JPS6212968B2 - - Google Patents
Info
- Publication number
- JPS6212968B2 JPS6212968B2 JP61014566A JP1456686A JPS6212968B2 JP S6212968 B2 JPS6212968 B2 JP S6212968B2 JP 61014566 A JP61014566 A JP 61014566A JP 1456686 A JP1456686 A JP 1456686A JP S6212968 B2 JPS6212968 B2 JP S6212968B2
- Authority
- JP
- Japan
- Prior art keywords
- frozen
- freezing
- clams
- water
- flavor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 235000011187 glycerol Nutrition 0.000 claims description 4
- 235000000346 sugar Nutrition 0.000 claims description 4
- 150000008163 sugars Chemical class 0.000 claims description 4
- 241000237852 Mollusca Species 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 24
- 235000020639 clam Nutrition 0.000 description 15
- 238000007710 freezing Methods 0.000 description 14
- 230000008014 freezing Effects 0.000 description 14
- 241000237519 Bivalvia Species 0.000 description 13
- 238000010438 heat treatment Methods 0.000 description 13
- 235000013372 meat Nutrition 0.000 description 13
- 239000000796 flavoring agent Substances 0.000 description 12
- 235000019634 flavors Nutrition 0.000 description 12
- 238000000034 method Methods 0.000 description 11
- 235000015170 shellfish Nutrition 0.000 description 11
- 238000002347 injection Methods 0.000 description 8
- 239000007924 injection Substances 0.000 description 8
- 239000000243 solution Substances 0.000 description 6
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 238000010411 cooking Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000013505 freshwater Substances 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000004576 sand Substances 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 241000251468 Actinopterygii Species 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 241000945534 Hamana Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241000237536 Mytilus edulis Species 0.000 description 1
- 241000237503 Pectinidae Species 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000020638 mussel Nutrition 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 235000020995 raw meat Nutrition 0.000 description 1
- 235000020637 scallop Nutrition 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
Landscapes
- Meat, Egg Or Seafood Products (AREA)
Description
本発明は新規な二枚貝の冷凍保存方法、より詳
細には長期凍結保存後も、生で食する時の肉質や
風味、食味を呈することができる二枚貝の冷凍保
存方法に関するものである。
従来、アサリ、ハマグリ、シジミ等の二枚貝
は、殻付きのまま開かずに冷凍すれば貝が死んで
しまい、その結果煮ても焼いても殻が閉じられた
状態か又開いても身肉が殻と接着して食べ難いた
め使用できないとされ、採取後ある程度水中に生
かしておける短期間内に売買する以外は、長期保
存には開殻してむき身にして冷凍することが一般
的である。しかし、むき身の冷凍の場合、むき身
にするのに手間がかかるし、味も落ちてしまう
し、料理の部分的材料にすると、他の材料にかく
れてその存在も強調できないとともに見せ場の風
情もなくなつてしまうのでむき身の冷凍保存はあ
まり行なわれていない。
周知のように貝の採取量は季節によつて大きく
変動する。かくて貝類を年間を通して安定に供給
するにはどうしても大量に採取できたときに殻付
きのまま冷凍して長期間の保存をはかることが必
要であり、貝類を殻付きのまま冷凍保存する方法
もいくつか提案されている。例えば特開昭56−
68342号公報記載の方法では、塩水で砂抜きした
二枚貝類を生きているうちに−40℃のエアブラス
ト凍結かドライアイス中−78℃で凍結し、そのま
まの状態で−20℃以下で数ケ月貯蔵し、開口する
ときはその貝類を水に入れその水を沸騰させて加
熱解凍して開口させている。しかしこの方法では
生のときの肉質や旨味、風味等が失なわれて殻割
れや凍結保存中の品質変化を生ずる惧れがあると
ともに保存後沸騰水中で煮熱する等加熱して開殻
させるときの開殻率が十分でなく、閉殻したまま
冷凍保存する方法として満足すべきものでなかつ
た。
かくて、本発明は二枚貝を閉殻したまま品質変
化することなく長期間冷凍保存して、常に生で食
する時の肉質、旨味、風味を保持することができ
且保存後調理時の開殻率の高い二枚貝の冷凍保存
方法を提供することを目的とするものであつて、
本発明者が鋭意研究、実験を重ねた結果、かかる
目的は二枚貝を口が開かない程度に加熱殺菌した
後食塩水又はアルカリ性化合物、糖類、グリセリ
ンのいずれか1種又は数種を含む食塩水からなる
注水液に浸漬したまま凍結することによつて達成
されることが見出されたのである。
本発明を更に詳細に説明する。
まずアサリ、ハマグリ、シジミ或いはムール
貝、ホタテ貝等の二枚貝を採取後、海水又は食塩
水で洗い不純物を除いて砂抜きしてから本発明に
係る方法を行なう。
かかる砂抜きをした後口が開かない程度に加熱
殺菌する。口が開かない程度に抑えて行なうの
は、高温度又は長時間加熱して口を開かせると旨
味の成分乃至栄養分が逸失し、且つ肉質を劣化さ
せ風味を損なう惧れがあるからである。この加熱
は殻の表面に付着した細菌を殺菌して除去するた
めである。加熱の手段は温湯に浸漬したりガスオ
ーブン或いは電子レンヂで加熱したり任意の方法
で行なうことができるが、通常温湯浸漬で行なわ
れる。その場合60〜100℃の温度に加温された清
水又は1〜5%程度のうすい塩水に数十秒乃至10
分間浸漬するのが望ましい。貝の種類や大きさ等
によつて適当な加熱手段、条件を選択する。
本発明の方法ではこのように加熱した後に次に
示す注水液に浸漬のまま凍結する。注水液として
は、0.5〜3%の範囲の濃度の食塩水を用いる
か、アルカリ性化合物、糖類、グリセリンのいず
れか1種又は数種を含む前記程度の濃度の食塩水
が用いられる。アルカリ性化合物としてはナトリ
ウム、カリウム等のアルカリ金属の水酸化物、炭
酸塩、重炭酸塩等が用いられ、特に重炭酸ソーダ
が好んで用いられる。これらの化合物の添加量は
これらが添加された食塩水のPHが7〜9の弱アル
カリ性になる程度の量とするのが望ましい。糖類
としては蔗糖、果糖、ソルビツト等が好んで用い
られ、その量はほぼ2〜8%の範囲、特に5〜6
程度とするのが好ましい。又グリセリンの量は1
〜5%の範囲、特に2〜3%程度とするのが好ま
しい。これらの化合物は1種でもよく、又数種組
合わせて用いることもでき、特に重炭酸ソーダと
蔗糖とを組合わせ添加した食塩水が好んで用いら
れる。砂抜きされた凍結すべき貝類を予め容器に
入れそこへ上記のような注水液を注入して浸漬の
まま凍結しても、又さきに容器に上記注水液を入
れておきそこへ凍結すべき貝類を入れて浸漬した
まま凍結してもよくその順序は任意である。この
ように注水液で浸漬したままの凍結でも生のとき
の肉質等を失なうことなく長期間凍結保存し又調
理加熱時には無処理の場合に比べて高い開殻率で
開殻することができる。
本発明の方法では上記のように加熱と浸漬凍結
をこの順序で組合わせて行なう。即ち砂抜きされ
た二枚貝を温湯やガスオーブン、電子レンジ等で
上記のようにして予備加熱し、冷却したあと上記
の如き注水液に浸漬してそのまま凍結するのであ
る。このように処理することにより生のときの肉
質、旨味などを長期間保存することができるとと
もに、開殻率を上げて事実上100%にも向上させ
ることができる。
以下に例を挙げて本発明について更に詳細に説
明する。
例 1
浜名湖産のアサリを用い、貝のサイズは中形
(7〜8g/ケ)と小形(5〜g/ケ)の2種類
とした。
アサリ300gを各々下記の通り各温度の温湯に
浸漬して加熱後、冷水にて冷却した。
ポリ容器に入れたのち、一部には別表の成分を
含む水溶液を500ml入れ、一部はそのまま凍結し
た。
The present invention relates to a novel method for freezing and preserving bivalves, and more particularly, to a method for freezing and preserving bivalves that can retain the same meat quality, flavor, and taste as when eaten raw even after long-term frozen preservation. Conventionally, if clams, clams, freshwater clams, and other bivalves are frozen without opening them with their shells on, the shellfish will die, and as a result, when boiled or grilled, the shells remain closed or the flesh remains even when opened. It is said that it cannot be used because it adheres to the shell and is difficult to eat, so unless it is bought and sold within a short period of time after being collected so that it can be kept alive in water, for long-term storage it is generally opened, shucked and frozen. However, in the case of frozen shelled meat, it takes time to peel it and the taste deteriorates, and when it is used as a partial ingredient in a dish, it is hidden behind other ingredients and its presence cannot be emphasized, and it does not have the appearance of a highlight. The shelled meat is not often frozen and preserved because it gets old. As is well known, the amount of shellfish collected varies greatly depending on the season. Therefore, in order to provide a stable supply of shellfish throughout the year, it is necessary to preserve them for a long period of time by freezing them with their shells on when they can be collected in large quantities.There is also a method of freezing shellfish with their shells on. Some suggestions have been made. For example, JP-A-56-
In the method described in Publication No. 68342, bivalve molluscs are air-blast frozen at -40°C or frozen at -78°C in dry ice while they are still alive after removing sand from them in salt water, and then kept at -20°C or lower for several months in that state. To store and open the shellfish, put the shellfish in water, bring the water to a boil, heat and thaw the shellfish before opening. However, with this method, there is a risk that the meat quality, taste, flavor, etc. when raw will be lost, resulting in cracking of the shell and quality changes during frozen storage.After storage, the shell must be opened by heating, such as boiling in boiling water. The rate of opening of the shell was not sufficient, and it was not a satisfactory method for freezing and preserving the shell with the shell closed. Thus, the present invention allows bivalves to be frozen for a long period of time without any change in quality with their shells closed, thereby retaining the meat quality, flavor, and flavor when eaten raw, and reducing the open shell rate when cooked after storage. The purpose is to provide a method for freezing and preserving bivalves with high
As a result of extensive research and experimentation by the present inventor, this purpose was achieved by heating and sterilizing bivalves to such an extent that they cannot open their mouths, and then using salt water containing one or more of alkaline compounds, sugars, and glycerin. It was discovered that this can be achieved by freezing while immersed in a water injection solution. The present invention will be explained in more detail. First, after collecting bivalves such as clams, clams, freshwater clams, mussels, and scallops, they are washed with seawater or salt water to remove impurities and remove sand before carrying out the method according to the present invention. After removing the sand, it is heated and sterilized to the extent that it does not open. The reason why this is done is to prevent the mouth from opening at high temperatures or for long periods of time because if the mouth is opened by heating at high temperatures or for a long time, the flavor components and nutrients will be lost, and there is a risk that the quality of the meat will deteriorate and the flavor will be impaired. This heating is to sterilize and remove bacteria attached to the surface of the shell. Heating can be done by any method such as immersion in hot water, heating in a gas oven or microwave oven, but immersion in hot water is usually used. In that case, soak in fresh water heated to a temperature of 60 to 100℃ or dilute salt water of about 1 to 5% for several tens of seconds to 10 minutes.
It is recommended to soak for a minute. Select appropriate heating means and conditions depending on the type and size of the shellfish. In the method of the present invention, after heating as described above, the material is frozen while immersed in the following water injection solution. As the water injection solution, a saline solution having a concentration in the range of 0.5 to 3% is used, or a saline solution containing one or more of alkaline compounds, sugars, and glycerin and having the above concentration is used. As the alkaline compound, hydroxides, carbonates, bicarbonates, etc. of alkali metals such as sodium and potassium are used, and sodium bicarbonate is particularly preferably used. It is desirable that the amount of these compounds added is such that the pH of the saline solution to which they are added becomes slightly alkaline, ranging from 7 to 9. Sucrose, fructose, sorbitol, etc. are preferably used as sugars, and the amount thereof is approximately in the range of 2 to 8%, especially 5 to 6%.
It is preferable to set it as approximately. Also, the amount of glycerin is 1
It is preferably in the range of ~5%, particularly around 2-3%. These compounds may be used alone or in combination, and a saline solution containing a combination of sodium bicarbonate and sucrose is particularly preferred. Even if you put the sand-removed shellfish to be frozen in a container in advance and inject the above-mentioned water injection into it and freeze it while immersed, you should also first pour the above-mentioned water injection into the container and freeze it there. Shellfish may be added and frozen while soaked in any order. In this way, even when frozen while immersed in a water injection solution, the meat can be preserved for a long period of time without losing its raw flesh quality, and during cooking and heating, the shells open at a higher rate than when untreated. can. In the method of the present invention, heating and immersion freezing are performed in combination in this order as described above. That is, the sand-removed bivalves are preheated in hot water, a gas oven, a microwave oven, etc. as described above, cooled, and then immersed in the water injection solution as described above to be frozen. By processing in this way, it is possible to preserve the raw meat quality and flavor for a long period of time, and it is also possible to increase the shell opening rate to virtually 100%. The present invention will be explained in more detail with reference to examples below. Example 1 Clams from Lake Hamana were used, and the shellfish were of two sizes: medium (7 to 8 g/fish) and small (5 to 8 g/fish). 300 g of clams were heated by immersing them in hot water at various temperatures as described below, and then cooled with cold water. After placing it in a plastic container, 500 ml of an aqueous solution containing the ingredients listed in the attached table was added to one portion, and the other portion was frozen as is.
【表】
−25℃で10日間凍蔵したのち、解凍し、アサリ
をフライパンに入れ蓋をして3分間煮熟して煮熟
試験を行ない、開殻率を調べると同時に貝の肉
質、風味について官能試験を行なつて品質の優劣
を判別した。[Table] After freezing at -25℃ for 10 days, thawing the clams, placing the clams in a frying pan with a lid on and boiling for 3 minutes to perform a boiling test. A sensory test was conducted to determine the superiority and inferiority of quality.
【表】【table】
【表】
結果(2)肉質、風味の品質判定(官能検査)
食品の官能検査に熟練したパネル16名により判
定した。[Table] Results (2) Judgment of meat quality and flavor quality (sensory test) Judgment was made by a panel of 16 people who are skilled in food sensory tests.
【表】
この結果から、予備加熱及び注水液凍結する事
により開殻率を上げると同時に肉質風味の劣化防
止に効果のある事かが明らかである。
例 2
ハマグリ(平均重量59g)を用いて凍結試験を
行なつた。
(1) ハマグリ10ケを下記の通り温湯中にて加熱
後、冷水中にて冷却し、ポリ袋に入れ前例のA
液と同水溶液を加えて凍結した。10日間凍結後
解凍して加熱試験を行なつた。[Table] From these results, it is clear that preheating and freezing the water injection solution are effective in increasing the shell opening rate and at the same time preventing deterioration of meat flavor. Example 2 A freezing test was conducted using clams (average weight 59 g). (1) Heat 10 clams in hot water as shown below, cool them in cold water, and place them in a plastic bag.
The liquid and the same aqueous solution were added and frozen. After freezing for 10 days, the samples were thawed and a heating test was conducted.
【表】
70℃3分、又は80℃1分の予備加熱により効
果が見られる。試食結果、風味、肉質共に極め
て良好であつた。
例 3
アサリ各400g(約50〜60ケ)を用いて試験し
た。
調理用電子レンヂ、ナシヨナルNE―5500型で
下記の通り予備加熱後、直ちに水冷し、ポリ袋に
入れて例1のA液と同液を加注して凍結及び加熱
試験を行なつた。[Table] Effects can be seen by preheating at 70°C for 3 minutes or 80°C for 1 minute. The taste results showed that both flavor and meat quality were very good. Example 3 A test was conducted using 400 g of each clam (approximately 50 to 60 clams). After preheating using a cooking microwave oven model Nasional NE-5500 as described below, the mixture was immediately cooled with water, placed in a plastic bag, and the same liquid as Example 1 was added thereto for freezing and heating tests.
【表】
90秒の予備加熱で効果が認められた。尚、No.
4,5の肉質が若干硬く感じられた他は風味、肉
質とも良好。
例 4
アサリ各400g(50〜60ケ)を用いて試験し
た。
調理用ガスオーブン(リンナイ コンベツク)
レンジで予備加熱を行ない前例と同様凍結、加熱
試験を行なつた。[Table] Effects were observed with 90 seconds of preheating. Furthermore, No.
The flavor and quality of meat were good, except for the meat quality in Nos. 4 and 5, which felt a little tough. Example 4 A test was conducted using 400 g (50 to 60 pieces) of each clam. Gas oven for cooking (Rinnai Konbetsu)
The sample was preheated in the microwave and the freezing and heating tests were conducted in the same manner as in the previous example.
【表】
No.4、No.5では効果が認められ、風味、肉質と
も良好であつた。[Table] The effect was recognized in No. 4 and No. 5, and both flavor and meat quality were good.
Claims (1)
後、食塩水又はアルカリ性化合物、糖類、グリセ
リンのいずれか1種又は数種を含む食塩水からな
る注水液に浸漬したまま凍結することを特徴とす
る二枚貝の冷凍保存方法。1. A bivalve mollusc is heat sterilized to the extent that its mouth does not open, and then frozen while immersed in a saline solution or a saline solution containing one or more of alkaline compounds, sugars, and glycerin. How to freeze bivalves.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP61014566A JPS61166352A (en) | 1986-01-25 | 1986-01-25 | Method of freezing and preserving bivalve |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP61014566A JPS61166352A (en) | 1986-01-25 | 1986-01-25 | Method of freezing and preserving bivalve |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP58193646A Division JPS6083529A (en) | 1983-10-17 | 1983-10-17 | Freezing and preservation of bivalve |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS61166352A JPS61166352A (en) | 1986-07-28 |
JPS6212968B2 true JPS6212968B2 (en) | 1987-03-23 |
Family
ID=11864700
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP61014566A Granted JPS61166352A (en) | 1986-01-25 | 1986-01-25 | Method of freezing and preserving bivalve |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS61166352A (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0684494B2 (en) * | 1986-11-28 | 1994-10-26 | 東レ・ダウコーニング・シリコーン株式会社 | Silicone pressure sensitive adhesive composition |
JP2726618B2 (en) * | 1993-12-28 | 1998-03-11 | 日清食品株式会社 | Freeze drying method of mollusk raw meat |
JP7162296B2 (en) * | 2018-08-07 | 2022-10-28 | 一喜 下田 | Food freezing method and food freezing apparatus |
-
1986
- 1986-01-25 JP JP61014566A patent/JPS61166352A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS61166352A (en) | 1986-07-28 |
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