JPS62128410A - Hot cathode parts - Google Patents

Hot cathode parts

Info

Publication number
JPS62128410A
JPS62128410A JP60267843A JP26784385A JPS62128410A JP S62128410 A JPS62128410 A JP S62128410A JP 60267843 A JP60267843 A JP 60267843A JP 26784385 A JP26784385 A JP 26784385A JP S62128410 A JPS62128410 A JP S62128410A
Authority
JP
Japan
Prior art keywords
group
hot cathode
carbide
boride
ion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP60267843A
Other languages
Japanese (ja)
Inventor
Yoshitaka Enomoto
榎本 義隆
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Seiko Instruments Inc
Original Assignee
Seiko Instruments Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Seiko Instruments Inc filed Critical Seiko Instruments Inc
Priority to JP60267843A priority Critical patent/JPS62128410A/en
Publication of JPS62128410A publication Critical patent/JPS62128410A/en
Pending legal-status Critical Current

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  • Physical Vapour Deposition (AREA)
  • Electron Sources, Ion Sources (AREA)
  • Solid Thermionic Cathode (AREA)

Abstract

PURPOSE:To enhance the resistance against ion impact by forming, on a metallic or a heat resistant conductive base, a coating layer comprising carbide or boride of IVa group, Va group or La. CONSTITUTION:In hot cathode parts of an ion source used for vacuum deposition, a coating film of carbide or boride of IV2 group, Va group or La is applied on a hot cathode, whereby the spattering ratio by rare gas is reduced and the reaction with oxygen can hardly happen, thus making possible the increase in operation time.

Description

【発明の詳細な説明】 〔産業上の利用分野〕 この発明は、真空蒸着に用いるイオン源の熱陰極部品に
関する。
DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] This invention relates to a hot cathode component of an ion source used for vacuum evaporation.

〔発明の概要〕[Summary of the invention]

この発明は、金属等の基材に金属化合物液Hを施し、長
時間動作を可能とした熱陰極に関するものである。
The present invention relates to a hot cathode that can be operated for a long time by applying a metal compound liquid H to a base material such as metal.

〔従来の技術〕[Conventional technology]

従来、第2図に示すように、電子銃の熱電子発生源であ
る熱陰極は、タングステンを材料とし、フィラメント形
状の熱陰pitが使用されていた。
Conventionally, as shown in FIG. 2, a filament-shaped hot cathode pit made of tungsten has been used as a hot cathode, which is a source of thermionic electrons in an electron gun.

〔発明が解決しようとする問題点〕[Problem that the invention seeks to solve]

しかし、従来の電子ビーム型加熱源は、イオンブレーテ
ィングのように、プラズマ密度の高い状態で使用すると
、イオン衝撃を受けてフィラメント1が融解、切断され
て、その寿命が著しく短くなるという欠点があった。
However, when conventional electron beam heating sources are used in a state of high plasma density, such as in ion blating, the filament 1 is melted and cut by ion bombardment, resulting in a significantly shortened lifetime. there were.

そこで、この発明は従来のこのような欠点を解決するた
め、イオン衝撃に対して、抵抗力の強い熱陰極を得るこ
とを目的としている。
Therefore, in order to solve these conventional drawbacks, the present invention aims to provide a hot cathode that is highly resistant to ion bombardment.

〔間ツ点を解決するための手段〕[Means to resolve the gap]

上記問題点を解決するためにこの発明は、熱陰極に、■
1族、■、族又はり、の炭化物又はホウ化素被膜を施し
耐イオン衝撃性を高めるようにした。
In order to solve the above problems, this invention provides a hot cathode with:
A carbide or boride coating of Group 1, ■, Group or Poly was applied to improve ion impact resistance.

〔作用〕[Effect]

上記のように構成された熱陰極を使用すると希ガスによ
るスパッタリング率が減少し、酸素との反応も起こりに
くくなるため、動作時間を増加することが出来るのであ
る。
When a hot cathode configured as described above is used, the sputtering rate due to rare gas is reduced and reaction with oxygen becomes less likely to occur, so that the operating time can be increased.

〔実施例〕〔Example〕

以下にこの発明を実施例に基づいて説明する。 The present invention will be explained below based on examples.

実施例1 タングステンを熱陰極の第2図におけるフィラメントl
として加工し、イオンブレーティング装置に配置する。
Example 1 Tungsten was used as the filament l of the hot cathode in Figure 2.
and placed in an ion blating device.

イオンブレーティング装置をI X 10−’Torr
に排気後アルゴンガスをI X l O−”Torr導
入し、直流500Vの電圧を印加してボンバードを行う
Ion blating device at I x 10-'Torr
After exhausting, argon gas was introduced at IXlO-'' Torr, and bombardment was performed by applying a DC voltage of 500 V.

続いてTiを電子ビーム加熱で蒸発させ、さらにアセチ
レンガスを5 X 10−’Torr導入し、Tiと反
応させフィラメント1の上に第1図における金属化合物
被膜2として、TiCを3μmの厚みで形成する。上記
の方法で形成したフィラメントは、N2ガスI X 1
0−”Torr、電子銃入力電圧IQkV、200mA
のイオンブレーティング条件で、電子銃の陰極として使
用したところ200時間使用可能であった。これに対し
、従来のタングステンフィラメントは30時間で中央部
が融解した。
Next, Ti was evaporated by electron beam heating, and acetylene gas was introduced at 5 x 10-'Torr to react with Ti, forming TiC with a thickness of 3 μm as metal compound coating 2 in FIG. 1 on filament 1. do. The filament formed by the above method is N2 gas I
0-”Torr, electron gun input voltage IQkV, 200mA
When used as an electron gun cathode under ion blating conditions, it could be used for 200 hours. In contrast, the center of the conventional tungsten filament melted in 30 hours.

実施例2 第3図に示す。 c t〕yl電r銃のTaパイプ3に
温度1 0 0 0 ’C,Ticl、  流星  1
 0 0  mn/m1nC2112’LA’$  1
00 ml!/minの条件下でT i C>a 12
をCVD法により10μmの厚みに形成する。
Example 2 Shown in FIG. c t]yl Electric gun's Ta pipe 3 has a temperature of 1 0 0 0'C, Ticl, Meteor 1
0 0 mn/m1nC2112'LA'$ 1
00ml! /min T i C>a 12
is formed to a thickness of 10 μm using the CVD method.

(第4図に示ず)次にこの?AFS2処理を作ったTa
パイプを、N2流1500 ml/min、 HCD型
電子銃入力電圧30V、電流200Aの条件下でイオン
ブレーティング用熱陰極として使用したところ、150
時間使用可能であった。これに対し、従来のTaパイプ
は20時間で先端部分が融解し、使用不能となった。
(Not shown in Figure 4) Next, this? Ta who created AFS2 processing
When the pipe was used as a hot cathode for ion blating under the conditions of N2 flow of 1500 ml/min, HCD type electron gun input voltage of 30 V, and current of 200 A, 150
Time was available. In contrast, the tip of the conventional Ta pipe melted in 20 hours, making it unusable.

上記実施例の他にも、N1族、■□族及びり。In addition to the above examples, the N1 group, the ■□ group, and the like.

の炭化物、ホウ化物において同様な、長寿命化の効果が
見られた。
A similar effect of longer life was observed in carbides and borides.

〔発明の効果〕〔Effect of the invention〕

この発明は、以上説明したように、熱陰極の表面に金属
化合物の被膜処理を施すことにより、熱陰極の使用時間
を延長する効果がある。
As explained above, the present invention has the effect of extending the usage time of the hot cathode by applying a coating treatment with a metal compound to the surface of the hot cathode.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は、この発明にかかる電子ビーム加熱蒸発源の陰
極部品閲、第2図は、従来の電子ビーム加熱薄光源の陰
極部品図、第3図は、従来のHCD型電子ビーム加熱暴
発源の中空加熱陰極部品図、第4図は、この発明にかか
る陰極部品図である。 l・・・フィラメント基材 2・・・金属化合物被膜 3・・・Taパイプ 4・・・金属化合物被膜 以上
Fig. 1 is a view of the cathode parts of the electron beam heating evaporation source according to the present invention, Fig. 2 is a view of the cathode parts of the conventional electron beam heating thin light source, and Fig. 3 is a view of the cathode parts of the conventional HCD type electron beam heating evaporation source. FIG. 4 is a diagram of a hollow heating cathode component according to the present invention. l...Filament base material 2...Metal compound coating 3...Ta pipe 4...Metal compound coating or more

Claims (1)

【特許請求の範囲】[Claims] 金属又は耐熱性電導基材上に、IV_a族、V_a族又は
L_aの炭化物又はホウ化物からなる被膜層を形成した
ことを特徴とする熱陰極部品。
A hot cathode component characterized in that a coating layer made of a carbide or boride of IV_a group, V_a group, or L_a group is formed on a metal or a heat-resistant conductive base material.
JP60267843A 1985-11-28 1985-11-28 Hot cathode parts Pending JPS62128410A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP60267843A JPS62128410A (en) 1985-11-28 1985-11-28 Hot cathode parts

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP60267843A JPS62128410A (en) 1985-11-28 1985-11-28 Hot cathode parts

Publications (1)

Publication Number Publication Date
JPS62128410A true JPS62128410A (en) 1987-06-10

Family

ID=17450394

Family Applications (1)

Application Number Title Priority Date Filing Date
JP60267843A Pending JPS62128410A (en) 1985-11-28 1985-11-28 Hot cathode parts

Country Status (1)

Country Link
JP (1) JPS62128410A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0422622A (en) * 1990-05-17 1992-01-27 Ngk Insulators Ltd Composite material having boride coating layer
JPH0464311A (en) * 1990-07-03 1992-02-28 Kokuyo Co Ltd Housing furniture

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0422622A (en) * 1990-05-17 1992-01-27 Ngk Insulators Ltd Composite material having boride coating layer
JPH0464311A (en) * 1990-07-03 1992-02-28 Kokuyo Co Ltd Housing furniture

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