filter having an end seal according to claim 1, wherein the porous base material and the porous filtration layer are made of ceramics. 3. A porous filter having an end seal according to claim 1, wherein the sealing material is an inorganic material or an organic material. 4. The end seal according to claim 1, in which a thin plate made of a metal, a thin plate made of a ceramic with a small pore diameter, or a thin plate made of an organic material is bonded as the sealing material. Porous filter.
JP60270629A 1985-12-03 1985-12-03 Porous filter having sealed end part Pending JPS62132518A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP60270629A JPS62132518A (en) 1985-12-03 1985-12-03 Porous filter having sealed end part

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP60270629A JPS62132518A (en) 1985-12-03 1985-12-03 Porous filter having sealed end part

Publications (1)

Publication Number Publication Date
JPS62132518A true JPS62132518A (en) 1987-06-15

Family

ID=17488749

Family Applications (1)

Application Number Title Priority Date Filing Date
JP60270629A Pending JPS62132518A (en) 1985-12-03 1985-12-03 Porous filter having sealed end part

Country Status (1)

Country Link
JP (1) JPS62132518A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02172511A (en) * 1988-12-26 1990-07-04 Ngk Insulators Ltd Tubular ceramic filter, method and device for sealing its end
JP2008173601A (en) * 2007-01-22 2008-07-31 Ngk Insulators Ltd Ceramic filter and end face sealing method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5952511A (en) * 1982-04-28 1984-03-27 セラヴエ−ル Filter element and production thereof
JPS5982918A (en) * 1982-11-02 1984-05-14 Kanebo Ltd Filter medium of multi-layered structure

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5952511A (en) * 1982-04-28 1984-03-27 セラヴエ−ル Filter element and production thereof
JPS5982918A (en) * 1982-11-02 1984-05-14 Kanebo Ltd Filter medium of multi-layered structure

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02172511A (en) * 1988-12-26 1990-07-04 Ngk Insulators Ltd Tubular ceramic filter, method and device for sealing its end
JP2008173601A (en) * 2007-01-22 2008-07-31 Ngk Insulators Ltd Ceramic filter and end face sealing method thereof

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